Crystal structure of a new polyoxometalate (POM) com­pound with a high level of crystallographic disorder

Skorepova, E.; Harchani, A.; Ftini, M.M.; Dušek, M.; Haddad, A.

doi:10.1107/S2053229619015596

Crystal structure of a new polyoxometalate (POM) compound with a high level of crystallographic disorder

E. Skorepova, A. Harchani, M. M. Ftini, M. Dušek and A. Haddad

The crystal structure, Hirshfeld surface analysis and spectroscopic analysis of a new polyoxometalate (POM) compound, namely, nonakis(2-methoxyaniline) bis(diphosphopentamolybdate) trihydrate, (C₇H₉NO)₉[P₂Mo₅O₂₃]₂·3H₂O, is reported. The title compound was synthesized using the solution method and was structurally characterized by single-crystal X-ray diffraction, which revealed P $\overline{1}$ symmetry. A study of the intermolecular interactions using Hirshfeld surface analysis confirmed that the hydrogen-bonding interactions play the dominant role in the stability of the crystal structure. The refinement was complicated by extensive disorder affecting 11 of the 16 ions and molecules in the asymmetric unit. IR and UV–Vis spectroscopic techniques were used to identify the vibrational modes and to classify this compound as an insulator.

Keywords: disorder; rigid body; synthesis; crystal structure; polyoxometalate; POM; spectroscopic analysis; Hirshfeld surface; insulator.

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Supporting information

	Crystallographic Information File (CIF) https://doi.org/10.1107/S2053229619015596/yd3001sup1.cif Contains datablocks global, I
	Structure factor file (CIF format) https://doi.org/10.1107/S2053229619015596/yd3001Isup2.hkl Contains datablock I
	Portable Document Format (PDF) file https://doi.org/10.1107/S2053229619015596/yd3001sup3.pdf Supplementary material

CCDC reference: 1843280

Computing details top

Data collection: CrysAlis PRO (Rigaku OD, 2015); cell refinement: CrysAlis PRO (Rigaku OD, 2015); data reduction: CrysAlis PRO (Rigaku OD, 2015); program(s) used to solve structure: SUPERFLIP (Palatinus & Chapuis, 2007); program(s) used to refine structure: JANA2006 (Petříček et al., 2014); molecular graphics: DIAMOND3 (Brandenburg & Putz, 2005), Mercury (Macrae et al., 2008) and Discovery Studio Visualizer (https://www.3dsbiovia.com/).

Nonakis(2-methoxyaniline) bis(diphosphopentamolybdate) trihydrate top

Crystal data top

(C₇H₁₀NO)_8.5[P₂Mo₅O₂₃]₂·3H₂O	Z = 2
M_r = 2993.5	F(000) = 2950
Triclinic, P1	D_x = 1.996 Mg m⁻³
Hall symbol: -P 1	Cu Kα radiation, λ = 1.54184 Å
a = 14.8316 (2) Å	Cell parameters from 14565 reflections
b = 15.2679 (1) Å	θ = 4.0–73.6°
c = 23.2370 (2) Å	µ = 11.57 mm⁻¹
α = 89.1396 (7)°	T = 95 K
β = 78.1097 (7)°	Polygonal shape, white
γ = 75.4959 (8)°	0.08 × 0.07 × 0.06 mm
V = 4981.24 (9) Å³

Data collection top

Rigaku OD SuperNova Dual source diffractometer with an AtlasS2 detector	19576 independent reflections
Radiation source: X-ray tube	16182 reflections with I > 3σ(I)
Mirror monochromator	R_int = 0.032
Detector resolution: 5.2027 pixels mm^-1	θ_max = 74.2°, θ_min = 3.5°
ω scans	h = −17→18
Absorption correction: gaussian (CrysAlis PRO; Rigaku OD, 2015)	k = −12→18
T_min = 0.516, T_max = 0.641	l = −28→28
35243 measured reflections

Refinement top

Refinement on F²	252 constraints
R[F > 3σ(F)] = 0.083	H atoms treated by a mixture of independent and constrained refinement
wR(F) = 0.219	Weighting scheme based on measured s.u.'s w = 1/(σ²(I) + 0.0016I²)
S = 2.74	(Δ/σ)_max < 0.001
19576 reflections	Δρ_max = 7.49 e Å⁻³
557 parameters	Δρ_min = −4.98 e Å⁻³
38 restraints

Special details top

Refinement. A single crystal of 1 of size 0.08 × 0.07 × 0.06 mm was used for X-ray diffraction study at 95K on a SuperNova four-circle diffractometer equipped with a CCD Atlas S2 detector, using the mirrors-collimated Cu Kα radiation (λ = 1.54184 Å). The crystal structures were solved by charge flipping with program SUPERFLIP (Palatinus & Chapuis, 2007) and refined with the JANA2006 program package (Petricek et al., 2014). The refinement was carried out against all reflections.

The molecular structure plots were generated using DIAMOND3 (Brandenburg & Putz, 2005), Mercury (Macrae et al., 2008) and DiscoveryStudio Visualizer.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å²) top

	x	y	z	U_iso*/U_eq	Occ. (<1)
Mo1bx	0.32393 (13)	0.13233 (14)	−0.09859 (8)	0.02031 (17)	0.433 (2)
Mo4bx	0.24160 (18)	0.15664 (13)	0.05157 (10)	0.02353 (18)	0.433 (2)
Mo5bx	0.20789 (16)	−0.04434 (13)	0.10197 (9)	0.02499 (19)	0.433 (2)
Mo3bx	0.25395 (15)	−0.19654 (12)	−0.01073 (9)	0.02366 (19)	0.433 (2)
Mo2bx	0.29431 (15)	−0.08409 (13)	−0.13840 (9)	0.02338 (18)	0.433 (2)
P1bx	0.3943 (3)	−0.0461 (3)	−0.0141 (2)	0.0200 (5)	0.433 (2)
P2bx	0.1383 (3)	0.0335 (3)	−0.0247 (2)	0.0256 (5)	0.433 (2)
O3bx	0.4004 (7)	−0.1599 (9)	−0.1641 (7)	0.0315 (19)	0.433 (2)
O5bx	0.4760 (9)	−0.1187 (8)	0.0060 (7)	0.0247 (16)	0.433 (2)
O14bx	0.4291 (5)	0.0216 (7)	−0.0564 (6)	0.0212 (14)	0.433 (2)
O15bx	0.1655 (8)	−0.0505 (4)	0.0132 (3)	0.0233 (15)	0.433 (2)
O1bx	0.3161 (9)	0.1798 (8)	−0.0222 (3)	0.0228 (16)	0.433 (2)
O6bx	0.4257 (7)	0.1600 (11)	−0.1341 (7)	0.0274 (17)	0.433 (2)
O23bx	0.0999 (8)	−0.0616 (12)	0.1362 (7)	0.037 (2)	0.433 (2)
O17bx	0.3490 (8)	−0.1006 (8)	−0.0495 (3)	0.0209 (14)	0.433 (2)
O18bx	0.3388 (10)	0.0243 (6)	−0.1461 (4)	0.0275 (18)	0.433 (2)
O11bx	0.3265 (5)	−0.0019 (4)	0.0429 (4)	0.0221 (14)	0.433 (2)
O10bx	0.2792 (8)	−0.1613 (5)	0.0628 (4)	0.0242 (15)	0.433 (2)
O13bx	0.2400 (9)	0.2057 (9)	−0.1273 (7)	0.0311 (19)	0.433 (2)
O7bx	0.2704 (12)	−0.0501 (12)	0.1568 (6)	0.0339 (19)	0.433 (2)
O19bx	0.3477 (9)	−0.2925 (7)	−0.0206 (8)	0.034 (2)	0.433 (2)
O16bx	0.1578 (9)	−0.2380 (11)	0.0152 (8)	0.033 (2)	0.433 (2)
O20bx	0.3079 (10)	0.1745 (11)	0.1009 (6)	0.0292 (18)	0.433 (2)
O12bx	0.2369 (10)	−0.1697 (8)	−0.0894 (4)	0.0271 (18)	0.433 (2)
O21bx	0.1619 (6)	0.0830 (5)	0.0938 (6)	0.0293 (18)	0.433 (2)
O4bx	0.1484 (9)	0.2496 (8)	0.0592 (8)	0.0351 (19)	0.433 (2)
O2bx	0.2360 (11)	−0.0864 (12)	−0.1948 (6)	0.032 (2)	0.433 (2)
O22bx	0.2096 (7)	0.0941 (8)	−0.0275 (3)	0.0218 (15)	0.433 (2)
O9bx	0.0342 (6)	0.0829 (10)	0.0005 (7)	0.0298 (18)	0.433 (2)
O8bx	0.1536 (5)	−0.0068 (9)	−0.0863 (4)	0.0274 (17)	0.433 (2)
O1w	0.3950 (19)	0.3149 (16)	−0.0293 (14)	0.057 (3)*	0.47 (4)
O1w'	0.4136 (17)	0.3145 (14)	−0.0073 (12)	0.057 (3)*	0.53 (4)
O2w	0.450 (3)	0.305 (2)	0.0724 (15)	0.072 (4)*	0.40 (4)
O2w'	0.492 (2)	0.3031 (14)	0.0833 (10)	0.072 (4)*	0.60 (4)
O3w	0.9780 (11)	−0.2273 (10)	0.4134 (7)	0.038 (3)*	0.5
O4w	0.9709 (15)	0.7500 (14)	0.0598 (10)	0.059 (5)*	0.5
O24a	0.1148 (4)	0.3212 (3)	0.2592 (2)	0.0434 (11)
N1a	0.0837 (7)	0.3255 (6)	0.3760 (3)	0.0364 (12)
C1a	0.1827 (9)	0.0751 (5)	0.2807 (5)	0.0493 (18)
C2a	0.1180 (7)	0.2385 (6)	0.3430 (3)	0.0356 (13)
C3a	0.1348 (9)	0.1589 (6)	0.3732 (4)	0.0435 (16)
C4a	0.1671 (9)	0.0774 (6)	0.3414 (5)	0.0519 (19)
C5a	0.1664 (7)	0.1546 (5)	0.2504 (4)	0.0435 (16)
C6a	0.1286 (7)	0.3243 (6)	0.1960 (3)	0.053 (2)
C7a	0.1337 (6)	0.2372 (5)	0.2827 (3)	0.0351 (13)
H1c1a	0.205147	0.017905	0.259245	0.0591*
H1c3a	0.124071	0.160477	0.415428	0.0522*
H1c4a	0.178719	0.021766	0.361714	0.0623*
H1c5a	0.177316	0.152976	0.208244	0.0522*
H1c6a	0.108455	0.385863	0.185027	0.0637*
H2c6a	0.194752	0.300278	0.178655	0.0637*
H3c6a	0.091647	0.288789	0.182243	0.0637*
H1n1a	0.125835	0.332392	0.395452	0.0437*
H2n1a	0.074592	0.369092	0.351603	0.0437*
H3n1a	0.030391	0.326728	0.400411	0.0437*
O24b	1.094 (2)	0.026 (2)	0.5027 (5)	0.0434 (13)	0.5
N1b	0.924 (3)	0.142 (4)	0.5177 (9)	0.0364 (13)	0.5
C1b	0.956 (5)	−0.131 (3)	0.4706 (9)	0.049 (2)	0.5
C2b	0.9351 (13)	0.048 (2)	0.5013 (7)	0.0356 (15)	0.5
C3b	0.856 (3)	0.019 (4)	0.4942 (9)	0.0435 (18)	0.5
C4b	0.868 (5)	−0.070 (4)	0.4787 (10)	0.052 (2)	0.5
C5b	1.035 (2)	−0.103 (2)	0.4778 (7)	0.0435 (18)	0.5
C6b	1.189 (3)	−0.033 (4)	0.4944 (8)	0.053 (2)	0.5
C7b	1.0234 (7)	−0.0119 (6)	0.4936 (5)	0.0351 (15)	0.5
H1c1b	0.963027	−0.193057	0.459736	0.0591*	0.5
H1c3b	0.794419	0.061221	0.500009	0.0522*	0.5
H1c4b	0.813603	−0.091012	0.473482	0.0623*	0.5
H1c5b	1.0967	−0.144863	0.472195	0.0522*	0.5
H1c6b	1.232995	0.001972	0.49893	0.0637*	0.5
H2c6b	1.190318	−0.078689	0.523186	0.0637*	0.5
H3c6b	1.206906	−0.060909	0.455664	0.0637*	0.5
H1n1b	0.886026	0.155761	0.551976	0.0437*	0.5
H2n1b	0.979551	0.150734	0.519414	0.0437*	0.5
H3n1b	0.900638	0.176994	0.49157	0.0437*	0.5
O24c	0.3816 (6)	0.2185 (4)	0.2029 (3)	0.0434 (12)
N1c	0.4254 (10)	0.0500 (6)	0.1589 (5)	0.0364 (12)
C1c	0.4104 (11)	0.0974 (9)	0.3393 (4)	0.0493 (19)
C2c	0.4203 (8)	0.0662 (5)	0.2214 (4)	0.0356 (14)
C3c	0.4377 (11)	−0.0068 (7)	0.2574 (5)	0.0435 (16)
C4c	0.4327 (12)	0.0098 (9)	0.3164 (5)	0.052 (2)
C5c	0.3926 (8)	0.1705 (7)	0.3034 (4)	0.0435 (17)
C6c	0.3589 (10)	0.3117 (6)	0.2232 (5)	0.053 (2)
C7c	0.3977 (6)	0.1536 (5)	0.2436 (3)	0.0351 (14)
H1c1c	0.407183	0.107806	0.38035	0.0591*
H1c3c	0.453001	−0.067757	0.241619	0.0522*
H1c4c	0.444741	−0.04008	0.341837	0.0623*
H1c5c	0.377137	0.231373	0.319298	0.0522*
H1c6c	0.354211	0.350354	0.190444	0.0637*
H2c6c	0.299303	0.325771	0.251146	0.0637*
H3c6c	0.408177	0.321097	0.241717	0.0637*
H1n1c	0.382671	0.021877	0.154816	0.0437*
H2n1c	0.414953	0.101442	0.141642	0.0437*
H3n1c	0.481741	0.016893	0.142864	0.0437*
O24d	0.9347 (5)	0.1418 (4)	0.2316 (3)	0.0434 (14)
N1d	0.9622 (10)	0.1325 (7)	0.1150 (4)	0.0364 (14)
C1d	0.8754 (11)	0.3868 (6)	0.2054 (6)	0.049 (2)
C2d	0.9320 (8)	0.2208 (6)	0.1463 (3)	0.0356 (15)
C3d	0.9187 (11)	0.2990 (7)	0.1145 (4)	0.0435 (19)
C4d	0.8902 (12)	0.3819 (7)	0.1448 (6)	0.052 (2)
C5d	0.8889 (9)	0.3087 (6)	0.2372 (4)	0.043 (2)
C6d	0.9198 (10)	0.1414 (7)	0.2949 (4)	0.053 (2)
C7d	0.9179 (6)	0.2247 (5)	0.2065 (3)	0.0351 (16)
H1c1d	0.855475	0.444848	0.225777	0.0591*
H1c3d	0.929222	0.295682	0.072347	0.0522*
H1c4d	0.880481	0.436591	0.123401	0.0623*
H1c5d	0.878641	0.312068	0.279355	0.0522*
H1c6d	0.928802	0.080143	0.307394	0.0637*
H2c6d	0.964505	0.168442	0.307736	0.0637*
H3c6d	0.856124	0.175293	0.311773	0.0637*
H1n1d	1.017766	0.126798	0.092028	0.0437*
H2n1d	0.965678	0.089844	0.140364	0.0437*
H3n1d	0.921016	0.128182	0.094083	0.0437*
O24e	0.9380 (9)	0.6935 (8)	0.1745 (5)	0.0434 (14)	0.5
N1e	0.9697 (16)	0.8544 (11)	0.1474 (8)	0.0364 (14)	0.5
C1e	0.8244 (14)	0.8141 (13)	0.3178 (7)	0.049 (2)	0.5
C2e	0.9193 (12)	0.8406 (8)	0.2065 (6)	0.0356 (15)	0.5
C3e	0.8890 (16)	0.9118 (11)	0.2482 (7)	0.0435 (19)	0.5
C4e	0.8414 (16)	0.8975 (14)	0.3038 (7)	0.052 (2)	0.5
C5e	0.8549 (11)	0.7428 (10)	0.2763 (6)	0.043 (2)	0.5
C6e	0.9222 (15)	0.6049 (11)	0.1855 (7)	0.053 (2)	0.5
C7e	0.9032 (9)	0.7572 (7)	0.2200 (5)	0.0351 (16)	0.5
H1c1e	0.791219	0.805286	0.356632	0.0591*	0.5
H1c3e	0.900964	0.969735	0.238538	0.0522*	0.5
H1c4e	0.819856	0.946178	0.333036	0.0623*	0.5
H1c5e	0.843119	0.684771	0.286043	0.0522*	0.5
H1c6e	0.945061	0.567961	0.149862	0.0637*	0.5
H2c6e	0.95566	0.57741	0.21507	0.0637*	0.5
H3c6e	0.85527	0.610177	0.198984	0.0637*	0.5
H1n1e	1.02252	0.867994	0.149527	0.0437*	0.5
H2n1e	0.982483	0.804985	0.125819	0.0437*	0.5
H3n1e	0.934132	0.898351	0.131706	0.0437*	0.5
O24f	0.9199 (9)	0.7100 (8)	0.1902 (4)	0.0434 (14)	0.5
N1f	0.9239 (16)	0.8768 (10)	0.1576 (7)	0.0364 (14)	0.5
C1f	0.8398 (15)	0.8259 (12)	0.3370 (6)	0.049 (2)	0.5
C2f	0.8947 (12)	0.8593 (8)	0.2199 (6)	0.0356 (15)	0.5
C3f	0.8699 (16)	0.9302 (10)	0.2615 (7)	0.0435 (18)	0.5
C4f	0.8424 (16)	0.9125 (12)	0.3201 (7)	0.052 (2)	0.5
C5f	0.8649 (11)	0.7549 (9)	0.2955 (5)	0.0435 (19)	0.5
C6f	0.9182 (15)	0.6181 (9)	0.2043 (7)	0.053 (2)	0.5
C7f	0.8928 (9)	0.7728 (7)	0.2361 (5)	0.0351 (15)	0.5
H1c1f	0.820498	0.814679	0.377867	0.0591*	0.5
H1c3f	0.871868	0.990366	0.249783	0.0522*	0.5
H1c4f	0.824838	0.960859	0.349342	0.0623*	0.5
H1c5f	0.863094	0.694708	0.307261	0.0522*	0.5
H1c6f	0.933619	0.581641	0.168615	0.0637*	0.5
H2c6f	0.963973	0.594535	0.22805	0.0637*	0.5
H3c6f	0.855768	0.616937	0.225617	0.0637*	0.5
H1n1f	0.975201	0.896295	0.152399	0.0437*	0.5
H2n1f	0.935326	0.826941	0.136692	0.0437*	0.5
H3n1f	0.878581	0.917438	0.146806	0.0437*	0.5
O24g	0.6230 (11)	0.4067 (8)	0.2229 (6)	0.0434 (13)	0.5
N1g	0.5813 (18)	0.4718 (12)	0.3332 (7)	0.0364 (13)	0.5
C1g	0.6521 (17)	0.6373 (12)	0.1930 (9)	0.049 (2)	0.5
C2g	0.6059 (13)	0.5294 (9)	0.2846 (5)	0.0356 (15)	0.5
C3g	0.6065 (18)	0.6180 (12)	0.2967 (7)	0.0435 (18)	0.5
C4g	0.6300 (19)	0.6713 (13)	0.2503 (9)	0.052 (2)	0.5
C5g	0.6513 (13)	0.5489 (9)	0.1808 (7)	0.0435 (19)	0.5
C6g	0.6462 (17)	0.3661 (11)	0.1644 (6)	0.053 (2)	0.5
C7g	0.6274 (10)	0.4949 (7)	0.2278 (5)	0.0351 (15)	0.5
H1c1g	0.668341	0.675223	0.161199	0.0591*	0.5
H1c3g	0.590868	0.641724	0.33653	0.0522*	0.5
H1c4g	0.630882	0.732664	0.25797	0.0623*	0.5
H1c5g	0.666663	0.525274	0.140931	0.0522*	0.5
H1c6g	0.645488	0.303391	0.166673	0.0637*	0.5
H2c6g	0.600119	0.396899	0.142483	0.0637*	0.5
H3c6g	0.708403	0.370828	0.144922	0.0637*	0.5
H1n1g	0.523274	0.495098	0.352179	0.0437*	0.5
H2n1g	0.585763	0.417987	0.319263	0.0437*	0.5
H3n1g	0.620255	0.468219	0.356957	0.0437*	0.5
O24h	0.3853 (12)	0.7679 (7)	0.2214 (6)	0.0434 (13)	0.5
N1h	0.4380 (19)	0.7504 (13)	0.1048 (7)	0.0364 (13)	0.5
C1h	0.3992 (18)	0.5245 (9)	0.2043 (9)	0.049 (2)	0.5
C2h	0.4246 (14)	0.6720 (10)	0.1392 (5)	0.0356 (14)	0.5
C3h	0.4390 (19)	0.5890 (12)	0.1105 (7)	0.0435 (17)	0.5
C4h	0.426 (2)	0.5156 (11)	0.1437 (9)	0.052 (2)	0.5
C5h	0.3845 (14)	0.6074 (9)	0.2331 (7)	0.0435 (18)	0.5
C6h	0.3582 (18)	0.7824 (12)	0.2844 (6)	0.053 (2)	0.5
C7h	0.3975 (9)	0.6818 (8)	0.1994 (5)	0.0351 (15)	0.5
H1c1h	0.390634	0.472855	0.22671	0.0591*	0.5
H1c3h	0.457474	0.582784	0.068362	0.0522*	0.5
H1c4h	0.436003	0.457734	0.124426	0.0623*	0.5
H1c5h	0.365836	0.613637	0.275172	0.0522*	0.5
H1c6h	0.356683	0.84356	0.294533	0.0637*	0.5
H2c6h	0.296157	0.772169	0.298092	0.0637*	0.5
H3c6h	0.403529	0.741235	0.302447	0.0637*	0.5
H1n1h	0.397594	0.762413	0.081688	0.0437*	0.5
H2n1h	0.428607	0.796958	0.128509	0.0437*	0.5
H3n1h	0.495743	0.738654	0.083859	0.0437*	0.5
O24i	0.1360 (11)	0.7688 (8)	0.2868 (5)	0.0434 (12)	0.5
N1i	0.1180 (17)	0.6097 (10)	0.3284 (8)	0.0364 (12)	0.5
C1i	0.1755 (18)	0.6438 (14)	0.1452 (7)	0.049 (2)	0.5
C2i	0.1379 (12)	0.6213 (8)	0.2648 (6)	0.0356 (14)	0.5
C3i	0.1479 (17)	0.5487 (10)	0.2268 (8)	0.0435 (17)	0.5
C4i	0.1666 (19)	0.5610 (14)	0.1669 (8)	0.052 (2)	0.5
C5i	0.1658 (13)	0.7164 (10)	0.1832 (6)	0.0435 (17)	0.5
C6i	0.1433 (16)	0.8574 (10)	0.2676 (8)	0.053 (2)	0.5
C7i	0.1469 (9)	0.7039 (8)	0.2439 (5)	0.0351 (14)	0.5
H1c1i	0.188438	0.651266	0.103487	0.0591*	0.5
H1c3i	0.142001	0.491008	0.241777	0.0522*	0.5
H1c4i	0.173541	0.511389	0.14001	0.0623*	0.5
H1c5i	0.171966	0.77398	0.168118	0.0522*	0.5
H1c6i	0.129483	0.897915	0.301281	0.0637*	0.5
H2c6i	0.206632	0.853779	0.245797	0.0637*	0.5
H3c6i	0.098511	0.879684	0.242951	0.0637*	0.5
H1n1i	0.164881	0.569067	0.337705	0.0437*	0.5
H2n1i	0.111571	0.660858	0.346662	0.0437*	0.5
H3n1i	0.065661	0.592083	0.33857	0.0437*	0.5
O24j	0.1137 (11)	0.7893 (8)	0.2941 (5)	0.0434 (12)	0.5
N1j	0.1010 (17)	0.6282 (10)	0.3346 (8)	0.0364 (12)	0.5
C1j	0.1837 (18)	0.6594 (14)	0.1523 (7)	0.049 (2)	0.5
C2j	0.1297 (12)	0.6388 (8)	0.2713 (7)	0.0356 (14)	0.5
C3j	0.1507 (17)	0.5642 (10)	0.2330 (8)	0.0435 (17)	0.5
C4j	0.1776 (19)	0.5755 (13)	0.1734 (7)	0.052 (2)	0.5
C5j	0.1631 (13)	0.7339 (10)	0.1905 (6)	0.0435 (17)	0.5
C6j	0.1175 (16)	0.8790 (10)	0.2755 (8)	0.053 (2)	0.5
C7j	0.1359 (9)	0.7224 (8)	0.2510 (5)	0.0351 (14)	0.5
H1c1j	0.202492	0.666094	0.110725	0.0591*	0.5
H1c3j	0.146706	0.505882	0.247626	0.0522*	0.5
H1c4j	0.192196	0.524576	0.146294	0.0623*	0.5
H1c5j	0.167334	0.792171	0.175889	0.0522*	0.5
H1c6j	0.095924	0.920495	0.309054	0.0637*	0.5
H2c6j	0.181883	0.8788	0.257391	0.0637*	0.5
H3c6j	0.077313	0.897417	0.247719	0.0637*	0.5
H1n1j	0.14711	0.590674	0.346916	0.0437*	0.5
H2n1j	0.088208	0.680488	0.353016	0.0437*	0.5
H3n1j	0.050629	0.607134	0.34157	0.0437*	0.5
O24k	0.6169 (11)	0.4299 (8)	0.2277 (6)	0.0434 (13)	0.5
N1k	0.5830 (18)	0.4848 (12)	0.3398 (7)	0.0364 (13)	0.5
C1k	0.6471 (17)	0.6616 (12)	0.2053 (9)	0.049 (2)	0.5
C2k	0.6052 (13)	0.5463 (9)	0.2932 (5)	0.0356 (15)	0.5
C3k	0.6077 (18)	0.6332 (12)	0.3082 (7)	0.0435 (18)	0.5
C4k	0.6290 (19)	0.6903 (13)	0.2636 (9)	0.052 (2)	0.5
C5k	0.6443 (13)	0.5749 (9)	0.1903 (7)	0.0435 (19)	0.5
C6k	0.6358 (17)	0.3947 (12)	0.1680 (6)	0.053 (2)	0.5
C7k	0.6227 (9)	0.5170 (7)	0.2355 (5)	0.0351 (15)	0.5
H1c1k	0.661739	0.702141	0.174848	0.0591*	0.5
H1c3k	0.594931	0.653232	0.348663	0.0522*	0.5
H1c4k	0.631137	0.750571	0.273235	0.0623*	0.5
H1c5k	0.656862	0.554998	0.149783	0.0522*	0.5
H1c6k	0.634538	0.332186	0.168196	0.0637*	0.5
H2c6k	0.588163	0.428553	0.148218	0.0637*	0.5
H3c6k	0.697465	0.400071	0.147789	0.0637*	0.5
H1n1k	0.525908	0.507268	0.360456	0.0437*	0.5
H2n1k	0.585907	0.432462	0.324154	0.0437*	0.5
H3n1k	0.623934	0.477994	0.362521	0.0437*	0.5
O24l	0.3922 (12)	0.7831 (8)	0.2289 (6)	0.0434 (13)	0.5
N1l	0.4348 (19)	0.7623 (13)	0.1123 (7)	0.0364 (13)	0.5
C1l	0.3913 (18)	0.5425 (9)	0.2167 (9)	0.049 (2)	0.5
C2l	0.4197 (14)	0.6859 (10)	0.1484 (5)	0.0356 (14)	0.5
C3l	0.4272 (19)	0.6033 (12)	0.1213 (7)	0.0435 (17)	0.5
C4l	0.413 (2)	0.5318 (11)	0.1561 (9)	0.052 (2)	0.5
C5l	0.3834 (14)	0.6251 (9)	0.2439 (7)	0.0435 (18)	0.5
C6l	0.3708 (18)	0.7993 (12)	0.2917 (6)	0.053 (2)	0.5
C7l	0.3979 (9)	0.6975 (8)	0.2086 (5)	0.0351 (14)	0.5
H1c1l	0.381545	0.492153	0.240328	0.0591*	0.5
H1c3l	0.442054	0.595872	0.079184	0.0522*	0.5
H1c4l	0.418047	0.474179	0.138022	0.0623*	0.5
H1c5l	0.368362	0.632485	0.286029	0.0522*	0.5
H1c6l	0.373599	0.859636	0.300494	0.0637*	0.5
H2c6l	0.308047	0.792321	0.307834	0.0637*	0.5
H3c6l	0.416448	0.756562	0.308756	0.0637*	0.5
H1n1l	0.392089	0.775932	0.090695	0.0437*	0.5
H2n1l	0.429856	0.808812	0.134977	0.0437*	0.5
H3n1l	0.491272	0.74768	0.089654	0.0437*	0.5
O24m	0.5927 (12)	0.2004 (7)	0.3524 (5)	0.0434 (12)	0.5
N1m	0.5324 (19)	0.2950 (12)	0.4541 (7)	0.0364 (12)	0.5
C1m	0.616 (2)	0.0099 (11)	0.4527 (8)	0.0493 (19)	0.5
C2m	0.5613 (13)	0.1961 (9)	0.4538 (5)	0.0356 (14)	0.5
C3m	0.5575 (19)	0.1526 (11)	0.5068 (7)	0.0435 (16)	0.5
C4m	0.585 (2)	0.0592 (11)	0.5056 (8)	0.052 (2)	0.5
C5m	0.6200 (14)	0.0533 (9)	0.3997 (6)	0.0435 (17)	0.5
C6m	0.6232 (18)	0.1538 (10)	0.2956 (6)	0.053 (2)	0.5
C7m	0.5922 (9)	0.1480 (7)	0.4009 (5)	0.0351 (14)	0.5
H1c1m	0.634655	−0.054997	0.452683	0.0591*	0.5
H1c3m	0.536264	0.186818	0.543537	0.0522*	0.5
H1c4m	0.582564	0.028117	0.541918	0.0623*	0.5
H1c5m	0.641449	0.019024	0.363005	0.0522*	0.5
H1c6m	0.615787	0.196979	0.265364	0.0637*	0.5
H2c6m	0.68889	0.121245	0.290257	0.0637*	0.5
H3c6m	0.585135	0.112005	0.293212	0.0637*	0.5
H1n1m	0.569612	0.31713	0.470922	0.0437*	0.5
H2n1m	0.536485	0.312727	0.418126	0.0437*	0.5
H3n1m	0.473901	0.314083	0.473534	0.0437*	0.5
O24n	0.5835 (12)	0.2248 (7)	0.3520 (5)	0.0434 (12)	0.5
N1n	0.5282 (19)	0.2923 (12)	0.4620 (7)	0.0364 (12)	0.5
C1n	0.626 (2)	0.0100 (10)	0.4293 (9)	0.0493 (19)	0.5
C2n	0.5622 (13)	0.1944 (9)	0.4508 (5)	0.0356 (13)	0.5
C3n	0.5658 (19)	0.1375 (11)	0.4979 (6)	0.0435 (16)	0.5
C4n	0.598 (2)	0.0452 (11)	0.4865 (8)	0.052 (2)	0.5
C5n	0.6230 (14)	0.0667 (9)	0.3822 (6)	0.0435 (17)	0.5
C6n	0.6109 (18)	0.1932 (10)	0.2912 (6)	0.053 (2)	0.5
C7n	0.5904 (9)	0.1603 (7)	0.3938 (5)	0.0351 (13)	0.5
H1c1n	0.648436	−0.054331	0.422161	0.0591*	0.5
H1c3n	0.54638	0.161927	0.537648	0.0522*	0.5
H1c4n	0.60073	0.005003	0.518651	0.0623*	0.5
H1c5n	0.642674	0.042237	0.342479	0.0522*	0.5
H1c6n	0.598321	0.243807	0.266441	0.0637*	0.5
H2c6n	0.67758	0.163494	0.282058	0.0637*	0.5
H3c6n	0.574919	0.151413	0.284735	0.0637*	0.5
H1n1n	0.565771	0.310878	0.480485	0.0437*	0.5
H2n1n	0.527893	0.319118	0.428694	0.0437*	0.5
H3n1n	0.470771	0.305223	0.483431	0.0437*	0.5
O24o	1.0798 (17)	0.5427 (18)	0.0076 (6)	0.0434 (13)	0.5
N1o	0.929 (3)	0.681 (3)	0.0421 (9)	0.0364 (13)	0.5
C1o	0.894 (3)	0.432 (3)	−0.0127 (9)	0.049 (2)	0.5
C2o	0.9162 (15)	0.5945 (15)	0.0231 (7)	0.0356 (15)	0.5
C3o	0.825 (3)	0.585 (3)	0.0237 (9)	0.0435 (18)	0.5
C4o	0.815 (3)	0.503 (3)	0.0055 (10)	0.052 (2)	0.5
C5o	0.9845 (18)	0.4406 (19)	−0.0131 (7)	0.0435 (18)	0.5
C6o	1.165 (3)	0.472 (3)	−0.0113 (8)	0.053 (2)	0.5
C7o	0.9950 (7)	0.5237 (6)	0.0053 (5)	0.0351 (15)	0.5
H1c1o	0.885266	0.375094	−0.025242	0.0591*	0.5
H1c3o	0.770567	0.635036	0.036434	0.0522*	0.5
H1c4o	0.75252	0.496014	0.005516	0.0623*	0.5
H1c5o	1.039179	0.390743	−0.025785	0.0522*	0.5
H1c6o	1.219866	0.494183	−0.010585	0.0637*	0.5
H2c6o	1.164754	0.42213	0.01475	0.0637*	0.5
H3c6o	1.168097	0.450829	−0.050562	0.0637*	0.5
H1n1o	0.900107	0.692928	0.078808	0.0437*	0.5
H2n1o	0.988971	0.677351	0.038291	0.0437*	0.5
H3n1o	0.903951	0.723591	0.020536	0.0437*	0.5
Mo1a	0.86614 (5)	0.51382 (4)	0.37349 (3)	0.02031 (17)
Mo2a	0.79126 (8)	0.32862 (7)	0.42017 (5)	0.02338 (18)
Mo3a	0.69788 (8)	0.35455 (7)	0.56717 (5)	0.02366 (19)
Mo4a	0.75855 (8)	0.68570 (7)	0.49410 (5)	0.02353 (18)
Mo5a	0.69624 (8)	0.56496 (7)	0.61221 (5)	0.02499 (19)
P1a	0.88531 (15)	0.44883 (14)	0.50963 (9)	0.0200 (5)
P2a	0.64567 (15)	0.53115 (17)	0.47560 (10)	0.0256 (5)
O1a	0.8254 (4)	0.6222 (4)	0.4210 (2)	0.0228 (16)
O2a	0.7254 (4)	0.3216 (4)	0.3685 (3)	0.032 (2)
O3a	0.8633 (4)	0.2231 (4)	0.4218 (3)	0.0315 (19)
O4a	0.7032 (5)	0.7886 (4)	0.4731 (3)	0.0351 (19)
O5a	0.9538 (4)	0.4153 (4)	0.5531 (2)	0.0247 (16)
O6a	0.9779 (4)	0.5189 (4)	0.3378 (3)	0.0274 (17)
O7a	0.7659 (5)	0.5845 (5)	0.6584 (3)	0.0339 (19)
O8a	0.7369 (3)	0.4786 (3)	0.4320 (2)	0.0218 (15)
O9a	0.5599 (4)	0.5097 (4)	0.4569 (3)	0.0298 (18)
O10a	0.7357 (4)	0.4330 (3)	0.6172 (2)	0.0242 (15)
O11a	0.8151 (3)	0.5391 (3)	0.5338 (2)	0.0221 (14)
O12a	0.6875 (4)	0.3307 (4)	0.4882 (2)	0.0271 (18)
O13a	0.8008 (4)	0.5393 (4)	0.3208 (3)	0.0311 (19)
O14a	0.9444 (3)	0.4672 (4)	0.4510 (2)	0.0212 (14)
O15a	0.6466 (4)	0.5009 (3)	0.5399 (2)	0.0233 (15)
O16a	0.5850 (4)	0.3588 (4)	0.6034 (3)	0.033 (2)
O17a	0.8360 (3)	0.3729 (3)	0.5047 (2)	0.0209 (14)
O18a	0.8854 (4)	0.3832 (4)	0.3744 (2)	0.0275 (18)
O19a	0.7630 (5)	0.2509 (4)	0.5852 (3)	0.034 (2)
O20a	0.8535 (4)	0.7089 (4)	0.5174 (3)	0.0292 (18)
O21a	0.6801 (4)	0.6750 (4)	0.5706 (2)	0.0293 (18)
O22a	0.6407 (4)	0.6314 (4)	0.4715 (3)	0.0274 (17)
O23a	0.5831 (5)	0.5856 (4)	0.6545 (3)	0.037 (2)
Mo1b	0.33515 (12)	0.10535 (10)	−0.10590 (6)	0.02031 (18)	0.567 (2)
Mo2b	0.29590 (12)	−0.09900 (11)	−0.12710 (8)	0.02338 (18)	0.567 (2)
Mo3b	0.23039 (12)	−0.18659 (13)	0.00580 (8)	0.0237 (2)	0.567 (2)
Mo4b	0.23100 (14)	0.16836 (12)	0.05051 (9)	0.02353 (18)	0.567 (2)
Mo5b	0.20970 (13)	−0.02944 (13)	0.11226 (9)	0.02499 (19)	0.567 (2)
P1b	0.38974 (16)	−0.05211 (15)	−0.00819 (10)	0.0200 (5)	0.567 (2)
P2b	0.13747 (17)	0.0379 (2)	−0.01849 (13)	0.0256 (5)	0.567 (2)
O1b	0.2903 (4)	0.1670 (4)	−0.0312 (2)	0.0228 (16)	0.567 (2)
O2b	0.2221 (5)	−0.0702 (5)	−0.1761 (3)	0.032 (2)	0.567 (2)
O3b	0.3808 (5)	−0.1928 (4)	−0.1573 (3)	0.031 (2)	0.567 (2)
O4b	0.1589 (5)	0.2746 (4)	0.0637 (3)	0.035 (2)	0.567 (2)
O5b	0.4699 (4)	−0.1115 (4)	0.0208 (2)	0.0247 (17)	0.567 (2)
O6b	0.4367 (4)	0.1403 (4)	−0.1318 (3)	0.0274 (17)	0.567 (2)
O7b	0.2845 (5)	−0.0428 (5)	0.1607 (3)	0.0339 (19)	0.567 (2)
O8b	0.2251 (4)	0.0258 (3)	−0.0704 (2)	0.0218 (16)	0.567 (2)
O9b	0.0527 (4)	0.0289 (4)	−0.0442 (3)	0.0298 (18)	0.567 (2)
O10b	0.2669 (4)	−0.1508 (4)	0.0754 (2)	0.0242 (16)	0.567 (2)
O11b	0.3138 (3)	0.0091 (3)	0.0396 (2)	0.0221 (15)	0.567 (2)
O12b	0.2077 (4)	−0.1509 (4)	−0.0706 (3)	0.0271 (18)	0.567 (2)
O13b	0.2573 (5)	0.1643 (4)	−0.1454 (3)	0.031 (2)	0.567 (2)
O14b	0.4334 (3)	0.0096 (4)	−0.0514 (2)	0.0212 (14)	0.567 (2)
O15b	0.1552 (4)	−0.0364 (4)	0.0276 (2)	0.0233 (16)	0.567 (2)
O16b	0.1266 (5)	−0.2136 (5)	0.0352 (3)	0.033 (2)	0.567 (2)
O17b	0.3506 (4)	−0.1190 (3)	−0.0383 (2)	0.0209 (15)	0.567 (2)
O18b	0.3716 (4)	−0.0126 (4)	−0.1464 (2)	0.0275 (18)	0.567 (2)
O19b	0.3115 (5)	−0.2909 (4)	−0.0099 (3)	0.034 (2)	0.567 (2)
O20b	0.3254 (4)	0.1760 (4)	0.0810 (3)	0.0292 (19)	0.567 (2)
O21b	0.1709 (4)	0.0998 (4)	0.1110 (3)	0.0293 (18)	0.567 (2)
O22b	0.1184 (4)	0.1312 (4)	0.0100 (3)	0.0274 (18)	0.567 (2)
O23b	0.1046 (5)	−0.0460 (5)	0.1521 (3)	0.037 (2)	0.567 (2)

