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Two new members of the mero-plesiotype rhodesite series [Sr2Na2(Si8O19)·4H2O, abbreviated as TR09; SrNa4(Si8O19)·4H2O, TR10] have been hydrothermally synthesized in Teflon-lined autoclaves at 503 K and structurally characterized using X-ray diffraction single-crystal data. The crystal structures were solved by direct methods and refined to R = 0.021 [TR09; 3317 reflections with Io > 2σ(Io)] and R = 0.033 [TR10; 5007 reflections with Io > 2σ(Io)]. Both structures are based on a rhodesite-type microporous heteropolyhedral framework, where two types of channels are within the double silicate layer that alternates with an `octahedral' O sheet. The large Sr2+ cation constrains to the roughly ellipsoidal shape of the channels. The H2O molecules are located both in the O sheets and in the channels, where they are loosely hydrogen bonded. The crystal-chemical features that allow flexibility to the rhodesite-type microporous heteropolyhedral framework and make it interesting for possible technological applications are discussed.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S0108768109050009/wh5008sup1.cif
Contains datablocks TR09, TR010

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S0108768109050009/wh5008TR09sup2.hkl
Contains datablock TR09

fcf

Structure factor file (CIF format) https://doi.org/10.1107/S0108768109050009/wh5008TR010sup3.fcf
Contains datablock TR010

Computing details top

For both structures, data collection: CrysAlis CCD, Oxford Diffraction Ltd., Version 1.171.32.13 (release 29-11-2007 CrysAlis171 .NET) (compiled Nov 29 2007,17:23:28); cell refinement: CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.32.13 (release 29-11-2007 CrysAlis171 .NET) (compiled Nov 29 2007,17:23:28). Data reduction: CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.32.13 (release 29-11-2007 CrysAlis171 .NET) (compiled Nov 29 2007,17:23:28) for TR09; CrysAlis PRO 171.32.13 for TR010. Program(s) used to solve structure: SHELXS86 (Sheldrick, 1986) for TR09; SHELXL97 (Sheldrick, 1997) for TR010. For both structures, program(s) used to refine structure: SHELXL97 (Sheldrick, 1997). Molecular graphics: ORTEP-3 for Windows (Farrugia, 1997) for TR09; ATOMS 6.2 for TR010. Software used to prepare material for publication: WinGX publication routines (Farrugia, 1999) for TR09.

BisSodium BisStrontium Octasilicate TetraHydrate (TR09) top
Crystal data top
Na2O19Si8Sr24(H2O)F(000) = 1608
Mr = 822.00Dx = 2.549 Mg m3
Dm = 2.8 Mg m3
Dm measured by not measured
Monoclinic, C2/cMo Kα radiation, λ = 0.71073 Å
a = 22.7681 (2) ÅCell parameters from 18102 reflections
b = 6.9352 (1) Åθ = 3.0–32.6°
c = 13.5789 (1) ŵ = 5.58 mm1
β = 92.578 (1)°T = 293 K
V = 2141.96 (4) Å3Prism, colourless
Z = 40.1 × 0.1 × 0.06 mm
Data collection top
Oxford 'X Calibur Gemini Ultra
diffractometer
3801 independent reflections
Radiation source: fine-focus sealed tube3317 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.030
Detector resolution: 10.2890 pixels mm-1θmax = 32.7°, θmin = 3.0°
phi/ω scansh = 3434
Absorption correction: multi scan
CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.32.13 (release 29-11-2007 CrysAlis171 .NET) (compiled Nov 29 2007,17:23:28) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.
k = 1010
Tmin = 0.678, Tmax = 1.000l = 2020
33115 measured reflections
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.021H-atom parameters not defined
wR(F2) = 0.080 w = 1/[σ2(Fo2) + (0.1P)2]
where P = (Fo2 + 2Fc2)/3
S = 0.64(Δ/σ)max = 0.001
3801 reflectionsΔρmax = 0.67 e Å3
176 parametersΔρmin = 0.77 e Å3
0 restraints
Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Sr10.230255 (7)0.05478 (2)0.285074 (12)0.01166 (6)
Na1A0.2560 (5)0.205 (4)0.0103 (9)0.021 (2)0.41 (5)
Na1B0.25000.25000.00000.011 (4)*0.19 (10)
Na20.00000.4774 (2)0.25000.0256 (3)
Si10.38207 (2)0.22489 (7)0.34130 (3)0.00815 (10)
Si20.06306 (2)0.02662 (7)0.27778 (3)0.00617 (9)
Si30.12176 (2)0.00371 (7)0.48267 (3)0.00905 (10)
Si40.13289 (2)0.29376 (6)0.14488 (3)0.00692 (9)
O10.31879 (6)0.2654 (2)0.29484 (11)0.0174 (3)
O20.39274 (7)0.3042 (2)0.45335 (10)0.0177 (3)
O30.40168 (6)0.00207 (18)0.34627 (10)0.0124 (2)
O40.43473 (6)0.31930 (18)0.27663 (10)0.0129 (2)
O50.07045 (7)0.0026 (2)0.39463 (10)0.0154 (3)
O60.11451 (5)0.16453 (18)0.24108 (9)0.0110 (2)
O70.00000.1274 (3)0.25000.0104 (3)
O80.18615 (7)0.0043 (3)0.44556 (12)0.0236 (3)
O90.10550 (6)0.18733 (19)0.54689 (9)0.0151 (3)
O100.20195 (5)0.30527 (18)0.14957 (9)0.0107 (2)
OW10.05391 (13)0.4956 (3)0.40418 (17)0.0515 (7)
OW2A0.2010 (11)0.5637 (14)0.1123 (5)0.064 (4)0.73 (4)
OW2B0.2246 (6)0.5864 (16)0.0979 (13)0.024 (4)0.27 (4)
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Sr10.00849 (9)0.00975 (9)0.01653 (9)0.00028 (5)0.00171 (6)0.00336 (5)
Na1A0.0184 (15)0.028 (6)0.0157 (17)0.004 (3)0.0048 (11)0.005 (3)
Na20.0223 (7)0.0260 (6)0.0286 (7)0.0000.0005 (5)0.000
Si10.0083 (2)0.0057 (2)0.0104 (2)0.00050 (15)0.00076 (15)0.00063 (15)
Si20.0058 (2)0.00650 (19)0.00611 (19)0.00014 (14)0.00032 (15)0.00036 (14)
Si30.0106 (2)0.0097 (2)0.0069 (2)0.00078 (17)0.00033 (16)0.00024 (16)
Si40.0072 (2)0.0053 (2)0.00820 (18)0.00049 (15)0.00045 (15)0.00006 (14)
O10.0114 (6)0.0123 (6)0.0280 (7)0.0008 (5)0.0052 (5)0.0052 (5)
O20.0268 (8)0.0137 (6)0.0127 (6)0.0025 (5)0.0006 (5)0.0039 (5)
O30.0126 (6)0.0052 (5)0.0193 (6)0.0007 (4)0.0002 (5)0.0007 (4)
O40.0118 (6)0.0096 (5)0.0178 (6)0.0002 (5)0.0038 (5)0.0049 (5)
O50.0162 (6)0.0222 (6)0.0076 (5)0.0007 (5)0.0020 (5)0.0024 (5)
O60.0096 (5)0.0105 (5)0.0128 (5)0.0012 (4)0.0006 (4)0.0037 (4)
O70.0078 (7)0.0088 (8)0.0142 (8)0.0000.0027 (6)0.000
O80.0134 (7)0.0365 (9)0.0213 (7)0.0019 (6)0.0072 (6)0.0003 (6)
O90.0180 (7)0.0133 (6)0.0134 (5)0.0009 (5)0.0048 (5)0.0053 (5)
O100.0080 (5)0.0120 (6)0.0121 (5)0.0016 (4)0.0016 (4)0.0005 (4)
OW10.083 (2)0.0373 (10)0.0319 (11)0.0048 (12)0.0187 (12)0.0012 (9)
OW2A0.085 (11)0.065 (3)0.044 (2)0.028 (4)0.005 (4)0.009 (2)
OW2B0.005 (6)0.031 (5)0.036 (5)0.005 (3)0.001 (3)0.012 (3)
Geometric parameters (Å, º) top
Sr1—O10i2.4580 (12)O2—O9xii2.6577 (19)
Sr1—O82.4651 (16)O2—O8xii2.664 (2)
Sr1—O12.4882 (14)O2—OW1xiii3.096 (3)
