Supporting information
Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536807009270/dn2136sup1.cif | |
Structure factor file (CIF format) https://doi.org/10.1107/S1600536807009270/dn2136Isup2.hkl |
CCDC reference: 642970
Data collection: X-AREA (Stoe & Cie, 2000); cell refinement: X-AREA; data reduction: X-RED32 (Stoe & Cie, 2000); program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: ORTEP-32 (Farrugia, 1997); software used to prepare material for publication: SHELXL97.
[Rh2(C10H15)2Cl4]·3CHCl3 | F(000) = 1928 |
Mr = 976.16 | Dx = 1.792 Mg m−3 |
Monoclinic, P21/c | Mo Kα radiation, λ = 0.71073 Å |
Hall symbol: -P 2ybc | Cell parameters from 33620 reflections |
a = 16.2812 (8) Å | θ = 1.8–25.6° |
b = 16.7815 (6) Å | µ = 1.89 mm−1 |
c = 13.8303 (7) Å | T = 173 K |
β = 106.733 (4)° | Rod, orange |
V = 3618.8 (3) Å3 | 0.30 × 0.15 × 0.15 mm |
Z = 4 |
Stoe IPDS2 diffractometer | 6449 independent reflections |
Radiation source: sealed X-ray tube, 12 x 0.4 mm long-fine focus | 4874 reflections with I > 2σ(I) |
Plane graphite monochromator | Rint = 0.038 |
Detector resolution: 6.67 pixels mm-1 | θmax = 25.2°, θmin = 1.3° |
rotation method scans | h = −19→19 |
Absorption correction: multi-scan (Blessing, 1995) | k = −20→19 |
Tmin = 0.699, Tmax = 0.848 | l = −16→16 |
46686 measured reflections |
Refinement on F2 | Primary atom site location: structure-invariant direct methods |
Least-squares matrix: full | Secondary atom site location: difference Fourier map |
R[F2 > 2σ(F2)] = 0.027 | Hydrogen site location: inferred from neighbouring sites |
wR(F2) = 0.061 | H-atom parameters constrained |
S = 1.01 | w = 1/[σ2(Fo2) + (0.0333P)2] where P = (Fo2 + 2Fc2)/3 |
6449 reflections | (Δ/σ)max = 0.002 |
400 parameters | Δρmax = 0.56 e Å−3 |
0 restraints | Δρmin = −0.53 e Å−3 |
Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes. |
Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. |
x | y | z | Uiso*/Ueq | Occ. (<1) | |
C1 | 0.1894 (2) | 0.38898 (19) | 0.9304 (2) | 0.0317 (7) | |
C2 | 0.1130 (2) | 0.37387 (19) | 0.8496 (2) | 0.0315 (7) | |
C3 | 0.0794 (2) | 0.44999 (19) | 0.8069 (2) | 0.0296 (7) | |
C4 | 0.1331 (2) | 0.51115 (18) | 0.8632 (2) | 0.0314 (7) | |
C5 | 0.2010 (2) | 0.47307 (19) | 0.9400 (2) | 0.0309 (7) | |
C6 | 0.2475 (2) | 0.3287 (2) | 0.9940 (3) | 0.0465 (9) | |
H6A | 0.2174 | 0.2792 | 0.9911 | 0.070* | |
H6B | 0.2664 | 0.3471 | 1.0626 | 0.070* | |
H6C | 0.2963 | 0.3209 | 0.9693 | 0.070* | |
C7 | 0.0770 (2) | 0.2945 (2) | 0.8108 (3) | 0.0438 (9) | |
H7A | 0.0971 | 0.2797 | 0.7545 | 0.066* | |
H7B | 0.0155 | 0.2973 | 0.7895 | 0.066* | |
H7C | 0.0953 | 0.2554 | 0.8633 | 0.066* | |
C8 | 0.0033 (2) | 0.4633 (2) | 0.7193 (2) | 0.0437 (9) | |
H8A | −0.0206 | 0.5147 | 0.7248 | 0.066* | |
H8B | −0.0387 | 0.4229 | 0.7179 | 0.066* | |
H8C | 0.0200 | 0.4608 | 0.6582 | 0.066* | |
C9 | 0.1231 (3) | 0.5983 (2) | 0.8451 (3) | 0.0480 (9) | |
H9A | 0.1464 | 0.6129 | 0.7913 | 0.072* | |
H9B | 0.1531 | 0.6264 | 0.9054 | 0.072* | |
H9C | 0.0633 | 0.6120 | 0.8269 | 0.072* | |
C10 | 0.2723 (2) | 0.5157 (2) | 1.0137 (3) | 0.0487 (9) | |
H10A | 0.2940 | 0.4833 | 1.0728 | 0.073* | |
H10B | 0.2515 | 0.5652 | 1.0324 | 0.073* | |
H10C | 0.3174 | 0.5261 | 0.9835 | 0.073* | |
C11 | 0.69337 (17) | 0.49097 (15) | 0.69271 (17) | 0.0338 (15) | 0.65 |
C12 | 0.62085 (17) | 0.49233 (16) | 0.73023 (18) | 0.037 (2) | 0.65 |
