Supporting information
Crystallographic Information File (CIF) https://doi.org/10.1107/S2052520619015270/je5023sup1.cif | |
Structure factor file (CIF format) https://doi.org/10.1107/S2052520619015270/je5023Isup2.hkl |
CCDC reference: 1965233
Data collection: APEX2 (Bruker, 2012); cell refinement: SAINT (Bruker, 2012); data reduction: SAINT (Bruker, 2012); program(s) used to solve structure: SHELXS2014 (Sheldrick, 2015); program(s) used to refine structure: SHELXL2017/1 (Sheldrick, 2015); molecular graphics: DIAMOND (Brandenburg, 2008).
Ag3.11O36Rb8.89Sc2W9·0.03(Rb8)·0.06(Rb8)·8.16(Rb8) | Dx = 4.998 Mg m−3 |
Mr = 3415.87 | Mo Kα radiation, λ = 0.71073 Å |
Orthorhombic, Cmcm | Cell parameters from 3382 reflections |
a = 17.9269 (3) Å | θ = 3.4–59.3° |
b = 10.4520 (2) Å | µ = 33.84 mm−1 |
c = 24.2260 (5) Å | T = 296 K |
V = 4539.27 (15) Å3 | Fragment, colorless |
Z = 4 | 0.08 × 0.08 × 0.04 mm |
F(000) = 5884 |
Bruker APEX Duo CCD diffractometer | 2979 reflections with I > 2σ(I) |
\ f scans, frame data integration | Rint = 0.050 |
Absorption correction: multi-scan SADABS (Bruker, 2012) | θmax = 29.7°, θmin = 1.7° |
Tmin = 0.083, Tmax = 0.258 | h = −24→24 |
44834 measured reflections | k = −14→13 |
3382 independent reflections | l = −33→33 |
Refinement on F2 | Primary atom site location: structure-invariant direct methods |
Least-squares matrix: full | Secondary atom site location: difference Fourier map |
R[F2 > 2σ(F2)] = 0.019 | w = 1/[σ2(Fo2) + (0.0084P)2 + 23.1939P] where P = (Fo2 + 2Fc2)/3 |
wR(F2) = 0.035 | (Δ/σ)max = 0.033 |
S = 1.04 | Δρmax = 1.08 e Å−3 |
3382 reflections | Δρmin = −1.46 e Å−3 |
187 parameters | Extinction correction: SHELXL-2017/1 (Sheldrick 2015), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
37 restraints | Extinction coefficient: 0.0000339 (18) |
Geometry. All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. |
x | y | z | Uiso*/Ueq | Occ. (<1) | |
W1 | 0.500000 | 0.41301 (3) | 0.750000 | 0.01240 (7) | |
W2 | 0.500000 | 0.00984 (2) | 0.59409 (2) | 0.01412 (5) | |
W3 | 0.13335 (2) | 0.30585 (2) | 0.750000 | 0.01311 (5) | |
W4 | 0.16802 (2) | 0.00694 (2) | 0.59314 (2) | 0.01353 (4) | |
Rb1 | 0.33511 (2) | 0.17527 (4) | 0.66257 (2) | 0.02366 (9) | |
Rb2 | 0.33811 (11) | 0.16878 (15) | 0.47423 (6) | 0.0256 (2) | 0.973 (7) |
Rb3a | 0.500000 | 0.500000 | 0.500000 | 0.026 (11) | 0.090 (3) |
Rb3b | 0.500000 | 0.460 (2) | 0.5072 (12) | 0.020 (6) | 0.1045 (17) |
Rb3c | 0.500000 | 0.4011 (9) | 0.5152 (4) | 0.030 (4) | 0.2597 (17) |
Rb3d | 0.500000 | 0.359 (4) | 0.5193 (19) | 0.027 (6) | 0.0907 (17) |
Ag1 | 0.500000 | 0.06296 (7) | 0.750000 | 0.02914 (16) | |
Ag2 | 0.30578 (3) | 0.48034 (5) | 0.750000 | 0.02874 (11) | |
Ag3 | 0.361 (3) | 0.186 (3) | 0.4809 (13) | 0.012 (6) | 0.027 (7) |
Sc | 0.000000 | 0.17670 (9) | 0.64088 (4) | 0.01184 (19) | |
O1 | 0.4211 (2) | 0.3143 (4) | 0.750000 | 0.0253 (9) | |
O2 | 0.500000 | 0.5121 (4) | 0.68979 (19) | 0.0339 (11) | |
O3 | 0.4197 (2) | 0.0654 (3) | 0.56209 (16) | 0.0544 (12) | |
O4 | 0.500000 | 0.0708 (4) | 0.66199 (17) | 0.0358 (11) | |
O5 | 0.500000 | −0.1622 (4) | 0.59040 (17) | 0.0284 (10) | |
O6 | 0.2204 (2) | 0.2304 (4) | 0.750000 | 0.0280 (10) | |
O7 | 0.1471 (3) | 0.4730 (4) | 0.750000 | 0.0263 (10) | |