Sr1—O1i2.5184 (13)O3—Si4i1.6271 (13)
Sr1—O102.5907 (13)O3—O42.5479 (18)
Sr1—O62.7820 (13)O3—O9xiii2.6063 (18)
Sr1—OW2Bii2.952 (14)O3—O6i2.6172 (18)
Sr1—OW2Biii2.959 (10)O3—Na2xi2.6482 (14)
Sr1—OW2Aii2.993 (10)O3—O10i2.7143 (18)
Sr1—OW2Aiii3.077 (12)O3—OW1xiii3.492 (3)
Sr1—Si43.3024 (5)O4—Si2vi1.6184 (13)
Sr1—Na1Aiv3.576 (3)O4—Na2xi2.5729 (17)
Na1A—Na1Aii0.73 (7)O4—O7xi2.6371 (19)
Na1A—O8v2.299 (6)O4—O5vi2.6481 (19)
Na1A—OW2Bii2.38 (3)O4—O6vi2.6501 (18)
Na1A—O102.404 (6)O4—O4xiv3.090 (3)
Na1A—O10ii2.413 (6)O4—OW1vi3.305 (3)
Na1A—OW2Aii2.50 (3)O4—Sr1vi4.1469 (13)
Na1A—O8vi2.516 (15)O5—O92.5490 (18)
Na1A—OW2B3.09 (3)O5—O2xii2.5700 (19)
Na1A—OW2A3.21 (3)O5—O62.6083 (18)
Na1A—Si4ii3.365 (3)O5—O72.6262 (15)
Na1A—O9vi3.366 (4)O5—O4i2.6481 (19)
Na1A—Si3v3.387 (3)O5—O82.693 (2)
Na1B—Na1Aii0.36 (3)O5—OW13.479 (3)
Na1B—O10ii2.3809 (12)O6—O102.5851 (17)
Na1B—O102.3809 (12)O6—O3vi2.6172 (18)
Na1B—O8v2.3821 (18)O6—O72.6280 (12)
Na1B—O8vi2.3821 (18)O6—O9v2.6404 (17)
Na1B—OW2Bii2.734 (11)O6—O4i2.6501 (18)
Na1B—OW2B2.734 (11)O6—O1i3.2050 (19)
Na1B—OW2A2.855 (8)O6—OW2Aiii3.323 (13)
Na1B—OW2Aii2.855 (8)O6—O83.346 (2)
Na1B—Si4ii3.3977 (5)O7—Si2vii1.6261 (9)
Na1B—Si43.3977 (5)O7—O5vii2.6262 (15)
Na1B—O9vi3.4070 (14)O7—O6vii2.6280 (12)
Na2—OW12.382 (2)O7—O4viii2.6371 (19)
Na2—OW1vii2.382 (2)O7—O4i2.6371 (19)
Na2—O4i2.5729 (17)O7—Na2xv2.741 (2)
Na2—O4viii2.5729 (17)O8—Na1Aiv2.299 (6)
Na2—O3viii2.6482 (14)O8—Na1Bi2.3821 (18)
Na2—O3i2.6482 (14)O8—Na1Ai2.516 (15)
Na2—O7ix2.741 (2)O8—O2xii2.664 (2)
Na2—Si1i3.3186 (7)O8—O92.694 (2)
Na2—Si1viii3.3186 (7)O8—OW2Bi2.891 (19)
Na2—O6x3.6067 (16)O8—OW2Biii3.036 (11)
Na2—O6ix3.6067 (16)O8—OW2Aiii3.120 (8)
Si1—O11.5720 (14)O8—O10i3.219 (2)
Si1—O21.6256 (14)O9—Si4iv1.6216 (13)
Si1—O31.6367 (13)O9—O3xiii2.6063 (18)
Si1—O41.6530 (13)O9—O6iv2.6404 (17)
Si1—Na2xi3.3186 (7)O9—O2xii2.6577 (19)
Si1—Sr1vi3.7848 (5)O9—O10iv2.6758 (18)
Si2—O51.5968 (14)O9—OW13.082 (3)
Si2—O61.6085 (13)O9—Na1Ai3.366 (4)
Si2—O4i1.6183 (13)O9—Na1Bi3.4070 (14)
Si2—O71.6261 (9)O9—Na1Aiv3.486 (9)
Si3—O81.5715 (16)O10—Na1Aii2.413 (6)
Si3—O2xii1.6326 (14)O10—Sr1vi2.4580 (12)
Si3—O51.6335 (15)O10—O9v2.6758 (18)
Si3—O91.6377 (14)O10—O3vi2.7143 (18)
Si3—Na1Aiv3.387 (3)O10—O8vi3.219 (2)
Si3—Na1Bi3.4080 (5)O10—OW2Bii3.283 (10)
Si3—Na1Ai3.467 (8)OW1—O2xiii3.096 (3)
Si4—O101.5728 (13)OW1—O4i3.305 (3)
Si4—O9v1.6216 (13)OW1—OW2Aiv3.40 (3)
Si4—O3vi1.6271 (13)OW1—O3xiii3.492 (3)
Si4—O61.6534 (12)OW2A—OW2B0.585 (12)
Si4—Na1Aii3.365 (3)OW2A—Na1Aii2.50 (3)
Si4—Sr1vi3.6912 (5)OW2A—Sr1ii2.993 (10)
O1—Sr1vi2.5184 (13)OW2A—Sr1xvi3.077 (12)
O1—O22.686 (2)OW2A—O8xvi3.120 (8)
O1—O42.6884 (19)OW2A—O1xvi3.24 (2)
O1—O32.7152 (19)OW2A—O6xvi3.323 (13)
O1—OW2Biii2.839 (9)OW2A—O10xvi3.360 (5)
O1—O6vi3.2050 (19)OW2A—O8vi3.37 (2)
O1—OW2Aiii3.24 (2)OW2A—O1ii3.384 (13)
O1—O103.2515 (19)OW2B—Na1Aii2.38 (3)
O1—O10i3.3181 (18)OW2B—O1xvi2.839 (9)
O1—OW2Aii3.384 (13)OW2B—O8vi2.891 (19)
O2—Si3xii1.6326 (14)OW2B—Sr1ii2.952 (14)
O2—O5xii2.5700 (19)OW2B—Sr1xvi2.959 (10)
O2—O32.5869 (19)OW2B—O8xvi3.036 (11)
O2—O42.6249 (19)OW2B—O10ii3.283 (10)
O10i—Sr1—O881.67 (5)O2—O4—O5vi144.92 (7)
O10i—Sr1—O184.26 (4)O7xi—O4—O5vi59.59 (4)
O8—Sr1—O1113.42 (5)Si2vi—O4—O6vi34.67 (4)
O10i—Sr1—O1i81.59 (4)Si1—O4—O6vi95.28 (6)
O8—Sr1—O1i94.44 (6)O3—O4—O6vi133.88 (7)
O1—Sr1—O1i146.43 (3)Na2xi—O4—O6vi162.61 (6)
O10i—Sr1—O10149.385 (13)O2—O4—O6vi87.08 (6)
O8—Sr1—O10128.67 (5)O7xi—O4—O6vi59.61 (5)
O1—Sr1—O1079.59 (4)O5vi—O4—O6vi58.98 (5)
O1i—Sr1—O1097.87 (4)Si2vi—O4—O1102.48 (7)
O10i—Sr1—O6147.52 (4)Si1—O4—O132.59 (4)
O8—Sr1—O678.99 (5)O3—O4—O162.40 (5)
O1—Sr1—O6127.46 (4)Na2xi—O4—O1118.52 (6)
O1i—Sr1—O674.22 (4)O2—O4—O160.72 (5)
O10—Sr1—O657.39 (4)O7xi—O4—O1133.39 (6)
O10i—Sr1—OW2Bii80.8 (3)O5vi—O4—O198.18 (6)
O8—Sr1—OW2Bii152.3 (2)O6vi—O4—O173.79 (5)
O1—Sr1—OW2Bii85.9 (3)Si2vi—O4—O4xiv80.98 (5)
O1i—Sr1—OW2Bii61.9 (3)Si1—O4—O4xiv148.49 (7)
O10—Sr1—OW2Bii72.3 (2)O3—O4—O4xiv112.96 (5)
O6—Sr1—OW2Bii105.6 (3)Na2xi—O4—O4xiv53.09 (3)
O10i—Sr1—OW2Biii116.1 (4)O2—O4—O4xiv127.42 (8)
O8—Sr1—OW2Biii67.4 (3)O7xi—O4—O4xiv54.13 (4)
O1—Sr1—OW2Biii62.1 (2)O5vi—O4—O4xiv78.45 (6)
O1i—Sr1—OW2Biii150.7 (2)O6vi—O4—O4xiv112.72 (4)
O10—Sr1—OW2Biii78.6 (4)O1—O4—O4xiv168.58 (7)
O6—Sr1—OW2Biii79.7 (3)Si2vi—O4—OW1vi104.06 (7)
OW2Bii—Sr1—OW2Biii140.1 (4)Si1—O4—OW1vi102.47 (8)
O10i—Sr1—OW2Aii75.4 (2)O3—O4—OW1vi74.45 (6)
O8—Sr1—OW2Aii154.44 (11)Na2xi—O4—OW1vi45.75 (5)
O1—Sr1—OW2Aii75.6 (5)O2—O4—OW1vi134.16 (7)
O1i—Sr1—OW2Aii71.4 (4)O7xi—O4—OW1vi111.73 (6)
O10—Sr1—OW2Aii75.49 (15)O5vi—O4—OW1vi70.53 (6)
O6—Sr1—OW2Aii115.5 (4)O6vi—O4—OW1vi125.21 (7)
OW2Bii—Sr1—OW2Aii11.3 (2)O1—O4—OW1vi94.96 (7)
OW2Biii—Sr1—OW2Aii133.5 (4)O4xiv—O4—OW1vi73.62 (6)
O10i—Sr1—OW2Aiii126.0 (4)Si2vi—O4—Sr1vi66.69 (5)
O8—Sr1—OW2Aiii67.47 (11)Si1—O4—Sr1vi65.87 (4)
O1—Sr1—OW2Aiii70.3 (4)O3—O4—Sr1vi98.02 (5)
O1i—Sr1—OW2Aiii141.2 (4)Na2xi—O4—Sr1vi144.11 (5)
O10—Sr1—OW2Aiii72.1 (2)O2—O4—Sr1vi80.60 (4)
O6—Sr1—OW2Aiii68.9 (5)O7xi—O4—Sr1vi99.44 (4)
OW2Bii—Sr1—OW2Aiii140.0 (2)O5vi—O4—Sr1vi68.25 (4)
OW2Biii—Sr1—OW2Aiii10.89 (18)O6vi—O4—Sr1vi41.43 (3)
OW2Aii—Sr1—OW2Aiii136.2 (2)O1—O4—Sr1vi35.81 (3)
O10i—Sr1—Si4162.91 (3)O4xiv—O4—Sr1vi145.56 (5)
O8—Sr1—Si4106.93 (4)OW1vi—O4—Sr1vi102.16 (6)
O1—Sr1—Si4104.91 (3)Si2—O5—Si3140.05 (10)
O1i—Sr1—Si483.01 (3)Si2—O5—O9151.06 (9)
O10—Sr1—Si427.75 (3)Si3—O5—O938.87 (5)
O6—Sr1—Si430.01 (3)Si2—O5—O2xii139.43 (9)
OW2Bii—Sr1—Si485.5 (3)Si3—O5—O2xii38.09 (5)
OW2Biii—Sr1—Si481.0 (4)O9—O5—O2xii62.55 (5)
OW2Aii—Sr1—Si492.7 (3)Si2—O5—O635.69 (4)
OW2Aiii—Sr1—Si471.1 (4)Si3—O5—O6107.15 (7)
O10i—Sr1—Na1Aiv42.29 (16)O9—O5—O6138.88 (7)
O8—Sr1—Na1Aiv39.63 (10)O2xii—O5—O6107.11 (7)
O1—Sr1—Na1Aiv98.6 (4)Si2—O5—O735.80 (4)
O1i—Sr1—Na1Aiv91.1 (5)Si3—O5—O7159.78 (9)
O10—Sr1—Na1Aiv166.3 (4)O9—O5—O7159.29 (8)
O6—Sr1—Na1Aiv116.02 (13)O2xii—O5—O7126.50 (8)
OW2Bii—Sr1—Na1Aiv121.3 (4)O6—O5—O760.27 (4)
OW2Biii—Sr1—Na1Aiv88.5 (6)Si2—O5—O4i34.82 (5)
OW2Aii—Sr1—Na1Aiv117.4 (3)Si3—O5—O4i130.33 (8)
OW2Aiii—Sr1—Na1Aiv94.4 (5)O9—O5—O4i117.67 (7)
Si4—Sr1—Na1Aiv145.68 (8)O2xii—O5—O4i162.89 (8)
Na1Aii—Na1A—O8v98.8 (9)O6—O5—O4i60.55 (5)
Na1Aii—Na1A—OW2Bii167.2 (5)O7—O5—O4i60.00 (5)
O8v—Na1A—OW2Bii76.3 (9)Si2—O5—O8108.23 (8)
Na1Aii—Na1A—O1082.0 (9)Si3—O5—O832.12 (5)
