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In the title compound, C31H26IN2O6S2, mol­ecules are linked into a sheet parallel to the bc plane by C—H...O hydrogen bonds and C—H...π inter­actions. The sheets are inter­linked via C—H...O hydrogen bonds.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536806049488/wn2093sup1.cif
Contains datablocks global, I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S1600536806049488/wn2093Isup2.hkl
Contains datablock I

CCDC reference: 630507

Key indicators

  • Single-crystal X-ray study
  • T = 100 K
  • Mean [sigma](C-C) = 0.002 Å
  • R factor = 0.033
  • wR factor = 0.088
  • Data-to-parameter ratio = 33.4

checkCIF/PLATON results

No syntax errors found



Alert level B PLAT230_ALERT_2_B Hirshfeld Test Diff for C20 - C21 .. 8.89 su
Alert level C ABSTM02_ALERT_3_C The ratio of expected to reported Tmax/Tmin(RR) is > 1.10 Tmin and Tmax reported: 0.544 0.699 Tmin and Tmax expected: 0.475 0.681 RR = 1.114 Please check that your absorption correction is appropriate. PLAT060_ALERT_3_C Ratio Tmax/Tmin (Exp-to-Rep) (too) Large ....... 1.13 PLAT062_ALERT_4_C Rescale T(min) & T(max) by ..................... 0.98 PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density .... 2.58
0 ALERT level A = In general: serious problem 1 ALERT level B = Potentially serious problem 4 ALERT level C = Check and explain 0 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check

Computing details top

Data collection: APEX2 (Bruker, 2005); cell refinement: APEX2; data reduction: SAINT (Bruker, 2005); program(s) used to solve structure: SHELXTL (Sheldrick, 1998); program(s) used to refine structure: SHELXTL; molecular graphics: SHELXTL; software used to prepare material for publication: SHELXTL and PLATON (Spek, 2003).

Ethyl 2-{[N-(2-iodophenyl)phenylsulfonamido]methyl}-1-phenylsulfonyl- 1H-indole-3-carboxylate top
Crystal data top
C30H25IN2O6S2F(000) = 1408.0
Mr = 700.56Dx = 1.640 Mg m3
Monoclinic, P21/cMo Kα radiation, λ = 0.71073 Å
Hall symbol: -P 2ybcCell parameters from 8060 reflections
a = 10.9098 (2) Åθ = 2.1–40.6°
b = 22.7150 (4) ŵ = 1.32 mm1
c = 11.8579 (2) ÅT = 100 K
β = 105.011 (1)°Block, colourless
V = 2838.30 (9) Å30.58 × 0.53 × 0.29 mm
Z = 4
Data collection top
Bruker SMART APEX2 CCD
diffractometer
12373 independent reflections
Radiation source: fine-focus sealed tube10729 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.021
