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The structure of lead molybdenum oxide, Pb5MoO8, has been determined by single-crystal X-ray methods. The crystal structure is a 4:3:2 superstructure of tetragonal α-PbO (litharge), with embodied MoO42− tetrahedra. Infinite double chains of OPb4 tetrahedra are formed. Along these chains, the OPb4 tetrahedra share vertices. Two of the O atoms form three nearly coplanar bonds with Pb atoms.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablocks global, na1328

fcf

Structure factor file (CIF format)
Contains datablock na1328

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