C13 | 0.60045 (17) | 0.57320 (18) | 0.7429 (2) | 0.047 (3) | 0.65 |
C14 | 0.66036 (19) | 0.62182 (14) | 0.7132 (2) | 0.0369 (18) | 0.65 |
C15 | 0.71779 (16) | 0.57100 (16) | 0.68218 (18) | 0.0305 (16) | 0.65 |
C16 | 0.7369 (2) | 0.41737 (18) | 0.6683 (3) | 0.0563 (17) | 0.65 |
H16A | 0.6959 | 0.3749 | 0.6496 | 0.084* | 0.65 |
H16B | 0.7824 | 0.4018 | 0.7265 | 0.084* | 0.65 |
H16C | 0.7600 | 0.4286 | 0.6133 | 0.084* | 0.65 |
C17 | 0.5737 (3) | 0.4204 (2) | 0.7527 (3) | 0.070 (2) | 0.65 |
H17A | 0.6047 | 0.3986 | 0.8170 | 0.105* | 0.65 |
H17B | 0.5691 | 0.3810 | 0.7011 | 0.105* | 0.65 |
H17C | 0.5174 | 0.4360 | 0.7543 | 0.105* | 0.65 |
C18 | 0.5278 (2) | 0.6024 (3) | 0.7812 (3) | 0.077 (2) | 0.65 |
H18A | 0.5456 | 0.6020 | 0.8537 | 0.116* | 0.65 |
H18B | 0.4791 | 0.5680 | 0.7568 | 0.116* | 0.65 |
H18C | 0.5126 | 0.6556 | 0.7574 | 0.116* | 0.65 |
C19 | 0.6626 (3) | 0.71175 (14) | 0.7144 (3) | 0.071 (2) | 0.65 |
H19A | 0.6502 | 0.7313 | 0.6465 | 0.107* | 0.65 |
H19B | 0.7185 | 0.7296 | 0.7527 | 0.107* | 0.65 |
H19C | 0.6205 | 0.7316 | 0.7447 | 0.107* | 0.65 |
C20 | 0.7918 (2) | 0.5974 (3) | 0.6446 (3) | 0.0518 (16) | 0.65 |
H20A | 0.7760 | 0.6448 | 0.6048 | 0.078* | 0.65 |
H20B | 0.8056 | 0.5560 | 0.6041 | 0.078* | 0.65 |
H20C | 0.8408 | 0.6082 | 0.7012 | 0.078* | 0.65 |
C21 | 0.4231 (3) | 0.7787 (2) | 0.4769 (3) | 0.0556 (11) | |
H21 | 0.4552 | 0.7305 | 0.4707 | 0.067* | |
C22 | 0.2756 (2) | 0.4456 (2) | 0.6536 (3) | 0.0454 (9) | |
H22 | 0.3161 | 0.4371 | 0.6142 | 0.054* | |
C23 | 0.9142 (2) | 0.2258 (2) | 0.9655 (3) | 0.0446 (9) | |
H23 | 0.9495 | 0.2736 | 0.9864 | 0.054* | |
Cl1 | 0.08430 (6) | 0.34808 (5) | 1.09468 (6) | 0.0388 (2) | |
Cl2 | 0.07558 (5) | 0.55292 (5) | 1.07776 (5) | 0.03044 (17) | |
Cl3 | 0.58835 (5) | 0.65236 (5) | 0.46084 (5) | 0.03398 (18) | |
Cl4 | 0.42943 (5) | 0.55280 (5) | 0.53447 (5) | 0.03315 (17) | |
Cl5 | 0.35696 (8) | 0.80501 (7) | 0.35659 (9) | 0.0707 (3) | |
Cl6 | 0.49571 (8) | 0.85528 (8) | 0.52578 (9) | 0.0763 (4) | |
Cl7 | 0.35914 (10) | 0.75823 (8) | 0.55594 (11) | 0.0848 (4) | |
Cl8 | 0.23510 (10) | 0.54187 (8) | 0.63181 (12) | 0.0954 (5) | |
Cl9 | 0.32971 (8) | 0.43274 (9) | 0.78174 (8) | 0.0803 (4) | |
Cl10 | 0.19387 (8) | 0.37443 (8) | 0.61784 (10) | 0.0772 (3) | |
Cl11 | 0.83684 (7) | 0.24572 (6) | 0.85045 (7) | 0.0584 (3) | |
Cl12 | 0.86559 (7) | 0.20202 (6) | 1.05942 (8) | 0.0611 (3) | |
Cl13 | 0.98107 (7) | 0.14710 (6) | 0.95172 (9) | 0.0617 (3) | |
Rh1 | 0.081153 (15) | 0.442045 (14) | 0.962918 (15) | 0.02433 (7) | |
Rh2 | 0.586935 (15) | 0.554913 (15) | 0.588323 (16) | 0.02709 (7) | |
C11' | 0.6490 (4) | 0.4890 (2) | 0.7156 (3) | 0.042 (4) | 0.35 |
C12' | 0.5852 (3) | 0.5349 (3) | 0.7415 (3) | 0.029 (3) | 0.35 |
C13' | 0.6048 (3) | 0.6167 (2) | 0.7337 (3) | 0.029 (3) | 0.35 |
C14' | 0.6807 (3) | 0.6213 (3) | 0.7029 (4) | 0.032 (3) | 0.35 |
C15' | 0.7080 (3) | 0.5424 (3) | 0.6917 (4) | 0.034 (3) | 0.35 |
C16' | 0.6534 (6) | 0.3992 (2) | 0.7137 (5) | 0.081 (5) | 0.35 |
H16D | 0.7122 | 0.3827 | 0.7281 | 0.121* | 0.35 |
H16E | 0.6216 | 0.3801 | 0.6482 | 0.121* | 0.35 |
H16F | 0.6292 | 0.3776 | 0.7637 | 0.121* | 0.35 |
C17' | 0.5099 (4) | 0.5025 (4) | 0.7720 (5) | 0.054 (3) | 0.35 |
H17D | 0.4828 | 0.4609 | 0.7262 | 0.081* | 0.35 |
H17E | 0.4693 | 0.5445 | 0.7699 | 0.081* | 0.35 |
H17F | 0.5295 | 0.4815 | 0.8393 | 0.081* | 0.35 |
C18' | 0.5538 (5) | 0.6865 (3) | 0.7544 (5) | 0.054 (3) | 0.35 |