O8v—Na1A—O1096.54 (11)O9—O5—O861.79 (6)
OW2Bii—Na1A—O1086.7 (7)O2xii—O5—O860.76 (6)
Na1Aii—Na1A—O10ii80.6 (8)O6—O5—O878.25 (6)
O8v—Na1A—O10ii86.14 (10)O7—O5—O8138.41 (7)
OW2Bii—Na1A—O10ii110.6 (10)O4i—O5—O8103.42 (7)
O10—Na1A—O10ii162.6 (15)Si2—O5—OW197.71 (7)
Na1Aii—Na1A—OW2Aii168.5 (5)Si3—O5—OW193.02 (7)
O8v—Na1A—OW2Aii89.3 (11)O9—O5—OW159.14 (6)
OW2Bii—Na1A—OW2Aii13.5 (3)O2xii—O5—OW1121.34 (7)
O10—Na1A—OW2Aii88.9 (7)O6—O5—OW1120.25 (7)
O10ii—Na1A—OW2Aii108.4 (9)O7—O5—OW1106.97 (7)
Na1Aii—Na1A—O8vi64.6 (8)O4i—O5—OW163.60 (6)
O8v—Na1A—O8vi163.4 (15)O8—O5—OW195.81 (7)
OW2Bii—Na1A—O8vi119.9 (9)Si2—O5—Sr171.25 (5)
O10—Na1A—O8vi81.7 (4)Si3—O5—Sr168.90 (5)
O10ii—Na1A—O8vi90.8 (5)O9—O5—Sr195.25 (5)
OW2Aii—Na1A—O8vi107.2 (8)O2xii—O5—Sr188.99 (5)
Na1Aii—Na1A—OW2B9.8 (4)O6—O5—Sr143.64 (4)
O8v—Na1A—OW2B102.6 (9)O7—O5—Sr1103.10 (4)
OW2Bii—Na1A—OW2B177.0 (3)O4i—O5—Sr173.91 (4)
O10—Na1A—OW2B90.7 (9)O8—O5—Sr136.99 (4)
O10ii—Na1A—OW2B72.0 (7)OW1—O5—Sr1101.84 (6)
OW2Aii—Na1A—OW2B168.1 (3)Si2—O6—Si4141.33 (8)
O8vi—Na1A—OW2B61.0 (7)Si2—O6—O10163.87 (8)
Na1Aii—Na1A—OW2A8.9 (4)Si4—O6—O1035.69 (4)
O8v—Na1A—OW2A92.5 (8)Si2—O6—O535.39 (4)
OW2Bii—Na1A—OW2A167.5 (2)Si4—O6—O5170.08 (8)
O10—Na1A—OW2A89.0 (9)O10—O6—O5151.52 (7)
O10ii—Na1A—OW2A73.6 (7)Si2—O6—O3vi125.17 (7)
OW2Aii—Na1A—OW2A177.4 (3)Si4—O6—O3vi36.73 (4)
O8vi—Na1A—OW2A70.9 (9)O10—O6—O3vi62.89 (5)
OW2B—Na1A—OW2A10.4 (2)O5—O6—O3vi133.74 (7)
Na1Aii—Na1A—Si4ii92.0 (7)Si2—O6—O735.89 (5)
O8v—Na1A—Si4ii106.8 (2)Si4—O6—O7112.11 (6)
OW2Bii—Na1A—Si4ii100.7 (8)O10—O6—O7147.80 (6)
O10—Na1A—Si4ii156.6 (4)O5—O6—O760.20 (4)
O10ii—Na1A—Si4ii25.38 (9)O3vi—O6—O789.29 (6)
OW2Aii—Na1A—Si4ii93.5 (8)Si2—O6—O9v108.67 (7)
O8vi—Na1A—Si4ii75.33 (16)Si4—O6—O9v35.87 (4)
OW2B—Na1A—Si4ii82.2 (5)O10—O6—O9v61.59 (5)
OW2A—Na1A—Si4ii87.7 (6)O5—O6—O9v143.97 (7)
Na1Aii—Na1A—O9vi93.4 (7)O3vi—O6—O9v59.43 (5)
O8v—Na1A—O9vi133.7 (4)O7—O6—O9v91.10 (5)
OW2Bii—Na1A—O9vi98.5 (8)Si2—O6—O4i34.91 (4)
O10—Na1A—O9vi129.46 (15)Si4—O6—O4i122.62 (7)
O10ii—Na1A—O9vi52.04 (6)O10—O6—O4i129.00 (6)
OW2Aii—Na1A—O9vi86.8 (8)O5—O6—O4i60.47 (5)
O8vi—Na1A—O9vi52.12 (7)O3vi—O6—O4i134.97 (7)
OW2B—Na1A—O9vi84.3 (5)O7—O6—O4i59.95 (5)
OW2A—Na1A—O9vi93.2 (7)O9v—O6—O4i87.13 (6)
Si4ii—Na1A—O9vi27.88 (3)Si2—O6—Sr1117.82 (6)
Na1Aii—Na1A—Si3v90.2 (7)Si4—O6—Sr192.69 (5)
O8v—Na1A—Si3v23.44 (9)O10—O6—Sr157.58 (4)
OW2Bii—Na1A—Si3v80.7 (6)O5—O6—Sr196.04 (5)
O10—Na1A—Si3v73.73 (9)O3vi—O6—Sr1116.86 (5)
O10ii—Na1A—Si3v106.27 (15)O7—O6—Sr1153.57 (6)
OW2Aii—Na1A—Si3v94.1 (8)O9v—O6—Sr1105.14 (5)
O8vi—Na1A—Si3v147.1 (9)O4i—O6—Sr199.50 (5)
OW2B—Na1A—Si3v97.2 (7)Si2—O6—O1i83.70 (6)
OW2A—Na1A—Si3v86.9 (7)Si4—O6—O1i102.09 (6)
Si4ii—Na1A—Si3v129.17 (10)O10—O6—O1i82.67 (5)
O9vi—Na1A—Si3v156.8 (2)O5—O6—O1i87.23 (5)
Na1Aii—Na1B—O10ii89.3 (4)O3vi—O6—O1i138.77 (6)
Na1Aii—Na1B—O1090.7 (4)O7—O6—O1i113.60 (6)
O10ii—Na1B—O10180.00 (8)O9v—O6—O1i85.17 (5)
Na1Aii—Na1B—O8v107.5 (4)O4i—O6—O1i53.65 (4)
O10ii—Na1B—O8v85.04 (5)Sr1—O6—O1i49.13 (3)
O10—Na1B—O8v94.96 (5)Si2—O6—OW2Aiii124.88 (15)
Na1Aii—Na1B—O8vi72.5 (4)Si4—O6—OW2Aiii90.09 (10)
O10ii—Na1B—O8vi94.96 (5)O10—O6—OW2Aiii68.0 (2)
O10—Na1B—O8vi85.04 (5)O5—O6—OW2Aiii90.25 (12)
O8v—Na1B—O8vi180.00 (12)O3vi—O6—OW2Aiii80.7 (3)
Na1Aii—Na1B—OW2Bii168.9 (4)O7—O6—OW2Aiii126.2 (4)
O10ii—Na1B—OW2Bii100.5 (3)O9v—O6—OW2Aiii125.56 (11)
O10—Na1B—OW2Bii79.5 (3)O4i—O6—OW2Aiii143.5 (2)
O8v—Na1B—OW2Bii68.4 (4)Sr1—O6—OW2Aiii59.8 (4)
O8vi—Na1B—OW2Bii111.6 (4)O1i—O6—OW2Aiii108.0 (4)
Na1Aii—Na1B—OW2B11.1 (4)Si2—O6—O883.11 (5)
O10ii—Na1B—OW2B79.5 (3)Si4—O6—O8134.77 (7)
O10—Na1B—OW2B100.5 (3)O10—O6—O899.61 (5)
O8v—Na1B—OW2B111.6 (4)O5—O6—O852.00 (5)
O8vi—Na1B—OW2B68.4 (4)O3vi—O6—O8136.29 (6)
OW2Bii—Na1B—OW2B180.0 (11)O7—O6—O8112.14 (5)
Na1Aii—Na1B—OW2A10.1 (4)O9v—O6—O8149.50 (6)
O10ii—Na1B—OW2A81.40 (19)O4i—O6—O887.92 (5)
O10—Na1B—OW2A98.60 (19)Sr1—O6—O846.31 (3)
O8v—Na1B—OW2A100.4 (5)O1i—O6—O867.85 (5)
O8vi—Na1B—OW2A79.6 (5)OW2Aiii—O6—O855.8 (2)
OW2Bii—Na1B—OW2A168.2 (2)Si2vii—O7—Si2129.07 (12)
OW2B—Na1B—OW2A11.8 (2)Si2vii—O7—O5vii35.06 (4)
Na1Aii—Na1B—OW2Aii169.9 (4)Si2—O7—O5vii122.34 (8)
O10ii—Na1B—OW2Aii98.60 (19)Si2vii—O7—O5122.34 (8)
O10—Na1B—OW2Aii81.40 (19)Si2—O7—O535.06 (4)
O8v—Na1B—OW2Aii79.6 (5)O5vii—O7—O5141.49 (10)
O8vi—Na1B—OW2Aii100.4 (5)Si2vii—O7—O6vii35.44 (3)
OW2Bii—Na1B—OW2Aii11.8 (2)Si2—O7—O6vii154.01 (8)
OW2B—Na1B—OW2Aii168.2 (2)O5vii—O7—O6vii59.53 (4)
OW2A—Na1B—OW2Aii180.0 (11)O5—O7—O6vii124.87 (5)
Na1Aii—Na1B—Si4ii98.2 (4)Si2vii—O7—O6154.01 (8)
O10ii—Na1B—Si4ii24.36 (3)Si2—O7—O635.44 (3)
O10—Na1B—Si4ii155.64 (3)O5vii—O7—O6124.87 (5)
O8v—Na1B—Si4ii103.77 (4)O5—O7—O659.53 (4)
O8vi—Na1B—Si4ii76.23 (4)O6vii—O7—O6168.77 (9)
OW2Bii—Na1B—Si4ii92.91 (19)Si2vii—O7—O4viii35.53 (5)
OW2B—Na1B—Si4ii87.09 (19)Si2—O7—O4viii96.71 (8)
OW2A—Na1B—Si4ii93.2 (3)O5vii—O7—O4viii60.41 (5)
OW2Aii—Na1B—Si4ii86.8 (3)O5—O7—O4viii87.66 (6)
Na1Aii—Na1B—Si481.8 (4)O6vii—O7—O4viii60.44 (4)
O10ii—Na1B—Si4155.64 (3)O6—O7—O4viii130.69 (7)
O10—Na1B—Si424.36 (3)Si2vii—O7—O4i96.71 (8)
O8v—Na1B—Si476.23 (4)Si2—O7—O4i35.53 (5)
O8vi—Na1B—Si4103.77 (4)O5vii—O7—O4i87.66 (6)
OW2Bii—Na1B—Si487.09 (19)O5—O7—O4i60.41 (5)
OW2B—Na1B—Si492.91 (19)O6vii—O7—O4i130.69 (7)
OW2A—Na1B—Si486.8 (3)O6—O7—O4i60.44 (4)
OW2Aii—Na1B—Si493.2 (3)O4viii—O7—O4i71.73 (7)
Si4ii—Na1B—Si4180.000 (18)Si2vii—O7—Na2xv115.47 (6)
Na1Aii—Na1B—O9vi99.5 (4)Si2—O7—Na2xv115.47 (6)
O10ii—Na1B—O9vi51.42 (4)O5vii—O7—Na2xv109.26 (5)
O10—Na1B—O9vi128.58 (4)O5—O7—Na2xv109.26 (5)
O8v—Na1B—O9vi128.13 (4)O6vii—O7—Na2xv84.38 (5)
O8vi—Na1B—O9vi51.87 (4)O6—O7—Na2xv84.38 (5)
OW2Bii—Na1B—O9vi90.8 (3)O4viii—O7—Na2xv144.13 (4)
OW2B—Na1B—O9vi89.2 (3)O4i—O7—Na2xv144.13 (4)
OW2A—Na1B—O9vi99.2 (5)Si3—O8—Na1Aiv121.0 (3)
OW2Aii—Na1B—O9vi80.8 (5)Si3—O8—Na1Bi117.61 (9)
Si4ii—Na1B—O9vi27.57 (2)Na1Aiv—O8—Na1Bi8.7 (8)
Si4—Na1B—O9vi152.43 (2)Si3—O8—Sr1134.98 (10)
OW1—Na2—OW1vii173.90 (12)Na1Aiv—O8—Sr197.22 (10)
OW1—Na2—O4i83.57 (7)Na1Bi—O8—Sr196.45 (6)
OW1vii—Na2—O4i101.36 (7)Si3—O8—Na1Ai114.1 (3)
OW1—Na2—O4viii101.36 (7)Na1Aiv—O8—Na1Ai16.6 (15)
OW1vii—Na2—O4viii83.57 (7)Na1Bi—O8—Na1Ai7.9 (7)
O4i—Na2—O4viii73.82 (7)Sr1—O8—Na1Ai95.61 (10)
OW1—Na2—O3viii88.64 (8)Si3—O8—O2xii34.49 (5)
OW1vii—Na2—O3viii90.96 (8)Na1Aiv—O8—O2xii126.1 (3)