Atomic displacement parameters (Å²) top

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
Mo1bx	0.0210 (3)	0.0230 (3)	0.0162 (2)	−0.0051 (2)	−0.00310 (18)	0.0016 (2)
Mo4bx	0.0240 (3)	0.0229 (3)	0.0205 (3)	−0.0029 (2)	−0.0013 (2)	0.0009 (2)
Mo5bx	0.0293 (3)	0.0267 (3)	0.0164 (3)	−0.0093 (2)	0.0041 (2)	−0.0036 (2)
Mo3bx	0.0228 (3)	0.0278 (3)	0.0190 (3)	−0.0084 (2)	0.0015 (2)	−0.0015 (2)
Mo2bx	0.0252 (3)	0.0296 (3)	0.0157 (3)	−0.0078 (2)	−0.0039 (2)	0.0008 (2)
P1bx	0.0196 (7)	0.0263 (7)	0.0139 (7)	−0.0070 (6)	−0.0017 (6)	0.0005 (6)
P2bx	0.0171 (7)	0.0349 (9)	0.0232 (8)	−0.0057 (6)	−0.0016 (6)	−0.0008 (7)
O3bx	0.034 (3)	0.033 (3)	0.027 (3)	−0.010 (2)	−0.003 (2)	−0.007 (2)
O5bx	0.028 (2)	0.027 (2)	0.022 (3)	−0.0078 (19)	−0.011 (2)	0.001 (2)
O14bx	0.0165 (19)	0.029 (2)	0.016 (2)	−0.0049 (16)	0.0003 (16)	0.0009 (18)
O15bx	0.022 (2)	0.028 (2)	0.017 (2)	−0.0054 (19)	0.0009 (18)	−0.0043 (19)
O1bx	0.026 (3)	0.028 (2)	0.018 (2)	−0.0123 (19)	−0.0035 (19)	0.0021 (18)
O6bx	0.032 (3)	0.030 (3)	0.021 (2)	−0.008 (2)	−0.0068 (19)	0.007 (2)
O23bx	0.047 (3)	0.034 (3)	0.024 (3)	−0.014 (2)	0.008 (2)	−0.004 (2)
O17bx	0.026 (2)	0.028 (2)	0.011 (2)	−0.0126 (18)	−0.0019 (18)	0.0024 (18)
O18bx	0.031 (3)	0.027 (3)	0.024 (2)	0.000 (2)	−0.013 (2)	−0.004 (2)
O11bx	0.019 (2)	0.032 (2)	0.013 (2)	−0.0061 (18)	0.0007 (16)	0.0005 (18)
O10bx	0.029 (2)	0.024 (2)	0.017 (2)	−0.0079 (19)	0.0029 (19)	0.0011 (18)
O13bx	0.031 (3)	0.035 (3)	0.029 (3)	−0.007 (2)	−0.012 (2)	0.004 (2)
O7bx	0.048 (3)	0.036 (3)	0.019 (2)	−0.020 (2)	0.000 (2)	−0.003 (2)
O19bx	0.028 (3)	0.038 (3)	0.034 (3)	−0.009 (2)	−0.003 (2)	−0.002 (2)
O16bx	0.033 (3)	0.036 (3)	0.030 (3)	−0.015 (2)	0.000 (2)	0.002 (2)
O20bx	0.038 (3)	0.026 (2)	0.022 (3)	−0.010 (2)	0.001 (2)	0.000 (2)
O12bx	0.024 (3)	0.034 (3)	0.024 (3)	−0.010 (2)	−0.002 (2)	−0.003 (2)
O21bx	0.028 (3)	0.027 (3)	0.029 (3)	−0.005 (2)	0.000 (2)	−0.007 (2)
O4bx	0.043 (3)	0.026 (3)	0.032 (3)	−0.007 (2)	−0.002 (2)	0.004 (2)
O2bx	0.035 (3)	0.038 (3)	0.025 (3)	−0.012 (2)	−0.008 (2)	−0.005 (2)
O22bx	0.016 (2)	0.028 (2)	0.019 (2)	−0.0074 (18)	0.0028 (18)	−0.0012 (19)
O9bx	0.020 (2)	0.039 (3)	0.029 (3)	−0.007 (2)	−0.005 (2)	0.003 (2)
O8bx	0.018 (2)	0.033 (3)	0.029 (3)	−0.004 (2)	−0.003 (2)	−0.002 (2)
O24a	0.0464 (18)	0.0466 (19)	0.0339 (16)	−0.0068 (15)	−0.0067 (13)	−0.0006 (13)
N1a	0.0326 (17)	0.0444 (19)	0.0318 (17)	−0.0114 (14)	−0.0032 (14)	−0.0031 (14)
C1a	0.046 (3)	0.039 (3)	0.060 (3)	−0.009 (2)	−0.006 (2)	−0.011 (2)
C2a	0.0291 (18)	0.043 (2)	0.036 (2)	−0.0129 (16)	−0.0039 (15)	−0.0058 (17)
C3a	0.041 (2)	0.049 (3)	0.040 (2)	−0.0126 (19)	−0.0050 (19)	0.001 (2)
C4a	0.059 (3)	0.044 (3)	0.053 (3)	−0.013 (2)	−0.011 (2)	0.002 (2)
C5a	0.039 (2)	0.055 (3)	0.036 (2)	−0.015 (2)	−0.0052 (18)	−0.006 (2)
C6a	0.056 (3)	0.061 (4)	0.036 (2)	−0.007 (3)	−0.005 (2)	−0.002 (2)
C7a	0.0275 (18)	0.041 (2)	0.034 (2)	−0.0072 (16)	−0.0025 (15)	−0.0065 (17)
O24b	0.0373 (18)	0.0379 (16)	0.052 (3)	−0.0047 (12)	−0.0075 (16)	0.0030 (15)
N1b	0.038 (2)	0.0340 (16)	0.033 (3)	−0.0023 (13)	−0.0074 (17)	0.0032 (15)
C1b	0.068 (4)	0.036 (3)	0.047 (4)	−0.016 (2)	−0.013 (3)	−0.001 (2)
C2b	0.043 (2)	0.0331 (19)	0.027 (3)	−0.0039 (15)	−0.0065 (19)	0.0016 (17)
C3b	0.043 (3)	0.043 (2)	0.042 (3)	−0.0066 (18)	−0.011 (2)	0.004 (2)
C4b	0.052 (3)	0.049 (3)	0.057 (4)	−0.015 (2)	−0.014 (3)	−0.002 (2)
C5b	0.046 (3)	0.039 (2)	0.038 (3)	0.0000 (18)	−0.006 (2)	0.001 (2)
C6b	0.043 (3)	0.044 (3)	0.066 (5)	−0.001 (2)	−0.009 (3)	0.006 (3)
C7b	0.042 (2)	0.0291 (19)	0.031 (3)	−0.0043 (15)	−0.0057 (19)	0.0047 (17)
O24c	0.050 (2)	0.0368 (17)	0.0416 (17)	−0.0105 (14)	−0.0047 (14)	−0.0037 (12)
N1c	0.032 (2)	0.0367 (19)	0.0391 (17)	−0.0068 (15)	−0.0046 (14)	−0.0065 (13)
C1c	0.047 (3)	0.067 (3)	0.034 (2)	−0.014 (3)	−0.009 (2)	−0.001 (2)
C2c	0.027 (2)	0.042 (2)	0.0374 (19)	−0.0082 (17)	−0.0059 (15)	−0.0065 (15)
C3c	0.040 (3)	0.042 (3)	0.047 (2)	−0.007 (2)	−0.0065 (18)	−0.0028 (18)
C4c	0.058 (4)	0.052 (3)	0.047 (2)	−0.012 (3)	−0.015 (2)	0.005 (2)
C5c	0.038 (3)	0.044 (3)	0.047 (2)	−0.010 (2)	−0.006 (2)	−0.0107 (19)
C6c	0.062 (4)	0.041 (3)	0.051 (3)	−0.011 (2)	−0.002 (3)	−0.008 (2)
C7c	0.029 (2)	0.041 (2)	0.033 (2)	−0.0089 (17)	−0.0013 (15)	−0.0068 (15)
O24d	0.052 (3)	0.0460 (19)	0.0342 (16)	−0.0158 (18)	−0.0082 (16)	−0.0004 (14)
N1d	0.033 (3)	0.0441 (19)	0.0326 (18)	−0.0101 (18)	−0.0079 (17)	−0.0036 (14)
C1d	0.046 (4)	0.038 (2)	0.062 (3)	−0.007 (2)	−0.011 (3)	−0.011 (2)
C2d	0.027 (3)	0.042 (2)	0.037 (2)	−0.007 (2)	−0.0064 (19)	−0.0063 (17)
C3d	0.042 (3)	0.049 (2)	0.040 (3)	−0.012 (2)	−0.011 (2)	0.000 (2)
C4d	0.057 (4)	0.044 (3)	0.053 (3)	−0.009 (3)	−0.011 (3)	0.002 (2)
C5d	0.038 (4)	0.055 (3)	0.037 (2)	−0.011 (3)	−0.006 (2)	−0.007 (2)
C6d	0.067 (5)	0.060 (3)	0.037 (3)	−0.023 (3)	−0.011 (3)	−0.001 (2)
C7d	0.031 (3)	0.041 (2)	0.035 (2)	−0.012 (2)	−0.0071 (19)	−0.0065 (17)
O24e	0.052 (3)	0.0387 (17)	0.0425 (16)	−0.0168 (16)	−0.0110 (16)	0.0063 (12)
N1e	0.035 (3)	0.0354 (18)	0.0409 (16)	−0.0099 (17)	−0.0108 (15)	0.0095 (13)
C1e	0.044 (4)	0.064 (3)	0.036 (2)	−0.011 (3)	−0.003 (2)	0.007 (2)
C2e	0.028 (3)	0.040 (2)	0.0397 (18)	−0.0084 (19)	−0.0093 (17)	0.0100 (15)
C3e	0.044 (4)	0.040 (3)	0.047 (2)	−0.010 (2)	−0.012 (2)	0.0063 (17)
C4e	0.054 (4)	0.052 (3)	0.047 (2)	−0.012 (3)	−0.004 (2)	−0.002 (2)
C5e	0.040 (4)	0.044 (3)	0.050 (2)	−0.015 (2)	−0.012 (2)	0.0136 (19)
C6e	0.069 (5)	0.044 (3)	0.053 (3)	−0.022 (3)	−0.016 (3)	0.012 (2)
C7e	0.033 (3)	0.040 (2)	0.0349 (19)	−0.0107 (19)	−0.0114 (18)	0.0110 (15)
O24f	0.052 (3)	0.0374 (17)	0.0434 (18)	−0.0144 (16)	−0.0133 (17)	0.0071 (13)
N1f	0.033 (3)	0.0355 (18)	0.0411 (18)	−0.0085 (16)	−0.0101 (17)	0.0091 (13)
C1f	0.046 (4)	0.065 (3)	0.034 (2)	−0.012 (3)	−0.006 (2)	0.007 (2)
C2f	0.027 (3)	0.041 (2)	0.039 (2)	−0.0082 (18)	−0.0076 (19)	0.0094 (16)
C3f	0.042 (3)	0.040 (3)	0.048 (2)	−0.009 (2)	−0.012 (2)	0.0057 (18)
C4f	0.056 (4)	0.052 (3)	0.045 (2)	−0.013 (3)	−0.006 (2)	−0.001 (2)
C5f	0.039 (4)	0.043 (3)	0.050 (3)	−0.013 (2)	−0.011 (2)	0.014 (2)
C6f	0.068 (5)	0.042 (3)	0.055 (3)	−0.018 (3)	−0.020 (3)	0.013 (2)
C7f	0.032 (3)	0.040 (2)	0.036 (2)	−0.0096 (18)	−0.0116 (19)	0.0105 (16)
O24g	0.051 (3)	0.0438 (18)	0.0340 (16)	−0.0085 (16)	−0.0085 (16)	−0.0003 (12)
N1g	0.033 (3)	0.0457 (19)	0.0304 (17)	−0.0087 (16)	−0.0083 (17)	0.0015 (13)
C1g	0.048 (4)	0.053 (3)	0.050 (3)	−0.018 (2)	−0.012 (3)	0.019 (2)
C2g	0.027 (3)	0.047 (2)	0.033 (2)	−0.0095 (17)	−0.0072 (19)	0.0049 (15)
C3g	0.043 (3)	0.049 (2)	0.040 (2)	−0.011 (2)	−0.011 (2)	0.0004 (18)
C4g	0.058 (4)	0.048 (3)	0.052 (3)	−0.018 (3)	−0.010 (3)	0.004 (2)
C5g	0.038 (3)	0.058 (3)	0.034 (2)	−0.010 (2)	−0.007 (2)	0.0016 (18)
C6g	0.065 (5)	0.055 (3)	0.036 (2)	−0.009 (3)	−0.012 (3)	−0.002 (2)
C7g	0.031 (3)	0.044 (2)	0.030 (2)	−0.0064 (17)	−0.0090 (19)	0.0061 (15)
O24h	0.049 (2)	0.049 (2)	0.0341 (16)	−0.0170 (18)	−0.0054 (14)	0.0019 (14)
N1h	0.031 (2)	0.044 (2)	0.0321 (18)	−0.0087 (17)	−0.0044 (15)	0.0047 (15)
C1h	0.047 (3)	0.042 (3)	0.060 (3)	−0.014 (2)	−0.011 (2)	0.016 (2)
C2h	0.027 (2)	0.042 (2)	0.036 (2)	−0.0064 (19)	−0.0071 (16)	0.0084 (18)
C3h	0.039 (3)	0.049 (3)	0.040 (3)	−0.010 (2)	−0.005 (2)	0.001 (2)
C4h	0.058 (3)	0.044 (3)	0.053 (3)	−0.012 (3)	−0.011 (3)	0.003 (2)
C5h	0.038 (3)	0.056 (3)	0.036 (2)	−0.011 (2)	−0.007 (2)	0.009 (2)
C6h	0.060 (4)	0.064 (4)	0.036 (3)	−0.024 (3)	−0.003 (2)	0.002 (2)
C7h	0.028 (2)	0.043 (3)	0.034 (2)	−0.0117 (19)	−0.0054 (16)	0.0081 (18)
O24i	0.048 (2)	0.0375 (18)	0.0433 (18)	−0.0124 (15)	−0.0045 (15)	0.0057 (14)
N1i	0.0324 (19)	0.038 (2)	0.0400 (18)	−0.0118 (16)	−0.0076 (15)	0.0088 (14)
C1i	0.047 (3)	0.067 (4)	0.033 (3)	−0.015 (3)	−0.007 (2)	0.004 (2)
C2i	0.028 (2)	0.043 (2)	0.037 (2)	−0.0102 (17)	−0.0096 (16)	0.0096 (17)
C3i	0.041 (2)	0.044 (3)	0.047 (2)	−0.014 (2)	−0.0086 (19)	0.005 (2)
C4i	0.059 (3)	0.053 (4)	0.045 (3)	−0.016 (3)	−0.012 (2)	0.000 (2)
C5i	0.039 (3)	0.045 (3)	0.048 (3)	−0.013 (2)	−0.011 (2)	0.014 (2)
C6i	0.059 (4)	0.043 (3)	0.055 (3)	−0.017 (3)	−0.003 (3)	0.010 (2)
C7i	0.0280 (19)	0.041 (2)	0.035 (2)	−0.0095 (17)	−0.0040 (16)	0.0083 (17)
O24j	0.0470 (19)	0.0374 (18)	0.0443 (19)	−0.0120 (15)	−0.0045 (15)	0.0060 (14)
N1j	0.0332 (18)	0.038 (2)	0.040 (2)	−0.0129 (15)	−0.0089 (15)	0.0088 (15)
C1j	0.047 (3)	0.068 (4)	0.033 (3)	−0.016 (3)	−0.006 (2)	0.004 (2)
C2j	0.0294 (19)	0.043 (2)	0.037 (2)	−0.0121 (17)	−0.0110 (16)	0.0096 (17)
C3j	0.041 (2)	0.043 (3)	0.048 (3)	−0.014 (2)	−0.010 (2)	0.005 (2)
C4j	0.059 (3)	0.052 (3)	0.045 (3)	−0.015 (3)	−0.010 (2)	−0.001 (2)
C5j	0.040 (2)	0.046 (3)	0.048 (3)	−0.014 (2)	−0.012 (2)	0.014 (2)
C6j	0.058 (3)	0.043 (3)	0.057 (3)	−0.016 (2)	−0.003 (3)	0.010 (2)
C7j	0.0282 (18)	0.042 (2)	0.036 (2)	−0.0110 (16)	−0.0053 (16)	0.0087 (17)
O24k	0.051 (3)	0.0439 (18)	0.0340 (16)	−0.0087 (16)	−0.0090 (16)	0.0003 (12)
N1k	0.033 (2)	0.0455 (18)	0.0306 (18)	−0.0085 (15)	−0.0084 (17)	0.0024 (13)
C1k	0.048 (4)	0.051 (3)	0.052 (3)	−0.017 (2)	−0.012 (3)	0.019 (2)
C2k	0.027 (3)	0.047 (2)	0.033 (2)	−0.0090 (17)	−0.0070 (19)	0.0056 (15)
C3k	0.042 (3)	0.049 (2)	0.040 (2)	−0.011 (2)	−0.012 (2)	0.0009 (18)
C4k	0.058 (4)	0.048 (3)	0.052 (3)	−0.019 (3)	−0.010 (3)	0.004 (2)
C5k	0.038 (3)	0.057 (3)	0.034 (2)	−0.010 (2)	−0.007 (2)	0.0028 (19)
C6k	0.065 (5)	0.056 (3)	0.036 (3)	−0.009 (3)	−0.013 (3)	−0.001 (2)
C7k	0.031 (3)	0.043 (2)	0.031 (2)	−0.0058 (17)	−0.0089 (19)	0.0068 (15)
O24l	0.049 (2)	0.049 (2)	0.0338 (16)	−0.0170 (18)	−0.0059 (14)	0.0019 (14)
N1l	0.0314 (19)	0.044 (2)	0.0316 (18)	−0.0078 (17)	−0.0042 (15)	0.0041 (15)
C1l	0.047 (3)	0.042 (3)	0.059 (3)	−0.014 (2)	−0.010 (2)	0.016 (2)
C2l	0.027 (2)	0.042 (2)	0.035 (2)	−0.0052 (19)	−0.0063 (16)	0.0078 (18)
C3l	0.040 (3)	0.049 (3)	0.040 (3)	−0.010 (2)	−0.005 (2)	0.001 (2)
C4l	0.059 (3)	0.044 (3)	0.053 (3)	−0.013 (3)	−0.011 (3)	0.003 (2)
C5l	0.038 (3)	0.055 (3)	0.035 (2)	−0.009 (2)	−0.0070 (19)	0.008 (2)
C6l	0.060 (4)	0.065 (4)	0.036 (2)	−0.023 (3)	−0.004 (2)	0.001 (2)
C7l	0.028 (2)	0.043 (3)	0.034 (2)	−0.0106 (19)	−0.0046 (16)	0.0077 (18)
O24m	0.0466 (18)	0.0415 (19)	0.0387 (18)	−0.0049 (14)	−0.0081 (14)	−0.0048 (13)
N1m	0.0310 (18)	0.0371 (19)	0.0392 (19)	−0.0072 (14)	−0.0038 (14)	−0.0062 (13)
C1m	0.046 (3)	0.034 (3)	0.067 (3)	−0.008 (2)	−0.012 (2)	0.005 (2)
C2m	0.0276 (18)	0.035 (2)	0.045 (2)	−0.0094 (15)	−0.0050 (16)	−0.0049 (16)
C3m	0.039 (2)	0.046 (3)	0.043 (3)	−0.0093 (19)	−0.0050 (19)	−0.0028 (18)
C4m	0.059 (3)	0.046 (3)	0.051 (3)	−0.014 (2)	−0.010 (2)	0.006 (2)
C5m	0.038 (2)	0.043 (3)	0.048 (3)	−0.010 (2)	−0.0058 (19)	−0.0105 (19)
C6m	0.056 (3)	0.051 (3)	0.045 (3)	−0.002 (3)	−0.008 (2)	−0.010 (2)
C7m	0.0272 (18)	0.033 (2)	0.043 (2)	−0.0040 (16)	−0.0064 (16)	−0.0052 (16)
O24n	0.0461 (18)	0.0437 (19)	0.0367 (17)	−0.0053 (15)	−0.0072 (13)	−0.0041 (13)
N1n	0.0313 (17)	0.0397 (19)	0.0365 (19)	−0.0086 (14)	−0.0031 (14)	−0.0060 (14)
C1n	0.046 (3)	0.033 (3)	0.067 (3)	−0.007 (2)	−0.010 (2)	−0.001 (2)
C2n	0.0280 (18)	0.037 (2)	0.042 (2)	−0.0104 (15)	−0.0043 (15)	−0.0061 (16)
C3n	0.040 (2)	0.047 (3)	0.042 (3)	−0.0105 (19)	−0.0046 (19)	−0.0020 (19)
C4n	0.059 (3)	0.045 (3)	0.052 (3)	−0.013 (2)	−0.011 (2)	0.005 (2)
C5n	0.038 (2)	0.047 (3)	0.044 (3)	−0.011 (2)	−0.0048 (19)	−0.011 (2)
C6n	0.055 (3)	0.056 (3)	0.041 (3)	−0.003 (3)	−0.006 (2)	−0.009 (2)
C7n	0.0270 (17)	0.035 (2)	0.041 (2)	−0.0047 (16)	−0.0048 (15)	−0.0066 (17)
O24o	0.0399 (18)	0.0359 (14)	0.050 (3)	−0.0051 (11)	−0.0049 (16)	0.0000 (14)
N1o	0.041 (2)	0.0312 (15)	0.033 (3)	−0.0034 (12)	−0.0078 (17)	0.0022 (15)
C1o	0.066 (3)	0.041 (3)	0.048 (4)	−0.022 (2)	−0.017 (3)	0.001 (2)
C2o	0.046 (2)	0.0317 (18)	0.027 (3)	−0.0063 (14)	−0.0092 (19)	0.0020 (16)
C3o	0.045 (3)	0.041 (2)	0.043 (3)	−0.0063 (17)	−0.010 (2)	0.004 (2)
C4o	0.050 (3)	0.051 (3)	0.057 (4)	−0.016 (2)	−0.014 (3)	−0.002 (2)
C5o	0.051 (3)	0.036 (2)	0.037 (4)	−0.0024 (17)	−0.007 (2)	0.000 (2)
C6o	0.047 (3)	0.039 (2)	0.064 (5)	−0.0018 (18)	−0.005 (3)	0.001 (2)
C7o	0.045 (2)	0.0276 (18)	0.031 (3)	−0.0069 (14)	−0.0069 (18)	0.0038 (16)
Mo1a	0.0210 (3)	0.0230 (3)	0.0162 (2)	−0.0051 (2)	−0.00309 (18)	0.0016 (2)
Mo2a	0.0252 (3)	0.0296 (3)	0.0157 (3)	−0.0078 (2)	−0.0039 (2)	0.0008 (2)
Mo3a	0.0228 (3)	0.0278 (3)	0.0190 (3)	−0.0084 (2)	0.0015 (2)	−0.0015 (2)
Mo4a	0.0240 (3)	0.0229 (3)	0.0205 (3)	−0.0029 (2)	−0.0013 (2)	0.0009 (2)
Mo5a	0.0293 (3)	0.0267 (3)	0.0164 (3)	−0.0093 (2)	0.0041 (2)	−0.0036 (2)
P1a	0.0196 (7)	0.0263 (7)	0.0139 (7)	−0.0070 (6)	−0.0017 (6)	0.0005 (6)
P2a	0.0171 (7)	0.0349 (9)	0.0232 (8)	−0.0057 (6)	−0.0016 (6)	−0.0008 (7)
O1a	0.026 (3)	0.028 (2)	0.018 (2)	−0.0123 (19)	−0.0035 (19)	0.0021 (18)
O2a	0.035 (3)	0.038 (3)	0.025 (3)	−0.012 (2)	−0.008 (2)	−0.005 (2)
O3a	0.034 (3)	0.033 (3)	0.027 (3)	−0.010 (2)	−0.003 (2)	−0.007 (2)
O4a	0.043 (3)	0.026 (3)	0.032 (3)	−0.007 (2)	−0.002 (2)	0.004 (2)
O5a	0.028 (2)	0.027 (2)	0.022 (3)	−0.0078 (19)	−0.011 (2)	0.001 (2)
O6a	0.032 (3)	0.030 (3)	0.021 (2)	−0.008 (2)	−0.0068 (19)	0.007 (2)
O7a	0.048 (3)	0.036 (3)	0.019 (2)	−0.020 (2)	0.000 (2)	−0.003 (2)
O8a	0.016 (2)	0.028 (2)	0.019 (2)	−0.0074 (18)	0.0028 (18)	−0.0012 (19)
O9a	0.020 (2)	0.039 (3)	0.029 (3)	−0.007 (2)	−0.005 (2)	0.003 (2)
O10a	0.029 (2)	0.024 (2)	0.017 (2)	−0.0079 (19)	0.0029 (19)	0.0011 (18)
O11a	0.019 (2)	0.032 (2)	0.013 (2)	−0.0061 (18)	0.0007 (16)	0.0005 (18)
O12a	0.024 (3)	0.034 (3)	0.024 (3)	−0.010 (2)	−0.002 (2)	−0.003 (2)
O13a	0.031 (3)	0.035 (3)	0.028 (3)	−0.007 (2)	−0.012 (2)	0.004 (2)
O14a	0.0165 (19)	0.029 (2)	0.016 (2)	−0.0049 (16)	0.0003 (16)	0.0009 (18)
O15a	0.022 (2)	0.028 (2)	0.017 (2)	−0.0054 (19)	0.0009 (18)	−0.0043 (19)
O16a	0.033 (3)	0.036 (3)	0.030 (3)	−0.015 (2)	0.000 (2)	0.002 (2)
O17a	0.026 (2)	0.028 (2)	0.011 (2)	−0.0126 (18)	−0.0019 (18)	0.0024 (18)
O18a	0.031 (3)	0.027 (3)	0.024 (2)	0.000 (2)	−0.013 (2)	−0.004 (2)
O19a	0.028 (3)	0.038 (3)	0.034 (3)	−0.009 (2)	−0.003 (2)	−0.002 (2)
O20a	0.038 (3)	0.026 (2)	0.022 (3)	−0.010 (2)	0.001 (2)	0.000 (2)
O21a	0.028 (3)	0.027 (3)	0.029 (3)	−0.005 (2)	0.000 (2)	−0.007 (2)
O22a	0.018 (2)	0.033 (3)	0.029 (3)	−0.004 (2)	−0.003 (2)	−0.002 (2)
O23a	0.047 (3)	0.034 (3)	0.024 (3)	−0.014 (2)	0.008 (2)	−0.004 (2)
Mo1b	0.0212 (3)	0.0209 (3)	0.0187 (3)	−0.0055 (2)	−0.00384 (19)	0.0041 (2)
Mo2b	0.0258 (3)	0.0267 (3)	0.0190 (3)	−0.0083 (2)	−0.0061 (2)	0.0067 (2)
Mo3b	0.0250 (3)	0.0276 (3)	0.0195 (3)	−0.0117 (2)	−0.0013 (2)	0.0032 (2)
Mo4b	0.0241 (3)	0.0224 (3)	0.0216 (3)	−0.0046 (2)	−0.0006 (2)	0.0021 (2)
Mo5b	0.0321 (3)	0.0278 (3)	0.0157 (3)	−0.0135 (2)	0.0007 (2)	0.0027 (2)
P1b	0.0208 (7)	0.0238 (8)	0.0168 (8)	−0.0084 (6)	−0.0040 (6)	0.0058 (6)
P2b	0.0183 (7)	0.0341 (10)	0.0248 (9)	−0.0091 (6)	−0.0029 (6)	0.0052 (6)
O1b	0.027 (3)	0.024 (3)	0.021 (2)	−0.012 (2)	−0.0076 (19)	0.0054 (17)
O2b	0.036 (3)	0.040 (3)	0.023 (3)	−0.013 (2)	−0.010 (2)	0.003 (2)
O3b	0.036 (3)	0.038 (3)	0.022 (3)	−0.013 (2)	−0.005 (2)	−0.001 (2)
O4b	0.043 (3)	0.025 (3)	0.034 (3)	−0.008 (2)	−0.001 (2)	0.000 (2)
O5b	0.027 (2)	0.027 (3)	0.022 (3)	−0.005 (2)	−0.011 (2)	0.0030 (19)
O6b	0.031 (3)	0.023 (3)	0.028 (3)	−0.006 (2)	−0.0083 (19)	0.0085 (19)
O7b	0.052 (3)	0.035 (3)	0.020 (3)	−0.022 (2)	−0.007 (2)	0.0055 (19)
O8b	0.018 (2)	0.028 (3)	0.020 (2)	−0.0118 (18)	0.0000 (18)	0.0037 (18)
O9b	0.021 (3)	0.035 (3)	0.034 (3)	−0.009 (2)	−0.006 (2)	0.007 (2)
O10b	0.031 (2)	0.022 (3)	0.019 (2)	−0.0107 (19)	0.0004 (19)	0.0039 (17)
O11b	0.021 (2)	0.028 (3)	0.018 (2)	−0.0093 (18)	−0.0020 (17)	0.0084 (17)
O12b	0.026 (3)	0.035 (3)	0.023 (3)	−0.013 (2)	−0.005 (2)	0.003 (2)
O13b	0.030 (3)	0.032 (3)	0.032 (3)	−0.004 (2)	−0.011 (2)	0.005 (2)
O14b	0.0178 (19)	0.026 (2)	0.020 (2)	−0.0079 (17)	−0.0014 (16)	0.0067 (17)
O15b	0.024 (2)	0.030 (3)	0.016 (2)	−0.0092 (19)	−0.0005 (18)	0.0029 (18)
O16b	0.037 (3)	0.034 (3)	0.032 (3)	−0.018 (3)	−0.005 (2)	0.004 (2)
O17b	0.028 (2)	0.022 (2)	0.016 (2)	−0.0126 (18)	−0.0071 (18)	0.0083 (17)
O18b	0.028 (3)	0.032 (3)	0.020 (3)	0.001 (2)	−0.008 (2)	−0.001 (2)
O19b	0.030 (3)	0.040 (3)	0.032 (3)	−0.012 (2)	−0.005 (2)	0.001 (2)
O20b	0.039 (3)	0.026 (3)	0.022 (3)	−0.012 (2)	−0.002 (2)	0.002 (2)
O21b	0.030 (3)	0.034 (3)	0.023 (3)	−0.009 (2)	0.000 (2)	−0.004 (2)
O22b	0.019 (2)	0.035 (3)	0.027 (3)	−0.007 (2)	−0.002 (2)	0.001 (2)
O23b	0.052 (3)	0.036 (3)	0.023 (3)	−0.020 (3)	0.003 (2)	0.003 (2)