H18D | 0.5678 | 0.7334 | 0.7227 | 0.081* | 0.35 |
H18E | 0.5676 | 0.6950 | 0.8259 | 0.081* | 0.35 |
H18F | 0.4937 | 0.6754 | 0.7278 | 0.081* | 0.35 |
C19' | 0.7246 (5) | 0.6969 (4) | 0.6852 (6) | 0.072 (4) | 0.35 |
H19D | 0.6925 | 0.7421 | 0.6966 | 0.108* | 0.35 |
H19E | 0.7276 | 0.6977 | 0.6169 | 0.108* | 0.35 |
H19F | 0.7815 | 0.6987 | 0.7309 | 0.108* | 0.35 |
C20' | 0.7861 (4) | 0.5193 (5) | 0.6601 (5) | 0.073 (5) | 0.35 |
H20D | 0.7979 | 0.5599 | 0.6171 | 0.110* | 0.35 |
H20E | 0.7756 | 0.4697 | 0.6241 | 0.110* | 0.35 |
H20F | 0.8345 | 0.5136 | 0.7189 | 0.110* | 0.35 |
U11 | U22 | U33 | U12 | U13 | U23 | |
C1 | 0.0299 (18) | 0.0370 (18) | 0.0301 (16) | 0.0053 (14) | 0.0117 (14) | 0.0006 (13) |
C2 | 0.0358 (19) | 0.0326 (17) | 0.0285 (16) | 0.0004 (14) | 0.0129 (14) | −0.0066 (13) |
C3 | 0.0304 (17) | 0.0389 (18) | 0.0215 (14) | 0.0007 (14) | 0.0107 (12) | −0.0011 (13) |
C4 | 0.039 (2) | 0.0319 (18) | 0.0305 (16) | −0.0008 (14) | 0.0210 (14) | 0.0008 (13) |
C5 | 0.0305 (18) | 0.0372 (17) | 0.0273 (15) | −0.0049 (14) | 0.0119 (13) | −0.0041 (13) |
C6 | 0.043 (2) | 0.051 (2) | 0.044 (2) | 0.0192 (18) | 0.0098 (16) | 0.0062 (17) |
C7 | 0.050 (2) | 0.036 (2) | 0.047 (2) | −0.0050 (17) | 0.0169 (17) | −0.0183 (16) |
C8 | 0.039 (2) | 0.063 (2) | 0.0284 (17) | 0.0094 (18) | 0.0081 (15) | 0.0025 (15) |
C9 | 0.067 (3) | 0.037 (2) | 0.050 (2) | −0.0034 (19) | 0.033 (2) | 0.0050 (17) |
C10 | 0.042 (2) | 0.063 (3) | 0.0401 (19) | −0.0183 (19) | 0.0113 (16) | −0.0143 (18) |
C11 | 0.035 (4) | 0.038 (4) | 0.019 (3) | 0.004 (3) | −0.007 (2) | −0.002 (3) |
C12 | 0.041 (4) | 0.043 (5) | 0.021 (3) | −0.018 (3) | −0.001 (3) | 0.006 (3) |
C13 | 0.036 (4) | 0.077 (8) | 0.026 (3) | 0.003 (4) | 0.006 (3) | −0.014 (4) |
C14 | 0.048 (4) | 0.031 (4) | 0.026 (4) | 0.000 (3) | 0.001 (3) | −0.004 (3) |
C15 | 0.028 (3) | 0.035 (4) | 0.023 (3) | −0.003 (3) | 0.000 (2) | 0.003 (2) |
C16 | 0.056 (4) | 0.045 (3) | 0.054 (4) | 0.020 (3) | −0.008 (3) | 0.001 (3) |
C17 | 0.072 (5) | 0.080 (5) | 0.045 (4) | −0.043 (4) | −0.003 (3) | 0.020 (3) |
C18 | 0.053 (4) | 0.145 (8) | 0.036 (3) | 0.013 (5) | 0.016 (3) | −0.028 (4) |
C19 | 0.118 (7) | 0.033 (3) | 0.047 (4) | −0.013 (4) | −0.002 (4) | −0.013 (3) |
C20 | 0.027 (3) | 0.085 (5) | 0.038 (3) | −0.021 (3) | 0.000 (2) | 0.003 (3) |
C21 | 0.044 (2) | 0.052 (2) | 0.070 (3) | 0.0058 (19) | 0.015 (2) | −0.022 (2) |
C22 | 0.045 (2) | 0.048 (2) | 0.048 (2) | 0.0147 (18) | 0.0228 (17) | 0.0056 (17) |
C23 | 0.042 (2) | 0.0332 (19) | 0.049 (2) | −0.0023 (16) | −0.0023 (16) | −0.0016 (16) |
Cl1 | 0.0449 (5) | 0.0378 (5) | 0.0324 (4) | −0.0047 (4) | 0.0089 (4) | 0.0082 (3) |
Cl2 | 0.0298 (4) | 0.0321 (4) | 0.0302 (4) | −0.0053 (3) | 0.0100 (3) | −0.0109 (3) |
Cl3 | 0.0343 (5) | 0.0371 (4) | 0.0325 (4) | 0.0042 (3) | 0.0128 (3) | 0.0084 (3) |
Cl4 | 0.0252 (4) | 0.0433 (5) | 0.0312 (4) | −0.0018 (3) | 0.0086 (3) | −0.0069 (3) |
Cl5 | 0.0551 (7) | 0.0738 (8) | 0.0744 (7) | −0.0002 (6) | 0.0047 (5) | −0.0139 (6) |
Cl6 | 0.0552 (7) | 0.0870 (9) | 0.0845 (8) | −0.0159 (6) | 0.0165 (6) | −0.0407 (7) |
Cl7 | 0.1007 (10) | 0.0623 (7) | 0.1111 (10) | 0.0044 (7) | 0.0622 (9) | −0.0020 (7) |
Cl8 | 0.1109 (11) | 0.0633 (8) | 0.1343 (12) | 0.0493 (8) | 0.0707 (10) | 0.0364 (8) |
Cl9 | 0.0746 (8) | 0.1160 (11) | 0.0504 (6) | 0.0096 (8) | 0.0183 (6) | 0.0094 (6) |