Detector resolution: 8.33 pixels mm-1θmax = 35.0°, θmin = 2.1°
ω scansh = 1717
Absorption correction: multi-scan
(SADABS; Bruker, 2005)
k = 3636
Tmin = 0.544, Tmax = 0.699l = 1918
41126 measured reflections
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.033Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.088H-atom parameters constrained
S = 1.06 w = 1/[σ2(Fo2) + (0.0359P)2 + 3.3196P]
where P = (Fo2 + 2Fc2)/3
12373 reflections(Δ/σ)max = 0.002
371 parametersΔρmax = 2.87 e Å3
0 restraintsΔρmin = 1.11 e Å3
Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
I10.264926 (11)0.346622 (5)0.417725 (9)0.02271 (3)
S10.14800 (4)0.342294 (16)0.71017 (3)0.01549 (6)
S20.50750 (4)0.241016 (16)0.64432 (3)0.01447 (6)
O10.20478 (12)0.28628 (5)0.70389 (12)0.0209 (2)
O20.04383 (12)0.36178 (6)0.61772 (11)0.0229 (2)
O30.65847 (12)0.40863 (6)0.91439 (12)0.0215 (2)
O40.60997 (12)0.50463 (5)0.88870 (12)0.0231 (2)
O50.50354 (13)0.23470 (6)0.52301 (10)0.0223 (2)
O60.42901 (12)0.20541 (5)0.69639 (11)0.0196 (2)
N10.26379 (12)0.39327 (6)0.72267 (12)0.0147 (2)
N20.46947 (12)0.31061 (5)0.66078 (11)0.0134 (2)
C10.39333 (13)0.38439 (6)0.77872 (12)0.0132 (2)
C20.44572 (14)0.43777 (6)0.82027 (13)0.0141 (2)
C30.34730 (15)0.48222 (6)0.79264 (13)0.0153 (2)
C40.34448 (17)0.54288 (7)0.81452 (15)0.0190 (3)
H40.41920.56300.85510.023*
C50.23089 (18)0.57274 (7)0.77590 (17)0.0236 (3)
H50.22750.61360.79150.028*
C60.12110 (19)0.54367 (8)0.71432 (19)0.0266 (3)
H60.04470.56540.68780.032*
C70.12091 (17)0.48370 (8)0.69093 (17)0.0235 (3)
H70.04620.46400.64870.028*
C80.23525 (15)0.45375 (7)0.73225 (14)0.0160 (2)
C90.10602 (14)0.34746 (6)0.84327 (14)0.0155 (2)
C100.18832 (15)0.32499 (7)0.94415 (14)0.0180 (3)
H100.26700.30790.94160.022*
C110.15310 (17)0.32810 (8)1.04851 (16)0.0214 (3)
H110.20830.31341.11840.026*
C120.03679 (18)0.35271 (8)1.05051 (17)0.0227 (3)
H120.01310.35471.12210.027*
C130.04499 (17)0.37444 (8)0.94921 (17)0.0244 (3)
H130.12450.39080.95150.029*
C140.01026 (16)0.37226 (8)0.84436 (16)0.0211 (3)
H140.06500.38750.77470.025*
C150.58151 (15)0.44716 (7)0.87882 (13)0.0165 (2)
C160.74291 (17)0.51881 (8)0.94104 (17)0.0238 (3)
H16A0.77920.49031.00400.029*
H16B0.74950.55870.97590.029*
C170.81686 (19)0.51653 (9)0.84917 (17)0.0264 (3)
H17A0.90680.52400.88590.040*
H17B0.78430.54660.78960.040*
H17C0.80730.47750.81260.040*
C180.46043 (14)0.32667 (6)0.78026 (12)0.0133 (2)