Geometric parameters (Å, º) top

Mo1bx—O1bx	1.897 (8)	O24h—C7l	1.079 (17)
Mo1bx—O6bx	1.712 (13)	N1h—C2h	1.46 (2)
Mo1bx—O18bx	1.937 (10)	N1h—H1n1h	0.87 (6)
Mo1bx—O13bx	1.694 (14)	N1h—H2n1h	0.87 (5)
Mo1bx—Mo1b	0.427 (2)	N1h—N1l	0.25 (3)
Mo1bx—O1b	1.598 (5)	N1h—C2l	1.44 (2)
Mo1bx—O6b	1.724 (6)	N1h—H1n1l	0.80 (6)
Mo1bx—O13b	1.606 (7)	C1h—C4h	1.38 (3)
Mo4bx—O1bx	1.919 (9)	C1h—C5h	1.39 (2)
Mo4bx—O20bx	1.722 (16)	C1h—H1c1h	0.96
Mo4bx—O21bx	1.944 (10)	C1h—C1l	0.38 (3)
Mo4bx—O4bx	1.697 (11)	C1h—C4l	1.10 (3)
Mo4bx—Mo4b	0.211 (3)	C1h—H1c1l	0.988
Mo4bx—O1b	1.929 (5)	C2h—C3h	1.39 (2)
Mo4bx—O4b	1.895 (6)	C2h—C7h	1.373 (17)
Mo4bx—O20b	1.625 (8)	C2h—N1l	1.53 (3)
Mo4bx—O21b	1.893 (6)	C2h—C2l	0.291 (19)
Mo5bx—O23bx	1.716 (14)	C2h—C3l	1.12 (3)
Mo5bx—O10bx	1.959 (8)	C3h—C4h	1.38 (3)
Mo5bx—O7bx	1.712 (17)	C3h—H1c3h	0.96
Mo5bx—O21bx	1.913 (7)	C3h—C3l	0.33 (2)
Mo5bx—Mo5b	0.342 (3)	C3h—C4l	1.42 (3)
Mo5bx—O7b	1.950 (8)	C3h—H1c3l	0.7268
Mo5bx—O10b	1.698 (5)	C4h—H1c4h	0.96
Mo5bx—O15b	2.028 (6)	C4h—C3l	1.43 (3)
Mo5bx—O21b	2.132 (6)	C4h—C4l	0.37 (3)
Mo5bx—O23b	1.728 (7)	C4h—H1c4l	0.6897
Mo3bx—O10bx	1.935 (11)	C5h—C7h	1.401 (19)
Mo3bx—O19bx	1.730 (11)	C5h—H1c5h	0.96
Mo3bx—O16bx	1.698 (15)	C5h—C1l	1.04 (2)
Mo3bx—O12bx	1.922 (10)	C5h—C5l	0.37 (2)
Mo3bx—Mo3b	0.461 (2)	C5h—C7l	1.52 (2)
Mo3bx—O12b	1.738 (6)	C6h—H1c6h	0.96
Mo3bx—O16b	2.044 (7)	C6h—H2c6h	0.96
Mo3bx—O17b	2.078 (6)	C6h—H3c6h	0.96
Mo3bx—O19b	1.481 (6)	C6h—O24l	1.281 (19)
Mo2bx—O3bx	1.701 (10)	C6h—C6l	0.41 (3)
Mo2bx—O18bx	1.923 (12)	C6h—H2c6l	0.8114
Mo2bx—O12bx	1.960 (13)	C7h—C2l	1.166 (17)
Mo2bx—O2bx	1.717 (16)	C7h—C5l	1.358 (19)
Mo2bx—Mo2b	0.346 (3)	C7h—C7l	0.325 (19)
Mo2bx—O2b	1.493 (8)	H1c1h—H1c1l	0.4102
Mo2bx—O3b	1.822 (6)	H1c3h—H1c3l	0.3333
Mo2bx—O18b	1.753 (7)	H1c4h—H1c4l	0.4068
P1bx—O5bx	1.569 (14)	H1c5h—C5l	0.7522
P1bx—O14bx	1.525 (13)	H1c5h—H1c5l	0.3978
P1bx—O17bx	1.532 (13)	H1c6h—C6l	0.6592
P1bx—O11bx	1.537 (8)	H1c6h—H1c6l	0.4299
P1bx—P1b	0.176 (5)	H2c6h—H2c6l	0.4678
P1bx—O14b	1.352 (8)	H3c6h—C6l	0.951
P1bx—O17b	1.582 (8)	H3c6h—H3c6l	0.3824
P2bx—O15bx	1.560 (9)	H1n1h—H1n1l	0.28 (6)
P2bx—O22bx	1.562 (14)	H2n1h—N1l	0.65 (5)
P2bx—O9bx	1.535 (10)	H2n1h—H2n1l	0.23 (6)
P2bx—O8bx	1.519 (11)	O24i—C6i	1.44 (2)
P2bx—P2b	0.157 (6)	O24i—C7i	1.372 (18)
P2bx—O8b	1.471 (7)	O24i—O24j	0.402 (17)
P2bx—O9b	1.451 (9)	O24i—C7j	1.102 (19)
O3bx—Mo2b	1.662 (10)	N1i—C2i	1.46 (2)
O3bx—O3b	0.645 (16)	N1i—H1n1i	0.87 (5)
O5bx—P1b	1.514 (13)	N1i—H2n1i	0.87 (4)
O5bx—O5b	0.347 (16)	N1i—N1j	0.33 (2)
O14bx—Mo1b	2.151 (11)	N1i—C2j	1.38 (2)
O14bx—O14b	0.218 (13)	N1i—H1n1j	0.68 (5)
O15bx—Mo3b	2.053 (6)	C1i—C4i	1.38 (3)
O15bx—P2b	1.533 (7)	C1i—C5i	1.39 (3)
O15bx—O15b	0.383 (9)	C1i—H1c1i	0.96
O1bx—Mo4b	1.924 (9)	C1i—C1j	0.35 (4)
O1bx—O1b	0.547 (15)	C1i—C4j	1.22 (3)
O6bx—Mo1b	1.764 (14)	C1i—H1c1j	0.9213
O6bx—O6b	0.317 (16)	C2i—C3i	1.39 (2)
O23bx—Mo5b	1.794 (14)	C2i—C7i	1.373 (18)
O23bx—O23b	0.47 (2)	C2i—C2j	0.291 (17)
O17bx—Mo2b	2.107 (9)	C2i—C3j	1.11 (2)
O17bx—P1b	1.523 (12)	C2i—C7j	1.567 (17)
O17bx—O17b	0.380 (11)	C3i—C4i	1.38 (2)
O18bx—Mo1b	1.544 (11)	C3i—H1c3i	0.96
O18bx—Mo2b	2.147 (12)	C3i—C3j	0.30 (3)
O18bx—O18b	0.648 (12)	C3i—C4j	1.33 (3)
O11bx—P1b	1.444 (7)	C3i—H1c3j	0.809
O11bx—O11b	0.244 (8)	C4i—H1c4i	0.96
O10bx—Mo3b	1.726 (12)	C4i—C3j	1.50 (3)
O10bx—O10b	0.330 (10)	C4i—C4j	0.36 (4)
O13bx—Mo1b	1.941 (13)	C4i—H1c4j	0.7152
O13bx—O13b	0.724 (15)	C5i—C7i	1.401 (19)
O7bx—Mo5b	1.487 (16)	C5i—H1c5i	0.96
O7bx—O7b	0.29 (2)	C5i—C1j	1.08 (2)
O19bx—Mo3b	2.050 (11)	C5i—C5j	0.31 (2)
O19bx—O19b	0.540 (15)	C5i—C7j	1.543 (18)
O16bx—Mo3b	1.464 (16)	C6i—H1c6i	0.96
O16bx—O16b	0.629 (15)	C6i—H2c6i	0.96
O20bx—Mo4b	1.813 (16)	C6i—H3c6i	0.96
O20bx—O20b	0.486 (14)	C6i—O24j	1.32 (2)
O12bx—Mo2b	1.681 (13)	C6i—C6j	0.45 (2)
O12bx—O12b	0.571 (11)	C6i—H2c6j	0.7224
O21bx—Mo4b	1.992 (10)	C7i—C2j	1.225 (18)
O21bx—Mo5b	1.768 (8)	C7i—C5j	1.313 (19)
O21bx—O21b	0.533 (15)	C7i—C7j	0.316 (15)
O4bx—Mo4b	1.492 (11)	H1c1i—H1c1j	0.3989
O4bx—O4b	0.465 (17)	H1c3i—H1c3j	0.2971
O2bx—Mo2b	1.944 (16)	H1c4i—H1c4j	0.4287
O2bx—O2b	0.477 (15)	H1c5i—C5j	0.8152
O22bx—P2b	1.513 (13)	H1c5i—H1c5j	0.3174
O22bx—O8b	1.398 (11)	H1c6i—C6j	0.7461
O22bx—O22b	1.433 (10)	H1c6i—H1c6j	0.5292
O9bx—P2b	1.489 (9)	H2c6i—H2c6j	0.4962
O9bx—O9b	1.277 (17)	H3c6i—C6j	0.8535
O8bx—O8b	1.393 (13)	H3c6i—H3c6j	0.3611
O1w—O1w'	0.63 (5)	H1n1i—H1n1j	0.38 (6)
O2w—O2w'	0.71 (6)	H2n1i—N1j	0.58 (5)
O24a—C6a	1.441 (9)	H2n1i—H2n1j	0.38 (6)
O24a—C7a	1.372 (9)	O24j—C6j	1.44 (2)
N1a—C2a	1.462 (11)	O24j—C7j	1.372 (17)
N1a—H1n1a	0.87 (5)	N1j—C2j	1.46 (2)
N1a—H2n1a	0.87 (4)	N1j—H1n1j	0.87 (5)
C1a—C4a	1.381 (15)	N1j—H2n1j	0.87 (4)
C1a—C5a	1.386 (12)	C1j—C4j	1.38 (3)
C1a—H1c1a	0.96	C1j—C5j	1.39 (2)
C2a—C3a	1.387 (12)	C1j—H1c1j	0.96
C2a—C7a	1.373 (11)	C2j—C3j	1.39 (2)
C3a—C4a	1.382 (13)	C2j—C7j	1.373 (18)
C3a—H1c3a	0.96	C3j—C4j	1.38 (2)
C4a—H1c4a	0.96	C3j—H1c3j	0.96
C5a—C7a	1.401 (11)	C4j—H1c4j	0.96
C5a—H1c5a	0.96	C5j—C7j	1.401 (18)
C6a—H1c6a	0.96	C5j—H1c5j	0.96
C6a—H2c6a	0.96	C6j—H1c6j	0.96
C6a—H3c6a	0.96	C6j—H2c6j	0.96
O24b—C2bⁱ	1.32 (5)	C6j—H3c6j	0.96
O24b—C3bⁱ	0.89 (5)	O24k—C6k	1.44 (2)
O24b—C4bⁱ	1.12 (8)	O24k—C7k	1.372 (18)
O24b—C6b	1.44 (5)	N1k—C2k	1.46 (2)
O24b—C7b	1.37 (4)	N1k—H1n1k	0.87 (5)
N1b—C2b	1.46 (7)	N1k—H2n1k	0.87 (4)
N1b—C5bⁱ	0.76 (6)	C1k—C4k	1.38 (3)
N1b—H1c5bⁱ	0.3454	C1k—C5k	1.39 (3)
N1b—H1n1b	0.87 (6)	C1k—H1c1k	0.96
N1b—H2n1b	0.87 (10)	C2k—C3k	1.39 (3)
C1b—C4b	1.38 (8)	C2k—C7k	1.373 (17)
C1b—C5b	1.39 (8)	C3k—C4k	1.38 (3)
C1b—H1c1b	0.96	C3k—H1c3k	0.96
C2b—C3b	1.39 (6)	C4k—H1c4k	0.96
C2b—C5bⁱ	1.19 (5)	C5k—C7k	1.401 (19)
C2b—C7b	1.37 (2)	C5k—H1c5k	0.96
C2b—C7bⁱ	0.74 (3)	C6k—H1c6k	0.96
C3b—C4b	1.38 (8)	C6k—H2c6k	0.96
C3b—C6bⁱ	0.65 (5)	C6k—H3c6k	0.96
C3b—H1c3b	0.96	O24l—C6l	1.44 (2)
C4b—H1c4b	0.96	O24l—C7l	1.372 (18)
C5b—C7b	1.40 (3)	N1l—C2l	1.46 (2)
C5b—H1c5b	0.96	N1l—H1n1l	0.87 (6)
C5b—H2n1bⁱ	0.99 (8)	N1l—H2n1l	0.87 (5)
C6b—H1c3bⁱ	0.4713	C1l—C4l	1.38 (3)
C6b—H1c6b	0.96	C1l—C5l	1.39 (2)
C6b—H2c6b	0.96	C1l—H1c1l	0.96
C6b—H3c6b	0.96	C2l—C3l	1.39 (2)
C7b—C7bⁱ	0.705 (13)	C2l—C7l	1.373 (17)
H1c3b—H2c6bⁱ	0.6223	C3l—C4l	1.38 (3)
H1c5b—H1n1bⁱ	0.5574	C3l—H1c3l	0.96
O24c—C6c	1.441 (12)	C4l—H1c4l	0.96
O24c—C7c	1.372 (10)	C5l—C7l	1.40 (2)
N1c—C2c	1.462 (15)	C5l—H1c5l	0.96
N1c—H1n1c	0.87 (6)	C6l—H1c6l	0.96
N1c—H2n1c	0.87 (4)	C6l—H2c6l	0.96
C1c—C4c	1.381 (19)	C6l—H3c6l	0.96
C1c—C5c	1.386 (16)	O24m—C6m	1.441 (18)
C1c—H1c1c	0.96	O24m—C7m	1.372 (17)
C2c—C3c	1.387 (14)	O24m—O24n	0.365 (15)
C2c—C7c	1.373 (11)	O24m—C6n	1.390 (19)
C3c—C4c	1.382 (17)	O24m—C7n	1.131 (17)
C3c—H1c3c	0.96	N1m—C2m	1.46 (2)
C4c—H1c4c	0.96	N1m—H1n1m	0.87 (6)
C5c—C7c	1.401 (12)	N1m—H2n1m	0.87 (5)
C5c—H1c5c	0.96	N1m—N1n	0.19 (2)
C6c—H1c6c	0.96	N1m—C2n	1.49 (2)
C6c—H2c6c	0.96	N1m—H2n1n	0.73 (5)
C6c—H3c6c	0.96	C1m—C4m	1.38 (3)
O24d—C6d	1.441 (11)	C1m—C5m	1.39 (2)
O24d—C7d	1.372 (9)	C1m—H1c1m	0.96
N1d—C2d	1.462 (14)	C1m—C1n	0.54 (3)
N1d—H1n1d	0.87 (5)	C1m—C4n	0.91 (3)
N1d—H2n1d	0.87 (4)	C2m—C3m	1.39 (2)
C1d—C4d	1.381 (19)	C2m—C7m	1.373 (17)
C1d—C5d	1.386 (14)	C2m—N1n	1.43 (2)
C1d—H1c1d	0.96	C2m—C2n	0.072 (18)
C2d—C3d	1.387 (14)	C2m—C3n	1.35 (2)
C2d—C7d	1.373 (11)	C2m—C7n	1.444 (17)
C3d—C4d	1.382 (15)	C3m—C4m	1.38 (2)
C3d—H1c3d	0.96	C3m—H1c3m	0.96
C4d—H1c4d	0.96	C3m—C2n	1.43 (2)
C5d—C7d	1.401 (11)	C3m—C3n	0.30 (2)
C5d—H1c5d	0.96	C3m—H1c3n	0.7107
C6d—H1c6d	0.96	C4m—H1c4m	0.96
C6d—H2c6d	0.96	C4m—C3n	1.18 (2)
C6d—H3c6d	0.96	C4m—C4n	0.48 (3)
O24e—C6e	1.44 (2)	C4m—H1c4n	0.8707
O24e—C7e	1.372 (15)	C5m—C7m	1.401 (17)
O24e—O24f	0.444 (14)	C5m—H1c5m	0.96
O24e—C6f	1.40 (2)	C5m—C1n	0.95 (2)
N1e—C2e	1.46 (2)	C5m—C5n	0.45 (2)
N1e—H1n1e	0.87 (7)	C6m—H1c6m	0.96
N1e—H2n1e	0.87 (5)	C6m—H2c6m	0.96
N1e—N1f	0.67 (3)	C6m—H3c6m	0.96
N1e—H1n1f	0.75 (5)	C6m—C6n	0.60 (2)
C1e—C4e	1.38 (3)	C6m—H2c6n	0.852
C1e—C5e	1.39 (2)	C6m—H3c6n	0.8146
C1e—H1c1e	0.96	C7m—C2n	1.303 (16)
C1e—C1f	0.59 (3)	C7m—C5n	1.261 (17)
C1e—C5f	1.03 (2)	C7m—C7n	0.249 (16)
C2e—C3e	1.39 (2)	H1c1m—H1c1n	0.6993
C2e—C7e	1.373 (18)	H1c3m—H1c3n	0.3898
C2e—N1f	1.26 (2)	H1c4m—H1c4n	0.6248
C2e—C2f	0.461 (17)	H1c5m—C5n	0.815
C2e—C7f	1.328 (18)	H1c5m—H1c5n	0.5917
C3e—C4e	1.38 (2)	H1c6m—C6n	0.5957
C3e—H1c3e	0.96	H1c6m—H1c6n	0.6989
C3e—C2f	1.02 (2)	H2c6m—H2c6n	0.6626
C3e—C3f	0.42 (2)	H3c6m—H3c6n	0.6239
C4e—H1c4e	0.96	H1n1m—N1n	0.84 (6)
C4e—C1f	1.33 (3)	H1n1m—H1n1n	0.26 (6)
C4e—C3f	1.15 (2)	H2n1m—H2n1n	0.28 (6)
C4e—C4f	0.45 (3)	O24n—C6n	1.441 (18)
C5e—C7e	1.401 (17)	O24n—C7n	1.372 (16)
C5e—H1c5e	0.96	N1n—C2n	1.46 (2)
C5e—C5f	0.55 (2)	N1n—H1n1n	0.87 (6)
C5e—C7f	1.142 (18)	N1n—H2n1n	0.87 (5)
C5e—H1c5f	1.021	C1n—C4n	1.38 (3)
C6e—H1c6e	0.96	C1n—C5n	1.39 (2)
C6e—H2c6e	0.96	C1n—H1c1n	0.96
C6e—H3c6e	0.96	C2n—C3n	1.39 (2)
C6e—C6f	0.47 (2)	C2n—C7n	1.373 (16)
C6e—H1c6f	0.5045	C3n—C4n	1.38 (2)
C7e—O24f	0.956 (15)	C3n—H1c3n	0.96
C7e—C2f	1.534 (16)	C4n—H1c4n	0.96
C7e—C7f	0.427 (14)	C5n—C7n	1.401 (17)
H1c1e—C1f	0.8986	C5n—H1c5n	0.96
H1c1e—H1c1f	0.7592	C6n—H1c6n	0.96
H1c3e—C3f	0.9386	C6n—H2c6n	0.96
H1c3e—H1c3f	0.4889	C6n—H3c6n	0.96
H1c4e—C4f	0.5858	O24o—C1oⁱⁱ	0.65 (6)
H1c4e—H1c4f	0.4701	O24o—C4oⁱⁱ	1.51 (5)
H1c5e—H1c5f	0.665	O24o—C5oⁱⁱ	0.90 (3)
H1c6e—H1c6f	0.467	O24o—C6o	1.44 (4)
H2c6e—C6f	0.7948	O24o—C7o	1.37 (3)
H2c6e—H2c6f	0.4598	N1o—C2o	1.46 (5)
H3c6e—C6f	1.0063	N1o—H1n1o	0.87 (5)
H3c6e—H3c6f	0.6338	N1o—H2n1o	0.87 (7)
H1n1e—H1n1f	0.73 (7)	C1o—C4o	1.38 (6)
H2n1e—H2n1f	0.73 (6)	C1o—C5o	1.39 (6)
O24f—C6f	1.441 (19)	C1o—C6oⁱⁱ	1.56 (5)
O24f—C7f	1.372 (15)	C1o—H1c1o	0.96
N1f—C2f	1.46 (2)	C2o—C3o	1.39 (4)
N1f—H1n1f	0.87 (6)	C2o—C5oⁱⁱ	1.41 (3)
N1f—H2n1f	0.87 (5)	C2o—C7o	1.37 (2)
C1f—C4f	1.38 (3)	C2o—H1c5oⁱⁱ	0.7728
C1f—C5f	1.39 (2)	C3o—C4o	1.38 (7)
C1f—H1c1f	0.96	C3o—C6oⁱⁱ	0.88 (5)
C2f—C3f	1.387 (19)	C3o—H1c3o	0.96
C2f—C7f	1.373 (17)	C3o—H2c6oⁱⁱ	0.8673
C3f—C4f	1.38 (2)	C3o—H3c6oⁱⁱ	0.8408
C3f—H1c3f	0.96	C4o—C6oⁱⁱ	0.58 (7)
C4f—H1c4f	0.96	C4o—H1c4o	0.96
C5f—C7f	1.401 (16)	C4o—H1c6oⁱⁱ	0.4922
C5f—H1c5f	0.96	C5o—C7o	1.40 (3)
C6f—H1c6f	0.96	C5o—C7oⁱⁱ	0.74 (3)
C6f—H2c6f	0.96	C5o—H1c5o	0.96
C6f—H3c6f	0.96	C6o—H1c6o	0.96
O24g—C6g	1.44 (2)	C6o—H2c6o	0.96
O24g—C7g	1.372 (17)	C6o—H3c6o	0.96
O24g—O24k	0.358 (16)	C7o—C7oⁱⁱ	0.731 (14)
O24g—C6k	1.26 (2)	H1c4o—H1c6oⁱⁱ	0.5119
N1g—C2g	1.46 (2)	Mo1a—O1a	1.898 (5)
N1g—H1n1g	0.87 (5)	Mo1a—O6a	1.712 (5)
N1g—H2n1g	0.87 (4)	Mo1a—O13a	1.695 (7)
N1g—N1k	0.26 (3)	Mo1a—O18a	1.942 (6)
N1g—C2k	1.52 (2)	Mo2a—O2a	1.717 (7)
N1g—H2n1k	0.67 (4)	Mo2a—O3a	1.701 (5)
C1g—C4g	1.38 (3)	Mo2a—O12a	1.960 (5)
C1g—C5g	1.39 (2)	Mo2a—O18a	1.929 (6)
C1g—H1c1g	0.96	Mo3a—O10a	1.936 (6)
C1g—C1k	0.45 (3)	Mo3a—O12a	1.922 (6)
C1g—C5k	0.99 (3)	Mo3a—O16a	1.697 (6)
C2g—C3g	1.39 (2)	Mo3a—O19a	1.730 (6)
C2g—C7g	1.373 (17)	Mo4a—O1a	1.919 (5)
C2g—N1k	1.46 (2)	Mo4a—O4a	1.696 (6)
C2g—C2k	0.33 (2)	Mo4a—O20a	1.724 (7)
C2g—C7k	1.130 (17)	Mo4a—O21a	1.943 (5)
C3g—C4g	1.38 (3)	Mo5a—O7a	1.712 (8)
C3g—H1c3g	0.96	Mo5a—O10a	1.961 (5)
C3g—C2k	1.10 (2)	Mo5a—O21a	1.913 (6)
C3g—C3k	0.36 (3)	Mo5a—O23a	1.716 (6)
C3g—C4k	1.41 (3)	P1a—O5a	1.569 (7)
C4g—H1c4g	0.96	P1a—O11a	1.537 (5)
C4g—C1k	1.03 (3)	P1a—O14a	1.524 (5)
C4g—C3k	1.46 (3)	P1a—O17a	1.534 (6)
C4g—C4k	0.42 (3)	P2a—O8a	1.556 (5)
C5g—C7g	1.401 (19)	P2a—O9a	1.534 (7)
C5g—H1c5g	0.96	P2a—O15a	1.560 (5)
C5g—C5k	0.44 (2)	P2a—O22a	1.517 (6)
C5g—C7k	1.372 (19)	Mo1b—O1b	1.898 (5)
C5g—H1c5k	0.7209	Mo1b—O6b	1.712 (7)
C6g—H1c6g	0.96	Mo1b—O13b	1.695 (7)
C6g—H2c6g	0.96	Mo1b—O18b	1.942 (6)
C6g—H3c6g	0.96	Mo2b—O2b	1.717 (7)
C6g—C6k	0.43 (2)	Mo2b—O3b	1.701 (6)
C6g—H1c6k	0.5852	Mo2b—O12b	1.960 (6)
C6g—H3c6k	1.0302	Mo2b—O18b	1.929 (7)
C7g—O24k	1.040 (18)	Mo3b—O10b	1.936 (6)
C7g—C5k	1.537 (19)	Mo3b—O12b	1.922 (6)
C7g—C7k	0.369 (16)	Mo3b—O16b	1.697 (7)
H1c1g—C1k	1.0369	Mo3b—O19b	1.730 (6)
H1c1g—H1c1k	0.4991	Mo4b—O1b	1.919 (5)
H1c3g—C3k	0.6632	Mo4b—O4b	1.696 (6)
H1c3g—H1c3k	0.3586	Mo4b—O20b	1.724 (8)
H1c4g—C4k	0.6612	Mo4b—O21b	1.943 (6)
H1c4g—H1c4k	0.451	Mo5b—O7b	1.712 (8)
H1c5g—H1c5k	0.4779	Mo5b—O10b	1.961 (5)
H1c6g—H1c6k	0.4329	Mo5b—O21b	1.913 (6)
H2c6g—C6k	0.8591	Mo5b—O23b	1.716 (7)
H2c6g—H2c6k	0.4866	P1b—O5b	1.569 (6)
H3c6g—H3c6k	0.4395	P1b—O11b	1.537 (5)
H1n1g—N1k	0.83 (6)	P1b—O14b	1.524 (6)
H1n1g—H1n1k	0.28 (7)	P1b—O17b	1.534 (6)
H2n1g—H2n1k	0.24 (6)	P2b—O8b	1.556 (5)
O24h—C6h	1.441 (19)	P2b—O9b	1.534 (8)
O24h—C7h	1.372 (17)	P2b—O15b	1.560 (6)
O24h—O24l	0.34 (2)	P2b—O22b	1.517 (7)