O8 | 0.08314 (18) | 0.2601 (3) | 0.68974 (14) | 0.0357 (8) | |
O9 | 0.1572 (2) | −0.1323 (3) | 0.55405 (16) | 0.0447 (10) | |
O10 | 0.24084 (17) | 0.0984 (3) | 0.56573 (13) | 0.0361 (8) | |
O11 | 0.1943 (2) | −0.0378 (3) | 0.66059 (12) | 0.0370 (8) | |
O12 | 0.08316 (16) | 0.0990 (3) | 0.59024 (11) | 0.0249 (7) |
U11 | U22 | U33 | U12 | U13 | U23 | |
W1 | 0.01360 (15) | 0.01031 (14) | 0.01328 (14) | 0.000 | 0.000 | 0.000 |
W2 | 0.01516 (11) | 0.01511 (11) | 0.01208 (10) | 0.000 | 0.000 | 0.00020 (8) |
W3 | 0.01051 (10) | 0.01379 (11) | 0.01503 (10) | −0.00242 (9) | 0.000 | 0.000 |
W4 | 0.01322 (8) | 0.01537 (8) | 0.01198 (7) | 0.00174 (6) | 0.00082 (6) | −0.00040 (5) |
Rb1 | 0.0236 (2) | 0.0236 (2) | 0.0238 (2) | 0.00162 (17) | −0.00200 (16) | −0.00255 (15) |
Rb2 | 0.0308 (5) | 0.0225 (4) | 0.0236 (4) | 0.0049 (4) | 0.0016 (4) | 0.0011 (3) |
Rb3a | 0.020 (9) | 0.04 (3) | 0.020 (16) | 0.000 | 0.000 | −0.01 (2) |
Rb3b | 0.013 (5) | 0.026 (18) | 0.021 (11) | 0.000 | 0.000 | −0.013 (12) |
Rb3c | 0.023 (2) | 0.048 (13) | 0.021 (5) | 0.000 | 0.000 | −0.011 (8) |
Rb3d | 0.016 (5) | 0.034 (16) | 0.029 (5) | 0.000 | 0.000 | 0.004 (9) |
Ag1 | 0.0352 (4) | 0.0369 (4) | 0.0153 (3) | 0.000 | 0.000 | 0.000 |
Ag2 | 0.0331 (3) | 0.0345 (3) | 0.0186 (2) | 0.0003 (2) | 0.000 | 0.000 |
Ag3 | 0.021 (15) | 0.009 (8) | 0.007 (8) | 0.002 (9) | 0.006 (8) | −0.004 (5) |
Sc | 0.0111 (5) | 0.0132 (5) | 0.0112 (4) | 0.000 | 0.000 | 0.0006 (4) |
O1 | 0.023 (2) | 0.027 (2) | 0.026 (2) | −0.0084 (19) | 0.000 | 0.000 |
O2 | 0.043 (3) | 0.027 (2) | 0.032 (3) | 0.000 | 0.000 | 0.0170 (19) |
O3 | 0.062 (3) | 0.041 (2) | 0.061 (2) | 0.0283 (19) | −0.044 (2) | −0.0205 (18) |
O4 | 0.055 (3) | 0.036 (3) | 0.016 (2) | 0.000 | 0.000 | −0.0070 (18) |
O5 | 0.042 (3) | 0.018 (2) | 0.025 (2) | 0.000 | 0.000 | 0.0045 (17) |
O6 | 0.020 (2) | 0.030 (2) | 0.035 (2) | 0.0096 (19) | 0.000 | 0.000 |
O7 | 0.035 (3) | 0.015 (2) | 0.030 (2) | 0.0007 (18) | 0.000 | 0.000 |
O8 | 0.0330 (19) | 0.0390 (19) | 0.0352 (19) | −0.0077 (16) | −0.0147 (15) | −0.0066 (14) |
O9 | 0.059 (3) | 0.0278 (19) | 0.047 (2) | 0.0044 (17) | 0.0006 (18) | −0.0169 (16) |
O10 | 0.0229 (17) | 0.050 (2) | 0.0352 (18) | −0.0095 (16) | 0.0028 (14) | 0.0137 (15) |
O11 | 0.042 (2) | 0.051 (2) | 0.0180 (16) | 0.0083 (18) | −0.0047 (14) | 0.0085 (14) |
O12 | 0.0209 (16) | 0.0329 (17) | 0.0211 (14) | 0.0093 (13) | 0.0035 (12) | −0.0009 (12) |
W1—O1 | 1.751 (4) | Rb3b—O9ix | 3.186 (12) |
W1—O1i | 1.751 (4) | Rb3b—O9x | 3.660 (15) |
W1—O2ii | 1.789 (4) | Rb3b—O9vi | 3.660 (15) |
W1—O2 | 1.789 (4) | Rb3b—O5viii | 3.91 (3) |
W2—O3iii | 1.735 (3) | Rb3c—O12vi | 2.958 (8) |
W2—O3 | 1.735 (3) | Rb3c—O12x | 2.958 (8) |
W2—O4 | 1.764 (4) | Rb3c—O9ix | 2.991 (5) |
W2—O5 | 1.800 (4) | Rb3c—O9v | 2.991 (5) |
W3—O6 | 1.749 (4) | Rb3c—O12ix | 3.131 (9) |
W3—O7 | 1.765 (4) | Rb3c—O12v | 3.131 (9) |
W3—O8ii | 1.780 (3) | Rb3c—O5viii | 3.575 (10) |
W3—O8 | 1.780 (3) | Rb3c—Scvi | 3.868 (9) |
W4—O9 | 1.747 (3) | Rb3c—O3 | 3.959 (10) |
W4—O10 | 1.749 (3) | Rb3c—O3iii | 3.959 (10) |
W4—O11 | 1.764 (3) | Rb3c—O9x | 4.074 (8) |
W4—O12 | 1.801 (3) | Rb3c—O9vi | 4.074 (8) |
Rb1—O1 | 2.996 (3) | Rb3d—O9ix | 2.942 (14) |
Rb1—O10 | 3.001 (3) | Rb3d—O9v | 2.942 (14) |