Cl10 | 0.0591 (7) | 0.0926 (9) | 0.0859 (8) | −0.0114 (6) | 0.0305 (6) | −0.0146 (7) |
Cl11 | 0.0625 (7) | 0.0419 (5) | 0.0555 (6) | −0.0011 (5) | −0.0075 (5) | −0.0012 (4) |
Cl12 | 0.0702 (7) | 0.0509 (6) | 0.0640 (6) | −0.0008 (5) | 0.0220 (5) | −0.0021 (5) |
Cl13 | 0.0544 (6) | 0.0507 (6) | 0.0790 (7) | 0.0094 (5) | 0.0175 (5) | 0.0035 (5) |
Rh1 | 0.02839 (14) | 0.02360 (12) | 0.02181 (12) | −0.00172 (10) | 0.00850 (9) | −0.00325 (9) |
Rh2 | 0.02485 (14) | 0.03328 (14) | 0.02148 (12) | −0.00398 (11) | 0.00400 (9) | 0.00124 (10) |
C11' | 0.081 (11) | 0.023 (7) | 0.015 (5) | 0.015 (7) | 0.004 (7) | −0.009 (4) |
C12' | 0.028 (6) | 0.039 (8) | 0.011 (5) | −0.008 (5) | −0.007 (4) | 0.000 (4) |
C13' | 0.029 (6) | 0.036 (7) | 0.015 (5) | 0.006 (5) | −0.004 (4) | −0.010 (4) |
C14' | 0.023 (5) | 0.052 (10) | 0.013 (6) | −0.023 (6) | −0.006 (4) | 0.009 (5) |
C15' | 0.024 (6) | 0.034 (8) | 0.041 (7) | 0.004 (5) | 0.004 (5) | −0.012 (5) |
C16' | 0.145 (14) | 0.035 (6) | 0.032 (6) | 0.027 (8) | −0.024 (7) | 0.009 (5) |
C17' | 0.051 (7) | 0.088 (9) | 0.024 (5) | −0.035 (6) | 0.013 (5) | 0.010 (5) |
C18' | 0.072 (8) | 0.056 (7) | 0.032 (5) | 0.027 (6) | 0.013 (5) | −0.012 (5) |
C19' | 0.070 (10) | 0.086 (10) | 0.043 (7) | −0.058 (8) | −0.008 (6) | 0.006 (6) |
C20' | 0.028 (6) | 0.153 (14) | 0.035 (6) | 0.040 (8) | 0.003 (5) | 0.009 (7) |
C1—C5 | 1.425 (5) | C19—H19A | 0.9600 |
C1—C2 | 1.435 (4) | C19—H19B | 0.9600 |
C1—C6 | 1.488 (4) | C19—H19C | 0.9600 |
C1—Rh1 | 2.135 (3) | C20—H20A | 0.9600 |
C2—C3 | 1.447 (4) | C20—H20B | 0.9600 |
C2—C7 | 1.491 (4) | C20—H20C | 0.9600 |
C2—Rh1 | 2.121 (3) | C21—Cl6 | 1.746 (4) |
C3—C4 | 1.425 (4) | C21—Cl7 | 1.747 (4) |
C3—C8 | 1.479 (4) | C21—Cl5 | 1.758 (4) |
C3—Rh1 | 2.153 (3) | C21—H21 | 0.9800 |
C4—C5 | 1.444 (5) | C22—Cl8 | 1.738 (4) |
C4—C9 | 1.485 (5) | C22—Cl10 | 1.750 (4) |
C4—Rh1 | 2.152 (3) | C22—Cl9 | 1.751 (4) |
C5—C10 | 1.490 (4) | C22—H22 | 0.9800 |
C5—Rh1 | 2.129 (3) | C23—Cl12 | 1.751 (4) |
C6—H6A | 0.9600 | C23—Cl11 | 1.754 (3) |
C6—H6B | 0.9600 | C23—Cl13 | 1.756 (4) |
C6—H6C | 0.9600 | C23—H23 | 0.9800 |
C7—H7A | 0.9600 | Cl1—Rh1 | 2.3991 (8) |
C7—H7B | 0.9600 | Cl2—Rh1i | 2.4512 (8) |
C7—H7C | 0.9600 | Cl2—Rh1 | 2.4649 (7) |
C8—H8A | 0.9600 | Cl3—Rh2 | 2.4097 (8) |
C8—H8B | 0.9600 | Cl4—Rh2ii | 2.4416 (8) |
C8—H8C | 0.9600 | Cl4—Rh2 | 2.4560 (8) |
C9—H9A | 0.9600 | Rh1—Cl2i | 2.4512 (8) |
C9—H9B | 0.9600 | Rh1—Rh1i | 3.6578 (5) |
C9—H9C | 0.9600 | Rh2—Cl4ii | 2.4416 (8) |
C10—H10A | 0.9600 | Rh2—Rh2ii | 3.6601 (5) |
C10—H10B | 0.9600 | C11'—C12' | 1.4200 |
C10—H10C | 0.9600 | C11'—C15' | 1.4200 |
C11—C12 | 1.4200 | C11'—C16' | 1.5095 |
C11—C15 | 1.4200 | C12'—C13' | 1.4200 |
C11—C16 | 1.5095 | C12'—C17' | 1.5095 |
C11—Rh2 | 2.191 (2) | C13'—C14' | 1.4200 |
C12—C13 | 1.4200 | C13'—C18' | 1.5095 |
C12—C17 | 1.5095 | C14'—C15' | 1.4200 |
C12—Rh2 | 2.153 (2) | C14'—C19' | 1.5095 |
C13—C14 | 1.4200 | C15'—C20' | 1.5095 |
C13—C18 | 1.5095 | C16'—H16D | 0.9600 |
C13—Rh2 | 2.107 (3) | C16'—H16E | 0.9600 |
C14—C15 | 1.4200 | C16'—H16F | 0.9600 |
C14—C19 | 1.5095 | C17'—H17D | 0.9600 |
C14—Rh2 | 2.117 (3) | C17'—H17E | 0.9600 |
C15—C20 | 1.5095 | C17'—H17F | 0.9600 |
C15—Rh2 | 2.169 (2) | C18'—H18D | 0.9600 |
C16—H16A | 0.9600 | C18'—H18E | 0.9600 |
C16—H16B | 0.9600 | C18'—H18F | 0.9600 |
C16—H16C | 0.9600 | C19'—H19D | 0.9600 |
C17—H17A | 0.9600 | C19'—H19E | 0.9600 |