H18A0.54680.32940.83330.016*
H18B0.41370.29550.81030.016*
C190.52240 (15)0.35388 (6)0.59786 (13)0.0145 (2)
C200.64464 (15)0.37566 (7)0.64359 (13)0.0175 (3)
H200.69370.36180.71700.021*
C210.69500 (17)0.41701 (8)0.58348 (15)0.0221 (3)
H210.77850.43140.61560.027*
C220.62399 (18)0.43799 (8)0.47551 (16)0.0237 (3)
H220.65930.46640.43420.028*
C230.50164 (17)0.41716 (8)0.42884 (15)0.0222 (3)
H230.45280.43140.35560.027*
C240.45079 (15)0.37527 (7)0.49001 (13)0.0174 (3)
C250.66565 (14)0.23023 (6)0.72639 (13)0.0146 (2)
C260.76415 (16)0.23909 (7)0.67325 (16)0.0199 (3)
H260.74640.25000.59330.024*
C270.88897 (17)0.23168 (7)0.73890 (18)0.0235 (3)
H270.95710.23900.70450.028*
C280.91403 (17)0.21366 (8)0.85430 (18)0.0248 (3)
H280.99930.20860.89870.030*
C290.81501 (17)0.20293 (8)0.90539 (15)0.0233 (3)
H290.83300.18940.98380.028*
C300.68978 (15)0.21190 (7)0.84254 (14)0.0180 (3)
H300.62200.20570.87790.022*
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
I10.01751 (5)0.03065 (6)0.01720 (5)0.00143 (4)0.00051 (3)0.00486 (4)
S10.01187 (14)0.01606 (15)0.01743 (15)0.00141 (11)0.00180 (12)0.00284 (11)
S20.01486 (14)0.01377 (14)0.01406 (14)0.00078 (11)0.00246 (11)0.00240 (11)
O10.0187 (5)0.0152 (5)0.0290 (6)0.0021 (4)0.0067 (5)0.0069 (4)
O20.0158 (5)0.0294 (6)0.0200 (5)0.0011 (4)0.0018 (4)0.0018 (5)
O30.0156 (5)0.0196 (5)0.0266 (6)0.0003 (4)0.0007 (4)0.0020 (4)
O40.0189 (5)0.0170 (5)0.0324 (6)0.0049 (4)0.0049 (5)0.0045 (4)
O50.0279 (6)0.0233 (5)0.0142 (5)0.0048 (5)0.0028 (4)0.0049 (4)
O60.0165 (5)0.0151 (5)0.0270 (6)0.0026 (4)0.0051 (4)0.0006 (4)
N10.0119 (5)0.0137 (5)0.0182 (5)0.0007 (4)0.0033 (4)0.0003 (4)
N20.0155 (5)0.0126 (5)0.0125 (5)0.0013 (4)0.0043 (4)0.0000 (4)
C10.0125 (5)0.0139 (5)0.0132 (5)0.0011 (4)0.0035 (4)0.0001 (4)
C20.0140 (6)0.0135 (5)0.0148 (5)0.0001 (4)0.0040 (5)0.0009 (4)
C30.0174 (6)0.0129 (5)0.0170 (6)0.0009 (5)0.0071 (5)0.0005 (4)
C40.0236 (7)0.0131 (6)0.0223 (7)0.0003 (5)0.0098 (6)0.0001 (5)
C50.0276 (8)0.0145 (6)0.0321 (8)0.0052 (6)0.0137 (7)0.0038 (6)
C60.0232 (8)0.0196 (7)0.0382 (10)0.0077 (6)0.0100 (7)0.0065 (7)
C70.0173 (7)0.0199 (7)0.0325 (8)0.0043 (5)0.0050 (6)0.0045 (6)
C80.0160 (6)0.0140 (5)0.0184 (6)0.0023 (5)0.0051 (5)0.0015 (5)
C90.0125 (5)0.0145 (5)0.0193 (6)0.0007 (4)0.0037 (5)0.0011 (5)
C100.0157 (6)0.0161 (6)0.0220 (7)0.0022 (5)0.0045 (5)0.0025 (5)
C110.0226 (7)0.0199 (7)0.0224 (7)0.0018 (6)0.0069 (6)0.0057 (5)
C120.0234 (7)0.0223 (7)0.0255 (8)0.0003 (6)0.0118 (6)0.0035 (6)