Rb1—O6 | 3.008 (3) | Rb3d—O12vi | 3.08 (4) |
Rb1—O7iv | 3.009 (3) | Rb3d—O12x | 3.08 (4) |
Rb1—O11v | 3.046 (4) | Rb3d—O5viii | 3.36 (5) |
Rb1—O3 | 3.089 (4) | Rb3d—O12ix | 3.39 (4) |
Rb1—O4 | 3.1510 (16) | Rb3d—O12v | 3.39 (4) |
Rb1—O9v | 3.313 (4) | Rb3d—O3 | 3.54 (3) |
Rb1—O11 | 3.366 (4) | Rb3d—O3iii | 3.54 (3) |
Rb2—O3 | 2.800 (4) | Ag1—O4ii | 2.134 (4) |
Rb2—O9v | 2.841 (4) | Ag1—O4 | 2.134 (4) |
Rb2—O10 | 2.915 (3) | Ag1—O7iv | 2.800 (4) |
Rb2—O10vi | 2.977 (4) | Ag1—O7xii | 2.800 (4) |
Rb2—O3vii | 2.985 (4) | Ag1—O1 | 2.984 (4) |
Rb2—O12vi | 3.213 (3) | Ag1—O1i | 2.984 (4) |
Rb2—O5viii | 3.298 (3) | Ag2—O11v | 2.174 (3) |
Rb2—O9vii | 3.337 (4) | Ag2—O11xiii | 2.174 (3) |
Rb2—O10vii | 3.432 (4) | Ag2—O6xiii | 2.656 (4) |
Rb3a—O12vi | 2.841 (3) | Ag2—O1 | 2.699 (4) |
Rb3a—O12ix | 2.841 (3) | Ag2—O7 | 2.846 (5) |
Rb3a—O12v | 2.841 (3) | Ag2—O6 | 3.027 (4) |
Rb3a—O12x | 2.841 (3) | Ag3—O3 | 2.57 (4) |
Rb3a—O9v | 3.401 (4) | Ag3—O9v | 2.62 (3) |
Rb3a—O9x | 3.401 (4) | Ag3—O12vi | 3.01 (3) |
Rb3a—O9vi | 3.401 (4) | Ag3—O3vii | 3.02 (3) |
Rb3a—O9ix | 3.401 (4) | Ag3—O5viii | 3.05 (3) |
Rb3a—Scvi | 3.8806 (10) | Ag3—O10vi | 3.11 (4) |
Rb3a—Scix | 3.8806 (10) | Ag3—O10 | 3.11 (3) |
Rb3a—O5viii | 4.155 (4) | Sc—O5xiv | 2.081 (4) |
Rb3a—O5xi | 4.155 (4) | Sc—O2xv | 2.089 (4) |
Rb3b—O12vi | 2.86 (3) | Sc—O8 | 2.093 (3) |
Rb3b—O12x | 2.86 (3) | Sc—O8xvi | 2.094 (3) |
Rb3b—O12ix | 2.90 (2) | Sc—O12xvi | 2.095 (3) |
Rb3b—O12v | 2.90 (2) | Sc—O12 | 2.095 (3) |
Rb3b—O9v | 3.186 (12) | ||
O1—W1—O1i | 107.8 (3) | O11v—Ag2—O11xiii | 170.01 (19) |
O1—W1—O2ii | 109.94 (10) | O11v—Ag2—O6xiii | 94.91 (10) |
O1i—W1—O2ii | 109.93 (10) | O11xiii—Ag2—O6xiii | 94.91 (10) |
O1—W1—O2 | 109.94 (10) | O11v—Ag2—O1 | 86.83 (10) |
O1i—W1—O2 | 109.93 (10) | O11xiii—Ag2—O1 | 86.83 (10) |
O2ii—W1—O2 | 109.3 (3) | O6xiii—Ag2—O1 | 140.21 (13) |
O3iii—W2—O3 | 112.1 (3) | O11v—Ag2—O7 | 89.82 (10) |
O3iii—W2—O4 | 107.20 (15) | O11xiii—Ag2—O7 | 89.82 (10) |
O3—W2—O4 | 107.20 (14) | O6xiii—Ag2—O7 | 81.35 (12) |
O3iii—W2—O5 | 108.20 (14) | O1—Ag2—O7 | 138.45 (12) |
O3—W2—O5 | 108.20 (14) | O11v—Ag2—O6 | 85.67 (9) |
O4—W2—O5 | 114.0 (2) | O11xiii—Ag2—O6 | 85.67 (9) |
O6—W3—O7 | 108.8 (2) | O6xiii—Ag2—O6 | 139.45 (4) |
O6—W3—O8ii | 109.28 (13) | O1—Ag2—O6 | 80.35 (12) |
O7—W3—O8ii | 109.67 (13) | O7—Ag2—O6 | 58.10 (11) |
O6—W3—O8 | 109.28 (13) | O3—Ag3—O9v | 83.5 (10) |
O7—W3—O8 | 109.67 (13) | O3—Ag3—O12vi | 131.9 (18) |
O8ii—W3—O8 | 110.2 (2) | O9v—Ag3—O12vi | 83.5 (10) |
O9—W4—O10 | 109.42 (17) | O3—Ag3—O3vii | 72.0 (8) |
O9—W4—O11 | 108.14 (17) | O9v—Ag3—O3vii | 155.2 (16) |
O10—W4—O11 | 107.28 (16) | O12vi—Ag3—O3vii | 109.6 (9) |
O9—W4—O12 | 109.26 (16) | O3—Ag3—O5viii | 93.2 (12) |
O10—W4—O12 | 108.87 (15) | O9v—Ag3—O5viii | 122.8 (16) |
O11—W4—O12 | 113.79 (15) | O12vi—Ag3—O5viii | 57.4 (6) |
O1—Rb1—O10 | 166.49 (10) | O3vii—Ag3—O5viii | 56.3 (5) |
O1—Rb1—O6 | 76.16 (10) | O3—Ag3—O10vi | 151.2 (11) |
O10—Rb1—O6 | 102.53 (9) | O9v—Ag3—O10vi | 69.4 (7) |
O1—Rb1—O7iv | 77.80 (9) | O12vi—Ag3—O10vi | 56.4 (6) |
O10—Rb1—O7iv | 114.95 (9) | O3vii—Ag3—O10vi | 135.4 (13) |
O6—Rb1—O7iv | 73.22 (10) | O5viii—Ag3—O10vi | 109.5 (9) |
O1—Rb1—O11v | 67.82 (10) | O3—Ag3—O10 | 68.5 (7) |
