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This structure determination shows that in the two molybdenum complexes of the title, (I), [Mo(C2F3O2)(C3H5)(C12H8N2)(CO)2] and (II), [Mo(C2F3O2)(C4H7)(C12H8N2)(CO)2], the phenanthroline ligand is perpendicular to the molybdenum-dicarbonyl plane. This is in contrast to similar molybdenum complexes, where the ligand is in the plane.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablocks I, II, global

fcf

Structure factor file (CIF format)
Contains datablock I

fcf

Structure factor file (CIF format)
Contains datablock mo2_15a

CCDC references: 126205; 126206

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