C130.0171 (7)0.0272 (8)0.0311 (8)0.0035 (6)0.0104 (6)0.0022 (6)
C140.0138 (6)0.0241 (7)0.0251 (7)0.0028 (5)0.0042 (5)0.0013 (6)
C150.0157 (6)0.0169 (6)0.0170 (6)0.0022 (5)0.0044 (5)0.0033 (5)
C160.0200 (7)0.0234 (7)0.0277 (8)0.0084 (6)0.0055 (6)0.0065 (6)
C170.0248 (8)0.0268 (8)0.0285 (8)0.0058 (6)0.0089 (7)0.0004 (7)
C180.0141 (5)0.0136 (5)0.0121 (5)0.0012 (4)0.0033 (4)0.0001 (4)
C190.0157 (6)0.0159 (6)0.0125 (5)0.0019 (4)0.0046 (5)0.0006 (4)
C200.0180 (6)0.0196 (6)0.0150 (6)0.0006 (5)0.0043 (5)0.0006 (5)
C210.0182 (7)0.0253 (7)0.0217 (7)0.0021 (6)0.0030 (6)0.0025 (6)
C220.0259 (8)0.0260 (8)0.0208 (7)0.0031 (6)0.0093 (6)0.0051 (6)
C230.0244 (8)0.0251 (7)0.0176 (6)0.0016 (6)0.0065 (6)0.0069 (5)
C240.0175 (6)0.0198 (6)0.0151 (6)0.0021 (5)0.0046 (5)0.0027 (5)
C250.0141 (6)0.0136 (5)0.0164 (6)0.0019 (4)0.0043 (5)0.0009 (4)
C260.0206 (7)0.0168 (6)0.0257 (7)0.0022 (5)0.0122 (6)0.0024 (5)
C270.0173 (7)0.0172 (6)0.0388 (9)0.0012 (5)0.0123 (7)0.0033 (6)
C280.0150 (7)0.0224 (7)0.0347 (9)0.0030 (5)0.0020 (6)0.0090 (6)
C290.0206 (7)0.0282 (8)0.0188 (7)0.0079 (6)0.0009 (6)0.0035 (6)
C300.0165 (6)0.0218 (6)0.0159 (6)0.0040 (5)0.0046 (5)0.0006 (5)
Geometric parameters (Å, º) top
I1—C242.0903 (16)C11—H110.95
S1—O11.4255 (13)C12—C131.388 (3)
S1—O21.4296 (13)C12—H120.95
S1—N11.6915 (13)C13—C141.391 (3)
S1—C91.7576 (16)C13—H130.95
S2—O61.4291 (13)C14—H140.95
S2—O51.4352 (12)C16—C171.515 (3)
S2—N21.6587 (13)C16—H16A0.99
S2—C251.7648 (15)C16—H16B0.99
O3—C151.210 (2)C17—H17A0.98
O4—C151.3398 (19)C17—H17B0.98
O4—C161.458 (2)C17—H17C0.98
N1—C11.4118 (19)C18—H18A0.99
N1—C81.4198 (19)C18—H18B0.99
N2—C191.4420 (19)C19—C201.394 (2)
N2—C181.4907 (18)C19—C241.402 (2)
C1—C21.376 (2)C20—C211.377 (2)
C1—C181.499 (2)C20—H200.95
C2—C31.448 (2)C21—C221.397 (3)
C2—C151.480 (2)C21—H210.95
C3—C41.404 (2)C22—C231.389 (3)
C3—C81.404 (2)C22—H220.95
C4—C51.383 (2)C23—C241.396 (2)
C4—H40.95C23—H230.95
C5—C61.397 (3)C25—C261.394 (2)
C5—H50.95C25—C301.397 (2)
C6—C71.390 (3)C26—C271.393 (3)
C6—H60.95C26—H260.95
C7—C81.394 (2)C27—C281.386 (3)
C7—H70.95C27—H270.95
C9—C141.391 (2)C28—C291.390 (3)
C9—C101.393 (2)C28—H280.95
C10—C111.389 (2)C29—C301.391 (2)
C10—H100.95C29—H290.95
C11—C121.392 (3)C30—H300.95
O1—S1—O2120.41 (8)C9—C14—H14120.6
O1—S1—N1106.90 (7)C13—C14—H14120.6
O2—S1—N1106.42 (7)O3—C15—O4123.35 (15)
O1—S1—C9108.93 (8)O3—C15—C2125.38 (14)
O2—S1—C9109.13 (8)O4—C15—C2111.26 (14)