C17—H17B | 0.9600 | C19'—H19F | 0.9600 |
C17—H17C | 0.9600 | C20'—H20D | 0.9600 |
C18—H18A | 0.9600 | C20'—H20E | 0.9600 |
C18—H18B | 0.9600 | C20'—H20F | 0.9600 |
C18—H18C | 0.9600 | ||
C5—C1—C2 | 108.0 (3) | C5—Rh1—Cl1 | 116.97 (9) |
C5—C1—C6 | 125.0 (3) | C1—Rh1—Cl1 | 92.72 (9) |
C2—C1—C6 | 127.0 (3) | C4—Rh1—Cl1 | 156.12 (9) |
C5—C1—Rh1 | 70.26 (18) | C3—Rh1—Cl1 | 142.45 (9) |
C2—C1—Rh1 | 69.80 (17) | C2—Rh1—Cl2i | 107.99 (9) |
C6—C1—Rh1 | 125.6 (2) | C5—Rh1—Cl2i | 153.56 (9) |
C1—C2—C3 | 107.6 (3) | C1—Rh1—Cl2i | 146.51 (9) |
C1—C2—C7 | 126.9 (3) | C4—Rh1—Cl2i | 114.16 (9) |
C3—C2—C7 | 125.3 (3) | C3—Rh1—Cl2i | 93.15 (8) |
C1—C2—Rh1 | 70.80 (17) | Cl1—Rh1—Cl2i | 89.43 (3) |
C3—C2—Rh1 | 71.41 (16) | C2—Rh1—Cl2 | 160.94 (9) |
C7—C2—Rh1 | 126.4 (2) | C5—Rh1—Cl2 | 96.69 (8) |
C4—C3—C2 | 108.2 (3) | C1—Rh1—Cl2 | 129.52 (9) |
C4—C3—C8 | 125.2 (3) | C4—Rh1—Cl2 | 95.75 (8) |
C2—C3—C8 | 126.6 (3) | C3—Rh1—Cl2 | 127.33 (9) |
C4—C3—Rh1 | 70.62 (16) | Cl1—Rh1—Cl2 | 90.19 (3) |
C2—C3—Rh1 | 69.02 (16) | Cl2i—Rh1—Cl2 | 83.85 (3) |
C8—C3—Rh1 | 126.7 (2) | C13—Rh2—C14 | 39.3 |
C3—C4—C5 | 107.6 (3) | C13—Rh2—C12 | 38.9 |
C3—C4—C9 | 126.7 (3) | C14—Rh2—C12 | 65.09 (6) |
C5—C4—C9 | 125.7 (3) | C13—Rh2—C15 | 64.98 (6) |
C3—C4—Rh1 | 70.71 (17) | C14—Rh2—C15 | 38.7 |
C5—C4—Rh1 | 69.43 (17) | C12—Rh2—C15 | 64.23 (6) |
C9—C4—Rh1 | 126.5 (2) | C13—Rh2—C11 | 64.60 (6) |
C1—C5—C4 | 108.5 (3) | C14—Rh2—C11 | 64.44 (6) |
C1—C5—C10 | 126.6 (3) | C12—Rh2—C11 | 38.2 |
C4—C5—C10 | 124.9 (3) | C15—Rh2—C11 | 38.0 |
C1—C5—Rh1 | 70.69 (18) | C13—Rh2—Cl3 | 128.55 (9) |
C4—C5—Rh1 | 71.16 (18) | C14—Rh2—Cl3 | 96.59 (8) |
C10—C5—Rh1 | 125.7 (2) | C12—Rh2—Cl3 | 160.74 (7) |
C12—C11—C15 | 108.0 | C15—Rh2—Cl3 | 97.98 (7) |
C12—C11—C16 | 126.0 | C11—Rh2—Cl3 | 129.96 (8) |
C15—C11—C16 | 126.0 | C13—Rh2—Cl4ii | 140.53 (9) |
C12—C11—Rh2 | 69.50 (8) | C14—Rh2—Cl4ii | 151.98 (8) |
C15—C11—Rh2 | 70.17 (8) | C12—Rh2—Cl4ii | 102.76 (8) |
C16—C11—Rh2 | 125.91 (8) | C15—Rh2—Cl4ii | 113.59 (8) |
C13—C12—C11 | 108.0 | C11—Rh2—Cl4ii | 90.17 (7) |
C13—C12—C17 | 126.0 | Cl3—Rh2—Cl4ii | 90.89 (3) |
C11—C12—C17 | 126.0 | C13—Rh2—Cl4 | 96.01 (8) |
C13—C12—Rh2 | 68.80 (8) | C14—Rh2—Cl4 | 123.37 (9) |
C11—C12—Rh2 | 72.35 (8) | C12—Rh2—Cl4 | 103.93 (7) |
C17—C12—Rh2 | 124.44 (8) | C15—Rh2—Cl4 | 160.60 (7) |
C12—C13—C14 | 108.0 | C11—Rh2—Cl4 | 138.73 (8) |
C12—C13—C18 | 126.0 | Cl3—Rh2—Cl4 | 90.97 (3) |
C14—C13—C18 | 126.0 | Cl4ii—Rh2—Cl4 | 83.28 (3) |
C12—C13—Rh2 | 72.28 (8) | C12'—C11'—C15' | 108.0 |
C14—C13—Rh2 | 70.74 (9) | C12'—C11'—C16' | 126.0 |
C18—C13—Rh2 | 122.65 (8) | C15'—C11'—C16' | 126.0 |
C15—C14—C13 | 108.0 | C11'—C12'—C13' | 108.0 |
C15—C14—C19 | 126.0 | C11'—C12'—C17' | 126.0 |
C13—C14—C19 | 126.0 | C13'—C12'—C17' | 126.0 |
C15—C14—Rh2 | 72.63 (8) | C12'—C13'—C14' | 108.0 |
C13—C14—Rh2 | 69.98 (8) | C12'—C13'—C18' | 126.0 |
C19—C14—Rh2 | 123.04 (8) | C14'—C13'—C18' | 126.0 |
C14—C15—C11 | 108.0 | C15'—C14'—C13' | 108.0 |
C14—C15—C20 | 126.0 | C15'—C14'—C19' | 126.0 |
C11—C15—C20 | 126.0 | C13'—C14'—C19' | 126.0 |
C14—C15—Rh2 | 68.70 (8) | C14'—C15'—C11' | 108.0 |
C11—C15—Rh2 | 71.82 (8) | C14'—C15'—C20' | 126.0 |
C20—C15—Rh2 | 125.06 (8) | C11'—C15'—C20' | 126.0 |
Cl6—C21—Cl7 | 111.2 (2) | C11'—C16'—H16D | 109.5 |
Cl6—C21—Cl5 | 110.1 (2) | C11'—C16'—H16E | 109.5 |
Cl7—C21—Cl5 | 109.2 (2) | H16D—C16'—H16E | 109.5 |
Cl6—C21—H21 | 108.8 | C11'—C16'—H16F | 109.5 |