O1bx—Mo1bx—O6bx	98.8 (7)	C6j—O24j—C7j	117.1 (12)
O1bx—Mo1bx—O18bx	145.9 (5)	N1i—N1j—H2n1i	143 (9)
O1bx—Mo1bx—O13bx	106.3 (6)	N1i—N1j—C2j	70 (4)
O1bx—Mo1bx—Mo1b	130.4 (5)	N1i—N1j—H1n1j	45 (5)
O1bx—Mo1bx—O1b	15.1 (5)	N1i—N1j—H2n1j	163 (8)
O1bx—Mo1bx—O6b	99.7 (5)	H2n1i—N1j—C2j	122 (5)
O1bx—Mo1bx—O13b	130.7 (4)	H2n1i—N1j—H1n1j	104 (6)
O6bx—Mo1bx—O18bx	97.4 (7)	H2n1i—N1j—H2n1j	20 (6)
O6bx—Mo1bx—O13bx	101.4 (7)	C2j—N1j—H1n1j	111 (3)
O6bx—Mo1bx—Mo1b	90.0 (6)	C2j—N1j—H2n1j	118 (3)
O6bx—Mo1bx—O1b	113.6 (6)	H1n1j—N1j—H2n1j	120 (5)
O6bx—Mo1bx—O6b	10.6 (5)	C1i—C1j—C5i	147 (6)
O6bx—Mo1bx—O13b	100.2 (6)	C1i—C1j—C4j	55 (4)
O18bx—Mo1bx—O13bx	99.6 (6)	C1i—C1j—C5j	149 (6)
O18bx—Mo1bx—Mo1b	20.2 (5)	C1i—C1j—H1c1j	73.15
O18bx—Mo1bx—O1b	139.1 (4)	C5i—C1j—C4j	118.9 (17)
O18bx—Mo1bx—O6b	91.2 (5)	C5i—C1j—C5j	2.1 (11)
O18bx—Mo1bx—O13b	74.9 (4)	C5i—C1j—H1c1j	121.44
O13bx—Mo1bx—Mo1b	119.6 (7)	C4j—C1j—C5j	120.8 (15)
O13bx—Mo1bx—O1b	99.5 (5)	C4j—C1j—H1c1j	119.6
O13bx—Mo1bx—O6b	111.0 (5)	C5j—C1j—H1c1j	119.6
O13bx—Mo1bx—O13b	25.2 (6)	N1i—C2j—C2i	100 (4)
Mo1b—Mo1bx—O1b	129.5 (4)	N1i—C2j—C7i	139.5 (16)
Mo1b—Mo1bx—O6b	81.3 (4)	N1i—C2j—N1j	13.1 (9)
Mo1b—Mo1bx—O13b	94.6 (4)	N1i—C2j—C3j	108.7 (13)
O1b—Mo1bx—O6b	114.8 (3)	N1i—C2j—C7j	129.5 (14)
O1b—Mo1bx—O13b	121.7 (3)	C2i—C2j—C7i	115 (4)
O6b—Mo1bx—O13b	106.9 (3)	C2i—C2j—N1j	112 (4)
O1bx—Mo4bx—O20bx	102.4 (6)	C2i—C2j—C3j	14 (5)
O1bx—Mo4bx—O21bx	147.0 (6)	C2i—C2j—C7j	127 (4)
O1bx—Mo4bx—O4bx	100.0 (7)	C7i—C2j—N1j	130.6 (14)
O1bx—Mo4bx—Mo4b	88.2 (9)	C7i—C2j—C3j	109.7 (14)
O1bx—Mo4bx—O1b	16.3 (4)	C7i—C2j—C7j	12.4 (7)
O1bx—Mo4bx—O4b	95.6 (4)	N1j—C2j—C3j	119.4 (13)
O1bx—Mo4bx—O20b	86.2 (5)	N1j—C2j—C7j	119.3 (12)
O1bx—Mo4bx—O21b	161.8 (4)	C3j—C2j—C7j	121.2 (14)
O20bx—Mo4bx—O21bx	103.7 (7)	C2i—C3j—C3i	160 (7)
O20bx—Mo4bx—O4bx	105.3 (8)	C2i—C3j—C4i	131.2 (17)
O20bx—Mo4bx—Mo4b	112.5 (11)	C2i—C3j—C2j	3.6 (11)
O20bx—Mo4bx—O1b	118.6 (5)	C2i—C3j—C4j	120.5 (18)
O20bx—Mo4bx—O4b	94.1 (5)	C2i—C3j—H1c3j	118.78
O20bx—Mo4bx—O20b	16.4 (5)	C3i—C3j—C4i	60 (5)
O20bx—Mo4bx—O21b	89.1 (5)	C3i—C3j—C2j	158 (7)
O21bx—Mo4bx—O4bx	92.2 (5)	C3i—C3j—C4j	73 (5)
O21bx—Mo4bx—Mo4b	100.0 (9)	C3i—C3j—H1c3j	51.32
O21bx—Mo4bx—O1b	132.3 (5)	C4i—C3j—C2j	128.9 (15)
O21bx—Mo4bx—O4b	102.2 (3)	C4i—C3j—C4j	13.4 (16)
O21bx—Mo4bx—O20b	118.1 (5)	C4i—C3j—H1c3j	109.78
O21bx—Mo4bx—O21b	15.9 (5)	C2j—C3j—C4j	118.7 (16)
O4bx—Mo4bx—Mo4b	12.6 (10)	C2j—C3j—H1c3j	120.64
O4bx—Mo4bx—O1b	96.7 (6)	C4j—C3j—H1c3j	120.64
O4bx—Mo4bx—O4b	13.5 (6)	C1i—C4j—C3i	141.2 (18)
O4bx—Mo4bx—O20b	110.5 (6)	C1i—C4j—C4i	110 (5)
O4bx—Mo4bx—O21b	90.3 (5)	C1i—C4j—C1j	13.6 (15)
Mo4b—Mo4bx—O1b	84.1 (8)	C1i—C4j—C3j	131.0 (18)
Mo4b—Mo4bx—O4b	18.8 (9)	C1i—C4j—H1c4j	108.6
Mo4b—Mo4bx—O20b	114.4 (10)	C3i—C4j—C4i	91 (5)
Mo4b—Mo4bx—O21b	100.5 (9)	C3i—C4j—C1j	132.1 (17)
O1b—Mo4bx—O4b	96.1 (3)	C3i—C4j—C3j	12.3 (12)
O1b—Mo4bx—O20b	102.3 (3)	C3i—C4j—H1c4j	108.05
O1b—Mo4bx—O21b	148.1 (3)	C4i—C4j—C1j	123 (5)
O4b—Mo4bx—O20b	97.7 (3)	C4i—C4j—C3j	103 (5)
O4b—Mo4bx—O21b	97.6 (3)	C4i—C4j—H1c4j	38.38
O20b—Mo4bx—O21b	104.3 (3)	C1j—C4j—C3j	120.6 (17)
O23bx—Mo5bx—O10bx	104.5 (7)	C1j—C4j—H1c4j	119.69
O23bx—Mo5bx—O7bx	104.7 (8)	C3j—C4j—H1c4j	119.69
O23bx—Mo5bx—O21bx	95.8 (6)	C5i—C5j—C7i	100 (4)
O23bx—Mo5bx—Mo5b	97.6 (8)	C5i—C5j—H1c5i	108.88
O23bx—Mo5bx—O7b	109.0 (6)	C5i—C5j—C1j	7 (4)
O23bx—Mo5bx—O10b	100.7 (6)	C5i—C5j—C7j	112 (4)
O23bx—Mo5bx—O15b	85.1 (6)	C5i—C5j—H1c5j	127.16
O23bx—Mo5bx—O21b	98.0 (6)	C7i—C5j—H1c5i	150.76
O23bx—Mo5bx—O23b	15.6 (7)	C7i—C5j—C1j	106.4 (14)
O10bx—Mo5bx—O7bx	96.6 (6)	C7i—C5j—C7j	12.9 (7)
O10bx—Mo5bx—O21bx	146.8 (5)	C7i—C5j—H1c5j	132.67
O10bx—Mo5bx—Mo5b	139.5 (6)	H1c5i—C5j—C1j	102.36
O10bx—Mo5bx—O7b	98.1 (4)	H1c5i—C5j—C7j	139.08
O10bx—Mo5bx—O10b	6.3 (3)	H1c5i—C5j—H1c5j	18.37
O10bx—Mo5bx—O15b	79.5 (4)	C1j—C5j—C7j	118.6 (14)
O10bx—Mo5bx—O21b	154.1 (3)	C1j—C5j—H1c5j	120.72
O10bx—Mo5bx—O23b	115.2 (4)	C7j—C5j—H1c5j	120.72
O7bx—Mo5bx—O21bx	103.4 (7)	C6i—C6j—H1c6i	104.45
O7bx—Mo5bx—Mo5b	44.4 (7)	C6i—C6j—H3c6i	89.56
O7bx—Mo5bx—O7b	5.2 (7)	C6i—C6j—O24j	66 (3)
O7bx—Mo5bx—O10b	92.9 (6)	C6i—C6j—H1c6j	137.58
O7bx—Mo5bx—O15b	170.1 (5)	C6i—C6j—H2c6j	45.65
O7bx—Mo5bx—O21b	89.6 (6)	C6i—C6j—H3c6j	111.53
O7bx—Mo5bx—O23b	91.7 (6)	H1c6i—C6j—H3c6i	157.01
O21bx—Mo5bx—Mo5b	60.3 (6)	H1c6i—C6j—O24j	101.42
O21bx—Mo5bx—O7b	99.8 (5)	H1c6i—C6j—H1c6j	33.23
O21bx—Mo5bx—O10b	153.1 (5)	H1c6i—C6j—H2c6j	82.95
O21bx—Mo5bx—O15b	76.4 (5)	H1c6i—C6j—H3c6j	139.57
O21bx—Mo5bx—O21b	13.8 (5)	H3c6i—C6j—O24j	100.91
O21bx—Mo5bx—O23b	90.6 (4)	H3c6i—C6j—H1c6j	131.02
Mo5b—Mo5bx—O7b	42.1 (5)	H3c6i—C6j—H2c6j	94.68
Mo5b—Mo5bx—O10b	136.8 (6)	H3c6i—C6j—H3c6j	21.97
Mo5b—Mo5bx—O15b	136.6 (5)	O24j—C6j—H1c6j	109.47
Mo5b—Mo5bx—O21b	46.5 (5)	O24j—C6j—H2c6j	109.47
Mo5b—Mo5bx—O23b	82.3 (5)	O24j—C6j—H3c6j	109.47
O7b—Mo5bx—O10b	94.7 (3)	H1c6j—C6j—H2c6j	109.47
O7b—Mo5bx—O15b	165.8 (3)	H1c6j—C6j—H3c6j	109.47
O7b—Mo5bx—O21b	86.2 (3)	H2c6j—C6j—H3c6j	109.47
O7b—Mo5bx—O23b	95.5 (3)	O24i—C7j—C2i	118.7 (13)
O10b—Mo5bx—O15b	84.0 (3)	O24i—C7j—C5i	136.8 (14)
O10b—Mo5bx—O21b	159.8 (3)	O24i—C7j—C7i	145 (4)
O10b—Mo5bx—O23b	110.4 (3)	O24i—C7j—O24j	13.9 (10)
O15b—Mo5bx—O21b	90.1 (2)	O24i—C7j—C2j	111.4 (13)
O15b—Mo5bx—O23b	98.2 (3)	O24i—C7j—C5j	126.5 (14)
O21b—Mo5bx—O23b	89.6 (3)	C2i—C7j—C5i	101.2 (10)
O10bx—Mo3bx—O19bx	93.1 (7)	C2i—C7j—C7i	48 (3)
O10bx—Mo3bx—O16bx	99.7 (7)	C2i—C7j—O24j	122.6 (11)
O10bx—Mo3bx—O12bx	150.4 (5)	C2i—C7j—C2j	8.5 (8)
O10bx—Mo3bx—Mo3b	56.7 (5)	C2i—C7j—C5j	111.9 (11)
O10bx—Mo3bx—O12b	141.5 (3)	C5i—C7j—C7i	58 (3)
O10bx—Mo3bx—O16b	88.2 (4)	C5i—C7j—O24j	136.1 (12)
O10bx—Mo3bx—O17b	77.7 (4)	C5i—C7j—C2j	109.4 (11)
O10bx—Mo3bx—O19b	93.5 (4)	C5i—C7j—C5j	10.7 (9)
O19bx—Mo3bx—O16bx	103.2 (7)	C7i—C7j—O24j	158 (4)
O19bx—Mo3bx—O12bx	103.2 (7)	C7i—C7j—C2j	56 (3)
O19bx—Mo3bx—Mo3b	128.8 (7)	C7i—C7j—C5j	68 (3)
O19bx—Mo3bx—O12b	119.8 (7)	O24j—C7j—C2j	114.5 (12)
O19bx—Mo3bx—O16b	115.4 (5)	O24j—C7j—C5j	125.5 (12)
O19bx—Mo3bx—O17b	89.1 (5)	C2j—C7j—C5j	120.1 (12)
O19bx—Mo3bx—O19b	17.2 (5)	C1i—H1c1j—H1c1i	83.25
O16bx—Mo3bx—O12bx	100.3 (8)	C1i—H1c1j—C1j	21.14
O16bx—Mo3bx—Mo3b	52.5 (7)	H1c1i—H1c1j—C1j	104.09
O16bx—Mo3bx—O12b	91.9 (6)	C3i—H1c3j—H1c3i	111.85
O16bx—Mo3bx—O16b	16.2 (6)	C3i—H1c3j—C3j	16.56
O16bx—Mo3bx—O17b	167.6 (5)	H1c3i—H1c3j—C3j	128.3
O16bx—Mo3bx—O19b	86.1 (6)	C4i—H1c4j—H1c4i	111.67
O12bx—Mo3bx—Mo3b	123.4 (5)	C4i—H1c4j—C4j	18.07
O12bx—Mo3bx—O12b	17.0 (4)	H1c4i—H1c4j—C4j	129.7
O12bx—Mo3bx—O16b	106.1 (5)	H1c5i—H1c5j—C5j	54.04
O12bx—Mo3bx—O17b	78.1 (5)	H1c6i—H1c6j—C6j	50.59
O12bx—Mo3bx—O19b	109.4 (4)	C6i—H2c6j—H2c6i	102.36
Mo3b—Mo3bx—O12b	106.6 (4)	C6i—H2c6j—C6j	26.2
Mo3b—Mo3bx—O16b	36.7 (4)	H2c6i—H2c6j—C6j	128.07
Mo3b—Mo3bx—O17b	118.1 (4)	H3c6i—H3c6j—C6j	62.19
Mo3b—Mo3bx—O19b	115.4 (4)	N1i—H1n1j—H1n1i	107 (12)
O12b—Mo3bx—O16b	94.0 (3)	N1i—H1n1j—N1j	20 (2)
O12b—Mo3bx—O17b	83.2 (3)	H1n1i—H1n1j—N1j	127 (12)
O12b—Mo3bx—O19b	124.0 (4)	H2n1i—H2n1j—N1j	31 (10)
O16b—Mo3bx—O17b	152.5 (2)	O24g—O24k—C7g	155 (4)
O16b—Mo3bx—O19b	98.2 (3)	O24g—O24k—C6k	54 (3)
O17b—Mo3bx—O19b	106.0 (3)	O24g—O24k—C7k	161 (4)
O3bx—Mo2bx—O18bx	98.1 (6)	C7g—O24k—C6k	110.0 (14)
O3bx—Mo2bx—O12bx	95.4 (6)	C7g—O24k—C7k	7.7 (8)
O3bx—Mo2bx—O2bx	102.0 (7)	C6k—O24k—C7k	117.1 (13)
O3bx—Mo2bx—Mo2b	77.6 (7)	N1g—N1k—C2g	86 (5)
O3bx—Mo2bx—O2b	117.0 (6)	N1g—N1k—H1n1g	90 (9)
O3bx—Mo2bx—O3b	20.7 (5)	N1g—N1k—C2k	99 (5)
O3bx—Mo2bx—O18b	79.5 (5)	N1g—N1k—H1n1k	109 (9)
O18bx—Mo2bx—O12bx	150.6 (4)	N1g—N1k—H2n1k	34 (7)
O18bx—Mo2bx—O2bx	106.4 (7)	C2g—N1k—H1n1g	115 (4)
O18bx—Mo2bx—Mo2b	126.5 (7)	C2g—N1k—C2k	12.8 (8)
O18bx—Mo2bx—O2b	104.2 (5)	C2g—N1k—H1n1k	118 (3)
O18bx—Mo2bx—O3b	118.7 (4)	C2g—N1k—H2n1k	106 (3)
O18bx—Mo2bx—O18b	19.6 (4)	H1n1g—N1k—C2k	113 (4)
O12bx—Mo2bx—O2bx	96.1 (7)	H1n1g—N1k—H1n1k	19 (5)
O12bx—Mo2bx—Mo2b	33.0 (6)	H1n1g—N1k—H2n1k	106 (6)
O12bx—Mo2bx—O2b	92.6 (5)	C2k—N1k—H1n1k	111 (3)
O12bx—Mo2bx—O3b	75.9 (4)	C2k—N1k—H2n1k	118 (3)
O12bx—Mo2bx—O18b	147.6 (4)	H1n1k—N1k—H2n1k	120 (5)
O2bx—Mo2bx—Mo2b	126.8 (8)	C1g—C1k—C4g	133 (4)
O2bx—Mo2bx—O2b	15.1 (5)	C1g—C1k—H1c1g	67.55
O2bx—Mo2bx—O3b	96.8 (6)	C1g—C1k—C4k	144 (4)
O2bx—Mo2bx—O18b	116.3 (6)	C1g—C1k—C5k	24 (3)
Mo2b—Mo2bx—O2b	125.5 (6)	C1g—C1k—H1c1k	96.15
Mo2b—Mo2bx—O3b	64.4 (4)	C4g—C1k—H1c1g	159.16
Mo2b—Mo2bx—O18b	115.8 (6)	C4g—C1k—C4k	11.3 (16)
O2b—Mo2bx—O3b	110.3 (4)	C4g—C1k—C5k	110 (2)
O2b—Mo2bx—O18b	118.4 (4)	C4g—C1k—H1c1k	130.76
O3b—Mo2bx—O18b	99.8 (3)	H1c1g—C1k—C4k	147.86
O5bx—P1bx—O14bx	114.3 (7)	H1c1g—C1k—C5k	91.18
O5bx—P1bx—O17bx	104.7 (7)	H1c1g—C1k—H1c1k	28.62
O5bx—P1bx—O11bx	105.5 (7)	C4k—C1k—C5k	120.8 (18)
O5bx—P1bx—P1b	69.0 (17)	C4k—C1k—H1c1k	119.6
O5bx—P1bx—O14b	109.0 (6)	C5k—C1k—H1c1k	119.6
O5bx—P1bx—O17b	94.1 (6)	N1g—C2k—C2g	73 (3)
O14bx—P1bx—O17bx	105.7 (6)	N1g—C2k—C3g	138.6 (14)
O14bx—P1bx—O11bx	113.7 (5)	N1g—C2k—N1k	9.8 (11)
O14bx—P1bx—P1b	168 (2)	N1g—C2k—C3k	129.0 (13)
O14bx—P1bx—O14b	5.3 (3)	N1g—C2k—C7k	109.7 (13)
O14bx—P1bx—O17b	118.8 (6)	C2g—C2k—C3g	148 (4)
O17bx—P1bx—O11bx	112.8 (5)	C2g—C2k—N1k	83 (3)
O17bx—P1bx—P1b	84 (2)	C2g—C2k—C3k	158 (4)
O17bx—P1bx—O14b	107.7 (5)	C2g—C2k—C7k	37 (3)
O17bx—P1bx—O17b	13.9 (4)	C3g—C2k—N1k	129.2 (15)
O11bx—P1bx—P1b	55.2 (15)	C3g—C2k—C3k	10.3 (11)
O11bx—P1bx—O14b	116.4 (5)	C3g—C2k—C7k	111.4 (14)
O11bx—P1bx—O17b	108.2 (5)	N1k—C2k—C3k	119.4 (13)
P1b—P1bx—O14b	168 (2)	N1k—C2k—C7k	119.3 (14)
P1b—P1bx—O17b	71 (2)	C3k—C2k—C7k	121.2 (13)
O14b—P1bx—O17b	120.3 (4)	C3g—C3k—C4g	70 (4)
O15bx—P2bx—O22bx	110.8 (6)	C3g—C3k—H1c3g	136.94
O15bx—P2bx—O9bx	107.7 (7)	C3g—C3k—C2k	33 (3)
O15bx—P2bx—O8bx	104.1 (6)	C3g—C3k—C4k	87 (4)
O15bx—P2bx—P2b	77 (2)	C3g—C3k—H1c3k	150.66
O15bx—P2bx—O8b	103.3 (5)	C4g—C3k—H1c3g	146.34
O15bx—P2bx—O9b	107.5 (6)	C4g—C3k—C2k	102.0 (14)
O22bx—P2bx—O9bx	114.1 (7)	C4g—C3k—C4k	16.8 (13)
O22bx—P2bx—O8bx	106.6 (6)	C4g—C3k—H1c3k	137.33
O22bx—P2bx—P2b	69 (2)	H1c3g—C3k—C2k	109.61
O22bx—P2bx—O8b	54.8 (4)	H1c3g—C3k—C4k	130.63
O22bx—P2bx—O9b	141.7 (6)	H1c3g—C3k—H1c3k	14.49
O9bx—P2bx—O8bx	113.0 (7)	C2k—C3k—C4k	118.7 (15)
O9bx—P2bx—P2b	70 (2)	C2k—C3k—H1c3k	120.64
O9bx—P2bx—O8b	148.9 (7)	C4k—C3k—H1c3k	120.64
O9bx—P2bx—O9b	50.6 (7)	C3g—C4k—C4g	77 (4)
O8bx—P2bx—P2b	176 (2)	C3g—C4k—H1c4g	156.95
O8bx—P2bx—O8b	55.5 (5)	C3g—C4k—C1k	106.0 (18)
O8bx—P2bx—O9b	64.3 (4)	C3g—C4k—C3k	14.8 (11)
P2b—P2bx—O8b	120 (2)	C3g—C4k—H1c4k	134.27
P2b—P2bx—O9b	119 (2)	C4g—C4k—H1c4g	123.45
O8b—P2bx—O9b	117.0 (5)	C4g—C4k—C1k	29 (4)
Mo2bx—O3bx—Mo2b	11.72 (11)	C4g—C4k—C3k	92 (4)
Mo2bx—O3bx—O3b	90.2 (10)	C4g—C4k—H1c4k	147.87
Mo2b—O3bx—O3b	82.4 (10)	H1c4g—C4k—C1k	95.73
P1bx—O5bx—P1b	6.2 (2)	H1c4g—C4k—C3k	143.3
P1bx—O5bx—O5b	96 (2)	H1c4g—C4k—H1c4k	24.48
P1b—O5bx—O5b	93 (2)	C1k—C4k—C3k	120.6 (19)
P1bx—O14bx—Mo1b	120.4 (5)	C1k—C4k—H1c4k	119.69
P1bx—O14bx—O14b	35 (2)	C3k—C4k—H1c4k	119.69
Mo1b—O14bx—O14b	152 (3)	C1g—C5k—C5g	151 (4)
P2bx—O15bx—Mo3b	141.9 (5)	C1g—C5k—C7g	142.0 (19)
P2bx—O15bx—P2b	5.7 (2)	C1g—C5k—C1k	10.7 (14)
P2bx—O15bx—O15b	92.5 (13)	C1g—C5k—C7k	129.0 (19)
Mo3b—O15bx—P2b	147.3 (5)	C1g—C5k—H1c5k	110.25
Mo3b—O15bx—O15b	125.7 (14)	C5g—C5k—C7g	64 (3)
P2b—O15bx—O15b	87.0 (13)	C5g—C5k—C1k	161 (4)
Mo1bx—O1bx—Mo4bx	128.9 (8)	C5g—C5k—C7k	77 (3)
Mo1bx—O1bx—Mo4b	129.2 (8)	C5g—C5k—H1c5k	44.99
Mo1bx—O1bx—O1b	49.6 (8)	C7g—C5k—C1k	131.8 (14)
Mo4bx—O1bx—Mo4b	6.30 (9)	C7g—C5k—C7k	13.4 (6)
Mo4bx—O1bx—O1b	82.8 (12)	C7g—C5k—H1c5k	107.47
Mo4b—O1bx—O1b	81.2 (11)	C1k—C5k—C7k	118.6 (14)
Mo1bx—O6bx—Mo1b	14.01 (14)	C1k—C5k—H1c5k	120.72
Mo1bx—O6bx—O6b	87 (3)	C7k—C5k—H1c5k	120.72
Mo1b—O6bx—O6b	76 (3)	O24g—C6k—C6g	106 (3)
Mo5bx—O23bx—Mo5b	10.90 (14)	O24g—C6k—H2c6g	136.98
Mo5bx—O23bx—O23b	83.7 (19)	O24g—C6k—O24k	13.2 (7)
Mo5b—O23bx—O23b	73.0 (19)	O24g—C6k—H1c6k	96.68
P1bx—O17bx—Mo2b	142.4 (7)	O24g—C6k—H2c6k	118.51
P1bx—O17bx—P1b	6.6 (2)	O24g—C6k—H3c6k	112.33
P1bx—O17bx—O17b	90.5 (19)	C6g—C6k—H2c6g	89.69
Mo2b—O17bx—P1b	148.4 (7)	C6g—C6k—O24k	119 (3)
Mo2b—O17bx—O17b	127 (2)	C6g—C6k—H1c6k	22.79
P1b—O17bx—O17b	84.6 (18)	C6g—C6k—H2c6k	120.01
Mo1bx—O18bx—Mo2bx	137.6 (5)	C6g—C6k—H3c6k	86.69
Mo1bx—O18bx—Mo1b	5.49 (12)	H2c6g—C6k—O24k	133.26
Mo1bx—O18bx—Mo2b	132.7 (5)	H2c6g—C6k—H1c6k	82
Mo1bx—O18bx—O18b	124.4 (16)	H2c6g—C6k—H2c6k	30.39
Mo2bx—O18bx—Mo1b	137.1 (6)	H2c6g—C6k—H3c6k	108.45
Mo2bx—O18bx—Mo2b	7.43 (9)	O24k—C6k—H1c6k	109.47
Mo2bx—O18bx—O18b	65.2 (12)	O24k—C6k—H2c6k	109.47
Mo1b—O18bx—Mo2b	131.6 (5)	O24k—C6k—H3c6k	109.47
Mo1b—O18bx—O18b	118.9 (16)	H1c6k—C6k—H2c6k	109.47
Mo2b—O18bx—O18b	62.0 (11)	H1c6k—C6k—H3c6k	109.47
P1bx—O11bx—P1b	5.7 (2)	H2c6k—C6k—H3c6k	109.47
P1bx—O11bx—O11b	104 (2)	C2g—C7k—C5g	147.6 (15)
P1b—O11bx—O11b	108 (2)	C2g—C7k—C7g	125 (3)
Mo5bx—O10bx—Mo3bx	120.0 (5)	C2g—C7k—O24k	104.5 (13)
Mo5bx—O10bx—Mo3b	111.5 (6)	C2g—C7k—C2k	10.0 (10)
Mo5bx—O10bx—O10b	34.5 (15)	C2g—C7k—C5k	130.0 (14)
Mo3bx—O10bx—Mo3b	12.91 (11)	C5g—C7k—C7g	87 (3)
Mo3bx—O10bx—O10b	138 (3)	C5g—C7k—O24k	107.7 (11)
Mo3b—O10bx—O10b	125 (3)	C5g—C7k—C2k	137.6 (13)
Mo1bx—O13bx—Mo1b	11.02 (13)	C5g—C7k—C5k	18.1 (8)
Mo1bx—O13bx—O13b	70.7 (12)	C7g—C7k—O24k	22 (2)
Mo1b—O13bx—O13b	59.7 (11)	C7g—C7k—C2k	134 (3)
Mo5bx—O7bx—Mo5b	9.26 (17)	C7g—C7k—C5k	105 (3)
Mo5bx—O7bx—O7b	142 (4)	O24k—C7k—C2k	114.5 (12)
Mo5b—O7bx—O7b	137 (4)	O24k—C7k—C5k	125.5 (12)
Mo3bx—O19bx—Mo3b	10.10 (14)	C2k—C7k—C5k	120.1 (12)
Mo3bx—O19bx—O19b	54.3 (12)	H1c1g—H1c1k—C1k	84.28
Mo3b—O19bx—O19b	47.2 (11)	H1c3g—H1c3k—C3k	27.57
Mo3bx—O16bx—Mo3b	14.47 (17)	H1c4g—H1c4k—C4k	37.41
Mo3bx—O16bx—O16b	115 (2)	C5g—H1c5k—H1c5g	104.6
Mo3b—O16bx—O16b	101 (2)	C5g—H1c5k—C5k	25.32
Mo4bx—O20bx—Mo4b	6.18 (10)	H1c5g—H1c5k—C5k	129.82
Mo4bx—O20bx—O20b	71 (2)	C6g—H1c6k—H1c6g	140.66
Mo4b—O20bx—O20b	72 (2)	C6g—H1c6k—C6k	16.67
Mo3bx—O12bx—Mo2bx	123.9 (8)	H1c6g—H1c6k—C6k	156.85
Mo3bx—O12bx—Mo2b	118.1 (8)	H2c6g—H2c6k—C6k	63.26
Mo3bx—O12bx—O12b	62.9 (11)	C6g—H3c6k—H3c6g	68.43
Mo2bx—O12bx—Mo2b	6.44 (11)	C6g—H3c6k—C6k	24.82
Mo2bx—O12bx—O12b	110.3 (16)	H3c6g—H3c6k—C6k	93.22
Mo2b—O12bx—O12b	111.0 (16)	H1n1g—H1n1k—N1k	72 (14)
Mo4bx—O21bx—Mo5bx	122.7 (4)	N1g—H2n1k—N1k	13 (3)
Mo4bx—O21bx—Mo4b	6.00 (9)	O24h—O24l—C6h	112 (4)
Mo4bx—O21bx—Mo5b	122.1 (4)	O24h—O24l—C6l	128 (4)
Mo4bx—O21bx—O21b	76.6 (12)	O24h—O24l—C7l	26 (3)