O10—Rb1—O11v | 98.84 (9) | O9v—Ag3—O10 | 71.5 (7) |
O6—Rb1—O11v | 72.78 (10) | O12vi—Ag3—O10 | 146.2 (11) |
O7iv—Rb1—O11v | 136.15 (8) | O3vii—Ag3—O10 | 102.4 (10) |
O1—Rb1—O3 | 119.00 (10) | O5viii—Ag3—O10 | 156.4 (12) |
O10—Rb1—O3 | 63.96 (9) | O10vi—Ag3—O10 | 92.9 (10) |
O6—Rb1—O3 | 164.10 (11) | O5xiv—Sc—O2xv | 178.56 (18) |
O7iv—Rb1—O3 | 103.97 (9) | O5xiv—Sc—O8 | 89.74 (13) |
O11v—Rb1—O3 | 116.02 (9) | O2xv—Sc—O8 | 91.27 (13) |
O1—Rb1—O4 | 71.86 (11) | O5xiv—Sc—O8xvi | 89.74 (12) |
O10—Rb1—O4 | 115.60 (10) | O2xv—Sc—O8xvi | 91.27 (13) |
O6—Rb1—O4 | 135.30 (9) | O8—Sc—O8xvi | 90.79 (19) |
O7iv—Rb1—O4 | 70.15 (11) | O5xiv—Sc—O12xvi | 88.26 (12) |
O11v—Rb1—O4 | 120.24 (10) | O2xv—Sc—O12xvi | 90.73 (13) |
O3—Rb1—O4 | 53.64 (9) | O8—Sc—O12xvi | 177.99 (13) |
O1—Rb1—O9v | 104.18 (8) | O8xvi—Sc—O12xvi | 89.19 (12) |
O10—Rb1—O9v | 64.25 (8) | O5xiv—Sc—O12 | 88.26 (12) |
O6—Rb1—O9v | 118.10 (9) | O2xv—Sc—O12 | 90.73 (13) |
O7iv—Rb1—O9v | 168.68 (10) | O8—Sc—O12 | 89.19 (12) |
O11v—Rb1—O9v | 52.91 (8) | O8xvi—Sc—O12 | 177.99 (13) |
O3—Rb1—O9v | 65.16 (9) | O12xvi—Sc—O12 | 90.76 (17) |
O4—Rb1—O9v | 99.65 (10) | W1—O1—Ag2 | 103.90 (18) |
O1—Rb1—O11 | 135.79 (8) | W1—O1—Ag1 | 97.79 (17) |
O10—Rb1—O11 | 52.38 (8) | Ag2—O1—Ag1 | 158.32 (16) |
O6—Rb1—O11 | 67.93 (10) | W1—O1—Rb1 | 134.55 (6) |
O7iv—Rb1—O11 | 67.96 (9) | Ag2—O1—Rb1 | 85.29 (10) |
O11v—Rb1—O11 | 121.42 (5) | Ag1—O1—Rb1 | 79.44 (9) |
O3—Rb1—O11 | 96.38 (9) | W1—O1—Rb1ii | 134.55 (6) |
O4—Rb1—O11 | 118.30 (9) | Ag2—O1—Rb1ii | 85.29 (10) |
O9v—Rb1—O11 | 114.93 (8) | Ag1—O1—Rb1ii | 79.44 (9) |
O3—Rb2—O9v | 75.49 (11) | Rb1—O1—Rb1ii | 89.99 (11) |
O3—Rb2—O10 | 68.72 (12) | W1—O2—Scix | 159.9 (3) |
O9v—Rb2—O10 | 71.62 (11) | W2—O3—Ag3 | 148.2 (9) |
O3—Rb2—O10vi | 144.21 (11) | W2—O3—Rb2 | 154.5 (2) |
O9v—Rb2—O10vi | 68.73 (11) | Ag3—O3—Rb2 | 8.7 (10) |
O10—Rb2—O10vi | 99.73 (9) | W2—O3—Rb2vii | 105.29 (15) |
O3—Rb2—O3vii | 69.60 (14) | Ag3—O3—Rb2vii | 88.5 (10) |
O9v—Rb2—O3vii | 141.86 (14) | Rb2—O3—Rb2vii | 80.57 (11) |
O10—Rb2—O3vii | 108.10 (10) | W2—O3—Ag3vii | 98.9 (8) |
O10vi—Rb2—O3vii | 143.87 (12) | Ag3—O3—Ag3vii | 91.0 (13) |
O3—Rb2—O12vi | 115.57 (12) | Rb2—O3—Ag3vii | 83.7 (6) |
O9v—Rb2—O12vi | 76.40 (10) | Rb2vii—O3—Ag3vii | 8.9 (9) |
O10—Rb2—O12vi | 145.40 (10) | W2—O3—Rb1 | 100.35 (15) |
O10vi—Rb2—O12vi | 55.48 (8) | Ag3—O3—Rb1 | 102.6 (6) |
O3vii—Rb2—O12vi | 105.12 (9) | Rb2—O3—Rb1 | 101.48 (11) |
O3—Rb2—O5viii | 83.86 (12) | Rb2vii—O3—Rb1 | 107.25 (15) |
O9v—Rb2—O5viii | 108.20 (12) | Ag3vii—O3—Rb1 | 115.0 (9) |
O10—Rb2—O5viii | 151.91 (10) | W2—O3—Rb3d | 94.8 (4) |
O10vi—Rb2—O5viii | 106.33 (10) | Ag3—O3—Rb3d | 61.2 (11) |
O3vii—Rb2—O5viii | 53.95 (10) | Rb2—O3—Rb3d | 69.9 (5) |
O12vi—Rb2—O5viii | 53.02 (9) | Rb2vii—O3—Rb3d | 145.4 (8) |
O3—Rb2—O9vii | 128.31 (13) | Ag3vii—O3—Rb3d | 142.7 (10) |
O9v—Rb2—O9vii | 104.62 (9) | Rb1—O3—Rb3d | 96.2 (7) |
O10—Rb2—O9vii | 62.99 (10) | W2—O3—Rb3c | 97.09 (17) |
O10vi—Rb2—O9vii | 64.18 (9) | Ag3—O3—Rb3c | 59.7 (10) |
O3vii—Rb2—O9vii | 108.80 (11) | Rb2—O3—Rb3c | 68.28 (13) |
O12vi—Rb2—O9vii | 114.43 (9) | Rb2vii—O3—Rb3c | 145.14 (17) |
O5viii—Rb2—O9vii | 139.06 (10) | Ag3vii—O3—Rb3c | 143.2 (6) |
O3—Rb2—O10vii | 99.55 (10) | Rb1—O3—Rb3c | 94.31 (14) |