O4i—Na2—O3viii128.87 (6)Na1Bi—O8—O2xii128.72 (7)
O4viii—Na2—O3viii58.40 (4)Sr1—O8—O2xii134.08 (8)
OW1—Na2—O3i90.96 (8)Na1Ai—O8—O2xii130.28 (13)
OW1vii—Na2—O3i88.64 (8)Si3—O8—O533.55 (5)
O4i—Na2—O3i58.40 (4)Na1Aiv—O8—O5138.3 (7)
O4viii—Na2—O3i128.87 (6)Na1Bi—O8—O5130.73 (8)
O3viii—Na2—O3i172.58 (8)Sr1—O8—O5101.91 (6)
OW1—Na2—O7ix86.95 (6)Na1Ai—O8—O5123.6 (6)
OW1vii—Na2—O7ix86.95 (6)O2xii—O8—O557.33 (5)
O4i—Na2—O7ix143.09 (3)Si3—O8—O933.68 (5)
O4viii—Na2—O7ix143.09 (3)Na1Aiv—O8—O988.2 (4)
O3viii—Na2—O7ix86.29 (4)Na1Bi—O8—O984.07 (6)
O3i—Na2—O7ix86.29 (4)Sr1—O8—O9146.68 (8)
OW1—Na2—Si1i87.55 (7)Na1Ai—O8—O980.4 (3)
OW1vii—Na2—Si1i95.03 (7)O2xii—O8—O959.47 (5)
O4i—Na2—Si1i29.24 (3)O5—O8—O956.47 (5)
O4viii—Na2—Si1i101.34 (5)Si3—O8—OW2Bi114.0 (2)
O3viii—Na2—Si1i158.11 (6)Na1Aiv—O8—OW2Bi53.1 (8)
O3i—Na2—Si1i29.17 (3)Na1Bi—O8—OW2Bi61.6 (2)
O7ix—Na2—Si1i115.00 (2)Sr1—O8—OW2Bi107.7 (2)
OW1—Na2—Si1viii95.03 (7)Na1Ai—O8—OW2Bi69.4 (7)
OW1vii—Na2—Si1viii87.55 (7)O2xii—O8—OW2Bi90.10 (19)
O4i—Na2—Si1viii101.34 (5)O5—O8—OW2Bi146.39 (19)
O4viii—Na2—Si1viii29.24 (3)O9—O8—OW2Bi101.8 (2)
O3viii—Na2—Si1viii29.17 (3)Si3—O8—OW2Biii110.2 (2)
O3i—Na2—Si1viii158.11 (6)Na1Aiv—O8—OW2Biii117.7 (8)
O7ix—Na2—Si1viii115.00 (2)Na1Bi—O8—OW2Biii125.1 (3)
Si1i—Na2—Si1viii130.00 (4)Sr1—O8—OW2Biii64.1 (2)
OW1—Na2—O6x106.17 (7)Na1Ai—O8—OW2Biii131.7 (6)
OW1vii—Na2—O6x69.40 (7)O2xii—O8—OW2Biii80.84 (18)
O4i—Na2—O6x168.03 (5)O5—O8—OW2Biii104.0 (3)
O4viii—Na2—O6x97.06 (3)O9—O8—OW2Biii140.30 (18)
O3viii—Na2—O6x46.41 (4)OW2Bi—O8—OW2Biii75.8 (6)
O3i—Na2—O6x126.90 (5)Si3—O8—OW2Aiii101.3 (4)
O7ix—Na2—O6x46.48 (2)Na1Aiv—O8—OW2Aiii128.5 (9)
Si1i—Na2—O6x154.39 (3)Na1Bi—O8—OW2Aiii135.9 (5)
Si1viii—Na2—O6x71.35 (2)Sr1—O8—OW2Aiii65.66 (19)
OW1—Na2—O6ix69.40 (7)Na1Ai—O8—OW2Aiii142.2 (7)
OW1vii—Na2—O6ix106.17 (7)O2xii—O8—OW2Aiii74.6 (3)
O4i—Na2—O6ix97.06 (3)O5—O8—OW2Aiii93.2 (5)
O4viii—Na2—O6ix168.03 (5)O9—O8—OW2Aiii133.4 (4)
O3viii—Na2—O6ix126.90 (5)OW2Bi—O8—OW2Aiii84.9 (6)
O3i—Na2—O6ix46.41 (4)OW2Biii—O8—OW2Aiii10.8 (2)
O7ix—Na2—O6ix46.48 (2)Si3—O8—O10i153.40 (10)
Si1i—Na2—O6ix71.35 (2)Na1Aiv—O8—O10i48.42 (15)
Si1viii—Na2—O6ix154.39 (3)Na1Bi—O8—O10i47.47 (4)
O6x—Na2—O6ix92.96 (5)Sr1—O8—O10i49.07 (4)
O1—Si1—O2114.26 (8)Na1Ai—O8—O10i47.65 (9)
O1—Si1—O3115.59 (7)O2xii—O8—O10i170.00 (8)
O2—Si1—O3104.93 (7)O5—O8—O10i132.66 (7)
O1—Si1—O4112.92 (7)O9—O8—O10i124.28 (7)
O2—Si1—O4106.37 (8)OW2Bi—O8—O10i80.08 (19)
O3—Si1—O4101.52 (7)OW2Biii—O8—O10i94.75 (19)
O1—Si1—Na2xi131.91 (6)OW2Aiii—O8—O10i102.4 (4)
O2—Si1—Na2xi113.78 (6)Si4iv—O9—Si3135.84 (9)
O3—Si1—Na2xi52.06 (5)Si4iv—O9—O5174.58 (9)
O4—Si1—Na2xi49.50 (5)Si3—O9—O538.75 (5)
O1—Si1—Sr131.04 (5)Si4iv—O9—O3xiii36.72 (4)
O2—Si1—Sr1113.57 (6)Si3—O9—O3xiii170.53 (9)
O3—Si1—Sr187.27 (5)O5—O9—O3xiii148.58 (7)
O4—Si1—Sr1135.23 (5)Si4iv—O9—O6iv36.68 (4)
Na2xi—Si1—Sr1123.52 (2)Si3—O9—O6iv118.30 (7)
O1—Si1—Sr1vi28.54 (5)O5—O9—O6iv141.86 (7)
O2—Si1—Sr1vi106.83 (6)O3xiii—O9—O6iv59.84 (5)
O3—Si1—Sr1vi141.03 (5)Si4iv—O9—O2xii116.80 (7)
O4—Si1—Sr1vi90.64 (5)Si3—O9—O2xii35.58 (5)
Na2xi—Si1—Sr1vi128.877 (17)O5—O9—O2xii59.11 (5)
Sr1—Si1—Sr1vi59.546 (7)O3xiii—O9—O2xii145.94 (7)
O5—Si2—O6108.93 (7)O6iv—O9—O2xii86.61 (5)
O5—Si2—O4i110.90 (8)Si4iv—O9—O10iv32.54 (4)
O6—Si2—O4i110.42 (7)Si3—O9—O10iv108.95 (7)
O5—Si2—O7109.14 (6)O5—O9—O10iv143.15 (7)
O6—Si2—O7108.67 (7)O3xiii—O9—O10iv61.83 (5)
O4i—Si2—O7108.74 (7)O6iv—O9—O10iv58.19 (5)
O5—Si2—Sr185.36 (6)O2xii—O9—O10iv107.11 (6)
O6—Si2—Sr140.24 (5)Si4iv—O9—O8113.44 (8)
O4i—Si2—Sr190.34 (5)Si3—O9—O832.15 (5)
O7—Si2—Sr1148.77 (5)O5—O9—O861.74 (6)
O8—Si3—O2xii112.48 (9)O3xiii—O9—O8138.87 (7)
O8—Si3—O5114.33 (8)O6iv—O9—O8117.15 (7)
O2xii—Si3—O5103.79 (8)O2xii—O9—O859.70 (6)
O8—Si3—O9114.18 (9)O10iv—O9—O881.65 (6)
O2xii—Si3—O9108.72 (8)Si4iv—O9—OW1108.77 (7)
O5—Si3—O9102.38 (7)Si3—O9—OW1108.38 (7)
O8—Si3—Na1Aiv35.6 (2)O5—O9—OW175.63 (6)
O2xii—Si3—Na1Aiv119.6 (5)O3xiii—O9—OW175.23 (6)
O5—Si3—Na1Aiv133.7 (4)O6iv—O9—OW1132.82 (7)
O9—Si3—Na1Aiv79.6 (3)O2xii—O9—OW1134.28 (6)
O8—Si3—Na1Bi38.27 (7)O10iv—O9—OW1113.34 (7)
O2xii—Si3—Na1Bi125.30 (6)O8—O9—OW1105.68 (8)
O5—Si3—Na1Bi129.07 (6)Si4iv—O9—Na1Ai76.04 (7)
O9—Si3—Na1Bi76.06 (5)Si3—O9—Na1Ai79.6 (3)
Na1Aiv—Si3—Na1Bi6.1 (6)O5—O9—Na1Ai100.93 (8)
O8—Si3—Na1Ai41.5 (3)O3xiii—O9—Na1Ai91.6 (3)
O2xii—Si3—Na1Ai130.9 (5)O6iv—O9—Na1Ai102.3 (3)
O5—Si3—Na1Ai124.3 (4)O2xii—O9—Na1Ai101.9 (5)
O9—Si3—Na1Ai72.7 (3)O10iv—O9—Na1Ai45.32 (14)
Na1Aiv—Si3—Na1Ai12.1 (11)O8—O9—Na1Ai47.5 (3)
Na1Bi—Si3—Na1Ai6.0 (5)OW1—O9—Na1Ai92.1 (5)
O8—Si3—Sr127.75 (6)Si4iv—O9—Na1Bi75.90 (5)
O2xii—Si3—Sr1117.38 (6)Si3—O9—Na1Bi76.13 (5)
O5—Si3—Sr187.09 (5)O5—O9—Na1Bi100.60 (5)
O9—Si3—Sr1129.07 (6)O3xiii—O9—Na1Bi94.81 (5)
Na1Aiv—Si3—Sr159.93 (6)O6iv—O9—Na1Bi99.32 (5)
Na1Bi—Si3—Sr160.502 (8)O2xii—O9—Na1Bi96.46 (5)
Na1Ai—Si3—Sr161.41 (11)O10iv—O9—Na1Bi44.08 (3)
O10—Si4—O9v113.78 (7)O8—O9—Na1Bi44.06 (4)
O10—Si4—O3vi116.03 (7)OW1—O9—Na1Bi97.92 (7)
O9v—Si4—O3vi106.69 (7)Na1Ai—O9—Na1Bi6.1 (6)
O10—Si4—O6106.47 (7)Si4iv—O9—Na1Aiv75.91 (7)
O9v—Si4—O6107.45 (7)Si3—O9—Na1Aiv72.9 (3)
O3vi—Si4—O6105.84 (7)O5—O9—Na1Aiv100.17 (8)
O10—Si4—Sr150.07 (5)O3xiii—O9—Na1Aiv97.8 (3)
O9v—Si4—Sr1117.90 (5)O6iv—O9—Na1Aiv96.4 (3)
O3vi—Si4—Sr1135.12 (5)O2xii—O9—Na1Aiv91.2 (5)
O6—Si4—Sr157.30 (5)O10iv—O9—Na1Aiv43.50 (5)
O10—Si4—Na1Aii41.1 (3)O8—O9—Na1Aiv41.2 (2)
O9v—Si4—Na1Aii76.08 (7)OW1—O9—Na1Aiv103.6 (5)
O3vi—Si4—Na1Aii115.1 (5)Na1Ai—O9—Na1Aiv12.1 (11)
O6—Si4—Na1Aii136.1 (6)Na1Bi—O9—Na1Aiv5.9 (5)
Sr1—Si4—Na1Aii81.8 (5)Si4—O10—Na1B117.01 (6)
O10—Si4—Na1B38.63 (4)Si4—O10—Na1A120.0 (2)
O9v—Si4—Na1B76.53 (5)Na1B—O10—Na1A8.7 (8)
O3vi—Si4—Na1B121.01 (5)Si4—O10—Na1Aii113.5 (3)
O6—Si4—Na1B129.95 (5)Na1B—O10—Na1Aii8.7 (8)
Sr1—Si4—Na1B76.407 (10)Na1A—O10—Na1Aii17.4 (15)
Na1Aii—Si4—Na1B6.2 (6)Si4—O10—Sr1vi131.36 (7)
O10—Si4—Na1A36.91 (13)Na1B—O10—Sr1vi96.67 (4)
O9v—Si4—Na1A77.12 (9)Na1A—O10—Sr1vi98.7 (2)
O3vi—Si4—Na1A126.7 (5)Na1Aii—O10—Sr1vi94.5 (2)
O6—Si4—Na1A124.0 (5)Si4—O10—O637.83 (4)
Sr1—Si4—Na1A71.2 (5)Na1B—O10—O6137.96 (6)
Na1Aii—Si4—Na1A12.1 (11)Na1A—O10—O6134.5 (4)
Na1B—Si4—Na1A6.0 (5)Na1Aii—O10—O6140.05 (15)
O10—Si4—Sr1vi29.99 (5)Sr1vi—O10—O6125.24 (6)
O9v—Si4—Sr1vi136.36 (6)Si4—O10—Sr1102.18 (6)
O3vi—Si4—Sr1vi87.69 (5)Na1B—O10—Sr1112.87 (5)