Mo5bx—O21bx—Mo4b	128.5 (4)	C6h—O24l—C6l	15.9 (15)
Mo5bx—O21bx—Mo5b	9.67 (11)	C6h—O24l—C7l	104.1 (13)
Mo5bx—O21bx—O21b	107.2 (14)	C6l—O24l—C7l	117.1 (13)
Mo4b—O21bx—Mo5b	128.1 (4)	N1h—N1l—C2h	68 (6)
Mo4b—O21bx—O21b	77.0 (12)	N1h—N1l—H2n1h	148 (11)
Mo5b—O21bx—O21b	97.6 (14)	N1h—N1l—C2l	79 (6)
Mo4bx—O4bx—Mo4b	1.77 (14)	N1h—N1l—H1n1l	66 (8)
Mo4bx—O4bx—O4b	108.3 (19)	N1h—N1l—H2n1l	152 (10)
Mo4b—O4bx—O4b	108.3 (19)	C2h—N1l—H2n1h	131 (5)
Mo2bx—O2bx—Mo2b	8.18 (13)	C2h—N1l—C2l	10.8 (7)
Mo2bx—O2bx—O2b	54.7 (19)	C2h—N1l—H1n1l	106 (4)
Mo2b—O2bx—O2b	55.2 (19)	C2h—N1l—H2n1l	128 (3)
P2bx—O22bx—P2b	5.5 (2)	H2n1h—N1l—C2l	121 (5)
P2bx—O22bx—O8b	59.3 (6)	H2n1h—N1l—H1n1l	119 (6)
P2bx—O22bx—O22b	66.2 (6)	H2n1h—N1l—H2n1l	5 (5)
P2b—O22bx—O8b	64.5 (6)	C2l—N1l—H1n1l	111 (4)
P2b—O22bx—O22b	61.9 (5)	C2l—N1l—H2n1l	118 (3)
O8b—O22bx—O22b	122.9 (9)	H1n1l—N1l—H2n1l	120 (5)
P2bx—O9bx—P2b	5.7 (3)	C1h—C1l—C5h	151 (5)
P2bx—O9bx—O9b	61.3 (6)	C1h—C1l—C4l	37 (4)
P2b—O9bx—O9b	66.9 (6)	C1h—C1l—C5l	156 (5)
P2bx—O8bx—O8b	60.5 (5)	C1h—C1l—H1c1l	82.96
C6a—O24a—C7a	117.1 (6)	C5h—C1l—C4l	115.2 (19)
C2a—N1a—H1n1a	111 (3)	C5h—C1l—C5l	5.9 (11)
C2a—N1a—H2n1a	118 (3)	C5h—C1l—H1c1l	125.15
H1n1a—N1a—H2n1a	120 (4)	C4l—C1l—C5l	120.8 (16)
C4a—C1a—C5a	120.8 (8)	C4l—C1l—H1c1l	119.6
C4a—C1a—H1c1a	119.6	C5l—C1l—H1c1l	119.6
C5a—C1a—H1c1a	119.6	N1h—C2l—C2h	89 (4)
N1a—C2a—C3a	119.4 (7)	N1h—C2l—C7h	140.1 (16)
N1a—C2a—C7a	119.3 (7)	N1h—C2l—N1l	9.6 (10)
C3a—C2a—C7a	121.2 (8)	N1h—C2l—C3l	109.8 (13)
C2a—C3a—C4a	118.7 (8)	N1h—C2l—C7l	129.0 (15)
C2a—C3a—H1c3a	120.64	C2h—C2l—C7h	130 (5)
C4a—C3a—H1c3a	120.64	C2h—C2l—N1l	99 (4)
C1a—C4a—C3a	120.6 (9)	C2h—C2l—C3l	21 (4)
C1a—C4a—H1c4a	119.69	C2h—C2l—C7l	141 (4)
C3a—C4a—H1c4a	119.69	C7h—C2l—N1l	130.5 (15)
C1a—C5a—C7a	118.6 (8)	C7h—C2l—C3l	110.0 (15)
C1a—C5a—H1c5a	120.72	C7h—C2l—C7l	11.4 (9)
C7a—C5a—H1c5a	120.72	N1l—C2l—C3l	119.4 (13)
O24a—C6a—H1c6a	109.47	N1l—C2l—C7l	119.3 (14)
O24a—C6a—H2c6a	109.47	C3l—C2l—C7l	121.2 (14)
O24a—C6a—H3c6a	109.47	C2h—C3l—C3h	140 (7)
H1c6a—C6a—H2c6a	109.47	C2h—C3l—C4h	137.5 (17)
H1c6a—C6a—H3c6a	109.47	C2h—C3l—C2l	5.4 (9)
H2c6a—C6a—H3c6a	109.47	C2h—C3l—C4l	123.9 (16)
O24a—C7a—C2a	114.5 (7)	C2h—C3l—H1c3l	115.47
O24a—C7a—C5a	125.5 (7)	C3h—C3l—C4h	74 (5)
C2a—C7a—C5a	120.1 (7)	C3h—C3l—C2l	145 (7)
C2bⁱ—O24b—C3bⁱ	75 (4)	C3h—C3l—C4l	89 (5)
C2bⁱ—O24b—C4bⁱ	155 (3)	C3h—C3l—H1c3l	37.03
C2bⁱ—O24b—C6b	87 (3)	C4h—C3l—C2l	132.6 (15)
C2bⁱ—O24b—C7b	31.9 (13)	C4h—C3l—C4l	15.0 (11)
C3bⁱ—O24b—C4bⁱ	86 (5)	C4h—C3l—H1c3l	106.47
C3bⁱ—O24b—C6b	17 (3)	C2l—C3l—C4l	118.7 (15)
C3bⁱ—O24b—C7b	107 (5)	C2l—C3l—H1c3l	120.64
C4bⁱ—O24b—C6b	79 (4)	C4l—C3l—H1c3l	120.64
C4bⁱ—O24b—C7b	161 (3)	C1h—C4l—C3h	144 (2)
C6b—O24b—C7b	117 (3)	C1h—C4l—C4h	132 (5)
C2b—N1b—C5bⁱ	54 (5)	C1h—C4l—C1l	12.1 (10)
C2b—N1b—H1c5bⁱ	96.12	C1h—C4l—C3l	132 (2)
C2b—N1b—H1n1b	111 (8)	C1h—C4l—H1c4l	107.91
C2b—N1b—H2n1b	118 (6)	C3h—C4l—C4h	77 (4)
C5bⁱ—N1b—H1c5bⁱ	115.21	C3h—C4l—C1l	132.9 (18)
C5bⁱ—N1b—H1n1b	113 (6)	C3h—C4l—C3l	13.3 (9)
C5bⁱ—N1b—H2n1b	74 (6)	C3h—C4l—H1c4l	107.17
H1c5bⁱ—N1b—H1n1b	19.82	C4h—C4l—C1l	144 (5)
H1c5bⁱ—N1b—H2n1b	139.71	C4h—C4l—C3l	90 (4)
H1n1b—N1b—H2n1b	120 (9)	C4h—C4l—H1c4l	34.94
C4b—C1b—C5b	121 (5)	C1l—C4l—C3l	120.6 (17)
C4b—C1b—H1c1b	119.6	C1l—C4l—H1c4l	119.69
C5b—C1b—H1c1b	119.6	C3l—C4l—H1c4l	119.69
O24bⁱ—C2b—N1b	155 (3)	C5h—C5l—C7h	89 (3)
O24bⁱ—C2b—C3b	38 (3)	C5h—C5l—H1c5h	113.7
O24bⁱ—C2b—C5bⁱ	159 (2)	C5h—C5l—C1l	17 (3)
O24bⁱ—C2b—C7b	84 (2)	C5h—C5l—C7l	102 (4)
O24bⁱ—C2b—C7bⁱ	78 (3)	C5h—C5l—H1c5l	136.51
N1b—C2b—C3b	119 (3)	C7h—C5l—H1c5h	154.68
N1b—C2b—C5bⁱ	31 (2)	C7h—C5l—C1l	105.3 (14)
N1b—C2b—C7b	119 (3)	C7h—C5l—C7l	13.4 (8)
N1b—C2b—C7bⁱ	121 (3)	C7h—C5l—H1c5l	133.98
C3b—C2b—C5bⁱ	147 (3)	H1c5h—C5l—C1l	98.56
C3b—C2b—C7b	121 (3)	H1c5h—C5l—C7l	142.33
C3b—C2b—C7bⁱ	116 (4)	H1c5h—C5l—H1c5l	23.03
C5bⁱ—C2b—C7b	90 (2)	C1l—C5l—C7l	118.6 (15)
C5bⁱ—C2b—C7bⁱ	90 (3)	C1l—C5l—H1c5l	120.72
C7b—C2b—C7bⁱ	17.7 (11)	C7l—C5l—H1c5l	120.72
O24bⁱ—C3b—C2b	67 (4)	C6h—C6l—H1c6h	126.59
O24bⁱ—C3b—C4b	54 (5)	C6h—C6l—H3c6h	78.91
O24bⁱ—C3b—C6bⁱ	139 (8)	C6h—C6l—O24l	59 (3)
O24bⁱ—C3b—H1c3b	164.62	C6h—C6l—H1c6l	148.53
C2b—C3b—C4b	119 (4)	C6h—C6l—H2c6l	56.73
C2b—C3b—C6bⁱ	134 (7)	C6h—C6l—H3c6l	101.97
C2b—C3b—H1c3b	120.64	H1c6h—C6l—H3c6h	153.17
C4b—C3b—C6bⁱ	103 (8)	H1c6h—C6l—O24l	102.35
C4b—C3b—H1c3b	120.64	H1c6h—C6l—H1c6l	22.26
C6bⁱ—C3b—H1c3b	25.94	H1c6h—C6l—H2c6l	93.29
O24bⁱ—C4b—C1b	82 (5)	H1c6h—C6l—H3c6l	130.85
O24bⁱ—C4b—C3b	40 (3)	H3c6h—C6l—O24l	98.38
O24bⁱ—C4b—H1c4b	155.77	H3c6h—C6l—H1c6l	132.48
C1b—C4b—C3b	121 (6)	H3c6h—C6l—H2c6l	95.67
C1b—C4b—H1c4b	119.69	H3c6h—C6l—H3c6l	23.08
C3b—C4b—H1c4b	119.69	O24l—C6l—H1c6l	109.47
N1bⁱ—C5b—C1b	112 (6)	O24l—C6l—H2c6l	109.47
N1bⁱ—C5b—C2bⁱ	94 (6)	O24l—C6l—H3c6l	109.47
N1bⁱ—C5b—C7b	126 (6)	H1c6l—C6l—H2c6l	109.47
N1bⁱ—C5b—H1c5b	19	H1c6l—C6l—H3c6l	109.47
N1bⁱ—C5b—H2n1bⁱ	58 (6)	H2c6l—C6l—H3c6l	109.47
C1b—C5b—C2bⁱ	147 (3)	O24h—C7l—C5h	142.1 (13)
C1b—C5b—C7b	119 (3)	O24h—C7l—C7h	151 (4)
C1b—C5b—H1c5b	120.72	O24h—C7l—O24l	7.9 (11)
C1b—C5b—H2n1bⁱ	57 (5)	O24h—C7l—C2l	110.3 (13)
C2bⁱ—C5b—C7b	31.9 (15)	O24h—C7l—C5l	129.1 (13)
C2bⁱ—C5b—H1c5b	90.53	C5h—C7l—C7h	62 (3)
C2bⁱ—C5b—H2n1bⁱ	136 (5)	C5h—C7l—O24l	139.0 (12)
C7b—C5b—H1c5b	120.72	C5h—C7l—C2l	106.6 (12)
C7b—C5b—H2n1bⁱ	149 (3)	C5h—C7l—C5l	13.6 (9)
H1c5b—C5b—H2n1bⁱ	72.63	C7h—C7l—O24l	157 (3)
O24b—C6b—C3bⁱ	24 (5)	C7h—C7l—C2l	45 (3)
O24b—C6b—H1c3bⁱ	140.64	C7h—C7l—C5l	76 (3)
O24b—C6b—H1c6b	109.47	O24l—C7l—C2l	114.5 (12)
O24b—C6b—H2c6b	109.47	O24l—C7l—C5l	125.5 (12)
O24b—C6b—H3c6b	109.47	C2l—C7l—C5l	120.1 (13)
C3bⁱ—C6b—H1c3bⁱ	116.99	C1h—H1c1l—H1c1h	74.04
C3bⁱ—C6b—H1c6b	122.12	C1h—H1c1l—C1l	22.4
C3bⁱ—C6b—H2c6b	85.8	H1c1h—H1c1l—C1l	96.44
C3bⁱ—C6b—H3c6b	117.15	C3h—H1c3l—H1c3h	125.65
H1c3bⁱ—C6b—H1c6b	99.39	C3h—H1c3l—C3l	15.67
H1c3bⁱ—C6b—H2c6b	33.28	H1c3h—H1c3l—C3l	140.82
H1c3bⁱ—C6b—H3c6b	84.24	C4h—H1c4l—H1c4h	119.97
H1c6b—C6b—H2c6b	109.47	C4h—H1c4l—C4l	17.92
H1c6b—C6b—H3c6b	109.47	H1c4h—H1c4l—C4l	137.8
H2c6b—C6b—H3c6b	109.47	H1c5h—H1c5l—C5l	47.69
O24b—C7b—C2b	114.5 (19)	H1c6h—H1c6l—C6l	35.51
O24b—C7b—C2bⁱ	70 (3)	C6h—H2c6l—H2c6h	93.36
O24b—C7b—C5b	125 (2)	C6h—H2c6l—C6l	24.86
O24b—C7b—C7bⁱ	116.4 (18)	H2c6h—H2c6l—C6l	118.22
C2b—C7b—C2bⁱ	162 (2)	H3c6h—H3c6l—C6l	77.14
C2b—C7b—C5b	120 (2)	N1h—H1n1l—H1n1h	95 (15)
C2b—C7b—C7bⁱ	18.6 (13)	N1h—H1n1l—N1l	16 (2)
C2bⁱ—C7b—C5b	58 (3)	H1n1h—H1n1l—N1l	111 (16)
C2bⁱ—C7b—C7bⁱ	144 (2)	H2n1h—H2n1l—N1l	14 (15)
C5b—C7b—C7bⁱ	115 (2)	C6m—O24m—C7m	117.1 (11)
C3b—H1c3b—C6bⁱ	37.06	C6m—O24m—O24n	115 (3)
C3b—H1c3b—H2c6bⁱ	87.27	C6m—O24m—C6n	24.4 (9)
C6bⁱ—H1c3b—H2c6bⁱ	122.16	C6m—O24m—C7n	119.9 (12)
N1bⁱ—H1c5b—C5b	45.79	C7m—O24m—O24n	128 (3)
N1bⁱ—H1c5b—H1n1bⁱ	148.05	C7m—O24m—C6n	141.4 (12)
C5b—H1c5b—H1n1bⁱ	125.51	C7m—O24m—C7n	2.8 (7)
C6b—H2c6b—H1c3bⁱ	24.56	O24n—O24m—C6n	91 (3)
N1b—H1n1b—H1c5bⁱ	12.13	O24n—O24m—C7n	125 (3)
N1b—H2n1b—C5bⁱ	48 (5)	C6n—O24m—C7n	144.2 (13)
C6c—O24c—C7c	117.1 (7)	C2m—N1m—H1n1m	111 (3)
C2c—N1c—H1n1c	111 (3)	C2m—N1m—H2n1m	118 (3)
C2c—N1c—H2n1c	118 (3)	C2m—N1m—N1n	76 (7)
H1n1c—N1c—H2n1c	120 (5)	C2m—N1m—C2n	2.6 (7)
C4c—C1c—C5c	120.8 (10)	C2m—N1m—H2n1n	130 (4)
C4c—C1c—H1c1c	119.6	H1n1m—N1m—H2n1m	120 (5)
C5c—C1c—H1c1c	119.6	H1n1m—N1m—N1n	75 (11)
N1c—C2c—C3c	119.4 (8)	H1n1m—N1m—C2n	113 (3)
N1c—C2c—C7c	119.3 (8)	H1n1m—N1m—H2n1n	115 (5)
C3c—C2c—C7c	121.2 (9)	H2n1m—N1m—N1n	147 (12)
C2c—C3c—C4c	118.7 (10)	H2n1m—N1m—C2n	115 (3)
C2c—C3c—H1c3c	120.64	H2n1m—N1m—H2n1n	17 (4)
C4c—C3c—H1c3c	120.64	N1n—N1m—C2n	78 (7)
C1c—C4c—C3c	120.6 (11)	N1n—N1m—H2n1n	131 (11)
C1c—C4c—H1c4c	119.69	C2n—N1m—H2n1n	128 (4)
C3c—C4c—H1c4c	119.69	C4m—C1m—C5m	120.8 (15)
C1c—C5c—C7c	118.6 (9)	C4m—C1m—H1c1m	119.6
C1c—C5c—H1c5c	120.72	C4m—C1m—C1n	148 (3)
C7c—C5c—H1c5c	120.72	C4m—C1m—C4n	4 (2)
O24c—C6c—H1c6c	109.47	C5m—C1m—H1c1m	119.6
O24c—C6c—H2c6c	109.47	C5m—C1m—C1n	28 (2)
O24c—C6c—H3c6c	109.47	C5m—C1m—C4n	117.9 (19)
H1c6c—C6c—H2c6c	109.47	H1c1m—C1m—C1n	92.08
H1c6c—C6c—H3c6c	109.47	H1c1m—C1m—C4n	122.46
H2c6c—C6c—H3c6c	109.47	C1n—C1m—C4n	145 (4)
O24c—C7c—C2c	114.5 (7)	N1m—C2m—C3m	119.4 (12)
O24c—C7c—C5c	125.5 (7)	N1m—C2m—C7m	119.3 (12)
C2c—C7c—C5c	120.1 (8)	N1m—C2m—N1n	7.5 (9)
C6d—O24d—C7d	117.1 (7)	N1m—C2m—C2n	110 (15)
C2d—N1d—H1n1d	111 (3)	N1m—C2m—C3n	131.8 (13)
C2d—N1d—H2n1d	118 (3)	N1m—C2m—C7n	109.6 (11)
H1n1d—N1d—H2n1d	120 (4)	C3m—C2m—C7m	121.2 (12)
C4d—C1d—C5d	120.8 (9)	C3m—C2m—N1n	112.1 (12)
C4d—C1d—H1c1d	119.6	C3m—C2m—C2n	129 (15)
C5d—C1d—H1c1d	119.6	C3m—C2m—C3n	12.4 (9)
N1d—C2d—C3d	119.4 (8)	C3m—C2m—C7n	130.9 (12)
N1d—C2d—C7d	119.3 (8)	C7m—C2m—N1n	126.6 (12)
C3d—C2d—C7d	121.2 (8)	C7m—C2m—C2n	13 (17)
C2d—C3d—C4d	118.7 (10)	C7m—C2m—C3n	108.9 (12)
C2d—C3d—H1c3d	120.64	C7m—C2m—C7n	9.7 (6)
C4d—C3d—H1c3d	120.64	N1n—C2m—C2n	117 (15)
C1d—C4d—C3d	120.6 (10)	N1n—C2m—C3n	124.5 (13)
C1d—C4d—H1c4d	119.69	N1n—C2m—C7n	116.9 (12)
C3d—C4d—H1c4d	119.69	C2n—C2m—C3n	117 (15)
C1d—C5d—C7d	118.6 (9)	C2n—C2m—C7n	10 (20)
C1d—C5d—H1c5d	120.72	C3n—C2m—C7n	118.6 (12)
C7d—C5d—H1c5d	120.72	C2m—C3m—C4m	118.7 (14)
O24d—C6d—H1c6d	109.47	C2m—C3m—H1c3m	120.64
O24d—C6d—H2c6d	109.47	C2m—C3m—C2n	2.2 (8)
O24d—C6d—H3c6d	109.47	C2m—C3m—C3n	77 (4)
H1c6d—C6d—H2c6d	109.47	C2m—C3m—H1c3n	141.52
H1c6d—C6d—H3c6d	109.47	C4m—C3m—H1c3m	120.64
H2c6d—C6d—H3c6d	109.47	C4m—C3m—C2n	116.5 (14)
O24d—C7d—C2d	114.5 (7)	C4m—C3m—C3n	42 (4)
O24d—C7d—C5d	125.5 (8)	C4m—C3m—H1c3n	99.75
C2d—C7d—C5d	120.1 (8)	H1c3m—C3m—C2n	122.81
C6e—O24e—C7e	117.1 (11)	H1c3m—C3m—C3n	161.98
C6e—O24e—O24f	103 (2)	H1c3m—C3m—H1c3n	20.9
C6e—O24e—C6f	19.1 (9)	C2n—C3m—C3n	75 (4)
C7e—O24e—O24f	17 (2)	C2n—C3m—H1c3n	143.7
C7e—O24e—C6f	99.0 (10)	C3n—C3m—H1c3n	141.14
O24f—O24e—C6f	86 (2)	C1m—C4m—C3m	120.6 (16)
C2e—N1e—H1n1e	111 (3)	C1m—C4m—H1c4m	119.69
C2e—N1e—H2n1e	118 (4)	C1m—C4m—C3n	111.0 (17)
C2e—N1e—N1f	59 (2)	C1m—C4m—C4n	7 (4)
C2e—N1e—H1n1f	99 (3)	C1m—C4m—H1c4n	80.34
H1n1e—N1e—H2n1e	120 (5)	C3m—C4m—H1c4m	119.69
H1n1e—N1e—N1f	126 (4)	C3m—C4m—C3n	9.6 (9)
H1n1e—N1e—H1n1f	53 (5)	C3m—C4m—C4n	115 (3)
H2n1e—N1e—N1f	108 (5)	C3m—C4m—H1c4n	158.72
H2n1e—N1e—H1n1f	139 (5)	H1c4m—C4m—C3n	129.3
N1f—N1e—H1n1f	75 (5)	H1c4m—C4m—C4n	125.08
C4e—C1e—C5e	120.8 (15)	H1c4m—C4m—H1c4n	39.53
C4e—C1e—H1c1e	119.6	C3n—C4m—C4n	105 (3)
C4e—C1e—C1f	72 (3)	C3n—C4m—H1c4n	167.83
C4e—C1e—C5f	122.8 (19)	C4n—C4m—H1c4n	85.55
C5e—C1e—H1c1e	119.6	C1m—C5m—C7m	118.6 (13)
C5e—C1e—C1f	135 (3)	C1m—C5m—H1c5m	120.72
C5e—C1e—C5f	19.9 (12)	C1m—C5m—C1n	15.3 (13)
H1c1e—C1e—C1f	65.9	C1m—C5m—C5n	177 (4)
H1c1e—C1e—C5f	113.81	C7m—C5m—H1c5m	120.72
C1f—C1e—C5f	115 (3)	C7m—C5m—C1n	133.6 (18)
N1e—C2e—C3e	119.4 (14)	C7m—C5m—C5n	63 (2)
N1e—C2e—C7e	119.3 (12)	H1c5m—C5m—C1n	105.62
N1e—C2e—N1f	27.3 (12)	H1c5m—C5m—C5n	57.87
N1e—C2e—C2f	132 (3)	C1n—C5m—C5n	162 (3)
N1e—C2e—C7f	137.4 (13)	O24m—C6m—H1c6m	109.47
C3e—C2e—C7e	121.2 (13)	O24m—C6m—H2c6m	109.47
C3e—C2e—N1f	105.6 (13)	O24m—C6m—H3c6m	109.47
C3e—C2e—C2f	31 (3)	O24m—C6m—C6n	73.0 (19)
C3e—C2e—C7f	103.2 (12)	O24m—C6m—H2c6n	103.83
C7e—C2e—N1f	127.3 (15)	O24m—C6m—H3c6n	106.36
C7e—C2e—C2f	102 (3)	H1c6m—C6m—H2c6m	109.47
C7e—C2e—C7f	18.1 (6)	H1c6m—C6m—H3c6m	109.47
N1f—C2e—C2f	107 (3)	H1c6m—C6m—C6n	36.44
N1f—C2e—C7f	142.7 (18)	H1c6m—C6m—H2c6n	72.52
C2f—C2e—C7f	86 (2)	H1c6m—C6m—H3c6n	73.49
C2e—C3e—C4e	118.7 (17)	H2c6m—C6m—H3c6m	109.47
C2e—C3e—H1c3e	120.64	H2c6m—C6m—C6n	122.85
C2e—C3e—C2f	13.5 (12)	H2c6m—C6m—H2c6n	42.37
C2e—C3e—C3f	158 (5)	H2c6m—C6m—H3c6n	140.1
C4e—C3e—H1c3e	120.64	H3c6m—C6m—C6n	123.63
C4e—C3e—C2f	111 (2)	H3c6m—C6m—H2c6n	143.14
C4e—C3e—C3f	49 (3)	H3c6m—C6m—H3c6n	40.13
H1c3e—C3e—C2f	127.41	C6n—C6m—H2c6n	80.75
H1c3e—C3e—C3f	74.29	C6n—C6m—H3c6n	84.01
C2f—C3e—C3f	144 (6)	H2c6n—C6m—H3c6n	140.3
C1e—C4e—C3e	120.6 (16)	O24m—C7m—C2m	114.5 (10)
C1e—C4e—H1c4e	119.69	O24m—C7m—C5m	125.5 (11)
C1e—C4e—C1f	25.1 (12)	O24m—C7m—C2n	114.0 (11)
C1e—C4e—C3f	135.3 (19)	O24m—C7m—C5n	106.8 (11)
C1e—C4e—C4f	111 (4)	O24m—C7m—C7n	13 (3)
C3e—C4e—H1c4e	119.69	C2m—C7m—C5m	120.1 (11)
C3e—C4e—C1f	135.1 (17)	C2m—C7m—C2n	0.7 (10)
C3e—C4e—C3f	16.2 (10)	C2m—C7m—C5n	138.7 (13)
C3e—C4e—C4f	122 (5)	C2m—C7m—C7n	102 (4)
H1c4e—C4e—C1f	101.5	C5m—C7m—C2n	120.6 (12)
H1c4e—C4e—C3f	104.56	C5m—C7m—C5n	18.7 (9)
H1c4e—C4e—C4f	25.11	C5m—C7m—C7n	138 (4)
C1f—C4e—C3f	151.2 (19)	C2n—C7m—C5n	139.2 (13)
C1f—C4e—C4f	88 (3)	C2n—C7m—C7n	101 (4)
C3f—C4e—C4f	112 (4)	C5n—C7m—C7n	120 (4)
C1e—C5e—C7e	118.6 (14)	C1m—H1c1m—H1c1n	87.25
C1e—C5e—H1c5e	120.72	C3m—H1c3m—H1c3n	40.58
C1e—C5e—C5f	39.7 (19)	C4m—H1c4m—H1c4n	62.5
C1e—C5e—C7f	103.2 (15)	C5m—H1c5m—C5n	28.09
C1e—C5e—H1c5f	93.32	C5m—H1c5m—H1c5n	112.57
C7e—C5e—H1c5e	120.72	C5n—H1c5m—H1c5n	84.48
C7e—C5e—C5f	119 (3)	C6m—H1c6m—C6n	36.75
C7e—C5e—C7f	15.4 (7)	C6m—H1c6m—H1c6n	132.13
C7e—C5e—H1c5f	137.33	C6n—H1c6m—H1c6n	95.4
H1c5e—C5e—C5f	106.32	C6m—H2c6m—H2c6n	60.07
H1c5e—C5e—C7f	136.07	C6m—H3c6m—H3c6n	57.29
H1c5e—C5e—H1c5f	39.07	N1m—H1n1m—N1n	12.7 (18)
C5f—C5e—C7f	107 (3)	N1m—H1n1m—H1n1n	100 (19)
C5f—C5e—H1c5f	67.9	N1n—H1n1m—H1n1n	87 (18)
C7f—C5e—H1c5f	145.01	N1m—H2n1m—H2n1n	52 (12)
O24e—C6e—H1c6e	109.47	O24m—O24n—C6n	75 (3)
O24e—C6e—H2c6e	109.47	O24m—O24n—C7n	43 (2)
O24e—C6e—H3c6e	109.47	C6n—O24n—C7n	117.1 (11)
O24e—C6e—C6f	75 (3)	N1m—N1n—C2m	97 (7)
O24e—C6e—H1c6f	117.65	N1m—N1n—H1n1m	92 (12)
H1c6e—C6e—H2c6e	109.47	N1m—N1n—C2n	94 (7)
H1c6e—C6e—H3c6e	109.47	N1m—N1n—H1n1n	109 (13)
H1c6e—C6e—C6f	164.48	N1m—N1n—H2n1n	39 (9)
H1c6e—C6e—H1c6f	8.49	C2m—N1n—H1n1m	117 (4)
H2c6e—C6e—H3c6e	109.47	C2m—N1n—C2n	2.5 (7)
H2c6e—C6e—C6f	55.55	C2m—N1n—H1n1n	110 (3)
H2c6e—C6e—H1c6f	103.36	C2m—N1n—H2n1n	120 (3)
H3c6e—C6e—C6f	81.64	H1n1m—N1n—C2n	118 (4)
H3c6e—C6e—H1c6f	107.09	H1n1m—N1n—H1n1n	17 (4)
C6f—C6e—H1c6f	158.86	H1n1m—N1n—H2n1n	105 (5)
O24e—C7e—C2e	114.5 (10)	C2n—N1n—H1n1n	111 (3)
O24e—C7e—C5e	125.5 (12)	C2n—N1n—H2n1n	118 (3)
O24e—C7e—O24f	7.7 (10)	H1n1n—N1n—H2n1n	120 (5)
O24e—C7e—C2f	129.6 (10)	C1m—C1n—C5m	137 (3)
O24e—C7e—C7f	170 (2)	C1m—C1n—C4n	22 (2)
C2e—C7e—C5e	120.1 (11)	C1m—C1n—C5n	142 (3)
C2e—C7e—O24f	120.5 (13)	C1m—C1n—H1c1n	97.75
C2e—C7e—C2f	17.1 (8)	C5m—C1n—C4n	115.4 (17)
C2e—C7e—C7f	75 (2)	C5m—C1n—C5n	5.6 (10)
C5e—C7e—O24f	119.2 (14)	C5m—C1n—H1c1n	124.94
C5e—C7e—C2f	104.4 (10)	C4n—C1n—C5n	120.8 (14)
C5e—C7e—C7f	45 (2)	C4n—C1n—H1c1n	119.6