Cl7—C21—H21 | 108.8 | H16D—C16'—H16F | 109.5 |
Cl5—C21—H21 | 108.8 | H16E—C16'—H16F | 109.5 |
Cl8—C22—Cl10 | 111.5 (2) | C12'—C17'—H17D | 109.5 |
Cl8—C22—Cl9 | 110.2 (2) | C12'—C17'—H17E | 109.5 |
Cl10—C22—Cl9 | 108.8 (2) | H17D—C17'—H17E | 109.5 |
Cl8—C22—H22 | 108.8 | C12'—C17'—H17F | 109.5 |
Cl10—C22—H22 | 108.8 | H17D—C17'—H17F | 109.5 |
Cl9—C22—H22 | 108.8 | H17E—C17'—H17F | 109.5 |
Cl12—C23—Cl11 | 110.9 (2) | C13'—C18'—H18D | 109.5 |
Cl12—C23—Cl13 | 109.63 (19) | C13'—C18'—H18E | 109.5 |
Cl11—C23—Cl13 | 110.5 (2) | H18D—C18'—H18E | 109.5 |
Cl12—C23—H23 | 108.6 | C13'—C18'—H18F | 109.5 |
Cl11—C23—H23 | 108.6 | H18D—C18'—H18F | 109.5 |
Cl13—C23—H23 | 108.6 | H18E—C18'—H18F | 109.5 |
Rh1i—Cl2—Rh1 | 96.15 (3) | C14'—C19'—H19D | 109.5 |
Rh2ii—Cl4—Rh2 | 96.72 (3) | C14'—C19'—H19E | 109.5 |
C2—Rh1—C5 | 65.97 (12) | H19D—C19'—H19E | 109.5 |
C2—Rh1—C1 | 39.40 (12) | C14'—C19'—H19F | 109.5 |
C5—Rh1—C1 | 39.04 (12) | H19D—C19'—H19F | 109.5 |
C2—Rh1—C4 | 65.97 (12) | H19E—C19'—H19F | 109.5 |
C5—Rh1—C4 | 39.41 (12) | C15'—C20'—H20D | 109.5 |
C1—Rh1—C4 | 65.77 (12) | C15'—C20'—H20E | 109.5 |
C2—Rh1—C3 | 39.57 (12) | H20D—C20'—H20E | 109.5 |
C5—Rh1—C3 | 65.46 (11) | C15'—C20'—H20F | 109.5 |
C1—Rh1—C3 | 65.71 (11) | H20D—C20'—H20F | 109.5 |
C4—Rh1—C3 | 38.66 (12) | H20E—C20'—H20F | 109.5 |
C2—Rh1—Cl1 | 104.49 (9) | ||
C5—C1—C2—C3 | 2.2 (3) | C9—C4—Rh1—Cl2i | 59.5 (3) |
C6—C1—C2—C3 | −177.7 (3) | C3—C4—Rh1—Cl2 | −148.18 (17) |
Rh1—C1—C2—C3 | 62.3 (2) | C5—C4—Rh1—Cl2 | 93.54 (17) |
C5—C1—C2—C7 | 178.2 (3) | C9—C4—Rh1—Cl2 | −26.3 (3) |
C6—C1—C2—C7 | −1.6 (5) | C4—C3—Rh1—C2 | −119.3 (3) |
Rh1—C1—C2—C7 | −121.6 (3) | C8—C3—Rh1—C2 | 120.7 (4) |
C5—C1—C2—Rh1 | −60.1 (2) | C4—C3—Rh1—C5 | −37.92 (19) |
C6—C1—C2—Rh1 | 120.0 (3) | C2—C3—Rh1—C5 | 81.36 (19) |
C1—C2—C3—C4 | −1.9 (3) | C8—C3—Rh1—C5 | −157.9 (3) |
C7—C2—C3—C4 | −178.0 (3) | C4—C3—Rh1—C1 | −81.0 (2) |
Rh1—C2—C3—C4 | 60.0 (2) | C2—C3—Rh1—C1 | 38.30 (18) |
C1—C2—C3—C8 | 177.3 (3) | C8—C3—Rh1—C1 | 159.1 (3) |
C7—C2—C3—C8 | 1.1 (5) | C2—C3—Rh1—C4 | 119.3 (3) |
Rh1—C2—C3—C8 | −120.8 (3) | C8—C3—Rh1—C4 | −120.0 (4) |
C1—C2—C3—Rh1 | −61.9 (2) | C4—C3—Rh1—Cl1 | −140.87 (16) |
C7—C2—C3—Rh1 | 121.9 (3) | C2—C3—Rh1—Cl1 | −21.6 (2) |
C2—C3—C4—C5 | 0.9 (3) | C8—C3—Rh1—Cl1 | 99.2 (3) |
C8—C3—C4—C5 | −178.3 (3) | C4—C3—Rh1—Cl2i | 125.95 (17) |
Rh1—C3—C4—C5 | 59.9 (2) | C2—C3—Rh1—Cl2i | −114.76 (17) |
C2—C3—C4—C9 | 179.3 (3) | C8—C3—Rh1—Cl2i | 6.0 (3) |
C8—C3—C4—C9 | 0.1 (5) | C4—C3—Rh1—Cl2 | 41.3 (2) |
Rh1—C3—C4—C9 | −121.7 (3) | C2—C3—Rh1—Cl2 | 160.57 (15) |
C2—C3—C4—Rh1 | −59.0 (2) | C8—C3—Rh1—Cl2 | −78.7 (3) |
C8—C3—C4—Rh1 | 121.8 (3) | Rh1i—Cl2—Rh1—C2 | 129.7 (3) |
C2—C1—C5—C4 | −1.6 (3) | Rh1i—Cl2—Rh1—C5 | 153.40 (9) |
C6—C1—C5—C4 | 178.2 (3) | Rh1i—Cl2—Rh1—C1 | 176.90 (11) |
Rh1—C1—C5—C4 | −61.5 (2) | Rh1i—Cl2—Rh1—C4 | 113.75 (9) |
C2—C1—C5—C10 | −179.5 (3) | Rh1i—Cl2—Rh1—C3 | 89.28 (11) |
C6—C1—C5—C10 | 0.3 (5) | Rh1i—Cl2—Rh1—Cl1 | −89.41 (3) |
Rh1—C1—C5—C10 | 120.6 (3) | Rh1i—Cl2—Rh1—Cl2i | 0.0 |
C2—C1—C5—Rh1 | 59.8 (2) | C12—C13—Rh2—C14 | −117.1 |
C6—C1—C5—Rh1 | −120.3 (3) | C18—C13—Rh2—C14 | 121.0 |
C3—C4—C5—C1 | 0.5 (3) | C14—C13—Rh2—C12 | 117.1 |
C9—C4—C5—C1 | −178.0 (3) | C18—C13—Rh2—C12 | −121.9 |
Rh1—C4—C5—C1 | 61.2 (2) | C12—C13—Rh2—C15 | −79.3 |
C3—C4—C5—C10 | 178.4 (3) | C14—C13—Rh2—C15 | 37.8 |
C9—C4—C5—C10 | −0.1 (5) | C18—C13—Rh2—C15 | 158.8 |