O6—Si4—Sr1vi107.64 (5)Na1A—O10—Sr1104.2 (8)
Sr1—Si4—Sr1vi63.932 (8)Na1Aii—O10—Sr1121.5 (8)
Na1Aii—Si4—Sr1vi60.69 (5)Sr1vi—O10—Sr194.79 (4)
Na1B—Si4—Sr1vi61.158 (8)O6—O10—Sr165.03 (4)
Na1A—Si4—Sr1vi61.96 (10)Si4—O10—O9v33.68 (4)
Si1—O1—Sr1129.95 (8)Na1B—O10—O9v84.50 (5)
Si1—O1—Sr1vi134.11 (8)Na1A—O10—O9v86.49 (19)
Sr1—O1—Sr1vi95.88 (4)Na1Aii—O10—O9v82.64 (17)
Si1—O1—O233.49 (5)Sr1vi—O10—O9v152.96 (6)
Sr1—O1—O2125.35 (7)O6—O10—O9v60.22 (5)
Sr1vi—O1—O2121.03 (6)Sr1—O10—O9v109.71 (5)
Si1—O1—O434.49 (5)Si4—O10—O3vi32.59 (4)
Sr1—O1—O4150.83 (7)Na1B—O10—O3vi122.02 (6)
Sr1vi—O1—O4105.54 (6)Na1A—O10—O3vi129.4 (6)
O2—O1—O458.47 (5)Na1Aii—O10—O3vi114.5 (7)
Si1—O1—O332.93 (4)Sr1vi—O10—O3vi100.27 (5)
Sr1—O1—O399.47 (5)O6—O10—O3vi59.13 (5)
Sr1vi—O1—O3160.88 (7)Sr1—O10—O3vi120.27 (5)
O2—O1—O357.23 (5)O9v—O10—O3vi57.83 (5)
O4—O1—O356.26 (5)Si4—O10—O8vi144.43 (7)
Si1—O1—OW2Biii124.0 (4)Na1B—O10—O8vi47.50 (4)
Sr1—O1—OW2Biii67.1 (2)Na1A—O10—O8vi50.7 (3)
Sr1vi—O1—OW2Biii66.6 (4)Na1Aii—O10—O8vi45.44 (15)
O2—O1—OW2Biii90.8 (4)Sr1vi—O10—O8vi49.26 (4)
O4—O1—OW2Biii139.9 (3)O6—O10—O8vi174.49 (6)
O3—O1—OW2Biii130.4 (4)Sr1—O10—O8vi113.36 (5)
Si1—O1—O6vi77.50 (6)O9v—O10—O8vi124.60 (6)
Sr1—O1—O6vi152.53 (6)O3vi—O10—O8vi120.11 (6)
Sr1vi—O1—O6vi56.65 (4)Si4—O10—O1144.04 (7)
O2—O1—O6vi75.60 (5)Na1B—O10—O196.26 (5)
O4—O1—O6vi52.56 (4)Na1A—O10—O191.1 (5)
O3—O1—O6vi107.49 (6)Na1Aii—O10—O1101.3 (4)
OW2Biii—O1—O6vi98.0 (2)Sr1vi—O10—O150.01 (3)
Si1—O1—OW2Aiii132.0 (3)O6—O10—O1107.64 (5)
Sr1—O1—OW2Aiii63.42 (15)Sr1—O10—O148.82 (3)
Sr1vi—O1—OW2Aiii61.13 (19)O9v—O10—O1156.93 (6)
O2—O1—OW2Aiii98.7 (3)O3vi—O10—O1135.85 (6)
O4—O1—OW2Aiii144.94 (19)O8vi—O10—O168.85 (5)
O3—O1—OW2Aiii136.7 (2)Si4—O10—OW2Bii117.9 (3)
OW2Biii—O1—OW2Aiii8.1 (2)Na1B—O10—OW2Bii55.0 (2)
O6vi—O1—OW2Aiii98.60 (10)Na1A—O10—OW2Bii46.3 (8)
Si1—O1—O10165.65 (9)Na1Aii—O10—OW2Bii63.6 (8)
Sr1—O1—O1051.60 (3)Sr1vi—O10—OW2Bii110.0 (3)
Sr1vi—O1—O1048.40 (3)O6—O10—OW2Bii101.61 (17)
O2—O1—O10160.73 (7)Sr1—O10—OW2Bii58.9 (3)
O4—O1—O10135.43 (6)O9v—O10—OW2Bii92.9 (4)
O3—O1—O10138.97 (6)O3vi—O10—OW2Bii149.7 (3)
OW2Biii—O1—O1070.4 (4)O8vi—O10—OW2Bii81.31 (18)
O6vi—O1—O10102.40 (5)O1—O10—OW2Bii69.4 (4)
OW2Aiii—O1—O1062.3 (3)Na2—OW1—O9133.03 (9)
Si1—O1—O10i82.76 (6)Na2—OW1—O2xiii139.30 (10)
Sr1—O1—O10i47.48 (3)O9—OW1—O2xiii87.64 (7)
Sr1vi—O1—O10i143.08 (5)Na2—OW1—O4i50.68 (5)
O2—O1—O10i90.25 (5)O9—OW1—O4i88.18 (6)
O4—O1—O10i107.75 (5)O2xiii—OW1—O4i151.56 (11)
O3—O1—O10i52.32 (4)Na2—OW1—OW2Aiv114.81 (17)
OW2Biii—O1—O10i96.5 (2)O9—OW1—OW2Aiv77.82 (11)
O6vi—O1—O10i159.80 (5)O2xiii—OW1—OW2Aiv65.50 (17)
OW2Aiii—O1—O10i97.74 (11)O4i—OW1—OW2Aiv86.13 (17)
O10—O1—O10i95.67 (5)Na2—OW1—O588.10 (7)
Si1—O1—OW2Aii105.2 (4)O9—OW1—O545.22 (4)
Sr1—O1—OW2Aii58.9 (4)O2xiii—OW1—O5132.04 (8)
Sr1vi—O1—OW2Aii100.37 (17)O4i—OW1—O545.87 (4)
O2—O1—OW2Aii135.4 (3)OW2Aiv—OW1—O591.53 (13)
O4—O1—OW2Aii97.2 (4)Na2—OW1—O3xiii165.52 (12)
O3—O1—OW2Aii78.2 (3)O9—OW1—O3xiii46.19 (4)
OW2Biii—O1—OW2Aii122.7 (2)O2xiii—OW1—O3xiii45.75 (4)
O6vi—O1—OW2Aii121.3 (3)O4i—OW1—O3xiii134.02 (8)
OW2Aiii—O1—OW2Aii116.5 (2)OW2Aiv—OW1—O3xiii79.64 (15)
O10—O1—OW2Aii62.3 (3)O5—OW1—O3xiii90.78 (6)
O10i—O1—OW2Aii60.16 (13)OW2B—OW2A—Na1Aii71.6 (13)
Si1—O2—Si3xii138.48 (10)OW2B—OW2A—Na1B72.3 (13)
Si1—O2—O5xii163.28 (9)Na1Aii—OW2A—Na1B1.46 (16)
Si3xii—O2—O5xii38.12 (5)OW2B—OW2A—Sr1ii80 (2)
Si1—O2—O337.68 (5)Na1Aii—OW2A—Sr1ii91.4 (4)
Si3xii—O2—O3172.78 (10)Na1B—OW2A—Sr1ii90.2 (3)
O5xii—O2—O3148.06 (8)OW2B—OW2A—Sr1xvi72.9 (18)
Si1—O2—O437.17 (5)Na1Aii—OW2A—Sr1xvi143.7 (11)
Si3xii—O2—O4122.99 (8)Na1B—OW2A—Sr1xvi144.1 (10)
O5xii—O2—O4126.47 (7)Sr1ii—OW2A—Sr1xvi75.5 (3)
O3—O2—O458.53 (5)OW2B—OW2A—O8xvi76.4 (15)
Si1—O2—O9xii109.79 (7)Na1Aii—OW2A—O8xvi128.4 (6)
Si3xii—O2—O9xii35.70 (5)Na1B—OW2A—O8xvi129.9 (5)
O5xii—O2—O9xii58.34 (5)Sr1ii—OW2A—O8xvi121.8 (5)
O3—O2—O9xii144.94 (7)Sr1xvi—OW2A—O8xvi46.87 (15)
O4—O2—O9xii87.29 (6)OW2B—OW2A—Na1A72.9 (13)
Si1—O2—O8xii125.10 (9)Na1Aii—OW2A—Na1A2.6 (3)
Si3xii—O2—O8xii33.03 (5)Na1B—OW2A—Na1A1.14 (10)
O5xii—O2—O8xii61.91 (6)Sr1ii—OW2A—Na1A89.4 (3)
O3—O2—O8xii140.43 (8)Sr1xvi—OW2A—Na1A144.3 (9)
O4—O2—O8xii137.13 (7)O8xvi—OW2A—Na1A131.0 (5)
O9xii—O2—O8xii60.84 (6)OW2B—OW2A—O1xvi43 (2)
Si1—O2—O132.25 (5)Na1Aii—OW2A—O1xvi100.3 (7)
Si3xii—O2—O1111.94 (8)Na1B—OW2A—O1xvi100.2 (7)
O5xii—O2—O1149.98 (8)Sr1ii—OW2A—O1xvi47.5 (3)
O3—O2—O161.95 (5)Sr1xvi—OW2A—O1xvi46.3 (3)
O4—O2—O160.81 (5)O8xvi—OW2A—O1xvi81.2 (5)
O9xii—O2—O196.20 (6)Na1A—OW2A—O1xvi100.1 (6)
O8xii—O2—O192.86 (7)OW2B—OW2A—O6xvi123.9 (18)
Si1—O2—OW1xiii112.90 (8)Na1Aii—OW2A—O6xvi164.4 (10)
Si3xii—O2—OW1xiii108.34 (7)Na1B—OW2A—O6xvi163.6 (9)
O5xii—O2—OW1xiii75.76 (6)Sr1ii—OW2A—O6xvi90.17 (17)
O3—O2—OW1xiii75.24 (6)Sr1xvi—OW2A—O6xvi51.35 (9)
O4—O2—OW1xiii116.75 (8)O8xvi—OW2A—O6xvi62.49 (13)
O9xii—O2—OW1xiii133.34 (7)Na1A—OW2A—O6xvi162.8 (8)
O8xii—O2—OW1xiii106.10 (8)O1xvi—OW2A—O6xvi92.2 (2)
O1—O2—OW1xiii130.23 (7)OW2B—OW2A—O10xvi102 (2)
Si4i—O3—Si1135.08 (9)Na1Aii—OW2A—O10xvi135.8 (3)
Si4i—O3—O4160.15 (9)Na1B—OW2A—O10xvi134.5 (3)
Si1—O3—O439.47 (5)Sr1ii—OW2A—O10xvi45.07 (8)
Si4i—O3—O2128.49 (8)Sr1xvi—OW2A—O10xvi47.22 (9)
Si1—O3—O237.39 (5)O8xvi—OW2A—O10xvi89.31 (15)
O4—O3—O261.48 (5)Na1A—OW2A—O10xvi133.5 (3)
Si4i—O3—O9xiii36.58 (4)O1xvi—OW2A—O10xvi59.0 (2)
Si1—O3—O9xiii142.56 (8)O6xvi—OW2A—O10xvi45.51 (12)
O4—O3—O9xiii163.04 (7)OW2B—OW2A—O8vi31.5 (15)
O2—O3—O9xiii110.93 (7)Na1Aii—OW2A—O8vi43.0 (3)
Si4i—O3—O6i37.43 (4)Na1B—OW2A—O8vi44.0 (3)
Si1—O3—O6i142.98 (8)Sr1ii—OW2A—O8vi94.8 (6)
O4—O3—O6i129.98 (7)Sr1xvi—OW2A—O8vi103.6 (7)
O2—O3—O6i165.23 (8)O8xvi—OW2A—O8vi92.1 (5)
O9xiii—O3—O6i60.73 (5)Na1A—OW2A—O8vi44.8 (2)
Si4i—O3—Na2xi121.01 (7)O1xvi—OW2A—O8vi71.8 (5)
Si1—O3—Na2xi98.77 (7)O6xvi—OW2A—O8vi152.2 (6)
O4—O3—Na2xi59.32 (5)O10xvi—OW2A—O8vi129.9 (7)
O2—O3—Na2xi108.30 (6)OW2B—OW2A—O1ii121 (2)
O9xiii—O3—Na2xi113.82 (6)Na1Aii—OW2A—O1ii86.5 (3)
O6i—O3—Na2xi86.47 (6)Na1B—OW2A—O1ii85.03 (18)
Si4i—O3—O10i31.38 (4)Sr1ii—OW2A—O1ii45.42 (11)
Si1—O3—O10i103.80 (7)Sr1xvi—OW2A—O1ii105.83 (15)
O4—O3—O10i135.22 (7)O8xvi—OW2A—O1ii145.1 (4)
O2—O3—O10i107.58 (6)Na1A—OW2A—O1ii83.90 (19)
O9xiii—O3—O10i60.35 (5)O1xvi—OW2A—O1ii92.7 (2)
O6i—O3—O10i57.97 (5)O6xvi—OW2A—O1ii83.6 (4)