O24f—C7e—C2f	134.7 (12)	C5n—C1n—H1c1n	119.6
O24f—C7e—C7f	165 (3)	N1m—C2n—C2m	67 (14)
C2f—C7e—C7f	60 (2)	N1m—C2n—C3m	114.7 (12)
C1e—H1c1e—C1f	36.89	N1m—C2n—C7m	122.4 (12)
C1e—H1c1e—H1c1f	106.62	N1m—C2n—N1n	7.4 (9)
C1f—H1c1e—H1c1f	70.2	N1m—C2n—C3n	126.6 (12)
C3e—H1c3e—C3f	25.77	N1m—C2n—C7n	112.1 (11)
C3e—H1c3e—H1c3f	101.96	C2m—C2n—C3m	48 (15)
C3f—H1c3e—H1c3f	77.52	C2m—C2n—C7m	167 (18)
C4e—H1c4e—C4f	18.95	C2m—C2n—N1n	60 (14)
C4e—H1c4e—H1c4f	149.28	C2m—C2n—C3n	60 (15)
C4f—H1c4e—H1c4f	130.46	C2m—C2n—C7n	170 (20)
C5e—H1c5e—H1c5f	75.42	C3m—C2n—C7m	122.9 (12)
C6e—H1c6e—H1c6f	9.18	C3m—C2n—N1n	107.5 (11)
C6e—H2c6e—C6f	29.33	C3m—C2n—C3n	11.9 (9)
C6e—H2c6e—H2c6f	121.6	C3m—C2n—C7n	133.1 (12)
C6f—H2c6e—H2c6f	96.16	C7m—C2n—N1n	129.6 (12)
C6e—H3c6e—C6f	27.65	C7m—C2n—C3n	111.0 (12)
C6e—H3c6e—H3c6f	93.91	C7m—C2n—C7n	10.2 (7)
C6f—H3c6e—H3c6f	67.27	N1n—C2n—C3n	119.4 (12)
N1e—H1n1e—H1n1f	55 (6)	N1n—C2n—C7n	119.3 (12)
N1e—H2n1e—H2n1f	73 (5)	C3n—C2n—C7n	121.2 (12)
O24e—O24f—C7e	156 (3)	C2m—C3n—C3m	90 (4)
O24e—O24f—C6f	76 (2)	C2m—C3n—C4m	140.7 (16)
O24e—O24f—C7f	159 (3)	C2m—C3n—C2n	2.6 (8)
C7e—O24f—C6f	121.7 (13)	C2m—C3n—C4n	121.3 (14)
C7e—O24f—C7f	4.8 (8)	C2m—C3n—H1c3n	118.05
C6f—O24f—C7f	117.1 (10)	C3m—C3n—C4m	129 (5)
N1e—N1f—C2e	94 (2)	C3m—C3n—C2n	93 (4)
N1e—N1f—C2f	110 (2)	C3m—C3n—C4n	148 (5)
N1e—N1f—H1n1f	57 (4)	C3m—C3n—H1c3n	27.68
N1e—N1f—H2n1f	76 (4)	C4m—C3n—C2n	138.0 (16)
C2e—N1f—C2f	17.5 (8)	C4m—C3n—C4n	19.5 (12)
C2e—N1f—H1n1f	109 (4)	C4m—C3n—H1c3n	101.27
C2e—N1f—H2n1f	108 (3)	C2n—C3n—C4n	118.7 (14)
C2f—N1f—H1n1f	111 (3)	C2n—C3n—H1c3n	120.64
C2f—N1f—H2n1f	118 (3)	C4n—C3n—H1c3n	120.64
H1n1f—N1f—H2n1f	120 (5)	C1m—C4n—C4m	169 (6)
C1e—C1f—C4e	83 (3)	C1m—C4n—C1n	13.0 (14)
C1e—C1f—H1c1e	77.21	C1m—C4n—C3n	133 (2)
C1e—C1f—C4f	101 (3)	C1m—C4n—H1c4n	107.07
C1e—C1f—C5f	42 (2)	C4m—C4n—C1n	174 (5)
C1e—C1f—H1c1f	124.6	C4m—C4n—C3n	55 (3)
C4e—C1f—H1c1e	131.36	C4m—C4n—H1c4n	64.72
C4e—C1f—C4f	18.9 (12)	C1n—C4n—C3n	120.6 (16)
C4e—C1f—C5f	102.8 (13)	C1n—C4n—H1c4n	119.69
C4e—C1f—H1c1f	137.13	C3n—C4n—H1c4n	119.69
H1c1e—C1f—C4f	130.06	C5m—C5n—C7m	98 (3)
H1c1e—C1f—C5f	90.94	C5m—C5n—H1c5m	94.04
H1c1e—C1f—H1c1f	48.08	C5m—C5n—C1n	12 (2)
C4f—C1f—C5f	120.8 (13)	C5m—C5n—C7n	107 (3)
C4f—C1f—H1c1f	119.6	C5m—C5n—H1c5n	131.88
C5f—C1f—H1c1f	119.6	C7m—C5n—H1c5m	167.13
C2e—C2f—C3e	135 (4)	C7m—C5n—C1n	109.7 (13)
C2e—C2f—C7e	61 (2)	C7m—C5n—C7n	8.9 (7)
C2e—C2f—N1f	55 (2)	C7m—C5n—H1c5n	129.6
C2e—C2f—C3f	146 (4)	H1c5m—C5n—C1n	82.96
C2e—C2f—C7f	75 (2)	H1c5m—C5n—C7n	158.35
C3e—C2f—C7e	139.8 (15)	H1c5m—C5n—H1c5n	37.84
C3e—C2f—N1f	114.9 (16)	C1n—C5n—C7n	118.6 (13)
C3e—C2f—C3f	10.2 (16)	C1n—C5n—H1c5n	120.72
C3e—C2f—C7f	124.8 (15)	C7n—C5n—H1c5n	120.72
C7e—C2f—N1f	103.7 (10)	O24m—C6n—C6m	83 (2)
C7e—C2f—C3f	136.9 (12)	O24m—C6n—H1c6m	170.58
C7e—C2f—C7f	15.7 (6)	O24m—C6n—O24n	14.7 (6)
N1f—C2f—C3f	119.4 (12)	O24m—C6n—H1c6n	124.14
N1f—C2f—C7f	119.3 (11)	O24m—C6n—H2c6n	101.58
C3f—C2f—C7f	121.2 (12)	O24m—C6n—H3c6n	101.85
C3e—C3f—C4e	114 (3)	C6m—C6n—H1c6m	106.81
C3e—C3f—H1c3e	79.94	C6m—C6n—O24n	97 (2)
C3e—C3f—C2f	25 (4)	C6m—C6n—H1c6n	153.22
C3e—C3f—C4f	126 (3)	C6m—C6n—H2c6n	61.16
C3e—C3f—H1c3f	108.17	C6m—C6n—H3c6n	57.56
C4e—C3f—H1c3e	156.01	H1c6m—C6n—O24n	155.91
C4e—C3f—C2f	102.6 (16)	H1c6m—C6n—H1c6n	46.45
C4e—C3f—C4f	17.5 (15)	H1c6m—C6n—H2c6n	83.96
C4e—C3f—H1c3f	136.22	H1c6m—C6n—H3c6n	83.18
H1c3e—C3f—C2f	97.67	O24n—C6n—H1c6n	109.47
H1c3e—C3f—C4f	138.67	O24n—C6n—H2c6n	109.47
H1c3e—C3f—H1c3f	29.81	O24n—C6n—H3c6n	109.47
C2f—C3f—C4f	118.7 (15)	H1c6n—C6n—H2c6n	109.47
C2f—C3f—H1c3f	120.64	H1c6n—C6n—H3c6n	109.47
C4f—C3f—H1c3f	120.64	H2c6n—C6n—H3c6n	109.47
C4e—C4f—H1c4e	135.94	O24m—C7n—C2m	127.0 (11)
C4e—C4f—C1f	74 (4)	O24m—C7n—C7m	164 (4)
C4e—C4f—C3f	51 (3)	O24m—C7n—O24n	12.6 (7)
C4e—C4f—H1c4f	157.63	O24m—C7n—C2n	127.0 (12)
H1c4e—C4f—C1f	125.34	O24m—C7n—C5n	112.9 (12)
H1c4e—C4f—C3f	109.92	C2m—C7n—C7m	69 (4)
H1c4e—C4f—H1c4f	21.87	C2m—C7n—O24n	114.4 (10)
C1f—C4f—C3f	120.6 (15)	C2m—C7n—C2n	0.5 (11)
C1f—C4f—H1c4f	119.69	C2m—C7n—C5n	120.1 (11)
C3f—C4f—H1c4f	119.69	C7m—C7n—O24n	177 (4)
C1e—C5f—C5e	120 (3)	C7m—C7n—C2n	69 (4)
C1e—C5f—C1f	22.6 (15)	C7m—C7n—C5n	51 (3)
C1e—C5f—C7f	108.9 (15)	O24n—C7n—C2n	114.5 (10)
C1e—C5f—H1c5f	125.84	O24n—C7n—C5n	125.5 (11)
C5e—C5f—C1f	143 (3)	C2n—C7n—C5n	120.1 (12)
C5e—C5f—C7f	51 (2)	H1c1m—H1c1n—C1n	82.92
C5e—C5f—H1c5f	80.2	C3m—H1c3n—H1c3m	118.52
C1f—C5f—C7f	118.6 (13)	C3m—H1c3n—C3n	11.18
C1f—C5f—H1c5f	120.72	H1c3m—H1c3n—C3n	129.68
C7f—C5f—H1c5f	120.72	C4m—H1c4n—H1c4m	77.97
O24e—C6f—C6e	86 (3)	C4m—H1c4n—C4n	29.73
O24e—C6f—H2c6e	126.84	H1c4m—H1c4n—C4n	107.7
O24e—C6f—H3c6e	109.77	H1c5m—H1c5n—C5n	57.67
O24e—C6f—O24f	17.9 (6)	H1c6m—H1c6n—C6n	38.15
O24e—C6f—H1c6f	92.75	C6m—H2c6n—H2c6m	77.55
O24e—C6f—H2c6f	111.04	C6m—H2c6n—C6n	38.09
O24e—C6f—H3c6f	123	H2c6m—H2c6n—C6n	115.41
C6e—C6f—H2c6e	95.12	C6m—H3c6n—H3c6m	82.58
C6e—C6f—H3c6e	70.7	C6m—H3c6n—C6n	38.43
C6e—C6f—O24f	101 (3)	H3c6m—H3c6n—C6n	120.54
C6e—C6f—H1c6f	10.93	H1n1m—H1n1n—N1n	75 (17)
C6e—C6f—H2c6f	119.84	N1m—H2n1n—H2n1m	111 (13)
C6e—C6f—H3c6f	106.79	N1m—H2n1n—N1n	10 (2)
H2c6e—C6f—H3c6e	120.55	H2n1m—H2n1n—N1n	120 (13)
H2c6e—C6f—O24f	132.59	C1oⁱⁱ—O24o—C4oⁱⁱ	66 (4)
H2c6e—C6f—H1c6f	84.23	C1oⁱⁱ—O24o—C5oⁱⁱ	125 (5)
H2c6e—C6f—H2c6f	28.43	C1oⁱⁱ—O24o—C6o	88 (4)
H2c6e—C6f—H3c6f	107.65	C1oⁱⁱ—O24o—C7o	155 (4)
H3c6e—C6f—O24f	106.85	C4oⁱⁱ—O24o—C5oⁱⁱ	169 (4)
H3c6e—C6f—H1c6f	75.81	C4oⁱⁱ—O24o—C6o	22 (3)
H3c6e—C6f—H2c6f	138.45	C4oⁱⁱ—O24o—C7o	139 (3)
H3c6e—C6f—H3c6f	37.51	C5oⁱⁱ—O24o—C6o	147 (4)
O24f—C6f—H1c6f	109.47	C5oⁱⁱ—O24o—C7o	30 (2)
O24f—C6f—H2c6f	109.47	C6o—O24o—C7o	117 (3)
O24f—C6f—H3c6f	109.47	C2o—N1o—H1n1o	111 (6)
H1c6f—C6f—H2c6f	109.47	C2o—N1o—H2n1o	118 (5)
H1c6f—C6f—H3c6f	109.47	H1n1o—N1o—H2n1o	120 (7)
H2c6f—C6f—H3c6f	109.47	O24oⁱⁱ—C1o—C4o	89 (5)
C2e—C7f—C5e	153.3 (13)	O24oⁱⁱ—C1o—C5o	32 (3)
C2e—C7f—C7e	87 (2)	O24oⁱⁱ—C1o—C6oⁱⁱ	67 (4)
C2e—C7f—O24f	97.7 (10)	O24oⁱⁱ—C1o—H1c1o	151.67
C2e—C7f—C2f	19.6 (8)	C4o—C1o—C5o	121 (4)
C2e—C7f—C5f	135.7 (12)	C4o—C1o—C6oⁱⁱ	22 (3)
C5e—C7f—C7e	119 (3)	C4o—C1o—H1c1o	119.6
C5e—C7f—O24f	108.5 (12)	C5o—C1o—C6oⁱⁱ	99 (4)
C5e—C7f—C2f	134.4 (12)	C5o—C1o—H1c1o	119.6
C5e—C7f—C5f	22.0 (11)	C6oⁱⁱ—C1o—H1c1o	141.14
C7e—C7f—O24f	11 (2)	N1o—C2o—C3o	119 (2)
C7e—C7f—C2f	104 (2)	N1o—C2o—C5oⁱⁱ	89 (2)
C7e—C7f—C5f	136 (2)	N1o—C2o—C7o	119 (2)
O24f—C7f—C2f	114.5 (10)	N1o—C2o—H1c5oⁱⁱ	48.38
O24f—C7f—C5f	125.5 (11)	C3o—C2o—C5oⁱⁱ	152 (3)
C2f—C7f—C5f	120.1 (11)	C3o—C2o—C7o	121 (2)
H1c1e—H1c1f—C1f	61.72	C3o—C2o—H1c5oⁱⁱ	167.71
H1c3e—H1c3f—C3f	72.67	C5oⁱⁱ—C2o—C7o	30.7 (13)
H1c4e—H1c4f—C4f	27.66	C5oⁱⁱ—C2o—H1c5oⁱⁱ	40.26
C5e—H1c5f—H1c5e	65.5	C7o—C2o—H1c5oⁱⁱ	70.97
C5e—H1c5f—C5f	31.9	C2o—C3o—C4o	119 (3)
H1c5e—H1c5f—C5f	96.89	C2o—C3o—C6oⁱⁱ	104 (4)
C6e—H1c6f—H1c6e	162.33	C2o—C3o—H1c3o	120.64
C6e—H1c6f—C6f	10.22	C2o—C3o—H2c6oⁱⁱ	93.41
H1c6e—H1c6f—C6f	168.3	C2o—C3o—H3c6oⁱⁱ	87.99
H2c6e—H2c6f—C6f	55.4	C4o—C3o—C6oⁱⁱ	15 (3)
H3c6e—H3c6f—C6f	75.21	C4o—C3o—H1c3o	120.64
N1e—H1n1f—H1n1e	72 (6)	C4o—C3o—H2c6oⁱⁱ	66.79
N1e—H1n1f—N1f	48 (4)	C4o—C3o—H3c6oⁱⁱ	71.72
H1n1e—H1n1f—N1f	119 (7)	C6oⁱⁱ—C3o—H1c3o	135.71
H2n1e—H2n1f—N1f	103 (8)	C6oⁱⁱ—C3o—H2c6oⁱⁱ	66.57
C6g—O24g—C7g	117.1 (12)	C6oⁱⁱ—C3o—H3c6oⁱⁱ	67.69
C6g—O24g—O24k	130 (3)	H1c3o—C3o—H2c6oⁱⁱ	109.17
C6g—O24g—C6k	16.8 (10)	H1c3o—C3o—H3c6oⁱⁱ	110
C7g—O24g—O24k	19 (3)	H2c6oⁱⁱ—C3o—H3c6oⁱⁱ	133.2
C7g—O24g—C6k	101.8 (13)	O24oⁱⁱ—C4o—C1o	26 (3)
O24k—O24g—C6k	113 (3)	O24oⁱⁱ—C4o—C3o	95 (4)
C2g—N1g—H1n1g	111 (3)	O24oⁱⁱ—C4o—C6oⁱⁱ	72 (5)
C2g—N1g—H2n1g	118 (3)	O24oⁱⁱ—C4o—H1c4o	145.29
C2g—N1g—N1k	83 (6)	O24oⁱⁱ—C4o—H1c6oⁱⁱ	158.19
C2g—N1g—C2k	12.3 (8)	C1o—C4o—C3o	121 (4)
C2g—N1g—H2n1k	120 (4)	C1o—C4o—C6oⁱⁱ	97 (6)
H1n1g—N1g—H2n1g	120 (5)	C1o—C4o—H1c4o	119.69
H1n1g—N1g—N1k	72 (8)	C1o—C4o—H1c6oⁱⁱ	133.9
H1n1g—N1g—C2k	105 (3)	C3o—C4o—C6oⁱⁱ	23 (4)
H1n1g—N1g—H2n1k	123 (6)	C3o—C4o—H1c4o	119.69
H2n1g—N1g—N1k	142 (8)	C3o—C4o—H1c6oⁱⁱ	104.59
H2n1g—N1g—C2k	129 (3)	C6oⁱⁱ—C4o—H1c4o	143.03
H2n1g—N1g—H2n1k	9 (6)	C6oⁱⁱ—C4o—H1c6oⁱⁱ	127.18
N1k—N1g—C2k	71 (5)	H1c4o—C4o—H1c6oⁱⁱ	17.4
N1k—N1g—H2n1k	133 (9)	O24oⁱⁱ—C5o—C1o	23 (3)
C2k—N1g—H2n1k	130 (4)	O24oⁱⁱ—C5o—C2oⁱⁱ	175 (4)
C4g—C1g—C5g	120.8 (18)	O24oⁱⁱ—C5o—C7o	96 (3)
C4g—C1g—H1c1g	119.6	O24oⁱⁱ—C5o—C7oⁱⁱ	113 (3)
C4g—C1g—C1k	33 (3)	O24oⁱⁱ—C5o—H1c5o	143.41
C4g—C1g—C5k	113 (2)	C1o—C5o—C2oⁱⁱ	152 (3)
C5g—C1g—H1c1g	119.6	C1o—C5o—C7o	119 (2)
C5g—C1g—C1k	154 (4)	C1o—C5o—C7oⁱⁱ	136 (3)
C5g—C1g—C5k	8.9 (11)	C1o—C5o—H1c5o	120.72
H1c1g—C1g—C1k	86.59	C2oⁱⁱ—C5o—C7o	89 (2)
H1c1g—C1g—C5k	127.43	C2oⁱⁱ—C5o—C7oⁱⁱ	72 (2)
C1k—C1g—C5k	145 (4)	C2oⁱⁱ—C5o—H1c5o	31.35
N1g—C2g—C3g	119.4 (13)	C7o—C5o—C7oⁱⁱ	17.5 (12)
N1g—C2g—C7g	119.3 (14)	C7o—C5o—H1c5o	120.72
N1g—C2g—N1k	10.3 (12)	C7oⁱⁱ—C5o—H1c5o	103.29
N1g—C2g—C2k	95 (3)	O24o—C6o—C1oⁱⁱ	25 (2)
N1g—C2g—C7k	131.9 (16)	O24o—C6o—C3oⁱⁱ	132 (5)
C3g—C2g—C7g	121.2 (13)	O24o—C6o—C4oⁱⁱ	86 (5)
C3g—C2g—N1k	109.4 (13)	O24o—C6o—H1c6o	109.47
C3g—C2g—C2k	25 (3)	O24o—C6o—H2c6o	109.47
C3g—C2g—C7k	108.6 (14)	O24o—C6o—H3c6o	109.47
C7g—C2g—N1k	129.4 (14)	C1oⁱⁱ—C6o—C3oⁱⁱ	157 (5)
C7g—C2g—C2k	145 (4)	C1oⁱⁱ—C6o—C4oⁱⁱ	61 (5)
C7g—C2g—C7k	12.8 (8)	C1oⁱⁱ—C6o—H1c6o	84.78
N1k—C2g—C2k	85 (3)	C1oⁱⁱ—C6o—H2c6o	118.37
N1k—C2g—C7k	142.0 (16)	C1oⁱⁱ—C6o—H3c6o	121.6
C2k—C2g—C7k	133 (4)	C3oⁱⁱ—C6o—C4oⁱⁱ	141 (7)
C2g—C3g—C4g	118.7 (15)	C3oⁱⁱ—C6o—H1c6o	118.04
C2g—C3g—H1c3g	120.64	C3oⁱⁱ—C6o—H2c6o	55.99
C2g—C3g—C2k	7.2 (9)	C3oⁱⁱ—C6o—H3c6o	54.12
C2g—C3g—C3k	144 (4)	C4oⁱⁱ—C6o—H1c6o	24.11
C2g—C3g—C4k	135.8 (15)	C4oⁱⁱ—C6o—H2c6o	114.51
C4g—C3g—H1c3g	120.64	C4oⁱⁱ—C6o—H3c6o	124.64
C4g—C3g—C2k	125.7 (17)	H1c6o—C6o—H2c6o	109.47
C4g—C3g—C3k	95 (4)	H1c6o—C6o—H3c6o	109.47
C4g—C3g—C4k	17.3 (13)	H2c6o—C6o—H3c6o	109.47
H1c3g—C3g—C2k	113.62	O24o—C7o—C2o	114.5 (16)
H1c3g—C3g—C3k	28.15	O24o—C7o—C5o	125.5 (15)
H1c3g—C3g—C4k	103.46	O24o—C7o—C5oⁱⁱ	37 (2)
C2k—C3g—C3k	137 (4)	O24o—C7o—C7oⁱⁱ	107.9 (16)
C2k—C3g—C4k	142.7 (17)	C2o—C7o—C5o	120.1 (17)
C3k—C3g—C4k	78 (4)	C2o—C7o—C5oⁱⁱ	77 (2)
C1g—C4g—C3g	120.6 (19)	C2o—C7o—C7oⁱⁱ	137.7 (19)
C1g—C4g—H1c4g	119.69	C5o—C7o—C5oⁱⁱ	163 (2)
C1g—C4g—C1k	13.9 (14)	C5o—C7o—C7oⁱⁱ	17.6 (14)
C1g—C4g—C3k	134.5 (19)	C5oⁱⁱ—C7o—C7oⁱⁱ	145 (2)
C1g—C4g—C4k	153 (5)	C4o—H1c4o—H1c6oⁱⁱ	16.71
C3g—C4g—H1c4g	119.69	C2oⁱⁱ—H1c5o—C5o	108.39
C3g—C4g—C1k	134 (2)	C4oⁱⁱ—H1c6o—C6o	28.71
C3g—C4g—C3k	14.3 (12)	C4oⁱⁱ—H1c6o—H1c4oⁱⁱ	145.88
C3g—C4g—C4k	85 (4)	C6o—H1c6o—H1c4oⁱⁱ	167.79
H1c4g—C4g—C1k	105.84	C3oⁱⁱ—H2c6o—C6o	57.44
H1c4g—C4g—C3k	105.71	C3oⁱⁱ—H3c6o—C6o	58.19
H1c4g—C4g—C4k	35.08	O1a—Mo1a—O6a	101.5 (3)
C1k—C4g—C3k	148 (2)	O1a—Mo1a—O13a	102.1 (3)
C1k—C4g—C4k	140 (5)	O1a—Mo1a—O18a	144.5 (2)
C3k—C4g—C4k	71 (4)	O6a—Mo1a—O13a	103.5 (3)
C1g—C5g—C7g	118.6 (14)	O6a—Mo1a—O18a	99.3 (3)
C1g—C5g—H1c5g	120.72	O13a—Mo1a—O18a	100.5 (3)
C1g—C5g—C5k	20 (3)	O2a—Mo2a—O3a	105.8 (3)
C1g—C5g—C7k	103.4 (14)	O2a—Mo2a—O12a	95.2 (3)
C1g—C5g—H1c5k	93.36	O2a—Mo2a—O18a	99.8 (3)
C7g—C5g—H1c5g	120.72	O3a—Mo2a—O12a	102.3 (3)
C7g—C5g—C5k	100 (3)	O3a—Mo2a—O18a	97.5 (3)
C7g—C5g—C7k	15.2 (7)	O12a—Mo2a—O18a	150.9 (3)
C7g—C5g—H1c5k	146.8	O10a—Mo3a—O12a	144.9 (3)
H1c5g—C5g—C5k	138.37	O10a—Mo3a—O16a	101.6 (3)
H1c5g—C5g—C7k	135.84	O10a—Mo3a—O19a	99.3 (3)
H1c5g—C5g—H1c5k	28.8	O12a—Mo3a—O16a	99.9 (3)
C5k—C5g—C7k	85 (3)	O12a—Mo3a—O19a	102.3 (3)
C5k—C5g—H1c5k	109.69	O16a—Mo3a—O19a	103.5 (3)
C7k—C5g—H1c5k	159.84	O1a—Mo4a—O4a	103.6 (3)
O24g—C6g—H1c6g	109.47	O1a—Mo4a—O20a	99.1 (3)
O24g—C6g—H2c6g	109.47	O1a—Mo4a—O21a	144.2 (2)
O24g—C6g—H3c6g	109.47	O4a—Mo4a—O20a	101.9 (3)
O24g—C6g—C6k	58 (3)	O4a—Mo4a—O21a	102.9 (3)
O24g—C6g—H1c6k	103.03	O20a—Mo4a—O21a	98.6 (3)
O24g—C6g—H3c6k	95.81	O7a—Mo5a—O10a	93.9 (3)
H1c6g—C6g—H2c6g	109.47	O7a—Mo5a—O21a	100.6 (3)
H1c6g—C6g—H3c6g	109.47	O7a—Mo5a—O23a	105.4 (3)
H1c6g—C6g—C6k	156.68	O10a—Mo5a—O21a	153.6 (2)
H1c6g—C6g—H1c6k	16.61	O10a—Mo5a—O23a	99.6 (3)
H1c6g—C6g—H3c6k	134.67	O21a—Mo5a—O23a	97.6 (3)
H2c6g—C6g—H3c6g	109.47	O5a—P1a—O11a	109.2 (3)
H2c6g—C6g—C6k	63.49	O5a—P1a—O14a	108.5 (3)
H2c6g—C6g—H1c6k	98.49	O5a—P1a—O17a	106.0 (3)
H2c6g—C6g—H3c6k	95.77	O11a—P1a—O14a	107.2 (3)
H3c6g—C6g—C6k	93.64	O11a—P1a—O17a	113.0 (3)
H3c6g—C6g—H1c6k	125.81	O14a—P1a—O17a	112.8 (3)
H3c6g—C6g—H3c6k	25.2	O8a—P2a—O9a	107.5 (3)
C6k—C6g—H1c6k	140.54	O8a—P2a—O15a	111.4 (3)
C6k—C6g—H3c6k	68.48	O8a—P2a—O22a	108.0 (3)
H1c6k—C6g—H3c6k	150.94	O9a—P2a—O15a	108.7 (3)
O24g—C7g—C2g	114.5 (11)	O9a—P2a—O22a	110.8 (3)
O24g—C7g—C5g	125.5 (12)	O15a—P2a—O22a	110.4 (3)
O24g—C7g—O24k	6.4 (9)	Mo1a—O1a—Mo4a	149.6 (3)
O24g—C7g—C5k	141.4 (12)	Mo3a—O10a—Mo5a	120.7 (3)
O24g—C7g—C7k	156 (3)	Mo2a—O12a—Mo3a	122.3 (3)
C2g—C7g—C5g	120.1 (12)	Mo1a—O18a—Mo2a	121.3 (2)
C2g—C7g—O24k	109.8 (13)	Mo4a—O21a—Mo5a	122.7 (3)
C2g—C7g—C5k	104.1 (11)	Mo1bx—Mo1b—O14bx	112.6 (5)
C2g—C7g—C7k	43 (2)	Mo1bx—Mo1b—O6bx	76.0 (6)
C5g—C7g—O24k	129.8 (14)	Mo1bx—Mo1b—O18bx	154.3 (6)
C5g—C7g—C5k	16.2 (8)	Mo1bx—Mo1b—O13bx	49.3 (6)
C5g—C7g—C7k	78 (3)	Mo1bx—Mo1b—O1b	40.5 (3)
O24k—C7g—C5k	145.3 (14)	Mo1bx—Mo1b—O6b	84.4 (4)
O24k—C7g—C7k	150 (3)	Mo1bx—Mo1b—O13b	70.8 (4)
C5k—C7g—C7k	62 (2)	Mo1bx—Mo1b—O18b	171.3 (4)
C1g—H1c1g—C1k	25.87	O14bx—Mo1b—O6bx	89.1 (5)
C1g—H1c1g—H1c1k	92.96	O14bx—Mo1b—O18bx	92.3 (5)
C1k—H1c1g—H1c1k	67.11	O14bx—Mo1b—O13bx	161.2 (6)
C3g—H1c3g—C3k	14.92	O14bx—Mo1b—O1b	79.7 (3)
C3g—H1c3g—H1c3k	152.04	O14bx—Mo1b—O6b	80.1 (3)
C3k—H1c3g—H1c3k	137.93	O14bx—Mo1b—O13b	175.4 (4)
C4g—H1c4g—C4k	21.47	O14bx—Mo1b—O18b	75.9 (4)
C4g—H1c4g—H1c4k	139.55	O6bx—Mo1b—O18bx	112.1 (7)
C4k—H1c4g—H1c4k	118.12	O6bx—Mo1b—O13bx	90.6 (6)
C5g—H1c5g—H1c5k	46.61	O6bx—Mo1b—O1b	98.3 (5)
C6g—H1c6g—H1c6k	22.73	O6bx—Mo1b—O6b	10.3 (5)
C6g—H2c6g—C6k	26.83	O6bx—Mo1b—O13b	94.8 (5)
C6g—H2c6g—H2c6k	113.12	O6bx—Mo1b—O18b	106.7 (5)
C6k—H2c6g—H2c6k	86.36	O18bx—Mo1b—O13bx	105.2 (7)
C6g—H3c6g—H3c6k	86.37	O18bx—Mo1b—O1b	148.6 (5)
N1g—H1n1g—N1k	18 (2)	O18bx—Mo1b—O6b	107.0 (5)
N1g—H1n1g—H1n1k	106 (17)	O18bx—Mo1b—O13b	84.0 (5)
N1k—H1n1g—H1n1k	89 (16)	O18bx—Mo1b—O18b	17.0 (5)
N1g—H2n1g—H2n1k	27 (16)	O13bx—Mo1b—O1b	81.8 (5)
C6h—O24h—C7h	117.1 (12)	O13bx—Mo1b—O6b	100.7 (5)
C6h—O24h—O24l	56 (3)	O13bx—Mo1b—O13b	21.6 (5)
C6h—O24h—C7l	111.4 (14)	O13bx—Mo1b—O18b	122.0 (5)
C7h—O24h—O24l	152 (4)	O1b—Mo1b—O6b	101.5 (3)
C7h—O24h—C7l	6.7 (9)	O1b—Mo1b—O13b	102.1 (3)