O9v—Rb2—O10vii | 143.39 (11) | Rb3d—O3—Rb3c | 2.8 (4) |
O10—Rb2—O10vii | 72.86 (12) | W2—O4—Ag1 | 156.6 (3) |
O10vi—Rb2—O10vii | 109.38 (8) | W2—O4—Rb1 | 97.43 (9) |
O3vii—Rb2—O10vii | 59.90 (10) | Ag1—O4—Rb1 | 90.51 (8) |
O12vi—Rb2—O10vii | 134.50 (9) | W2—O4—Rb1iii | 97.43 (9) |
O5viii—Rb2—O10vii | 107.23 (9) | Ag1—O4—Rb1iii | 90.51 (8) |
O9vii—Rb2—O10vii | 49.85 (8) | Rb1—O4—Rb1iii | 139.46 (16) |
O12vi—Rb3a—O12ix | 180.0 | W2—O5—Scxii | 141.2 (2) |
O12vi—Rb3a—O12v | 116.70 (11) | W2—O5—Ag3vii | 96.3 (6) |
O12ix—Rb3a—O12v | 63.30 (11) | Scxii—O5—Ag3vii | 105.5 (6) |
O12vi—Rb3a—O12x | 63.30 (11) | W2—O5—Ag3viii | 96.3 (7) |
O12ix—Rb3a—O12x | 116.70 (11) | Scxii—O5—Ag3viii | 105.5 (6) |
O12v—Rb3a—O12x | 180.0 | Ag3vii—O5—Ag3viii | 110.2 (16) |
O12vi—Rb3a—O9v | 73.35 (8) | W2—O5—Rb2vii | 92.55 (10) |
O12ix—Rb3a—O9v | 106.65 (8) | Scxii—O5—Rb2vii | 105.19 (9) |
O12v—Rb3a—O9v | 54.34 (8) | Ag3vii—O5—Rb2vii | 7.2 (8) |
O12x—Rb3a—O9v | 125.66 (8) | Ag3viii—O5—Rb2vii | 116.8 (8) |
O12vi—Rb3a—O9x | 106.65 (8) | W2—O5—Rb2viii | 92.55 (10) |
O12ix—Rb3a—O9x | 73.35 (8) | Scxii—O5—Rb2viii | 105.19 (9) |
O12v—Rb3a—O9x | 125.66 (8) | Ag3vii—O5—Rb2viii | 116.8 (8) |
O12x—Rb3a—O9x | 54.34 (8) | Ag3viii—O5—Rb2viii | 7.2 (8) |
O9v—Rb3a—O9x | 180.0 | Rb2vii—O5—Rb2viii | 123.26 (14) |
O12vi—Rb3a—O9vi | 54.34 (8) | W2—O5—Rb3dviii | 130.5 (6) |
O12ix—Rb3a—O9vi | 125.66 (8) | Scxii—O5—Rb3dviii | 88.3 (6) |
O12v—Rb3a—O9vi | 73.35 (8) | Ag3vii—O5—Rb3dviii | 60.1 (8) |
O12x—Rb3a—O9vi | 106.65 (8) | Ag3viii—O5—Rb3dviii | 60.1 (8) |
O9v—Rb3a—O9vi | 68.10 (13) | Rb2vii—O5—Rb3dviii | 67.1 (2) |
O9x—Rb3a—O9vi | 111.90 (13) | Rb2viii—O5—Rb3dviii | 67.1 (2) |
O12vi—Rb3a—O9ix | 125.66 (8) | W2—O5—Rb3cviii | 137.2 (2) |
O12ix—Rb3a—O9ix | 54.34 (8) | Scxii—O5—Rb3cviii | 81.69 (19) |
O12v—Rb3a—O9ix | 106.65 (8) | Ag3vii—O5—Rb3cviii | 62.5 (8) |
O12x—Rb3a—O9ix | 73.35 (8) | Ag3viii—O5—Rb3cviii | 62.5 (8) |
O9v—Rb3a—O9ix | 111.90 (13) | Rb2vii—O5—Rb3cviii | 69.25 (9) |
O9x—Rb3a—O9ix | 68.10 (13) | Rb2viii—O5—Rb3cviii | 69.25 (9) |
O9vi—Rb3a—O9ix | 180.00 (12) | Rb3dviii—O5—Rb3cviii | 6.6 (7) |
O12vi—Rb3a—O5viii | 44.35 (7) | W2—O5—Rb3bviii | 145.6 (4) |
O12ix—Rb3a—O5viii | 135.65 (7) | Scxii—O5—Rb3bviii | 73.2 (4) |
O12v—Rb3a—O5viii | 135.65 (7) | Ag3vii—O5—Rb3bviii | 65.9 (8) |
O12x—Rb3a—O5viii | 44.35 (7) | Ag3viii—O5—Rb3bviii | 65.9 (8) |
O9v—Rb3a—O5viii | 81.81 (6) | Rb2vii—O5—Rb3bviii | 72.30 (17) |
O9x—Rb3a—O5viii | 98.19 (6) | Rb2viii—O5—Rb3bviii | 72.30 (16) |
O9vi—Rb3a—O5viii | 98.19 (6) | Rb3dviii—O5—Rb3bviii | 15.1 (7) |
O9ix—Rb3a—O5viii | 81.81 (6) | Rb3cviii—O5—Rb3bviii | 8.4 (4) |
O12vi—Rb3a—O5xi | 135.65 (7) | W2—O5—Rb3axviii | 151.04 (18) |
O12ix—Rb3a—O5xi | 44.35 (7) | Scxii—O5—Rb3axviii | 67.80 (11) |
O12v—Rb3a—O5xi | 44.35 (7) | Ag3vii—O5—Rb3axviii | 68.4 (7) |
O12x—Rb3a—O5xi | 135.65 (7) | Ag3viii—O5—Rb3axviii | 68.4 (7) |
O9v—Rb3a—O5xi | 98.19 (6) | Rb2vii—O5—Rb3axviii | 74.46 (8) |
O9x—Rb3a—O5xi | 81.81 (6) | Rb2viii—O5—Rb3axviii | 74.46 (8) |
O9vi—Rb3a—O5xi | 81.81 (6) | Rb3dviii—O5—Rb3axviii | 20.5 (6) |
O9ix—Rb3a—O5xi | 98.19 (6) | Rb3cviii—O5—Rb3axviii | 13.89 (15) |
O5viii—Rb3a—O5xi | 180.00 (10) | Rb3bviii—O5—Rb3axviii | 5.5 (4) |
O12vi—Rb3b—O12x | 62.8 (6) | W3—O6—Ag2iv | 106.61 (19) |