Na2xi—O3—O10i142.85 (6)O10xvi—OW2A—O1ii58.94 (15)
Si4i—O3—O1106.30 (7)O8vi—OW2A—O1ii118.8 (3)
Si1—O3—O131.48 (4)OW2A—OW2B—Na1Aii94.9 (14)
O4—O3—O161.34 (5)OW2A—OW2B—Na1B95.9 (14)
O2—O3—O160.81 (5)Na1Aii—OW2B—Na1B1.70 (19)
O9xiii—O3—O1130.36 (7)OW2A—OW2B—O1xvi129 (2)
O6i—O3—O1113.89 (6)Na1Aii—OW2B—O1xvi115.9 (5)
Na2xi—O3—O1114.96 (6)Na1B—OW2B—O1xvi114.2 (4)
O10i—O3—O175.34 (5)OW2A—OW2B—O8vi142.4 (18)
Si4i—O3—OW1xiii92.54 (7)Na1Aii—OW2B—O8vi50.6 (4)
Si1—O3—OW1xiii96.37 (7)Na1B—OW2B—O8vi50.0 (3)
O4—O3—OW1xiii106.66 (6)O1xvi—OW2B—O8vi85.1 (4)
O2—O3—OW1xiii59.01 (6)OW2A—OW2B—Sr1ii88 (2)
O9xiii—O3—OW1xiii58.59 (5)Na1Aii—OW2B—Sr1ii94.8 (4)
O6i—O3—OW1xiii117.67 (6)Na1B—OW2B—Sr1ii93.5 (3)
Na2xi—O3—OW1xiii105.37 (7)O1xvi—OW2B—Sr1ii51.51 (18)
O10i—O3—OW1xiii101.04 (7)O8vi—OW2B—Sr1ii106.8 (4)
O1—O3—OW1xiii114.85 (7)OW2A—OW2B—Sr1xvi96.2 (18)
Si4i—O3—Sr168.16 (5)Na1Aii—OW2B—Sr1xvi166.5 (5)
Si1—O3—Sr168.43 (5)Na1B—OW2B—Sr1xvi164.9 (5)
O4—O3—Sr198.01 (5)O1xvi—OW2B—Sr1xvi50.78 (16)
O2—O3—Sr186.26 (5)O8vi—OW2B—Sr1xvi120.3 (6)
O9xiii—O3—Sr196.48 (5)Sr1ii—OW2B—Sr1xvi77.9 (3)
O6i—O3—Sr182.87 (4)OW2A—OW2B—O8xvi92.9 (14)
Na2xi—O3—Sr1137.27 (5)Na1Aii—OW2B—O8xvi138.3 (7)
O10i—O3—Sr137.50 (3)Na1B—OW2B—O8xvi139.5 (6)
O1—O3—Sr138.15 (3)O1xvi—OW2B—O8xvi89.6 (3)
OW1xiii—O3—Sr1116.24 (6)O8vi—OW2B—O8xvi104.2 (6)
Si2vi—O4—Si1129.24 (9)Sr1ii—OW2B—O8xvi126.3 (4)
Si2vi—O4—O3164.23 (8)Sr1xvi—OW2B—O8xvi48.55 (16)
Si1—O4—O339.01 (4)OW2A—OW2B—Na1A96.7 (14)
Si2vi—O4—Na2xi128.05 (7)Na1Aii—OW2B—Na1A3.0 (3)
Si1—O4—Na2xi101.26 (6)Na1B—OW2B—Na1A1.30 (12)
O3—O4—Na2xi62.28 (5)O1xvi—OW2B—Na1A112.9 (4)
Si2vi—O4—O2118.22 (7)O8vi—OW2B—Na1A49.6 (3)
Si1—O4—O236.46 (5)Sr1ii—OW2B—Na1A92.5 (3)
O3—O4—O259.99 (5)Sr1xvi—OW2B—Na1A163.6 (4)
Na2xi—O4—O2109.44 (5)O8xvi—OW2B—Na1A140.3 (6)
Si2vi—O4—O7xi35.73 (4)OW2A—OW2B—O10ii100.0 (17)
Si1—O4—O7xi145.13 (8)Na1Aii—OW2B—O10ii47.0 (3)
O3—O4—O7xi159.62 (7)Na1B—OW2B—O10ii45.49 (16)
Na2xi—O4—O7xi107.23 (5)O1xvi—OW2B—O10ii77.6 (2)
O2—O4—O7xi112.86 (6)O8vi—OW2B—O10ii69.0 (3)
Si2vi—O4—O5vi34.29 (4)Sr1ii—OW2B—O10ii48.75 (17)
Si1—O4—O5vi130.69 (8)Sr1xvi—OW2B—O10ii123.1 (3)
O3—O4—O5vi138.03 (7)O8xvi—OW2B—O10ii165.8 (5)
Na2xi—O4—O5vi105.28 (6)Na1A—OW2B—O10ii44.36 (18)
Symmetry codes: (i) x+1/2, y1/2, z+1/2; (ii) x+1/2, y+1/2, z; (iii) x, y+1, z+1/2; (iv) x, y, z+1/2; (v) x, y, z1/2; (vi) x+1/2, y+1/2, z+1/2; (vii) x, y, z+1/2; (viii) x1/2, y1/2, z; (ix) x, y1, z; (x) x, y1, z+1/2; (xi) x+1/2, y+1/2, z; (xii) x+1/2, y+1/2, z+1; (xiii) x+1/2, y1/2, z+1; (xiv) x+1, y, z+1/2; (xv) x, y+1, z; (xvi) x, y+1, z1/2.
TetraSodium BisStrontium OctaSilicate TetraHydrate (TR010) top
Crystal data top
Na4SrSi8O19·4(H2O)F(000) = 1512
Mr = 780.36Dx = 2.474 Mg m3
Monoclinic, P2/cMo Kα radiation, λ = 0.71073 Å
Hall symbol: P -2ycCell parameters from 9594 reflections
a = 22.4102 (3) Åθ = 3.0–32.7°
b = 7.0292 (1) ŵ = 3.23 mm1
c = 13.3140 (2) ÅT = 293 K
β = 92.538 (1)°Prismatic, colourless
V = 2095.24 (5) Å30.23 × 0.14 × 0.04 mm
Z = 4
Data collection top
Oxford 'X Calibur Gemini Ultra
diffractometer
7245 independent reflections
Radiation source: fine-focus sealed tube5007 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.034
Detector resolution: 10.2890 pixels mm-1θmax = 32.7°, θmin = 3.0°
phi/ω scansh = 3332
Absorption correction: multi-scan
CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.32.13 (release 29-11-2007 CrysAlis171 .NET) (compiled Nov 29 2007,17:23:28) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.
k = 1010
Tmin = 0.448, Tmax = 1.000l = 2014
27441 measured reflections
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.033H-atom parameters not defined
wR(F2) = 0.065 w = 1/[σ2(Fo2) + (0.010P)2]
where P = (Fo2 + 2Fc2)/3
S = 1.62(Δ/σ)max = 0.001
7245 reflectionsΔρmax = 0.83 e Å3
327 parametersΔρmin = 0.93 e Å3
0 restraints
Special details top

Experimental. CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.32.13 (release 29–11-2007 CrysAlis171. NET) (compiled Nov 29 2007,17:23:28) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
Sr10.00000.02754 (5)0.25000.01172 (9)
Sr20.50000.00893 (4)0.25000.01063 (9)
Na10.00496 (5)0.76608 (18)0.47772 (8)0.0251 (3)
Na20.00000.5291 (2)0.25000.0259 (5)
Na30.49055 (5)0.24008 (19)0.00146 (7)0.0287 (3)
Na40.50000.51130 (17)0.25000.0162 (4)
Na50.25125 (5)0.26751 (14)0.49402 (8)0.0265 (3)
Si10.18312 (4)0.01233 (8)0.28265 (5)0.00700 (16)
Si20.37147 (4)0.00519 (8)0.02473 (5)0.00738 (16)
Si30.38539 (3)0.28424 (9)0.14957 (5)0.00710 (14)
Si40.11008 (3)0.28539 (9)0.14217 (5)0.00703 (14)
Si50.37755 (3)0.28178 (9)0.14341 (5)0.00800 (14)
Si60.12330 (3)0.28393 (9)0.15658 (5)0.00757 (14)
Si70.31312 (4)0.01339 (8)0.21879 (5)0.00701 (16)
Si80.12836 (4)0.01182 (8)0.47964 (5)0.00784 (16)
O10.13332 (8)0.1576 (2)0.23846 (12)0.0128 (4)
O20.24693 (8)0.0787 (2)0.24506 (13)0.0142 (3)
O30.16788 (8)0.2024 (2)0.24823 (12)0.0143 (4)
O40.18471 (9)0.0184 (2)0.40380 (13)0.0097 (4)
O50.43424 (9)0.0360 (2)0.08009 (13)0.0154 (4)
O60.36439 (8)0.2022 (2)0.03000 (12)0.0142 (4)
O70.35336 (7)0.1680 (2)0.05897 (11)0.0104 (4)
O80.31448 (9)0.0215 (2)0.09876 (13)0.0102 (4)
O90.45563 (7)0.2713 (2)0.14818 (12)0.0113 (4)
O100.35727 (9)0.50340 (19)0.14519 (14)0.0114 (4)
O110.35819 (8)0.1856 (2)0.24648 (12)0.0130 (4)
O120.03971 (8)0.2884 (2)0.14271 (12)0.0112 (4)
O130.14143 (9)0.49257 (19)0.15163 (14)0.0120 (4)
O140.13704 (8)0.1876 (2)0.04208 (12)0.0139 (4)
O150.44475 (8)0.2448 (2)0.16721 (12)0.0150 (4)
O160.32975 (8)0.1789 (2)0.27831 (12)0.0163 (4)
O170.05532 (7)0.2379 (2)0.17074 (12)0.0120 (4)
O180.14839 (8)0.1858 (2)0.05515 (12)0.0135 (4)
O190.06478 (8)0.0309 (2)0.42553 (13)0.0153 (4)
OW10.06834 (13)0.4818 (3)0.40521 (18)0.0437 (7)
OW20.43056 (10)0.5481 (3)0.09837 (16)0.0363 (6)
OW30.20059 (13)0.5272 (3)0.4135 (2)0.0520 (8)
OW40.29162 (18)0.5038 (3)0.1051 (3)0.0912 (13)
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Sr10.0155 (2)0.00850 (16)0.0115 (2)0.0000.00482 (16)0.000
Sr20.0132 (2)0.00831 (16)0.01056 (19)0.0000.00319 (15)0.000
Na10.0208 (6)0.0363 (7)0.0177 (6)0.0045 (5)0.0058 (5)0.0031 (5)
Na20.0251 (11)0.0131 (7)0.0408 (12)0.0000.0169 (9)0.000
Na30.0253 (7)0.0388 (7)0.0211 (6)0.0058 (6)0.0099 (5)0.0030 (5)
Na40.0169 (10)0.0134 (7)0.0187 (9)0.0000.0058 (7)0.000