Rh1—C4—C5—C10 | −120.9 (3) | C12—C13—Rh2—C11 | −37.1 |
C3—C4—C5—Rh1 | −60.7 (2) | C14—C13—Rh2—C11 | 79.99 (5) |
C9—C4—C5—Rh1 | 120.8 (3) | C18—C13—Rh2—C11 | −159.0 |
C15—C11—C12—C13 | 0.0 | C12—C13—Rh2—Cl3 | −159.16 (10) |
C16—C11—C12—C13 | 180.0 | C14—C13—Rh2—Cl3 | −42.07 (9) |
Rh2—C11—C12—C13 | −59.84 (9) | C18—C13—Rh2—Cl3 | 78.96 (10) |
C15—C11—C12—C17 | 180.0 | C12—C13—Rh2—Cl4ii | 18.05 (12) |
C16—C11—C12—C17 | 0.0 | C14—C13—Rh2—Cl4ii | 135.14 (14) |
Rh2—C11—C12—C17 | 120.16 (9) | C18—C13—Rh2—Cl4ii | −103.83 (12) |
C15—C11—C12—Rh2 | 59.84 (9) | C12—C13—Rh2—Cl4 | 104.77 (8) |
C16—C11—C12—Rh2 | −120.16 (9) | C14—C13—Rh2—Cl4 | −138.14 (8) |
C11—C12—C13—C14 | 0.0 | C18—C13—Rh2—Cl4 | −17.11 (8) |
C17—C12—C13—C14 | 180.0 | C15—C14—Rh2—C13 | 117.3 |
Rh2—C12—C13—C14 | −62.10 (8) | C19—C14—Rh2—C13 | −120.6 |
C11—C12—C13—C18 | 180.0 | C15—C14—Rh2—C12 | 79.22 (5) |
C17—C12—C13—C18 | 0.0 | C13—C14—Rh2—C12 | −38.1 |
Rh2—C12—C13—C18 | 117.90 (8) | C19—C14—Rh2—C12 | −158.7 |
C11—C12—C13—Rh2 | 62.10 (8) | C13—C14—Rh2—C15 | −117.3 |
C17—C12—C13—Rh2 | −117.90 (8) | C19—C14—Rh2—C15 | 122.1 |
C12—C13—C14—C15 | 0.0 | C15—C14—Rh2—C11 | 36.9 |
C18—C13—C14—C15 | 180.0 | C13—C14—Rh2—C11 | −80.43 (5) |
Rh2—C13—C14—C15 | −63.09 (8) | C19—C14—Rh2—C11 | 159.0 |
C12—C13—C14—C19 | 180.0 | C15—C14—Rh2—Cl3 | −94.54 (8) |
C18—C13—C14—C19 | 0.0 | C13—C14—Rh2—Cl3 | 148.16 (9) |
Rh2—C13—C14—C19 | 116.91 (8) | C19—C14—Rh2—Cl3 | 27.54 (8) |
C12—C13—C14—Rh2 | 63.09 (8) | C15—C14—Rh2—Cl4ii | 9.97 (19) |
C18—C13—C14—Rh2 | −116.91 (8) | C13—C14—Rh2—Cl4ii | −107.3 (2) |
C13—C14—C15—C11 | 0.0 | C19—C14—Rh2—Cl4ii | 132.06 (18) |
C19—C14—C15—C11 | 180.0 | C15—C14—Rh2—Cl4 | 169.91 (9) |
Rh2—C14—C15—C11 | −61.39 (8) | C13—C14—Rh2—Cl4 | 52.62 (8) |
C13—C14—C15—C20 | 180.0 | C19—C14—Rh2—Cl4 | −68.00 (9) |
C19—C14—C15—C20 | 0.0 | C11—C12—Rh2—C13 | −118.1 |
Rh2—C14—C15—C20 | 118.61 (8) | C17—C12—Rh2—C13 | 119.90 (5) |
C13—C14—C15—Rh2 | 61.39 (8) | C13—C12—Rh2—C14 | 38.4 |
C19—C14—C15—Rh2 | −118.61 (8) | C11—C12—Rh2—C14 | −79.69 (5) |
C12—C11—C15—C14 | 0.0 | C17—C12—Rh2—C14 | 158.3 |
C16—C11—C15—C14 | 180.0 | C13—C12—Rh2—C15 | 81.40 (6) |
Rh2—C11—C15—C14 | 59.42 (8) | C11—C12—Rh2—C15 | −36.7 |
C12—C11—C15—C20 | 180.0 | C17—C12—Rh2—C15 | −158.7 |
C16—C11—C15—C20 | 0.0 | C13—C12—Rh2—C11 | 118.1 |
Rh2—C11—C15—C20 | −120.58 (8) | C17—C12—Rh2—C11 | −122.0 |
C12—C11—C15—Rh2 | −59.42 (8) | C13—C12—Rh2—Cl3 | 57.5 (3) |
C16—C11—C15—Rh2 | 120.58 (8) | C11—C12—Rh2—Cl3 | −60.6 (3) |
C1—C2—Rh1—C5 | 37.16 (18) | C17—C12—Rh2—Cl3 | 177.4 (3) |
C3—C2—Rh1—C5 | −79.96 (19) | C13—C12—Rh2—Cl4ii | −168.35 (9) |
C7—C2—Rh1—C5 | 159.4 (3) | C11—C12—Rh2—Cl4ii | 73.54 (7) |
C3—C2—Rh1—C1 | −117.1 (3) | C17—C12—Rh2—Cl4ii | −48.45 (9) |
C7—C2—Rh1—C1 | 122.3 (4) | C13—C12—Rh2—Cl4 | −82.21 (8) |
C1—C2—Rh1—C4 | 80.5 (2) | C11—C12—Rh2—Cl4 | 159.68 (7) |
C3—C2—Rh1—C4 | −36.63 (18) | C17—C12—Rh2—Cl4 | 37.69 (9) |
C7—C2—Rh1—C4 | −157.2 (3) | C14—C15—Rh2—C13 | −38.4 |
C1—C2—Rh1—C3 | 117.1 (3) | C11—C15—Rh2—C13 | 80.12 (5) |
C7—C2—Rh1—C3 | −120.6 (4) | C20—C15—Rh2—C13 | −158.2 |
C1—C2—Rh1—Cl1 | −76.27 (18) | C11—C15—Rh2—C14 | 118.5 |
C3—C2—Rh1—Cl1 | 166.61 (16) | C20—C15—Rh2—C14 | −119.81 (5) |
C7—C2—Rh1—Cl1 | 46.0 (3) | C14—C15—Rh2—C12 | −81.65 (6) |
C1—C2—Rh1—Cl2i | −170.47 (16) | C11—C15—Rh2—C12 | 36.8 |
C3—C2—Rh1—Cl2i | 72.42 (18) | C20—C15—Rh2—C12 | 158.5 |
C7—C2—Rh1—Cl2i | −48.2 (3) | C14—C15—Rh2—C11 | −118.5 |