O12vi—Rb3b—O12ix | 161.8 (8) | W3—O6—Rb1ii | 134.15 (6) |
O12x—Rb3b—O12ix | 114.4 (2) | Ag2iv—O6—Rb1ii | 86.12 (10) |
O12vi—Rb3b—O12v | 114.4 (2) | W3—O6—Rb1 | 134.15 (6) |
O12x—Rb3b—O12v | 161.8 (8) | Ag2iv—O6—Rb1 | 86.12 (10) |
O12ix—Rb3b—O12v | 62.0 (6) | Rb1ii—O6—Rb1 | 89.53 (11) |
O12vi—Rb3b—O9v | 76.6 (3) | W3—O6—Ag2 | 93.56 (16) |
O12x—Rb3b—O9v | 133.7 (8) | Ag2iv—O6—Ag2 | 159.83 (16) |
O12ix—Rb3b—O9v | 111.1 (9) | Rb1ii—O6—Ag2 | 79.62 (9) |
O12v—Rb3b—O9v | 56.6 (3) | Rb1—O6—Ag2 | 79.62 (9) |
O12vi—Rb3b—O9ix | 133.7 (8) | W3—O7—Ag1xiv | 101.58 (19) |
O12x—Rb3b—O9ix | 76.6 (3) | W3—O7—Ag2 | 99.58 (17) |
O12ix—Rb3b—O9ix | 56.6 (3) | Ag1xiv—O7—Ag2 | 158.84 (16) |
O12v—Rb3b—O9ix | 111.1 (9) | W3—O7—Rb1xiii | 135.26 (5) |
O9v—Rb3b—O9ix | 124.4 (8) | Ag1xiv—O7—Rb1xiii | 82.18 (9) |
O12vi—Rb3b—O9x | 99.9 (8) | Ag2—O7—Rb1xiii | 82.83 (10) |
O12x—Rb3b—O9x | 50.9 (3) | W3—O7—Rb1v | 135.26 (5) |
O12ix—Rb3b—O9x | 68.8 (3) | Ag1xiv—O7—Rb1v | 82.18 (9) |
O12v—Rb3b—O9x | 115.5 (6) | Ag2—O7—Rb1v | 82.83 (10) |
O9v—Rb3b—O9x | 166.9 (6) | Rb1xiii—O7—Rb1v | 89.47 (11) |
O9ix—Rb3b—O9x | 67.19 (16) | W3—O8—Sc | 159.3 (2) |
O12vi—Rb3b—O9vi | 50.9 (3) | W4—O9—Ag3xix | 170.1 (7) |
O12x—Rb3b—O9vi | 99.9 (8) | W4—O9—Rb2xix | 167.3 (2) |
O12ix—Rb3b—O9vi | 115.5 (6) | Ag3xix—O9—Rb2xix | 8.7 (10) |
O12v—Rb3b—O9vi | 68.8 (3) | W4—O9—Rb3dxv | 106.8 (9) |
O9v—Rb3b—O9vi | 67.19 (16) | Ag3xix—O9—Rb3dxv | 70.5 (13) |
O9ix—Rb3b—O9vi | 166.9 (6) | Rb2xix—O9—Rb3dxv | 79.0 (9) |
O9x—Rb3b—O9vi | 100.7 (6) | W4—O9—Rb3cxv | 100.3 (2) |
O12vi—Rb3b—O5viii | 47.9 (4) | Ag3xix—O9—Rb3cxv | 76.0 (10) |
O12x—Rb3b—O5viii | 47.9 (4) | Rb2xix—O9—Rb3cxv | 84.2 (2) |
O12ix—Rb3b—O5viii | 145.1 (4) | Rb3dxv—O9—Rb3cxv | 8.8 (8) |
O12v—Rb3b—O5viii | 145.1 (4) | W4—O9—Rb3bxv | 92.3 (5) |
O9v—Rb3b—O5viii | 88.6 (4) | Ag3xix—O9—Rb3bxv | 82.6 (10) |
O9ix—Rb3b—O5viii | 88.6 (4) | Rb2xix—O9—Rb3bxv | 90.3 (5) |
O9x—Rb3b—O5viii | 98.4 (5) | Rb3dxv—O9—Rb3bxv | 20.1 (8) |
O9vi—Rb3b—O5viii | 98.4 (5) | Rb3cxv—O9—Rb3bxv | 11.4 (3) |
O12vi—Rb3c—O12x | 60.5 (2) | W4—O9—Rb1xix | 94.07 (15) |
O12vi—Rb3c—O9ix | 138.3 (3) | Ag3xix—O9—Rb1xix | 95.8 (7) |
O12x—Rb3c—O9ix | 78.28 (12) | Rb2xix—O9—Rb1xix | 95.42 (10) |
O12vi—Rb3c—O9v | 78.28 (12) | Rb3dxv—O9—Rb1xix | 104.3 (7) |
O12x—Rb3c—O9v | 138.3 (3) | Rb3cxv—O9—Rb1xix | 111.1 (2) |
O9ix—Rb3c—O9v | 140.8 (4) | Rb3bxv—O9—Rb1xix | 120.2 (4) |
O12vi—Rb3c—O12ix | 137.9 (3) | W4—O9—Rb2vii | 95.65 (15) |
O12x—Rb3c—O12ix | 105.17 (19) | Ag3xix—O9—Rb2vii | 84.0 (10) |
O9ix—Rb3c—O12ix | 56.36 (13) | Rb2xix—O9—Rb2vii | 75.38 (9) |
O9v—Rb3c—O12ix | 110.1 (3) | Rb3dxv—O9—Rb2vii | 150.3 (9) |
O12vi—Rb3c—O12v | 105.17 (19) | Rb3cxv—O9—Rb2vii | 149.8 (2) |
O12x—Rb3c—O12v | 137.9 (3) | Rb3bxv—O9—Rb2vii | 145.2 (5) |
O9ix—Rb3c—O12v | 110.1 (3) | Rb1xix—O9—Rb2vii | 93.04 (10) |
O9v—Rb3c—O12v | 56.36 (13) | W4—O9—Rb3axv | 87.83 (13) |
O12ix—Rb3c—O12v | 56.87 (19) | Ag3xix—O9—Rb3axv | 86.2 (9) |
O12vi—Rb3c—O5viii | 51.80 (16) | Rb2xix—O9—Rb3axv | 93.44 (11) |
O12x—Rb3c—O5viii | 51.80 (16) | Rb3dxv—O9—Rb3axv | 27.1 (7) |
O9ix—Rb3c—O5viii | 98.3 (2) | Rb3cxv—O9—Rb3axv | 18.37 (18) |
O9v—Rb3c—O5viii | 98.3 (2) | Rb3bxv—O9—Rb3axv | 7.0 (3) |
O12ix—Rb3c—O5viii | 151.26 (10) | Rb1xix—O9—Rb3axv | 125.94 (12) |
