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The structure of the title compound was determined previously by Jones & Templeton [Acta Cryst. (1958), 11, 484] at T = 278 K using the Weissenberg technique, and twice by Nahringbauer [Acta Chem. Scand. (1970), 24, 453-462] at T = 278 and 93 K. The present redetermination at T = 40 K provides data of higher precision, reflected in s.u.'s which are about one third those of Nahringbauer.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablocks global, qa0082

fcf

Structure factor file (CIF format)
Contains datablock aceto0r

CCDC reference: 131006

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