Na50.0195 (6)0.0261 (6)0.0337 (6)0.0014 (5)0.0029 (5)0.0013 (5)
Si10.0079 (4)0.0076 (3)0.0056 (4)0.0007 (3)0.0006 (3)0.0001 (2)
Si20.0084 (4)0.0084 (3)0.0054 (4)0.0004 (3)0.0011 (3)0.0002 (2)
Si30.0090 (4)0.0059 (3)0.0064 (3)0.0004 (3)0.0006 (3)0.0002 (3)
Si40.0084 (4)0.0058 (3)0.0069 (3)0.0004 (3)0.0000 (3)0.0003 (3)
Si50.0109 (4)0.0059 (3)0.0072 (3)0.0002 (3)0.0002 (3)0.0003 (3)
Si60.0092 (4)0.0059 (3)0.0076 (3)0.0006 (3)0.0005 (3)0.0001 (3)
Si70.0084 (4)0.0075 (3)0.0052 (4)0.0005 (3)0.0004 (3)0.0001 (2)
Si80.0088 (4)0.0091 (3)0.0058 (4)0.0001 (3)0.0010 (3)0.0002 (2)
O10.0122 (9)0.0153 (8)0.0108 (9)0.0038 (7)0.0001 (7)0.0036 (7)
O20.0112 (8)0.0161 (8)0.0158 (9)0.0022 (9)0.0054 (7)0.0023 (8)
O30.0184 (10)0.0108 (8)0.0131 (9)0.0014 (8)0.0060 (7)0.0022 (7)
O40.0102 (11)0.0136 (8)0.0052 (9)0.0004 (7)0.0003 (7)0.0002 (6)
O50.0110 (11)0.0227 (9)0.0123 (10)0.0015 (8)0.0028 (8)0.0019 (7)
O60.0246 (11)0.0089 (8)0.0093 (9)0.0005 (8)0.0043 (8)0.0015 (7)
O70.0093 (9)0.0119 (8)0.0103 (9)0.0006 (7)0.0028 (7)0.0037 (7)
O80.0112 (11)0.0140 (8)0.0056 (9)0.0031 (7)0.0024 (8)0.0019 (6)
O90.0084 (9)0.0130 (8)0.0126 (9)0.0007 (7)0.0011 (7)0.0006 (7)
O100.0108 (11)0.0047 (8)0.0187 (11)0.0006 (6)0.0009 (8)0.0008 (6)
O110.0161 (10)0.0149 (8)0.0080 (8)0.0061 (8)0.0012 (7)0.0017 (7)
O120.0093 (9)0.0127 (8)0.0116 (9)0.0003 (7)0.0006 (7)0.0009 (7)
O130.0134 (12)0.0055 (8)0.0170 (10)0.0000 (7)0.0011 (8)0.0005 (6)
O140.0193 (10)0.0115 (8)0.0112 (9)0.0006 (8)0.0051 (7)0.0037 (7)
O150.0141 (10)0.0136 (9)0.0174 (9)0.0030 (8)0.0032 (8)0.0020 (7)
O160.0218 (11)0.0125 (8)0.0140 (9)0.0007 (8)0.0052 (8)0.0030 (7)
O170.0097 (9)0.0129 (8)0.0137 (9)0.0001 (7)0.0028 (7)0.0010 (7)
O180.0161 (10)0.0135 (8)0.0112 (9)0.0020 (7)0.0042 (7)0.0047 (7)
O190.0081 (10)0.0256 (10)0.0121 (10)0.0026 (8)0.0009 (8)0.0015 (7)
OW10.0469 (19)0.0475 (15)0.0359 (15)0.0135 (11)0.0092 (12)0.0018 (10)
OW20.0307 (15)0.0438 (12)0.0334 (13)0.0082 (11)0.0079 (11)0.0022 (11)
OW30.056 (2)0.0430 (14)0.0572 (18)0.0081 (12)0.0010 (15)0.0193 (12)
OW40.096 (3)0.066 (2)0.106 (3)0.0153 (16)0.048 (2)0.0523 (17)
Geometric parameters (Å, º) top
Sr1—O172.4997 (16)O3—O182.591 (2)
Sr1—O17i2.4997 (16)O3—O42.602 (2)
Sr1—O12i2.5114 (15)O3—O172.694 (2)
Sr1—O122.5114 (16)O3—OW3ii2.975 (3)
Sr1—O19i2.6962 (19)O4—O18iii2.501 (2)
Sr1—O192.6962 (19)O4—O14iii2.608 (2)
Sr1—O13.1347 (17)O4—O192.717 (3)
Sr1—O1i3.1347 (17)O4—OW3ii3.473 (3)
Sr1—Si43.4272 (7)O5—Na3iv2.498 (2)
Sr1—Si4i3.4272 (7)O5—O62.683 (2)
Sr1—Na2ii3.5038 (14)O5—O72.698 (3)
Sr1—Na23.5254 (14)O5—O82.708 (3)
Sr2—O15iii2.4594 (16)O5—OW2ii2.935 (3)
Sr2—O15iv2.4594 (16)O5—O113.252 (2)
Sr2—O9iii2.5196 (16)O5—O15iv3.252 (3)
Sr2—O9iv2.5196 (16)O5—O9iv3.374 (2)
Sr2—O5v2.6634 (19)O6—O82.614 (2)
Sr2—O52.6634 (19)O6—O102.615 (2)
Sr2—O11v3.4104 (17)O6—O152.638 (2)
Sr2—O113.4104 (17)O6—O16xii2.640 (2)
Sr2—Na4ii3.4980 (12)O6—O72.641 (2)
Sr2—Si3iv3.5261 (7)O6—OW43.263 (4)
Sr2—Si3iii3.5261 (7)O6—OW23.287 (3)
Sr2—Na43.5312 (12)O7—Na5xii2.523 (2)
Na1—O12vi2.329 (2)O7—O82.528 (2)
Na1—O17vii2.344 (2)O7—O10ii2.583 (2)
Na1—O19viii2.414 (2)O7—O11xii2.600 (2)
Na1—O19ix2.513 (2)O7—O92.726 (2)
Na1—OW12.658 (3)O7—O16xii3.289 (2)
Na1—OW1ix2.897 (3)O7—OW2ii3.323 (3)
Na1—O14vi3.062 (2)O7—Na3iv3.584 (2)
Na1—Si4vi3.1651 (13)O8—Na5xii2.601 (2)
Na1—Si8viii3.2597 (13)O8—O112.603 (2)
Na1—Si6vii3.3358 (13)O8—O162.642 (2)
Na1—Na1x3.351 (2)O8—OW4ii3.377 (3)
Na1—Si8ix3.4403 (14)O9—Na3iv2.2606 (19)
Na2—O17viii2.3342 (18)O9—Na4iv2.4065 (18)
Na2—O17vii2.3342 (18)O9—Sr2iv2.5196 (16)
Na2—O122.4099 (18)O9—O11xii2.613 (2)
Na2—O12i2.4099 (18)O9—O10ii2.716 (2)
Na2—OW12.539 (3)O9—OW2iv3.253 (3)
Na2—OW1i2.539 (3)O9—O5iv3.374 (3)
Na2—Si6vii3.3488 (9)O9—O15ii3.419 (3)
Na2—Si6viii3.3488 (9)O9—O9xv3.433 (3)
Na2—Si43.3756 (9)O10—Si3viii1.6223 (15)
Na2—Si4i3.3756 (9)O10—O16xii2.562 (2)
Na2—Na1i3.4569 (13)O10—O7viii2.583 (2)
Na3—O9iv2.2606 (19)O10—O11xiii2.620 (2)
Na3—O152.428 (2)O10—O152.699 (2)
Na3—O5iv2.498 (2)O10—O9viii2.716 (2)
Na3—O52.563 (2)O10—Na5xiii3.473 (2)
Na3—OW2xi2.705 (3)O10—Na4xi3.5474 (18)
Na3—O62.852 (2)O11—Si3iii1.6410 (17)
Na3—OW22.883 (2)O11—O7iii2.600 (2)
Na3—Si53.1283 (13)O11—O9iii2.613 (2)
Na3—Si23.2035 (14)O11—O10vi2.620 (2)
Na3—Si3iv3.3509 (13)O11—O162.678 (2)
Na3—Na3iv3.402 (3)O11—OW43.244 (3)
Na3—O7iv3.584 (2)O12—Na1xiii2.329 (2)
Na4—O9iii2.4065 (18)O12—O132.692 (2)
Na4—O9iv2.4065 (18)O12—O142.704 (2)
Na4—O15xi2.4103 (19)O12—OW1i2.825 (3)
Na4—O15vi2.4103 (19)O12—O19i3.065 (2)
Na4—OW2v2.507 (2)O12—O17viii3.367 (2)
Na4—OW22.507 (2)O12—O12i3.432 (3)
Na4—Si3iv3.3520 (9)O12—Na1i3.835 (2)
Na4—Si3iii3.3520 (9)O13—Si6viii1.6248 (15)
Na4—Si5vi3.4648 (8)O13—O3viii2.556 (2)
Na4—Si5xi3.4648 (8)O13—O142.592 (2)
Na4—Sr2viii3.4980 (12)O13—O18viii2.608 (2)
Na5—OW4vi2.339 (3)O13—O17viii2.724 (2)
Na5—OW32.379 (3)O13—OW43.450 (5)
Na5—O7iii2.523 (2)O13—OW3xiii3.493 (3)
Na5—O18iii2.544 (2)O13—Na5xiii3.710 (2)
Na5—O42.564 (2)O14—Si8xii1.6368 (17)
Na5—O8iii2.601 (2)O14—O4xii2.608 (2)
Na5—Si2iii3.2754 (13)O14—O182.642 (2)
Na5—Si83.2871 (13)O14—O19xii2.677 (3)
Na5—O10vi3.473 (2)O14—OW3xiii3.032 (3)
Na5—O23.568 (2)O14—Na1xiii3.062 (2)
Na5—O13vi3.710 (2)O14—OW1xiii3.293 (3)
Si1—O11.6050 (18)O15—Na4xi2.4103 (19)
Si1—O21.6052 (19)O15—Sr2iv2.4594 (16)
Si1—O31.6098 (17)O15—O16xii2.686 (3)
Si1—O41.6124 (18)O15—OW2xi3.247 (3)
Si2—O51.574 (2)O15—O5iv3.252 (3)
Si2—O61.6346 (16)O15—O15xv3.388 (3)
Si2—O71.6359 (17)O15—O9viii3.419 (3)
Si2—O81.6515 (18)O15—OW2xiii3.446 (3)
Si2—Na5xii3.2754 (13)O16—Si5iii1.6303 (19)
Si3—O91.5758 (18)O16—O10iii2.562 (2)
Si3—O10ii1.6223 (15)O16—O6iii2.640 (2)
Si3—O11xii1.6410 (17)O16—O15iii2.686 (3)
Si3—O71.6477 (16)O16—O7iii3.289 (2)
Si3—Na3iv3.3509 (13)O16—OW4ii3.294 (4)
Si3—Na4iv3.3520 (9)O17—Na2ii2.3342 (18)
Si3—Sr2iv3.5261 (7)O17—Na1xiv2.344 (2)
Si4—O121.5775 (18)O17—O182.672 (2)
Si4—O131.6193 (16)O17—O13ii2.724 (2)
Si4—O11.6318 (17)O17—O17i3.326 (3)
Si4—O141.6385 (16)O17—O12ii3.367 (2)
Si4—Na1xiii3.1651 (13)O17—O19i3.486 (3)
Si5—O151.5743 (18)O18—Si8xii1.6334 (17)
Si5—O101.6226 (15)O18—O4xii2.501 (2)
Si5—O16xii1.6303 (19)O18—Na5xii2.544 (2)
Si5—O61.6488 (16)O18—O13ii2.608 (2)
Si5—Na4xi3.4648 (8)O18—O19xii2.718 (3)
Si5—Sr2iv3.7503 (7)O18—OW3xii3.298 (3)
Si6—O171.5770 (17)O18—OW1xii3.349 (3)