C1—C2—Rh1—Cl2 | 63.1 (3) | C20—C15—Rh2—C11 | 121.7 |
C3—C2—Rh1—Cl2 | −54.1 (4) | C14—C15—Rh2—Cl3 | 90.60 (8) |
C7—C2—Rh1—Cl2 | −174.7 (2) | C11—C15—Rh2—Cl3 | −150.90 (8) |
C1—C5—Rh1—C2 | −37.49 (17) | C20—C15—Rh2—Cl3 | −29.22 (9) |
C4—C5—Rh1—C2 | 80.81 (19) | C14—C15—Rh2—Cl4ii | −174.91 (9) |
C10—C5—Rh1—C2 | −159.2 (3) | C11—C15—Rh2—Cl4ii | −56.41 (8) |
C4—C5—Rh1—C1 | 118.3 (2) | C20—C15—Rh2—Cl4ii | 65.28 (9) |
C10—C5—Rh1—C1 | −121.7 (4) | C14—C15—Rh2—Cl4 | −26.1 (2) |
C1—C5—Rh1—C4 | −118.3 (2) | C11—C15—Rh2—Cl4 | 92.4 (2) |
C10—C5—Rh1—C4 | 120.0 (4) | C20—C15—Rh2—Cl4 | −145.9 (2) |
C1—C5—Rh1—C3 | −81.09 (19) | C12—C11—Rh2—C13 | 37.8 |
C4—C5—Rh1—C3 | 37.22 (17) | C15—C11—Rh2—C13 | −81.21 (6) |
C10—C5—Rh1—C3 | 157.2 (3) | C16—C11—Rh2—C13 | 158.1 |
C1—C5—Rh1—Cl1 | 57.12 (18) | C12—C11—Rh2—C14 | 81.56 (6) |
C4—C5—Rh1—Cl1 | 175.43 (14) | C15—C11—Rh2—C14 | −37.5 |
C10—C5—Rh1—Cl1 | −64.6 (3) | C16—C11—Rh2—C14 | −158.2 |
C1—C5—Rh1—Cl2i | −119.6 (2) | C15—C11—Rh2—C12 | −119.1 |
C4—C5—Rh1—Cl2i | −1.3 (3) | C16—C11—Rh2—C12 | 120.26 (5) |
C10—C5—Rh1—Cl2i | 118.7 (3) | C12—C11—Rh2—C15 | 119.1 |
C1—C5—Rh1—Cl2 | 150.76 (16) | C16—C11—Rh2—C15 | −120.68 (5) |
C4—C5—Rh1—Cl2 | −90.93 (16) | C12—C11—Rh2—Cl3 | 157.98 (11) |
C10—C5—Rh1—Cl2 | 29.0 (3) | C15—C11—Rh2—Cl3 | 38.92 (9) |
C5—C1—Rh1—C2 | 118.9 (3) | C16—C11—Rh2—Cl3 | −81.76 (11) |
C6—C1—Rh1—C2 | −121.7 (4) | C12—C11—Rh2—Cl4ii | −110.72 (8) |
C2—C1—Rh1—C5 | −118.9 (3) | C15—C11—Rh2—Cl4ii | 130.23 (8) |
C6—C1—Rh1—C5 | 119.5 (4) | C16—C11—Rh2—Cl4ii | 9.55 (9) |
C5—C1—Rh1—C4 | 37.80 (17) | C12—C11—Rh2—Cl4 | −30.74 (10) |
C2—C1—Rh1—C4 | −81.05 (19) | C15—C11—Rh2—Cl4 | −149.79 (12) |
C6—C1—Rh1—C4 | 157.3 (3) | C16—C11—Rh2—Cl4 | 89.53 (12) |
C5—C1—Rh1—C3 | 80.39 (19) | Rh2ii—Cl4—Rh2—C13 | −140.28 (9) |
C2—C1—Rh1—C3 | −38.47 (18) | Rh2ii—Cl4—Rh2—C14 | −170.66 (9) |
C6—C1—Rh1—C3 | −160.1 (3) | Rh2ii—Cl4—Rh2—C12 | −101.53 (8) |
C5—C1—Rh1—Cl1 | −131.47 (16) | Rh2ii—Cl4—Rh2—C15 | −151.4 (2) |
C2—C1—Rh1—Cl1 | 109.68 (17) | Rh2ii—Cl4—Rh2—C11 | −82.55 (10) |
C6—C1—Rh1—Cl1 | −12.0 (3) | Rh2ii—Cl4—Rh2—Cl3 | 90.79 (3) |
C5—C1—Rh1—Cl2i | 135.45 (16) | Rh2ii—Cl4—Rh2—Cl4ii | 0.0 |
C2—C1—Rh1—Cl2i | 16.6 (3) | C15'—C11'—C12'—C13' | 0.0 |
C6—C1—Rh1—Cl2i | −105.1 (3) | C16'—C11'—C12'—C13' | 180.0 |
C5—C1—Rh1—Cl2 | −39.0 (2) | C15'—C11'—C12'—C17' | 180.0 |
C2—C1—Rh1—Cl2 | −157.82 (15) | C16'—C11'—C12'—C17' | 0.0 |
C6—C1—Rh1—Cl2 | 80.5 (3) | C11'—C12'—C13'—C14' | 0.0 |
C3—C4—Rh1—C2 | 37.47 (18) | C17'—C12'—C13'—C14' | 180.0 |
C5—C4—Rh1—C2 | −80.81 (19) | C11'—C12'—C13'—C18' | 180.0 |
C9—C4—Rh1—C2 | 159.3 (3) | C17'—C12'—C13'—C18' | 0.0 |
C3—C4—Rh1—C5 | 118.3 (3) | C12'—C13'—C14'—C15' | 0.0 |
C9—C4—Rh1—C5 | −119.8 (4) | C18'—C13'—C14'—C15' | 180.0 |
C3—C4—Rh1—C1 | 80.82 (19) | C12'—C13'—C14'—C19' | 180.0 |
C5—C4—Rh1—C1 | −37.46 (18) | C18'—C13'—C14'—C19' | 0.0 |
C9—C4—Rh1—C1 | −157.3 (3) | C13'—C14'—C15'—C11' | 0.0 |
C5—C4—Rh1—C3 | −118.3 (3) | C19'—C14'—C15'—C11' | 180.0 |
C9—C4—Rh1—C3 | 121.9 (4) | C13'—C14'—C15'—C20' | 180.0 |
C3—C4—Rh1—Cl1 | 108.2 (2) | C19'—C14'—C15'—C20' | 0.0 |
C5—C4—Rh1—Cl1 | −10.1 (3) | C12'—C11'—C15'—C14' | 0.0 |
C9—C4—Rh1—Cl1 | −130.0 (3) | C16'—C11'—C15'—C14' | 180.0 |
C3—C4—Rh1—Cl2i | −62.35 (19) | C12'—C11'—C15'—C20' | 180.0 |
C5—C4—Rh1—Cl2i | 179.36 (15) | C16'—C11'—C15'—C20' | 0.0 |
Symmetry codes: (i) −x, −y+1, −z+2; (ii) −x+1, −y+1, −z+1. |