N1—S1—C9103.77 (7)O4—C16—C17110.04 (15)
O6—S2—O5120.70 (8)O4—C16—H16A109.7
O6—S2—N2107.00 (7)C17—C16—H16A109.7
O5—S2—N2105.65 (7)O4—C16—H16B109.7
O6—S2—C25107.03 (7)C17—C16—H16B109.7
O5—S2—C25108.07 (8)H16A—C16—H16B108.2
N2—S2—C25107.82 (7)C16—C17—H17A109.5
C15—O4—C16115.78 (14)C16—C17—H17B109.5
C1—N1—C8108.30 (12)H17A—C17—H17B109.5
C1—N1—S1125.26 (10)C16—C17—H17C109.5
C8—N1—S1119.68 (11)H17A—C17—H17C109.5
C19—N2—C18117.32 (12)H17B—C17—H17C109.5
C19—N2—S2116.28 (10)N2—C18—C1110.77 (11)
C18—N2—S2115.16 (9)N2—C18—H18A109.5
C2—C1—N1108.36 (12)C1—C18—H18A109.5
C2—C1—C18127.58 (13)N2—C18—H18B109.5
N1—C1—C18123.82 (12)C1—C18—H18B109.5
C1—C2—C3108.57 (13)H18A—C18—H18B108.1
C1—C2—C15124.58 (13)C20—C19—C24118.88 (14)
C3—C2—C15126.81 (13)C20—C19—N2120.78 (13)
C4—C3—C8119.24 (14)C24—C19—N2120.34 (14)
C4—C3—C2133.86 (15)C21—C20—C19120.72 (15)
C8—C3—C2106.91 (13)C21—C20—H20119.6
C5—C4—C3118.74 (16)C19—C20—H20119.6
C5—C4—H4120.6C20—C21—C22120.41 (16)
C3—C4—H4120.6C20—C21—H21119.8
C4—C5—C6121.00 (16)C22—C21—H21119.8
C4—C5—H5119.5C23—C22—C21119.76 (16)
C6—C5—H5119.5C23—C22—H22120.1
C7—C6—C5121.63 (16)C21—C22—H22120.1
C7—C6—H6119.2C22—C23—C24119.71 (15)
C5—C6—H6119.2C22—C23—H23120.1
C6—C7—C8116.95 (17)C24—C23—H23120.1
C6—C7—H7121.5C23—C24—C19120.53 (15)
C8—C7—H7121.5C23—C24—I1118.24 (12)
C7—C8—C3122.42 (15)C19—C24—I1121.23 (11)
C7—C8—N1129.72 (15)C26—C25—C30121.22 (14)
C3—C8—N1107.85 (13)C26—C25—S2119.26 (12)
C14—C9—C10121.79 (15)C30—C25—S2119.52 (11)
C14—C9—S1119.06 (13)C27—C26—C25119.11 (16)
C10—C9—S1119.12 (12)C27—C26—H26120.4
C11—C10—C9118.73 (15)C25—C26—H26120.4
C11—C10—H10120.6C28—C27—C26120.12 (16)
C9—C10—H10120.6C28—C27—H27119.9
C10—C11—C12119.93 (16)C26—C27—H27119.9
C10—C11—H11120.0C27—C28—C29120.35 (16)
C12—C11—H11120.0C27—C28—H28119.8
C13—C12—C11120.81 (16)C29—C28—H28119.8
C13—C12—H12119.6C28—C29—C30120.46 (17)
C11—C12—H12119.6C28—C29—H29119.8
C12—C13—C14119.86 (16)C30—C29—H29119.8
C12—C13—H13120.1C29—C30—C25118.67 (15)
C14—C13—H13120.1C29—C30—H30120.7
C9—C14—C13118.86 (16)C25—C30—H30120.7
O1—S1—N1—C131.48 (14)C9—C10—C11—C120.7 (3)
O2—S1—N1—C1161.34 (12)C10—C11—C12—C130.1 (3)
C9—S1—N1—C183.58 (13)C11—C12—C13—C140.7 (3)
O1—S1—N1—C8179.21 (12)C10—C9—C14—C130.2 (3)
O2—S1—N1—C850.92 (14)S1—C9—C14—C13177.84 (14)
C9—S1—N1—C864.16 (13)C12—C13—C14—C90.8 (3)
O6—S2—N2—C19170.17 (11)C16—O4—C15—O32.7 (2)
O5—S2—N2—C1940.37 (13)C16—O4—C15—C2177.59 (14)
