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The crystal structures of phase II and the metastable phases III' and III of cyclohexanol, C6H11OH, have been determined using high-resolution neutron powder and single-crystal X-ray diffraction techniques. Phase II crystallizes in a tetragonal structure, space group P\bar 42_1c, characterized by a hydrogen-bonded tetrameric ring motif. Phases III' and III are monoclinic, space groups P21/c and Pc, respectively, with molecules linked via hydrogen-bonded chains.
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