O12v—Rb3c—O5viii | 151.26 (10) | Rb2vii—O9—Rb3axv | 140.60 (13) |
O12vi—Rb3c—O3 | 93.7 (2) | W4—O9—Rb3bvi | 84.0 (4) |
O12x—Rb3c—O3 | 115.5 (3) | Ag3xix—O9—Rb3bvi | 89.4 (10) |
O9ix—Rb3c—O3 | 98.6 (2) | Rb2xix—O9—Rb3bvi | 96.2 (4) |
O9v—Rb3c—O3 | 57.58 (15) | Rb3dxv—O9—Rb3bvi | 33.1 (7) |
O12ix—Rb3c—O3 | 126.3 (3) | Rb3cxv—O9—Rb3bvi | 24.5 (4) |
O12v—Rb3c—O3 | 104.24 (19) | Rb3bxv—O9—Rb3bvi | 13.1 (6) |
O5viii—Rb3c—O3 | 65.56 (17) | Rb1xix—O9—Rb3bvi | 130.8 (4) |
O12vi—Rb3c—O3iii | 115.5 (3) | Rb2vii—O9—Rb3bvi | 136.2 (4) |
O12x—Rb3c—O3iii | 93.7 (2) | Rb3axv—O9—Rb3bvi | 6.1 (3) |
O9ix—Rb3c—O3iii | 57.58 (15) | W4—O9—Rb3cvi | 78.82 (18) |
O9v—Rb3c—O3iii | 98.6 (2) | Ag3xix—O9—Rb3cvi | 93.9 (8) |
O12ix—Rb3c—O3iii | 104.24 (19) | Rb2xix—O9—Rb3cvi | 100.04 (17) |
O12v—Rb3c—O3iii | 126.3 (3) | Rb3dxv—O9—Rb3cvi | 40.4 (6) |
O5viii—Rb3c—O3iii | 65.56 (17) | Rb3cxv—O9—Rb3cvi | 31.7 (3) |
O3—Rb3c—O3iii | 42.63 (14) | Rb3bxv—O9—Rb3cvi | 20.4 (4) |
O12vi—Rb3c—O9x | 89.6 (2) | Rb1xix—O9—Rb3cvi | 135.71 (14) |
O12x—Rb3c—O9x | 45.23 (12) | Rb2vii—O9—Rb3cvi | 130.96 (15) |
O9ix—Rb3c—O9x | 63.07 (15) | Rb3axv—O9—Rb3cvi | 13.38 (10) |
O9v—Rb3c—O9x | 148.3 (3) | Rb3bvi—O9—Rb3cvi | 7.3 (3) |
O12ix—Rb3c—O9x | 61.18 (13) | W4—O10—Rb2 | 150.83 (18) |
O12v—Rb3c—O9x | 100.2 (2) | W4—O10—Rb2vi | 102.44 (14) |
O5viii—Rb3c—O9x | 96.86 (18) | Rb2—O10—Rb2vi | 80.27 (9) |
O3—Rb3c—O9x | 153.6 (2) | W4—O10—Rb1 | 105.65 (13) |
O3iii—Rb3c—O9x | 113.11 (10) | Rb2—O10—Rb1 | 100.96 (10) |
O12vi—Rb3c—O9vi | 45.23 (12) | Rb2vi—O10—Rb1 | 107.66 (11) |
O12x—Rb3c—O9vi | 89.6 (2) | W4—O10—Ag3vi | 95.6 (8) |
O9ix—Rb3c—O9vi | 148.3 (3) | Rb2—O10—Ag3vi | 83.7 (6) |
O9v—Rb3c—O9vi | 63.07 (15) | Rb2vi—O10—Ag3vi | 8.5 (8) |
O12ix—Rb3c—O9vi | 100.2 (2) | Rb1—O10—Ag3vi | 114.8 (8) |
O12v—Rb3c—O9vi | 61.18 (13) | W4—O10—Ag3 | 158.0 (7) |
Ag3—Rb3c—O9vi | 77.7 (6) | Rb2—O10—Ag3 | 8.1 (8) |
Ag3iii—Rb3c—O9vi | 141.7 (5) | Rb2vi—O10—Ag3 | 82.7 (7) |
O5viii—Rb3c—O9vi | 96.86 (18) | Rb1—O10—Ag3 | 92.8 (8) |
W4ix—Rb3c—O9vi | 126.3 (3) | Ag3vi—O10—Ag3 | 87.1 (10) |
W4v—Rb3c—O9vi | 58.20 (9) | W4—O10—Rb2vii | 92.37 (13) |
Scvi—Rb3c—O9vi | 73.85 (14) | Rb2—O10—Rb2vii | 71.75 (8) |
Rb2—Rb3c—O9vi | 75.55 (8) | Rb2vi—O10—Rb2vii | 144.59 (12) |
Rb2iii—Rb3c—O9vi | 141.0 (2) | Rb1—O10—Rb2vii | 98.75 (9) |
O3—Rb3c—O9vi | 113.11 (10) | Ag3vi—O10—Rb2vii | 141.7 (6) |
O3iii—Rb3c—O9vi | 153.6 (2) | Ag3—O10—Rb2vii | 72.7 (6) |
O9x—Rb3c—O9vi | 87.5 (2) | W4—O11—Ag2iv | 154.1 (2) |
Rb3b—Rb3d—O9ix | 92.6 (12) | W4—O11—Rb1xix | 103.25 (14) |
Rb3a—Rb3d—O9ix | 93.2 (9) | Ag2iv—O11—Rb1xix | 94.01 (11) |
Rb3bxvii—Rb3d—O9ix | 93.5 (8) | W4—O11—Rb1 | 92.20 (13) |
Rb3cxvii—Rb3d—O9ix | 93.4 (7) | Ag2iv—O11—Rb1 | 85.92 (11) |
Rb3b—Rb3d—O9v | 92.6 (12) | Rb1xix—O11—Rb1 | 141.36 (12) |
Rb3a—Rb3d—O9v | 93.2 (9) | W4—O12—Sc | 141.76 (16) |
Rb3bxvii—Rb3d—O9v | 93.5 (8) | W4—O12—Rb3axv | 106.18 (12) |
Rb3cxvii—Rb3d—O9v | 93.4 (7) | Sc—O12—Rb3axv | 102.61 (11) |
O9ix—Rb3d—O9v | 146.5 (18) | W4—O12—Rb3bvi | 111.0 (3) |
O9ix—Rb3d—O12vi | 134.9 (12) | Sc—O12—Rb3bvi | 101.3 (3) |
O9v—Rb3d—O12vi | 77.2 (4) | Rb3axv—O12—Rb3bvi | 9.2 (4) |
O9ix—Rb3d—O12x | 77.2 (4) | W4—O12—Rb3bxv | 101.1 (3) |
O9v—Rb3d—O12x | 134.9 (12) | Sc—O12—Rb3bxv | 103.6 (3) |