C25—S2—N2—C1975.00 (12)C1—C2—C15—O312.8 (3)
O6—S2—N2—C1846.95 (12)C3—C2—C15—O3169.88 (16)
O5—S2—N2—C18176.75 (11)C1—C2—C15—O4167.55 (14)
C25—S2—N2—C1867.89 (12)C3—C2—C15—O49.8 (2)
C8—N1—C1—C21.22 (16)C15—O4—C16—C1783.85 (19)
S1—N1—C1—C2151.98 (11)C19—N2—C18—C152.53 (17)
C8—N1—C1—C18176.05 (13)S2—N2—C18—C1164.98 (10)
S1—N1—C1—C1833.2 (2)C2—C1—C18—N2106.94 (16)
N1—C1—C2—C31.17 (16)N1—C1—C18—N266.85 (17)
C18—C1—C2—C3175.74 (13)C18—N2—C19—C2058.46 (19)
N1—C1—C2—C15176.58 (13)S2—N2—C19—C2083.61 (16)
C18—C1—C2—C152.0 (2)C18—N2—C19—C24120.75 (15)
C1—C2—C3—C4178.73 (16)S2—N2—C19—C2497.18 (15)
C15—C2—C3—C43.6 (3)C24—C19—C20—C210.7 (2)
C1—C2—C3—C80.68 (17)N2—C19—C20—C21179.93 (15)
C15—C2—C3—C8177.01 (14)C19—C20—C21—C220.2 (3)
C8—C3—C4—C50.1 (2)C20—C21—C22—C230.3 (3)
C2—C3—C4—C5179.22 (17)C21—C22—C23—C240.2 (3)
C3—C4—C5—C61.2 (3)C22—C23—C24—C190.3 (3)
C4—C5—C6—C71.0 (3)C22—C23—C24—I1178.74 (14)
C5—C6—C7—C80.3 (3)C20—C19—C24—C230.8 (2)
C6—C7—C8—C31.4 (3)N2—C19—C24—C23179.98 (14)
C6—C7—C8—N1179.58 (17)C20—C19—C24—I1178.25 (11)
C4—C3—C8—C71.2 (2)N2—C19—C24—I11.0 (2)
C2—C3—C8—C7179.29 (15)O6—S2—C25—C26154.39 (12)
C4—C3—C8—N1179.59 (13)O5—S2—C25—C2622.96 (15)
C2—C3—C8—N10.08 (17)N2—S2—C25—C2690.80 (13)
C1—N1—C8—C7179.92 (17)O6—S2—C25—C3024.37 (14)
S1—N1—C8—C727.4 (2)O5—S2—C25—C30155.80 (13)
C1—N1—C8—C30.79 (16)N2—S2—C25—C3090.44 (13)
S1—N1—C8—C3153.46 (11)C30—C25—C26—C272.5 (2)
O1—S1—C9—C14137.96 (13)S2—C25—C26—C27178.74 (12)
O2—S1—C9—C144.70 (15)C25—C26—C27—C282.3 (2)
N1—S1—C9—C14108.44 (13)C26—C27—C28—C290.1 (3)
O1—S1—C9—C1040.10 (14)C27—C28—C29—C302.0 (3)
O2—S1—C9—C10173.36 (12)C28—C29—C30—C251.8 (3)
N1—S1—C9—C1073.50 (13)C26—C25—C30—C290.5 (2)
C14—C9—C10—C110.6 (2)S2—C25—C30—C29179.22 (13)
S1—C9—C10—C11178.60 (13)
Hydrogen-bond geometry (Å, º) top
D—H···AD—HH···AD···AD—H···A
C4—H4···O40.952.412.932 (2)114
C7—H7···O20.952.352.958 (2)121
C11—H11···O1i0.952.493.150 (2)127
C11—H11···O6i0.952.383.159 (2)139
C13—H13···O3ii0.952.333.248 (2)162
C18—H18A···O30.992.252.981 (2)130
C18—H18B···O10.992.312.852 (2)113
C18—H18B···O60.992.482.9184 (18)106
C18—H18B···O5i0.992.553.1223 (18)116
C5—H5···Cg1iii0.952.633.4645 (17)148
C16—H16A···Cg2iv0.992.923.638 (2)131
C16—H16B···Cg3iv0.992.833.655 (2)141
C22—H22···Cg2v0.952.813.635 (2)146
Symmetry codes: (i) x, y+1/2, z+1/2; (ii) x1, y, z; (iii) x+1, y+1/2, z+3/2; (iv) x+1, y+1, z+2; (v) x+1, y+1, z+1.
 

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