O24l—O24h—C7l	146 (4)	O1b—Mo1b—O18b	144.5 (3)
C2h—N1h—H1n1h	111 (4)	O6b—Mo1b—O13b	103.5 (3)
C2h—N1h—H2n1h	118 (3)	O6b—Mo1b—O18b	99.3 (3)
C2h—N1h—N1l	103 (6)	O13b—Mo1b—O18b	100.5 (3)
C2h—N1h—C2l	11.5 (8)	Mo2bx—Mo2b—O3bx	90.7 (7)
C2h—N1h—H1n1l	117 (5)	Mo2bx—Mo2b—O17bx	133.0 (6)
H1n1h—N1h—H2n1h	120 (5)	Mo2bx—Mo2b—O18bx	46.1 (6)
H1n1h—N1h—N1l	116 (9)	Mo2bx—Mo2b—O12bx	140.5 (7)
H1n1h—N1h—C2l	117 (4)	Mo2bx—Mo2b—O2bx	45.0 (8)
H1n1h—N1h—H1n1l	19 (4)	Mo2bx—Mo2b—O2b	45.1 (6)
H2n1h—N1h—N1l	24 (8)	Mo2bx—Mo2b—O3b	105.0 (4)
H2n1h—N1h—C2l	107 (3)	Mo2bx—Mo2b—O12b	136.6 (5)
H2n1h—N1h—H1n1l	104 (5)	Mo2bx—Mo2b—O18b	54.9 (5)
N1l—N1h—C2l	91 (6)	O3bx—Mo2b—O17bx	91.5 (6)
N1l—N1h—H1n1l	98 (9)	O3bx—Mo2b—O18bx	91.2 (6)
C2l—N1h—H1n1l	119 (5)	O3bx—Mo2b—O12bx	108.5 (6)
C4h—C1h—C5h	120.8 (16)	O3bx—Mo2b—O2bx	94.6 (7)
C4h—C1h—H1c1h	119.6	O3bx—Mo2b—O2b	107.6 (6)
C4h—C1h—C1l	141 (4)	O3bx—Mo2b—O3b	22.1 (5)
C4h—C1h—C4l	11.4 (11)	O3bx—Mo2b—O12b	123.2 (5)
C4h—C1h—H1c1l	143.74	O3bx—Mo2b—O18b	75.5 (5)
C5h—C1h—H1c1h	119.6	O17bx—Mo2b—O18bx	87.0 (5)
C5h—C1h—C1l	21 (4)	O17bx—Mo2b—O12bx	82.0 (5)
C5h—C1h—C4l	110.6 (17)	O17bx—Mo2b—O2bx	173.6 (5)
C5h—C1h—H1c1l	95.42	O17bx—Mo2b—O2b	160.5 (3)
H1c1h—C1h—C1l	98.9	O17bx—Mo2b—O3b	93.5 (4)
H1c1h—C1h—C4l	129.53	O17bx—Mo2b—O12b	77.3 (4)
H1c1h—C1h—H1c1l	24.26	O17bx—Mo2b—O18b	80.4 (4)
C1l—C1h—C4l	131 (4)	O18bx—Mo2b—O12bx	157.6 (4)
C1l—C1h—H1c1l	74.64	O18bx—Mo2b—O2bx	90.9 (6)
C4l—C1h—H1c1l	152.95	O18bx—Mo2b—O2b	88.3 (4)
N1h—C2h—C3h	119.4 (13)	O18bx—Mo2b—O3b	113.2 (4)
N1h—C2h—C7h	119.3 (13)	O18bx—Mo2b—O12b	141.9 (3)
N1h—C2h—N1l	9.0 (9)	O18bx—Mo2b—O18b	17.2 (4)
N1h—C2h—C2l	79 (4)	O12bx—Mo2b—O2bx	98.0 (7)
N1h—C2h—C3l	126.4 (15)	O12bx—Mo2b—O2b	95.6 (5)
C3h—C2h—C7h	121.2 (14)	O12bx—Mo2b—O3b	87.0 (4)
C3h—C2h—N1l	128.4 (13)	O12bx—Mo2b—O12b	15.8 (4)
C3h—C2h—C2l	161 (5)	O12bx—Mo2b—O18b	162.1 (4)
C3h—C2h—C3l	8.6 (14)	O2bx—Mo2b—O2b	13.2 (4)
C7h—C2h—N1l	110.4 (13)	O2bx—Mo2b—O3b	92.9 (5)
C7h—C2h—C2l	40 (4)	O2bx—Mo2b—O12b	101.0 (5)
C7h—C2h—C3l	114.0 (15)	O2bx—Mo2b—O18b	99.1 (6)
N1l—C2h—C2l	70 (4)	O2b—Mo2b—O3b	105.8 (3)
N1l—C2h—C3l	135.3 (14)	O2b—Mo2b—O12b	95.2 (3)
C2l—C2h—C3l	153 (5)	O2b—Mo2b—O18b	99.8 (3)
C2h—C3h—C4h	118.7 (14)	O3b—Mo2b—O12b	102.3 (3)
C2h—C3h—H1c3h	120.64	O3b—Mo2b—O18b	97.5 (3)
C2h—C3h—C3l	31 (6)	O12b—Mo2b—O18b	150.9 (3)
C2h—C3h—C4l	104.1 (13)	Mo3bx—Mo3b—O15bx	116.5 (4)
C2h—C3h—H1c3l	108.78	Mo3bx—Mo3b—O10bx	110.3 (5)
C4h—C3h—H1c3h	120.64	Mo3bx—Mo3b—O19bx	41.1 (6)
C4h—C3h—C3l	92 (5)	Mo3bx—Mo3b—O16bx	113.1 (7)
C4h—C3h—C4l	15.1 (10)	Mo3bx—Mo3b—O10b	118.2 (4)
C4h—C3h—H1c3l	130.98	Mo3bx—Mo3b—O12b	60.1 (4)
H1c3h—C3h—C3l	143.15	Mo3bx—Mo3b—O16b	133.9 (5)
H1c3h—C3h—C4l	135.04	Mo3bx—Mo3b—O19b	50.7 (4)
H1c3h—C3h—H1c3l	16.39	O15bx—Mo3b—O10bx	83.2 (4)
C3l—C3h—C4l	77 (5)	O15bx—Mo3b—O19bx	151.1 (5)
C3l—C3h—H1c3l	127.3	O15bx—Mo3b—O16bx	109.5 (6)
C4l—C3h—H1c3l	143.15	O15bx—Mo3b—O10b	78.5 (3)
C1h—C4h—C3h	120.6 (16)	O15bx—Mo3b—O12b	73.3 (3)
C1h—C4h—H1c4h	119.69	O15bx—Mo3b—O16b	92.2 (4)
C1h—C4h—C3l	108.0 (14)	O15bx—Mo3b—O19b	164.3 (4)
C1h—C4h—C4l	36 (4)	O10bx—Mo3b—O19bx	89.4 (6)
C1h—C4h—H1c4l	102.43	O10bx—Mo3b—O16bx	121.2 (8)
C3h—C4h—H1c4h	119.69	O10bx—Mo3b—O10b	8.0 (4)
C3h—C4h—C3l	13.1 (9)	O10bx—Mo3b—O12b	143.9 (4)
C3h—C4h—C4l	88 (4)	O10bx—Mo3b—O16b	108.1 (4)
C3h—C4h—H1c4l	134.93	O10bx—Mo3b—O19b	93.0 (4)
H1c4h—C4h—C3l	132.16	O19bx—Mo3b—O16bx	98.3 (7)
H1c4h—C4h—C4l	148.56	O19bx—Mo3b—O10b	96.6 (5)
H1c4h—C4h—H1c4l	21.54	O19bx—Mo3b—O12b	98.1 (5)
C3l—C4h—C4l	75 (4)	O19bx—Mo3b—O16b	116.7 (4)
C3l—C4h—H1c4l	144.84	O19bx—Mo3b—O19b	13.3 (4)
C4l—C4h—H1c4l	127.14	O16bx—Mo3b—O10b	116.4 (7)
C1h—C5h—C7h	118.6 (14)	O16bx—Mo3b—O12b	92.7 (7)
C1h—C5h—H1c5h	120.72	O16bx—Mo3b—O16b	21.4 (6)
C1h—C5h—C1l	7.5 (14)	O16bx—Mo3b—O19b	85.5 (6)
C1h—C5h—C5l	163 (4)	O10b—Mo3b—O12b	144.9 (3)
C1h—C5h—C7l	130.1 (14)	O10b—Mo3b—O16b	101.6 (3)
C7h—C5h—H1c5h	120.72	O10b—Mo3b—O19b	99.3 (3)
C7h—C5h—C1l	125.9 (18)	O12b—Mo3b—O16b	99.9 (3)
C7h—C5h—C5l	76 (3)	O12b—Mo3b—O19b	102.3 (3)
C7h—C5h—C7l	11.9 (7)	O16b—Mo3b—O19b	103.5 (3)
H1c5h—C5h—C1l	113.34	Mo4bx—Mo4b—O1bx	85.5 (9)
H1c5h—C5h—C5l	45.84	Mo4bx—Mo4b—O20bx	61.3 (10)
H1c5h—C5h—C7l	109.11	Mo4bx—Mo4b—O21bx	74.0 (9)
C1l—C5h—C5l	157 (4)	Mo4bx—Mo4b—O4bx	165.6 (11)
C1l—C5h—C7l	137.5 (18)	Mo4bx—Mo4b—O1b	89.6 (8)
C5l—C5h—C7l	64 (3)	Mo4bx—Mo4b—O4b	158.9 (10)
O24h—C6h—H1c6h	109.47	Mo4bx—Mo4b—O20b	59.2 (10)
O24h—C6h—H2c6h	109.47	Mo4bx—Mo4b—O21b	73.4 (8)
O24h—C6h—H3c6h	109.47	O1bx—Mo4b—O20bx	98.9 (6)
O24h—C6h—O24l	12.6 (10)	O1bx—Mo4b—O21bx	142.2 (5)
O24h—C6h—C6l	117 (4)	O1bx—Mo4b—O4bx	108.0 (7)
O24h—C6h—H2c6l	134.17	O1bx—Mo4b—O1b	16.4 (4)
H1c6h—C6h—H2c6h	109.47	O1bx—Mo4b—O4b	102.4 (4)
H1c6h—C6h—H3c6h	109.47	O1bx—Mo4b—O20b	83.4 (4)
H1c6h—C6h—O24l	98.29	O1bx—Mo4b—O21b	153.6 (4)
H1c6h—C6h—C6l	33.46	O20bx—Mo4b—O21bx	98.6 (6)
H1c6h—C6h—H2c6l	84.44	O20bx—Mo4b—O4bx	110.3 (8)
H2c6h—C6h—H3c6h	109.47	O20bx—Mo4b—O1b	114.6 (5)
H2c6h—C6h—O24l	119.96	O20bx—Mo4b—O4b	98.0 (5)
H2c6h—C6h—C6l	127.52	O20bx—Mo4b—O20b	15.5 (5)
H2c6h—C6h—H2c6l	29.11	O20bx—Mo4b—O21b	84.9 (5)
H3c6h—C6h—O24l	109.41	O21bx—Mo4b—O4bx	96.9 (6)
H3c6h—C6h—C6l	76.44	O21bx—Mo4b—O1b	129.8 (4)
H3c6h—C6h—H2c6l	105.89	O21bx—Mo4b—O4b	108.0 (3)
O24l—C6h—C6l	105 (4)	O21bx—Mo4b—O20b	111.0 (4)
O24l—C6h—H2c6l	141.22	O21bx—Mo4b—O21b	15.5 (5)
C6l—C6h—H2c6l	98.41	O4bx—Mo4b—O1b	104.8 (7)
O24h—C7h—C2h	114.5 (12)	O4bx—Mo4b—O4b	15.1 (6)
O24h—C7h—C5h	125.5 (12)	O4bx—Mo4b—O20b	116.1 (7)
O24h—C7h—C2l	105.2 (13)	O4bx—Mo4b—O21b	94.9 (6)
O24h—C7h—C5l	110.5 (12)	O1b—Mo4b—O4b	103.6 (3)
O24h—C7h—C7l	23 (3)	O1b—Mo4b—O20b	99.1 (3)
C2h—C7h—C5h	120.1 (13)	O1b—Mo4b—O21b	144.2 (3)
C2h—C7h—C2l	9.3 (10)	O4b—Mo4b—O20b	101.9 (4)
C2h—C7h—C5l	135.0 (13)	O4b—Mo4b—O21b	102.9 (3)
C2h—C7h—C7l	132 (3)	O20b—Mo4b—O21b	98.6 (3)
C5h—C7h—C2l	129.4 (14)	Mo5bx—Mo5b—O23bx	71.5 (7)
C5h—C7h—C5l	15.2 (10)	Mo5bx—Mo5b—O7bx	126.3 (8)
C5h—C7h—C7l	106 (3)	Mo5bx—Mo5b—O21bx	110.1 (7)
C2l—C7h—C5l	144.3 (14)	Mo5bx—Mo5b—O7b	130.2 (5)
C2l—C7h—C7l	124 (4)	Mo5bx—Mo5b—O10b	36.4 (5)
C5l—C7h—C7l	91 (3)	Mo5bx—Mo5b—O21b	126.0 (5)
C1h—H1c1h—H1c1l	81.7	Mo5bx—Mo5b—O23b	86.4 (6)
C3h—H1c3h—H1c3l	37.96	O23bx—Mo5b—O7bx	111.3 (9)
C4h—H1c4h—H1c4l	38.49	O23bx—Mo5b—O21bx	98.3 (6)
C5h—H1c5h—C5l	20.46	O23bx—Mo5b—O7b	116.9 (6)
C5h—H1c5h—H1c5l	129.56	O23bx—Mo5b—O10b	88.8 (6)
C5l—H1c5h—H1c5l	109.28	O23bx—Mo5b—O21b	103.8 (6)
C6h—H1c6h—C6l	19.95	O23bx—Mo5b—O23b	15.1 (6)
C6h—H1c6h—H1c6l	141.93	O7bx—Mo5b—O21bx	121.7 (9)
C6l—H1c6h—H1c6l	122.23	O7bx—Mo5b—O7b	6.6 (8)
C6h—H2c6h—H2c6l	57.54	O7bx—Mo5b—O10b	90.5 (7)
C6h—H3c6h—C6l	24.65	O7bx—Mo5b—O21b	105.9 (8)
C6h—H3c6h—H3c6l	104.4	O7bx—Mo5b—O23b	100.5 (7)
C6l—H3c6h—H3c6l	79.78	O21bx—Mo5b—O7b	116.2 (5)
N1h—H1n1h—H1n1l	67 (15)	O21bx—Mo5b—O10b	140.7 (5)
N1h—H2n1h—N1l	9 (3)	O21bx—Mo5b—O21b	16.0 (5)
N1h—H2n1h—H2n1l	170 (19)	O21bx—Mo5b—O23b	96.1 (4)
N1l—H2n1h—H2n1l	160 (20)	O7b—Mo5b—O10b	93.9 (3)
C6i—O24i—C7i	117.1 (12)	O7b—Mo5b—O21b	100.6 (3)
C6i—O24i—O24j	65 (3)	O7b—Mo5b—O23b	105.4 (4)
C6i—O24i—C7j	113.7 (14)	O10b—Mo5b—O21b	153.6 (3)
C7i—O24i—O24j	132 (4)	O10b—Mo5b—O23b	99.6 (3)
C7i—O24i—C7j	7.7 (8)	O21b—Mo5b—O23b	97.6 (3)
O24j—O24i—C7j	125 (4)	P1bx—P1b—O5bx	104.8 (18)
C2i—N1i—H1n1i	111 (3)	P1bx—P1b—O17bx	90 (2)
C2i—N1i—H2n1i	118 (3)	P1bx—P1b—O11bx	119.1 (17)
C2i—N1i—N1j	108 (5)	P1bx—P1b—O5b	112.1 (18)
C2i—N1i—C2j	11.3 (7)	P1bx—P1b—O11b	113.5 (16)
C2i—N1i—H1n1j	134 (4)	P1bx—P1b—O14b	10.2 (19)
H1n1i—N1i—H2n1i	120 (5)	P1bx—P1b—O17b	103 (2)
H1n1i—N1i—N1j	139 (6)	O5bx—P1b—O17bx	107.9 (7)
H1n1i—N1i—C2j	120 (3)	O5bx—P1b—O11bx	113.3 (7)
H1n1i—N1i—H1n1j	25 (5)	O5bx—P1b—O5b	12.8 (6)
H2n1i—N1i—N1j	23 (6)	O5bx—P1b—O11b	122.0 (6)
H2n1i—N1i—C2j	107 (3)	O5bx—P1b—O14b	103.2 (6)
H2n1i—N1i—H1n1j	96 (5)	O5bx—P1b—O17b	98.3 (6)
N1j—N1i—C2j	97 (5)	O17bx—P1b—O11bx	119.0 (5)
N1j—N1i—H1n1j	114 (7)	O17bx—P1b—O5b	117.3 (5)
C2j—N1i—H1n1j	141 (5)	O17bx—P1b—O11b	113.9 (4)
C4i—C1i—C5i	120.8 (15)	O17bx—P1b—O14b	99.8 (4)
C4i—C1i—H1c1i	119.6	O17bx—P1b—O17b	14.3 (4)
C4i—C1i—C1j	125 (5)	O11bx—P1b—O5b	100.6 (4)
C4i—C1i—C4j	14.1 (17)	O11bx—P1b—O11b	8.7 (4)
C4i—C1i—H1c1j	137.88	O11bx—P1b—O14b	111.8 (4)
C5i—C1i—H1c1i	119.6	O11bx—P1b—O17b	116.0 (4)
C5i—C1i—C1j	25 (4)	O5b—P1b—O11b	109.2 (3)
C5i—C1i—C4j	109.3 (16)	O5b—P1b—O14b	108.5 (3)
C5i—C1i—H1c1j	99.1	O5b—P1b—O17b	106.0 (3)
H1c1i—C1i—C1j	109.73	O11b—P1b—O14b	107.2 (3)
H1c1i—C1i—C4j	130.31	O11b—P1b—O17b	113.0 (3)
H1c1i—C1i—H1c1j	24.37	O14b—P1b—O17b	112.8 (3)
C1j—C1i—C4j	111 (5)	P2bx—P2b—O15bx	97 (2)
C1j—C1i—H1c1j	85.71	P2bx—P2b—O22bx	105 (2)
C4j—C1i—H1c1j	143.58	P2bx—P2b—O9bx	104 (2)
N1i—C2i—C3i	119.4 (14)	P2bx—P2b—O8b	55 (2)
N1i—C2i—C7i	119.3 (13)	P2bx—P2b—O9b	55 (2)
N1i—C2i—C2j	69 (4)	P2bx—P2b—O15b	111 (2)
N1i—C2i—C3j	121.8 (15)	P2bx—P2b—O22b	139 (2)
N1i—C2i—C7j	110.8 (12)	O15bx—P2b—O22bx	115.1 (6)
C3i—C2i—C7i	121.2 (14)	O15bx—P2b—O9bx	111.6 (7)
C3i—C2i—C2j	161 (6)	O15bx—P2b—O8b	100.7 (4)
C3i—C2i—C3j	4.2 (16)	O15bx—P2b—O9b	104.7 (5)
C3i—C2i—C7j	129.6 (13)	O15bx—P2b—O15b	14.2 (3)
C7i—C2i—C2j	54 (4)	O15bx—P2b—O22b	123.8 (4)
C7i—C2i—C3j	118.7 (16)	O22bx—P2b—O9bx	119.9 (7)
C7i—C2i—C7j	9.8 (6)	O22bx—P2b—O8b	54.2 (4)
C2j—C2i—C3j	163 (6)	O22bx—P2b—O9b	138.2 (5)
C2j—C2i—C7j	44 (4)	O22bx—P2b—O15b	113.0 (4)
C3j—C2i—C7j	127.4 (15)	O22bx—P2b—O22b	56.5 (4)
C2i—C3i—C4i	118.7 (16)	O9bx—P2b—O8b	144.0 (7)
C2i—C3i—H1c3i	120.64	O9bx—P2b—O9b	50.0 (7)
C2i—C3i—C3j	16 (5)	O9bx—P2b—O15b	103.2 (6)
C2i—C3i—C4j	105.8 (16)	O9bx—P2b—O22b	66.8 (6)
C2i—C3i—H1c3j	105.23	O8b—P2b—O9b	107.5 (4)
C4i—C3i—H1c3i	120.64	O8b—P2b—O15b	111.4 (3)
C4i—C3i—C3j	109 (5)	O8b—P2b—O22b	108.0 (3)
C4i—C3i—C4j	15.0 (17)	O9b—P2b—O15b	108.7 (4)
C4i—C3i—H1c3j	135.54	O9b—P2b—O22b	110.8 (4)
H1c3i—C3i—C3j	128.7	O15b—P2b—O22b	110.4 (4)
H1c3i—C3i—C4j	132.91	Mo1bx—O1b—Mo4bx	155.0 (4)
H1c3i—C3i—H1c3j	16.69	Mo1bx—O1b—O1bx	115.3 (10)
C3j—C3i—C4j	95 (5)	Mo1bx—O1b—Mo1b	10.00 (10)
C3j—C3i—H1c3j	112.12	Mo1bx—O1b—Mo4b	157.9 (4)
C4j—C3i—H1c3j	145.56	Mo4bx—O1b—O1bx	80.8 (10)
C1i—C4i—C3i	120.6 (18)	Mo4bx—O1b—Mo1b	145.8 (3)
C1i—C4i—H1c4i	119.69	Mo4bx—O1b—Mo4b	6.29 (8)
C1i—C4i—C3j	110.2 (17)	O1bx—O1b—Mo1b	116.6 (10)
C1i—C4i—C4j	56 (4)	O1bx—O1b—Mo4b	82.4 (9)
C1i—C4i—H1c4j	111.77	Mo1b—O1b—Mo4b	149.6 (4)
C3i—C4i—H1c4i	119.69	Mo2bx—O2b—O2bx	110 (2)
C3i—C4i—C3j	10.7 (11)	Mo2bx—O2b—Mo2b	9.43 (12)
C3i—C4i—C4j	74 (4)	O2bx—O2b—Mo2b	112 (2)
C3i—C4i—H1c4j	122.03	Mo2bx—O3b—O3bx	69.1 (10)
H1c4i—C4i—C3j	130.06	Mo2bx—O3b—Mo2b	10.56 (9)
H1c4i—C4i—C4j	148.02	O3bx—O3b—Mo2b	75.5 (10)
H1c4i—C4i—H1c4j	24.52	Mo4bx—O4b—O4bx	58.3 (16)
C3j—C4i—C4j	64 (4)	Mo4bx—O4b—Mo4b	2.30 (12)
C3j—C4i—H1c4j	129.65	O4bx—O4b—Mo4b	56.6 (16)
C4j—C4i—H1c4j	123.56	O5bx—O5b—P1b	75 (2)
C1i—C5i—C7i	118.6 (14)	Mo1bx—O6b—O6bx	83 (2)
C1i—C5i—H1c5i	120.72	Mo1bx—O6b—Mo1b	14.27 (10)
C1i—C5i—C1j	7.8 (18)	O6bx—O6b—Mo1b	94 (3)
C1i—C5i—C5j	173 (5)	Mo5bx—O7b—O7bx	32 (3)
C1i—C5i—C7j	128.3 (15)	Mo5bx—O7b—Mo5b	7.70 (9)
C7i—C5i—H1c5i	120.72	O7bx—O7b—Mo5b	36 (3)
C7i—C5i—C1j	120.6 (16)	P2bx—O8b—O22bx	65.9 (5)
C7i—C5i—C5j	67 (4)	P2bx—O8b—O8bx	64.0 (5)
C7i—C5i—C7j	11.0 (6)	P2bx—O8b—P2b	5.0 (3)
H1c5i—C5i—C1j	118.12	O22bx—O8b—O8bx	124.6 (7)
H1c5i—C5i—C5j	53.46	O22bx—O8b—P2b	61.3 (5)
H1c5i—C5i—C7j	110.77	O8bx—O8b—P2b	69.0 (4)
C1j—C5i—C5j	171 (5)	P2bx—O9b—O9bx	68.1 (6)
C1j—C5i—C7j	131.0 (17)	P2bx—O9b—P2b	5.1 (2)
C5j—C5i—C7j	57 (4)	O9bx—O9b—P2b	63.2 (5)
O24i—C6i—H1c6i	109.47	Mo5bx—O10b—O10bx	139.2 (18)
O24i—C6i—H2c6i	109.47	Mo5bx—O10b—Mo3b	114.0 (3)
O24i—C6i—H3c6i	109.47	Mo5bx—O10b—Mo5b	6.86 (11)
O24i—C6i—O24j	16.0 (8)	O10bx—O10b—Mo3b	47 (2)
O24i—C6i—C6j	112 (4)	O10bx—O10b—Mo5b	142.1 (18)
O24i—C6i—H2c6j	136.01	Mo3b—O10b—Mo5b	120.7 (3)
H1c6i—C6i—H2c6i	109.47	O11bx—O11b—P1b	63 (2)
H1c6i—C6i—H3c6i	109.47	Mo3bx—O12b—O12bx	100.1 (13)
H1c6i—C6i—O24j	98.69	Mo3bx—O12b—Mo2b	113.4 (3)
H1c6i—C6i—C6j	48.81	Mo3bx—O12b—Mo3b	13.29 (9)
H1c6i—C6i—H2c6j	84.16	O12bx—O12b—Mo2b	53.2 (14)
H2c6i—C6i—H3c6i	109.47	O12bx—O12b—Mo3b	113.2 (13)
H2c6i—C6i—O24j	125.15	Mo2b—O12b—Mo3b	122.3 (3)
H2c6i—C6i—C6j	137.85	Mo1bx—O13b—O13bx	84.2 (14)
H2c6i—C6i—H2c6j	30.33	Mo1bx—O13b—Mo1b	14.54 (11)
H3c6i—C6i—O24j	103.56	O13bx—O13b—Mo1b	98.7 (14)
H3c6i—C6i—C6j	62.76	P1bx—O14b—O14bx	140 (2)
H3c6i—C6i—H2c6j	104.21	P1bx—O14b—P1b	1.3 (2)
O24j—C6i—C6j	96 (4)	O14bx—O14b—P1b	140 (2)
O24j—C6i—H2c6j	149.3	Mo5bx—O15b—O15bx	128.8 (17)
C6j—C6i—H2c6j	108.16	Mo5bx—O15b—P2b	134.0 (4)
O24i—C7i—C2i	114.5 (12)	O15bx—O15b—P2b	78.8 (13)
O24i—C7i—C5i	125.5 (12)	Mo3bx—O16b—O16bx	48.9 (16)
O24i—C7i—C2j	104.2 (12)	Mo3bx—O16b—Mo3b	9.35 (10)
O24i—C7i—C5j	113.0 (12)	O16bx—O16b—Mo3b	57.9 (17)
O24i—C7i—C7j	28 (3)	Mo3bx—O17b—P1bx	141.0 (3)
C2i—C7i—C5i	120.1 (13)	Mo3bx—O17b—O17bx	127 (2)
C2i—C7i—C2j	11.1 (8)	Mo3bx—O17b—P1b	135.2 (3)
C2i—C7i—C5j	132.6 (13)	P1bx—O17b—O17bx	76 (2)
C2i—C7i—C7j	123 (3)	P1bx—O17b—P1b	6.22 (19)
C5i—C7i—C2j	130.2 (14)	O17bx—O17b—P1b	81 (2)
C5i—C7i—C5j	12.5 (9)	Mo2bx—O18b—O18bx	95.2 (14)
C5i—C7i—C7j	111 (3)	Mo2bx—O18b—Mo1b	121.8 (3)
C2j—C7i—C5j	142.5 (15)	Mo2bx—O18b—Mo2b	9.28 (9)
C2j—C7i—C7j	112 (3)	O18bx—O18b—Mo1b	44.1 (12)
C5j—C7i—C7j	100 (3)	O18bx—O18b—Mo2b	100.8 (14)
C1i—H1c1i—H1c1j	72.38	Mo1b—O18b—Mo2b	121.3 (3)
C3i—H1c3i—H1c3j	51.46	Mo3bx—O19b—O19bx	108.5 (14)
C4i—H1c4i—H1c4j	43.82	Mo3bx—O19b—Mo3b	13.94 (12)
C5i—H1c5i—C5j	17.66	O19bx—O19b—Mo3b	119.5 (14)
C5i—H1c5i—H1c5j	125.17	Mo4bx—O20b—O20bx	93 (2)
C5j—H1c5i—H1c5j	107.59	Mo4bx—O20b—Mo4b	6.41 (9)
C6i—H1c6i—C6j	26.74	O20bx—O20b—Mo4b	93 (2)
C6i—H1c6i—H1c6j	122.84	Mo4bx—O21b—Mo5bx	114.4 (3)
C6j—H1c6i—H1c6j	96.17	Mo4bx—O21b—O21bx	87.5 (13)
C6i—H2c6i—H2c6j	47.31	Mo4bx—O21b—Mo4b	6.14 (9)
C6i—H3c6i—C6j	27.68	Mo4bx—O21b—Mo5b	117.3 (3)
C6i—H3c6i—H3c6j	123.52	Mo5bx—O21b—O21bx	59.0 (11)
C6j—H3c6i—H3c6j	95.84	Mo5bx—O21b—Mo4b	119.2 (3)
N1i—H1n1i—H1n1j	48 (9)	Mo5bx—O21b—Mo5b	7.45 (9)
N1i—H2n1i—N1j	13 (3)	O21bx—O21b—Mo4b	87.5 (13)
N1i—H2n1i—H2n1j	143 (14)	O21bx—O21b—Mo5b	66.4 (11)
N1j—H2n1i—H2n1j	129 (15)	Mo4b—O21b—Mo5b	122.7 (3)
O24i—O24j—C6i	99 (3)	O22bx—O22b—P2b	61.6 (6)
O24i—O24j—C6j	117 (3)	Mo5bx—O23b—O23bx	80.8 (18)
O24i—O24j—C7j	41 (3)	Mo5bx—O23b—Mo5b	11.39 (11)
C6i—O24j—C6j	17.9 (11)	O23bx—O23b—Mo5b	92.0 (18)
C6i—O24j—C7j	104.8 (12)