O12vi—Rb3d—O12x | 58.0 (8) | Rb3axv—O12—Rb3bxv | 9.1 (4) |
O9ix—Rb3d—O5viii | 104.3 (9) | Rb3bvi—O12—Rb3bxv | 18.2 (8) |
O9v—Rb3d—O5viii | 104.3 (9) | W4—O12—Rb3cvi | 117.33 (18) |
O12vi—Rb3d—O5viii | 53.5 (8) | Sc—O12—Rb3cvi | 98.47 (15) |
O12x—Rb3d—O5viii | 53.5 (8) | Rb3axv—O12—Rb3cvi | 21.69 (18) |
O9ix—Rb3d—O12ix | 53.8 (6) | Rb3bvi—O12—Rb3cvi | 12.5 (4) |
O9v—Rb3d—O12ix | 104.6 (12) | Rb3bxv—O12—Rb3cvi | 30.7 (5) |
O12vi—Rb3d—O12ix | 122.9 (11) | W4—O12—Ag3vi | 97.9 (8) |
O12x—Rb3d—O12ix | 96.7 (7) | Sc—O12—Ag3vi | 106.5 (6) |
O5viii—Rb3d—O12ix | 148.7 (8) | Rb3axv—O12—Ag3vi | 90.4 (8) |
O9ix—Rb3d—O12v | 104.6 (12) | Rb3bvi—O12—Ag3vi | 82.1 (9) |
O9v—Rb3d—O12v | 53.8 (6) | Rb3bxv—O12—Ag3vi | 98.7 (9) |
O12vi—Rb3d—O12v | 96.7 (7) | Rb3cvi—O12—Ag3vi | 71.0 (9) |
O12x—Rb3d—O12v | 122.9 (11) | W4—O12—Rb3dvi | 121.3 (6) |
Rb3dxvii—Rb3d—O12v | 56.4 (13) | Sc—O12—Rb3dvi | 96.0 (6) |
O5viii—Rb3d—O12v | 148.7 (8) | Rb3axv—O12—Rb3dvi | 30.0 (7) |
O12ix—Rb3d—O12v | 52.2 (7) | Rb3bvi—O12—Rb3dvi | 20.9 (8) |
O9ix—Rb3d—O3 | 109.5 (9) | Rb3bxv—O12—Rb3dvi | 39.1 (8) |
O9v—Rb3d—O3 | 63.6 (5) | Rb3cvi—O12—Rb3dvi | 8.4 (8) |
O12vi—Rb3d—O3 | 100.4 (9) | Ag3vi—O12—Rb3dvi | 63.9 (10) |
O12x—Rb3d—O3 | 125.1 (14) | W4—O12—Rb3cxv | 94.12 (15) |
O5viii—Rb3d—O3 | 72.7 (8) | Sc—O12—Rb3cxv | 104.90 (14) |
O12ix—Rb3d—O3 | 132.2 (14) | Rb3axv—O12—Rb3cxv | 20.44 (17) |
O12v—Rb3d—O3 | 108.3 (8) | Rb3bvi—O12—Rb3cxv | 29.6 (5) |
O9ix—Rb3d—O3iii | 63.6 (5) | Rb3bxv—O12—Rb3cxv | 11.4 (4) |
O9v—Rb3d—O3iii | 109.5 (9) | Rb3cvi—O12—Rb3cxv | 42.1 (3) |
O12vi—Rb3d—O3iii | 125.1 (14) | Ag3vi—O12—Rb3cxv | 108.7 (8) |
O12x—Rb3d—O3iii | 100.4 (9) | Rb3dvi—O12—Rb3cxv | 50.5 (6) |
O5viii—Rb3d—O3iii | 72.7 (8) | W4—O12—Rb2vi | 92.95 (11) |
O12ix—Rb3d—O3iii | 108.3 (8) | Sc—O12—Rb2vi | 107.72 (11) |
O12v—Rb3d—O3iii | 132.2 (14) | Rb3axv—O12—Rb2vi | 97.56 (9) |
O3—Rb3d—O3iii | 48.0 (5) | Rb3bvi—O12—Rb2vi | 89.4 (4) |
O4ii—Ag1—O4 | 175.6 (2) | Rb3bxv—O12—Rb2vi | 105.6 (5) |
O4ii—Ag1—O7iv | 90.74 (4) | Rb3cvi—O12—Rb2vi | 78.56 (17) |
O4—Ag1—O7iv | 90.74 (4) | Ag3vi—O12—Rb2vi | 7.8 (9) |
O4ii—Ag1—O7xii | 90.74 (4) | Rb3dvi—O12—Rb2vi | 71.6 (5) |
O4—Ag1—O7xii | 90.74 (4) | Rb3cxv—O12—Rb2vi | 115.21 (18) |
O7iv—Ag1—O7xii | 140.76 (17) | W4—O12—Rb3dxv | 89.7 (3) |
O4ii—Ag1—O1 | 88.05 (11) | Sc—O12—Rb3dxv | 105.7 (4) |
O4—Ag1—O1 | 88.05 (11) | Rb3axv—O12—Rb3dxv | 27.0 (6) |
O7iv—Ag1—O1 | 81.32 (11) | Rb3bvi—O12—Rb3dxv | 36.2 (7) |
O7xii—Ag1—O1 | 137.92 (12) | Rb3bxv—O12—Rb3dxv | 18.0 (8) |
O4ii—Ag1—O1i | 88.05 (11) | Rb3cvi—O12—Rb3dxv | 48.7 (6) |
O4—Ag1—O1i | 88.05 (11) | Ag3vi—O12—Rb3dxv | 114.3 (10) |
O7iv—Ag1—O1i | 137.92 (12) | Rb3dvi—O12—Rb3dxv | 57.1 (11) |
O7xii—Ag1—O1i | 81.32 (11) | Rb3cxv—O12—Rb3dxv | 6.6 (7) |
O1—Ag1—O1i | 56.61 (16) | Rb2vi—O12—Rb3dxv | 120.4 (7) |
Symmetry codes: (i) −x+1, y, −z+3/2; (ii) x, y, −z+3/2; (iii) −x+1, y, z; (iv) −x+1/2, y−1/2, −z+3/2; (v) −x+1/2, y+1/2, z; (vi) −x+1/2, −y+1/2, −z+1; (vii) x, −y, −z+1; (viii) −x+1, −y, −z+1; (ix) x+1/2, y+1/2, z; (x) x+1/2, −y+1/2, −z+1; (xi) x, y+1, z; (xii) x+1/2, y−1/2, z; (xiii) −x+1/2, y+1/2, −z+3/2; (xiv) x−1/2, y+1/2, z; (xv) x−1/2, y−1/2, z; (xvi) −x, y, z; (xvii) −x+1, −y+1, −z+1; (xviii) x, y−1, z; (xix) −x+1/2, y−1/2, z. |