Symmetry codes: (i) −x+2, −y, −z+1; (ii) −x+2, −y+1, −z.

Hydrogen-bond geometry (Å, º) top

D—H···A	D—H	H···A	D···A	D—H···A
C1a—H1c1a···O7b	0.96	2.43	3.218 (11)	139.34
C5a—H1c5a···O21b	0.96	2.44	3.342 (11)	156.29
N1a—H1n1a···O20aⁱⁱⁱ	0.87 (5)	2.10 (4)	2.819 (11)	140 (4)
N1a—H2n1a···O24a	0.87 (4)	2.36 (4)	2.658 (9)	100 (2)
N1a—H2n1a···O6a^iv	0.87 (4)	2.34 (3)	3.187 (10)	163 (4)
N1a—H2n1a···O18a^iv	0.87 (4)	2.45 (5)	2.858 (12)	109 (3)
O3w—H1c1b···N1bⁱ	1.17	2.16	2.88 (5)	116.74
O3w—H1c1b···C1b	1.17	0.96	1.92 (5)	129.17
O3w—H1c1b···C4b	1.17	2.03	2.80 (5)	119.87
O3w—H1c1b···C5b	1.17	2.04	2.83 (4)	121.42
C1b—H1c1b···O3w	0.96	1.17	1.92 (5)	129.17
N1bⁱ—H1c5b···C3bⁱ	0.35	2.39	2.46 (8)	97.79
N1bⁱ—H1c5b···O19aⁱ	0.35	2.44	2.74 (4)	146.30
C5b—H1c5b···O19aⁱ	0.96	2.44	3.33 (3)	154.60
C6b—H2c6b···N1bⁱ	0.96	2.50	2.71 (8)	92.09
N1b—H1n1b···O19a	0.87 (6)	1.98 (6)	2.74 (4)	145 (7)
C5bⁱ—H1n1b···O19a	1.36 (6)	1.98 (6)	3.33 (3)	175 (6)
N1b—H2n1b···O3wⁱ	0.87 (10)	2.33 (7)	2.88 (5)	121 (4)
N1b—H2n1b···O24b	0.87 (10)	2.36 (7)	2.66 (5)	100 (6)
N1b—H2n1b···C1bⁱ	0.87 (10)	1.18 (9)	1.81 (8)	124 (8)
N1b—H2n1b···C4bⁱ	0.87 (10)	2.46 (9)	3.02 (8)	123 (6)
C1bⁱ—H2n1b···N1b	1.18 (9)	0.87 (10)	1.81 (8)	124 (8)
C1bⁱ—H2n1b···C2b	1.18 (9)	2.02 (9)	2.47 (7)	98 (5)
C5bⁱ—H2n1b···O3wⁱ	0.99 (8)	2.33 (7)	2.83 (4)	110 (4)
C6c—H2c6c···O7aⁱⁱⁱ	0.96	2.41	3.172 (11)	136.20
N1c—H1n1c···O7bx	0.87 (6)	2.22 (6)	3.07 (3)	166 (3)
N1c—H1n1c···O7b	0.87 (6)	1.95 (5)	2.799 (17)	164 (3)
N1c—H2n1c···O20bx	0.87 (4)	2.24 (5)	2.779 (19)	120 (4)
N1c—H2n1c···O24c	0.87 (4)	2.36 (4)	2.658 (12)	100 (2)
N1c—H2n1c···O20b	0.87 (4)	2.34 (4)	2.961 (13)	128 (5)
N1d—H1n1d···O21bx^v	0.87 (5)	2.16 (5)	2.811 (17)	131 (4)
N1d—H1n1d···O9bx^v	0.87 (5)	2.10 (5)	2.695 (17)	125 (5)
N1d—H1n1d···O21b^v	0.87 (5)	2.43 (6)	2.996 (17)	123 (4)
N1d—H1n1d···O22b^v	0.87 (5)	2.15 (4)	2.998 (13)	166 (5)
N1d—H2n1d···O24d	0.87 (4)	2.36 (5)	2.658 (11)	100 (3)
C5e—H1c5e···C6f	0.96	2.12	2.419 (19)	96.08
C5f—H1c5e···C6f	1.23	2.12	2.84 (2)	113.47
N1e—H1n1e···O23bx^vi	0.87 (7)	1.70 (6)	2.55 (3)	162 (5)
N1e—H1n1e···O23b^vi	0.87 (7)	1.97 (6)	2.82 (3)	164 (4)
N1f—H1n1e···O23bx^vi	1.38 (6)	1.70 (6)	2.94 (3)	145 (3)
N1f—H1n1e···O23b^vi	1.38 (6)	1.97 (6)	3.17 (2)	142 (3)
N1e—H2n1e···O4w	0.87 (5)	1.73 (5)	2.60 (3)	175 (4)
N1e—H2n1e···O24e	0.87 (5)	2.36 (5)	2.66 (2)	100 (3)
N1e—H2n1e···O24f	0.87 (5)	2.45 (4)	2.62 (2)	91 (3)
N1f—H2n1e···O4w	1.26 (4)	1.73 (5)	2.86 (3)	146 (4)
N1f—H2n1e···O24e	1.26 (4)	2.36 (5)	2.78 (2)	96 (2)
C3e—H1c3f···O2bx^vii	1.16	2.44	3.23 (2)	123.90
C3f—H1c3f···O2bx^vii	0.96	2.44	3.09 (2)	125.19
C6e—H3c6f···C5e	1.19	2.27	2.84 (2)	106.76
N1e—H1n1f···O23bx^vi	0.75 (5)	2.08 (6)	2.55 (3)	120 (5)
N1e—H1n1f···C3e	0.75 (5)	2.31 (4)	2.46 (2)	93 (4)
N1e—H1n1f···O23b^vi	0.75 (5)	2.31 (6)	2.82 (3)	126 (5)
N1f—H1n1f···O23bx^vi	0.87 (6)	2.08 (6)	2.94 (3)	168 (4)
N1f—H1n1f···O23b^vi	0.87 (6)	2.31 (6)	3.17 (2)	168 (4)
N1e—H2n1f···O4w	0.96 (6)	2.04 (4)	2.60 (3)	115 (3)
N1e—H2n1f···O24e	0.96 (6)	2.38 (4)	2.66 (2)	96 (3)
N1e—H2n1f···O24f	0.96 (6)	2.36 (4)	2.62 (2)	94 (3)
N1f—H2n1f···O4w	0.87 (5)	2.04 (4)	2.86 (3)	157 (5)
N1f—H2n1f···O24e	0.87 (5)	2.38 (4)	2.78 (2)	109 (3)
N1f—H2n1f···O24f	0.87 (5)	2.36 (4)	2.66 (2)	100 (3)
C5g—H1c5g···C6k	0.96	2.21	2.45 (3)	92.76
C5k—H1c5g···C6k	1.32	2.21	2.84 (2)	104.84
C6g—H1c6g···O3bx^viii	0.96	2.46	3.39 (2)	163.83
C6g—H1c6g···O3b^viii	0.96	1.85	2.78 (2)	163.77
C6k—H1c6g···O3bx^viii	1.37	2.46	3.76 (2)	158.65
C6k—H1c6g···O3b^viii	1.37	1.85	3.17 (2)	160.45
N1g—H1n1g···O16aⁱⁱⁱ	0.87 (5)	2.47 (4)	3.219 (19)	145 (5)
N1g—H1n1g···O23aⁱⁱⁱ	0.87 (5)	2.34 (6)	2.75 (3)	109 (4)
N1k—H1n1g···O16aⁱⁱⁱ	0.83 (6)	2.47 (4)	3.074 (19)	131 (5)
N1k—H1n1g···O23aⁱⁱⁱ	0.83 (6)	2.34 (6)	2.91 (3)	127 (4)
N1g—H2n1g···O24g	0.87 (4)	2.36 (5)	2.66 (2)	100 (3)
N1g—H2n1g···O24k	0.87 (4)	2.28 (5)	2.46 (2)	92 (3)
N1g—H2n1g···O2a	0.87 (4)	2.42 (5)	2.95 (2)	120 (5)
N1k—H2n1g···O24g	1.09 (4)	2.36 (5)	2.87 (2)	107 (3)
N1k—H2n1g···O24k	1.09 (4)	2.28 (5)	2.66 (2)	98 (3)
N1k—H2n1g···O2a	1.09 (4)	2.42 (5)	3.00 (2)	112 (4)
C4h—H1c4h···O2w′	0.96	2.44	3.38 (3)	167.92
C4l—H1c4h···O2w′	1.29	2.44	3.71 (3)	167.42
C6h—H2c6h···O24i	0.96	2.46	3.34 (3)	153.24
C6l—H2c6h···O24i	1.25	2.46	3.65 (3)	157.76
C6l—H2c6h···C5l	1.25	2.50	2.84 (2)	92.69
C6l—H3c6h···C5l	0.95	2.37	2.84 (2)	110.43
N1h—H1n1h···O10bx^ix	0.87 (6)	2.04 (5)	2.77 (3)	141 (4)
N1h—H1n1h···O10b^ix	0.87 (6)	2.16 (5)	2.82 (3)	133 (4)
N1l—H1n1h···O10bx^ix	1.00 (6)	2.04 (5)	2.78 (3)	129 (3)
N1l—H1n1h···O10b^ix	1.00 (6)	2.16 (5)	2.81 (3)	121 (3)
N1h—H2n1h···O6bx^vii	0.87 (5)	2.22 (6)	2.90 (3)	135 (4)
N1h—H2n1h···O24h	0.87 (5)	2.36 (5)	2.66 (2)	100 (4)
N1h—H2n1h···O24l	0.87 (5)	2.46 (5)	2.85 (2)	108 (4)
N1h—H2n1h···O6b^vii	0.87 (5)	2.23 (6)	2.95 (3)	140 (4)
N1l—H2n1h···O6bx^vii	0.65 (5)	2.22 (6)	2.76 (3)	142 (5)
N1l—H2n1h···O24h	0.65 (5)	2.36 (5)	2.48 (2)	93 (4)
N1l—H2n1h···O24l	0.65 (5)	2.46 (5)	2.66 (2)	101 (5)
N1l—H2n1h···O6b^vii	0.65 (5)	2.23 (6)	2.80 (3)	148 (5)
C6i—H3c6i···O23b^ix	0.96	2.38	3.132 (19)	134.79
C6j—H3c6i···C5j	0.85	2.43	2.84 (2)	110.47
C6j—H3c6i···O23b^ix	0.85	2.38	3.097 (19)	141.76
N1i—H1n1i···O7aⁱⁱⁱ	0.87 (5)	2.28 (4)	3.084 (17)	154 (5)
N1i—H1n1i···O10aⁱⁱⁱ	0.87 (5)	2.04 (6)	2.68 (3)	129 (5)
N1j—H1n1i···O7aⁱⁱⁱ	1.14 (5)	2.28 (4)	3.372 (17)	160 (5)
N1j—H1n1i···O10aⁱⁱⁱ	1.14 (5)	2.04 (6)	2.82 (3)	122 (4)
N1i—H2n1i···O3w^x	0.87 (4)	2.37 (4)	3.20 (2)	159 (6)
N1i—H2n1i···O24i	0.87 (4)	2.36 (5)	2.66 (2)	100 (3)
N1i—H2n1i···O24j	0.87 (4)	2.44 (5)	2.83 (2)	108 (3)
N1j—H2n1i···O3w^x	0.58 (5)	2.37 (4)	2.88 (2)	147 (7)
N1j—H2n1i···O24i	0.58 (5)	2.36 (5)	2.52 (2)	100 (4)
N1j—H2n1i···O24j	0.58 (5)	2.44 (5)	2.66 (2)	106 (4)
C5i—H1c5j···O23bx^ix	1.17	2.46	3.51 (2)	148.52
C5i—H1c5j···C6i	1.17	2.29	2.84 (2)	105.93
C5j—H1c5j···O23bx^ix	0.96	2.46	3.33 (2)	152.17
C5j—H1c5j···C6i	0.96	2.29	2.54 (2)	93.87
C6i—H3c6j···O23b^ix	1.20	2.37	3.132 (19)	119.15
C6j—H3c6j···O23b^ix	0.96	2.37	3.097 (19)	132.21
N1i—H1n1j···O5aⁱⁱⁱ	0.68 (5)	2.46 (4)	2.795 (19)	113 (5)
N1i—H1n1j···O10aⁱⁱⁱ	0.68 (5)	2.09 (6)	2.68 (3)	146 (6)
N1j—H1n1j···O5aⁱⁱⁱ	0.87 (5)	2.46 (4)	2.694 (19)	96 (3)
N1j—H1n1j···O10aⁱⁱⁱ	0.87 (5)	2.09 (6)	2.82 (3)	141 (5)
N1i—H2n1j···O3w^x	1.19 (4)	2.02 (4)	3.20 (2)	169 (4)
N1i—H2n1j···O24i	1.19 (4)	2.35 (5)	2.66 (2)	91 (2)
N1i—H2n1j···O24j	1.19 (4)	2.36 (5)	2.83 (2)	101 (2)
N1j—H2n1j···O3w^x	0.87 (4)	2.02 (4)	2.88 (2)	167 (5)
N1j—H2n1j···O24i	0.87 (4)	2.35 (5)	2.52 (2)	91 (3)
N1j—H2n1j···O24j	0.87 (4)	2.36 (5)	2.66 (2)	100 (3)
C1g—H1c1k···O6bx^vii	1.10	2.46	3.39 (2)	141.18
C1g—H1c1k···O13bx^vii	1.10	2.38	3.39 (3)	151.16
C1k—H1c1k···O6bx^vii	0.96	2.46	3.23 (2)	136.73
C1k—H1c1k···O13bx^vii	0.96	2.38	3.25 (3)	150.31
C6g—H1c6k···O3b^viii	0.59	2.22	2.78 (2)	162.75
C6k—H1c6k···O3b^viii	0.96	2.22	3.17 (2)	171.45
C6g—H2c6k···C5g	1.24	2.45	2.84 (2)	95.46
C6g—H2c6k···C4h	1.24	2.46	3.61 (3)	153.63
C6k—H2c6k···C4h	0.96	2.46	3.35 (3)	153.78
C6g—H3c6k···C5g	1.03	2.30	2.84 (2)	111.51
N1g—H1n1k···O9a	0.99 (5)	2.29 (5)	2.873 (18)	117 (4)
N1g—H1n1k···O16aⁱⁱⁱ	0.99 (5)	2.32 (4)	3.219 (19)	151 (4)
N1k—H1n1k···O9a	0.87 (5)	2.29 (5)	2.690 (18)	108 (5)
N1k—H1n1k···O16aⁱⁱⁱ	0.87 (5)	2.32 (4)	3.074 (19)	146 (4)
N1g—H2n1k···O24g	0.67 (4)	2.47 (5)	2.66 (2)	99 (5)
N1g—H2n1k···O24k	0.67 (4)	2.36 (5)	2.46 (2)	91 (4)
N1g—H2n1k···O2a	0.67 (4)	2.44 (5)	2.95 (2)	135 (6)
N1k—H2n1k···O24g	0.87 (4)	2.47 (5)	2.87 (2)	108 (4)
N1k—H2n1k···O24k	0.87 (4)	2.36 (5)	2.66 (2)	100 (3)
N1k—H2n1k···O2a	0.87 (4)	2.44 (5)	3.00 (2)	122 (5)
C5h—H1c5l···C6h	1.25	2.26	2.84 (2)	104.54
C5l—H1c5l···C6h	0.96	2.26	2.50 (2)	93.22
N1h—H1n1l···O10bx^ix	0.80 (6)	1.98 (5)	2.77 (3)	166 (4)
N1h—H1n1l···O10b^ix	0.80 (6)	2.07 (5)	2.82 (3)	157 (4)
N1l—H1n1l···O10bx^ix	0.87 (6)	1.98 (5)	2.78 (3)	151 (4)
N1l—H1n1l···O10b^ix	0.87 (6)	2.07 (5)	2.81 (3)	142 (4)
N1h—H2n1l···O6bx^vii	1.09 (5)	2.09 (6)	2.90 (3)	129 (4)
N1h—H2n1l···O24h	1.09 (5)	2.29 (5)	2.66 (2)	97 (3)
N1h—H2n1l···O24l	1.09 (5)	2.36 (5)	2.85 (2)	105 (3)
N1h—H2n1l···O6b^vii	1.09 (5)	2.08 (6)	2.95 (3)	134 (4)
N1l—H2n1l···O6bx^vii	0.87 (5)	2.09 (6)	2.76 (3)	134 (4)
N1l—H2n1l···O24h	0.87 (5)	2.29 (5)	2.48 (2)	92 (3)
N1l—H2n1l···O24l	0.87 (5)	2.36 (5)	2.66 (2)	100 (4)
N1l—H2n1l···O6b^vii	0.87 (5)	2.08 (6)	2.80 (3)	140 (4)
C1m—H1c1m···O4a^xi	0.96	2.43	3.367 (17)	164.69
C1n—H1c1m···O4a^xi	1.12	2.43	3.494 (17)	158.50
C6m—H2c6m···O2bx^viii	0.96	2.28	2.81 (2)	114.26
C6n—H2c6m···O2bx^viii	1.38	2.28	3.00 (2)	107.84
C6n—H2c6m···C5n	1.38	2.38	2.84 (2)	94.48
C6n—H3c6m···C5n	1.39	2.31	2.84 (2)	97.53
N1m—H1n1m···O12a	0.87 (6)	1.98 (6)	2.76 (3)	149 (4)
N1n—H1n1m···O12a	0.84 (6)	1.98 (6)	2.76 (3)	154 (4)
N1m—H2n1m···O24m	0.87 (5)	2.36 (4)	2.658 (19)	100 (3)
N1m—H2n1m···O24n	0.87 (5)	2.11 (4)	2.506 (19)	107 (3)
N1n—H2n1m···O24m	1.04 (5)	2.36 (4)	2.796 (19)	104 (2)
N1n—H2n1m···O24n	1.04 (5)	2.11 (4)	2.658 (19)	110 (3)
C5m—H1c5n···C6m	1.31	2.00	2.84 (2)	117.25
C5n—H1c5n···C6m	0.96	2.00	2.39 (2)	102.34
C6m—H2c6n···O2bx^viii	0.85	2.33	2.81 (2)	116.61
C6n—H2c6n···O2bx^viii	0.96	2.33	3.00 (2)	127.12
N1m—H1n1n···O12a	0.95 (6)	2.01 (6)	2.76 (3)	134 (4)
N1n—H1n1n···O12a	0.87 (6)	2.01 (6)	2.76 (3)	144 (4)
N1m—H2n1n···O24n	0.73 (5)	2.36 (4)	2.506 (19)	93 (3)
N1n—H2n1n···O24n	0.87 (5)	2.36 (4)	2.658 (19)	100 (3)
C1o—H1c1o···O16bx^viii	0.96	2.33	3.23 (5)	155.69
C1o—H1c1o···O4wⁱⁱ	0.96	2.46	3.04 (4)	118.70
C3o—H1c3o···O1w^vii	0.96	2.41	3.21 (4)	140.93
N1oⁱⁱ—H1c5o···O24oⁱⁱ	1.11	1.77	2.66 (4)	133.58
N1oⁱⁱ—H1c5o···C1o	1.11	2.05	2.72 (5)	115.75
N1oⁱⁱ—H1c5o···C2oⁱⁱ	1.11	0.77	1.46 (5)	100.28
N1oⁱⁱ—H1c5o···C3oⁱⁱ	1.11	2.15	2.46 (6)	92.47
N1oⁱⁱ—H1c5o···C5o	1.11	0.96	2.01 (4)	151.27
N1oⁱⁱ—H1c5o···C7o	1.11	2.06	3.17 (4)	172.90
N1oⁱⁱ—H1c5o···C7oⁱⁱ	1.11	1.34	2.45 (4)	175.85
C2oⁱⁱ—H1c5o···O4wⁱⁱ	0.77	2.35	2.90 (3)	129.12
C2oⁱⁱ—H1c5o···O24oⁱⁱ	0.77	1.77	2.31 (3)	126.07
C2oⁱⁱ—H1c5o···N1oⁱⁱ	0.77	1.11	1.46 (5)	100.28
C2oⁱⁱ—H1c5o···C1o	0.77	2.05	2.71 (5)	143.91
C2oⁱⁱ—H1c5o···C5o	0.77	0.96	1.41 (3)	108.39
C5o—H1c5o···O4wⁱⁱ	0.96	2.35	2.98 (3)	122.49
C5o—H1c5o···N1oⁱⁱ	0.96	1.11	2.01 (4)	151.27
C5o—H1c5o···C2oⁱⁱ	0.96	0.77	1.41 (3)	108.39
C5o—H1c5o···C3oⁱⁱ	0.96	2.15	2.71 (4)	116.23
C7oⁱⁱ—H1c5o···O4wⁱⁱ	1.34	2.35	3.61 (2)	154.93
C7oⁱⁱ—H1c5o···N1oⁱⁱ	1.34	1.11	2.45 (4)	175.85
C3oⁱⁱ—H2c6o···C1oⁱⁱ	0.87	2.19	2.40 (6)	93.30
C4oⁱⁱ—H2c6o···C2oⁱⁱ	1.31	1.68	2.38 (6)	105.01
C3oⁱⁱ—H3c6o···C1oⁱⁱ	0.84	2.22	2.40 (6)	91.80
C4oⁱⁱ—H3c6o···C2oⁱⁱ	1.37	1.60	2.38 (6)	106.40
C4oⁱⁱ—H3c6o···C7oⁱⁱ	1.37	2.37	2.76 (5)	91.22
N1o—H1n1o···O13bx^vii	0.87 (5)	2.25 (5)	2.99 (3)	143 (6)
N1o—H1n1o···O24e	0.87 (5)	2.47 (6)	3.11 (3)	131 (6)
O4w—H2n1o···O24o	1.07 (6)	2.36 (6)	3.28 (3)	144 (5)
O4w—H2n1o···N1o	1.07 (6)	0.87 (7)	1.48 (5)	99 (5)
O4w—H2n1o···C1oⁱⁱ	1.07 (6)	2.24 (6)	3.04 (4)	130 (5)
O4w—H2n1o···C2o	1.07 (6)	2.02 (7)	2.90 (3)	138 (4)
O4w—H2n1o···C5oⁱⁱ	1.07 (6)	1.98 (6)	2.98 (3)	154 (5)
N1o—H2n1o···O4w	0.87 (7)	1.07 (6)	1.48 (5)	99 (5)
N1o—H2n1o···O24o	0.87 (7)	2.36 (6)	2.66 (4)	100 (5)
N1o—H2n1o···C1oⁱⁱ	0.87 (7)	2.24 (6)	2.72 (5)	115 (6)

Symmetry codes: (i) −x+2, −y, −z+1; (ii) −x+2, −y+1, −z; (iii) −x+1, −y+1, −z+1; (iv) x−1, y, z; (v) x+1, y, z; (vi) x+1, y+1, z; (vii) −x+1, −y+1, −z; (viii) −x+1, −y, −z; (ix) x, y+1, z; (x) x−1, y+1, z; (xi) x, y−1, z.

Mo—O bond lengths (Å) in [P₂Mo₅O₂₃]^6- top

	Terminal (Mo—O)	Bridging (Mo—O—Mo)	Bridging (Mo—O—P)
Min (this work)	1.626	1.798	2.221
Max (this work)	1.749	2.017	2.428
Average (this work)	1.707	1.922	2.311
Average (Qu et al., 2011)	1.694	1.926	2.298
Average (Ganesan & Natarajan, 2005)	1.763	1.977	2.270
Average (Liu et al., 2007)	1.711	2.077	2.293

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Crystal structure of a new polyoxometalate (POM) com­pound with a high level of crystallographic disorder

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Crystal structure of a new polyoxometalate (POM) compound with a high level of crystallographic disorder