Si6—O13ii1.6248 (15)O19—Na1ii2.414 (2)
Si6—O181.6379 (16)O19—Na1ix2.513 (2)
Si6—O31.6453 (18)O19—O14iii2.677 (3)
Si6—Na1xiv3.3358 (13)O19—O18iii2.718 (3)
Si6—Na2ii3.3488 (9)O19—O12i3.065 (2)
Si7—O161.6023 (17)O19—OW13.183 (3)
Si7—O21.6059 (19)O19—O17i3.486 (3)
Si7—O111.6089 (18)OW1—O12i2.825 (3)
Si7—O81.6184 (18)OW1—Na1ix2.897 (3)
Si8—O191.574 (2)OW1—OW32.978 (4)
Si8—O18iii1.6334 (17)OW1—O14vi3.293 (3)
Si8—O14iii1.6368 (17)OW1—O18iii3.349 (3)
Si8—O41.6521 (19)OW2—Na3xi2.705 (3)
Si8—Na1ii3.2597 (13)OW2—O5viii2.935 (3)
Si8—Na1ix3.4403 (14)OW2—OW43.135 (5)
O1—O122.576 (2)OW2—O15xi3.247 (3)
O1—O22.603 (3)OW2—O9iv3.253 (3)
O1—O42.628 (2)OW2—O7viii3.323 (3)
O1—O142.628 (2)OW2—O15vi3.446 (3)
O1—O132.633 (2)OW2—Sr2viii4.088 (2)
O1—O32.648 (2)OW3—O3viii2.975 (3)
O1—O193.114 (2)OW3—O14vi3.032 (3)
O1—O173.385 (2)OW3—OW4vi3.203 (4)
O1—O183.460 (2)OW3—O18iii3.298 (3)
O2—O112.603 (3)OW3—O4viii3.473 (3)
O2—O82.616 (2)OW3—O13vi3.493 (3)
O2—O162.617 (2)OW4—Na5xiii2.339 (3)
O2—O42.618 (2)OW4—OW3xiii3.203 (4)
O2—O32.656 (2)OW4—O16viii3.294 (4)
O3—O13ii2.556 (2)OW4—O8viii3.377 (3)
O17—Sr1—O17i83.42 (7)Si2—O7—O10ii156.37 (11)
O17—Sr1—O12i168.53 (5)Si3—O7—O10ii37.49 (5)
O17i—Sr1—O12i96.32 (5)Na5xii—O7—O10ii85.72 (7)
O17—Sr1—O1296.32 (5)O8—O7—O10ii138.87 (8)
O17i—Sr1—O12168.53 (5)Si2—O7—O11xii133.78 (9)
O12i—Sr1—O1286.21 (7)Si3—O7—O11xii37.67 (5)
O17—Sr1—O19i84.18 (5)Na5xii—O7—O11xii110.10 (8)
O17i—Sr1—O19i96.57 (5)O8—O7—O11xii151.40 (9)
O12i—Sr1—O19i107.22 (5)O10ii—O7—O11xii60.72 (6)
O12—Sr1—O19i72.03 (5)Si2—O7—O636.13 (5)
O17—Sr1—O1996.57 (5)Si3—O7—O6123.69 (8)
O17i—Sr1—O1984.18 (5)Na5xii—O7—O6108.21 (7)
O12i—Sr1—O1972.03 (5)O8—O7—O660.72 (6)
O12—Sr1—O19107.22 (5)O10ii—O7—O6160.30 (8)
O19i—Sr1—O19179.01 (7)O11xii—O7—O6100.64 (7)
O17—Sr1—O172.87 (5)Si2—O7—O532.11 (6)
O17i—Sr1—O1136.88 (5)Si3—O7—O5111.82 (9)
O12i—Sr1—O1100.23 (5)Na5xii—O7—O5119.57 (7)
O12—Sr1—O152.89 (5)O8—O7—O562.33 (7)
O19i—Sr1—O1115.64 (5)O10ii—O7—O5125.29 (9)
O19—Sr1—O164.03 (5)O11xii—O7—O5130.07 (8)
O17—Sr1—O1i136.88 (5)O6—O7—O560.34 (6)
O17i—Sr1—O1i72.87 (5)Si2—O7—O9107.17 (9)
O12i—Sr1—O1i52.89 (5)Si3—O7—O931.45 (5)
O12—Sr1—O1i100.23 (5)Na5xii—O7—O9146.96 (8)
O19i—Sr1—O1i64.03 (5)O8—O7—O9142.91 (9)
O19—Sr1—O1i115.64 (5)O10ii—O7—O961.46 (6)
O1—Sr1—O1i146.09 (6)O11xii—O7—O958.70 (6)
O17—Sr1—Si480.70 (4)O6—O7—O9104.55 (7)
O17i—Sr1—Si4162.04 (4)O5—O7—O980.70 (7)
O12i—Sr1—Si497.58 (4)Si2—O7—O16xii87.59 (7)
O12—Sr1—Si425.29 (4)Si3—O7—O16xii87.02 (7)
O19i—Sr1—Si490.13 (4)Na5xii—O7—O16xii105.57 (7)
O19—Sr1—Si489.34 (4)O8—O7—O16xii101.19 (7)
O1—Sr1—Si428.35 (3)O10ii—O7—O16xii112.20 (7)
O1i—Sr1—Si4124.87 (3)O11xii—O7—O16xii52.53 (5)
O17—Sr1—Si4i162.04 (4)O6—O7—O16xii51.46 (5)
O17i—Sr1—Si4i80.70 (4)O5—O7—O16xii106.30 (7)
O12i—Sr1—Si4i25.29 (4)O9—O7—O16xii91.40 (6)
O12—Sr1—Si4i97.58 (4)Si2—O7—OW2ii83.34 (8)
O19i—Sr1—Si4i89.34 (4)Si3—O7—OW2ii86.11 (8)
O19—Sr1—Si4i90.13 (4)Na5xii—O7—OW2ii96.34 (6)
O1—Sr1—Si4i124.87 (3)O8—O7—OW2ii84.82 (7)
O1i—Sr1—Si4i28.35 (3)O10ii—O7—OW2ii73.51 (7)
Si4—Sr1—Si4i116.14 (2)O11xii—O7—OW2ii123.77 (7)
O17—Sr1—Na2ii41.71 (4)O6—O7—OW2ii117.19 (8)
O17i—Sr1—Na2ii41.71 (4)O5—O7—OW2ii57.22 (6)
O12i—Sr1—Na2ii136.89 (4)O9—O7—OW2ii71.96 (6)
O12—Sr1—Na2ii136.89 (4)O16xii—O7—OW2ii157.59 (8)
O19i—Sr1—Na2ii90.50 (4)Si2—O7—Na3iv75.10 (7)
O19—Sr1—Na2ii90.50 (4)Si3—O7—Na3iv68.50 (6)
O1—Sr1—Na2ii106.95 (3)Na5xii—O7—Na3iv142.17 (7)
O1i—Sr1—Na2ii106.95 (3)O8—O7—Na3iv104.43 (7)
Si4—Sr1—Na2ii121.928 (12)O10ii—O7—Na3iv85.21 (6)
Si4i—Sr1—Na2ii121.928 (12)O11xii—O7—Na3iv97.05 (6)
O17—Sr1—Na2138.29 (4)O6—O7—Na3iv91.37 (6)
O17i—Sr1—Na2138.29 (4)O5—O7—Na3iv44.12 (5)
O12i—Sr1—Na243.11 (4)O9—O7—Na3iv39.10 (5)
O12—Sr1—Na243.11 (4)O16xii—O7—Na3iv111.87 (6)
O19i—Sr1—Na289.50 (4)OW2ii—O7—Na3iv45.92 (5)
O19—Sr1—Na289.50 (4)Si7—O8—Si2128.88 (13)
O1—Sr1—Na273.05 (3)Si7—O8—O7154.73 (11)
O1i—Sr1—Na273.05 (3)Si2—O8—O739.51 (6)
Si4—Sr1—Na258.072 (12)Si7—O8—Na5xii126.62 (9)
Si4i—Sr1—Na258.072 (12)Si2—O8—Na5xii98.26 (8)
Na2ii—Sr1—Na2180.0O7—O8—Na5xii58.91 (6)
O15iii—Sr2—O15iv87.05 (8)Si7—O8—O1136.11 (6)
O15iii—Sr2—O9iii94.08 (6)Si2—O8—O1197.87 (9)
O15iv—Sr2—O9iii172.08 (5)O7—O8—O11136.33 (9)
O15iii—Sr2—O9iv172.08 (5)Na5xii—O8—O11162.66 (8)
O15iv—Sr2—O9iv94.08 (6)Si7—O8—O6125.70 (9)
O9iii—Sr2—O9iv85.88 (7)Si2—O8—O637.07 (5)
O15iii—Sr2—O5v78.69 (6)O7—O8—O661.78 (6)
O15iv—Sr2—O5v91.38 (6)Na5xii—O8—O6106.69 (7)
O9iii—Sr2—O5v81.17 (5)O11—O8—O690.08 (7)
O9iv—Sr2—O5v109.09 (5)Si7—O8—O235.61 (6)
O15iii—Sr2—O591.38 (6)Si2—O8—O2156.05 (10)
O15iv—Sr2—O578.69 (6)O7—O8—O2163.80 (10)
O9iii—Sr2—O5109.09 (5)Na5xii—O8—O2105.00 (8)
O9iv—Sr2—O581.17 (5)O11—O8—O259.84 (6)
O5v—Sr2—O5166.38 (7)O6—O8—O2127.20 (7)
O15iii—Sr2—O11v138.17 (5)Si7—O8—O1634.67 (5)
O15iv—Sr2—O11v77.46 (5)Si2—O8—O16119.76 (11)
O9iii—Sr2—O11v96.65 (5)O7—O8—O16123.06 (8)
O9iv—Sr2—O11v49.54 (5)Na5xii—O8—O16104.62 (7)
O5v—Sr2—O11v63.34 (5)O11—O8—O1661.40 (7)
O5—Sr2—O11v122.35 (5)O6—O8—O16143.42 (10)
O15iii—Sr2—O1177.46 (5)O2—O8—O1659.68 (6)
O15iv—Sr2—O11138.17 (5)Si7—O8—O599.12 (10)
O9iii—Sr2—O1149.54 (5)Si2—O8—O532.01 (6)
O9iv—Sr2—O1196.65 (5)O7—O8—O561.91 (7)
O5v—Sr2—O11122.35 (5)Na5xii—O8—O5116.38 (7)
O5—Sr2—O1163.34 (5)O11—O8—O575.47 (7)
O11v—Sr2—O11137.29 (5)O6—O8—O560.52 (6)
O15iii—Sr2—Na4ii43.53 (4)O2—O8—O5133.39 (9)
O15iv—Sr2—Na4ii43.53 (4)O16—O8—O588.75 (8)
O9iii—Sr2—Na4ii137.06 (4)Si7—O8—OW4ii96.64 (9)
O9iv—Sr2—Na4ii137.06 (4)Si2—O8—OW4ii101.89 (10)
O5v—Sr2—Na4ii83.19 (4)O7—O8—OW4ii71.15 (8)
O5—Sr2—Na4ii83.19 (4)Na5xii—O8—OW4ii43.71 (7)
O11v—Sr2—Na4ii111.35 (3)O11—O8—OW4ii125.87 (9)
O11—Sr2—Na4ii111.35 (3)O6—O8—OW4ii132.90 (9)
O15iii—Sr2—Si3iv163.23 (4)O2—O8—OW4ii98.86 (9)
O15iv—Sr2—Si3iv80.70 (4)O16—O8—OW4ii65.01 (8)
O9iii—Sr2—Si3iv96.53 (4)O5—O8—OW4ii96.74 (9)
O9iv—Sr2—Si3iv23.47 (4)Si3—O9—Na3iv120.68 (9)
O5v—Sr2—Si3iv90.13 (4)Si3—O9—Na4iv112.99 (9)
O5—Sr2—Si3iv97.35 (4)Na3iv—O9—Na4iv109.69 (7)
O11v—Sr2—Si3iv27.30 (3)Si3—O9—Sr2iv116.97 (9)
O11—Sr2—Si3iv119.27 (3)Na3iv—O9—Sr2iv100.69 (7)
Na4ii—Sr2—Si3iv123.286 (11)Na4iv—O9—Sr2iv91.56 (5)
O15iii—Sr2—Si3iii80.70 (4)Si3—O9—O11xii36.53 (6)
O15iv—Sr2—Si3iii163.23 (4)Na3iv—O9—O11xii147.42 (8)
O9iii—Sr2—Si3iii23.47 (4)Na4iv—O9—O11xii102.46 (7)
O9iv—Sr2—Si3iii96.53 (4)Sr2iv—O9—O11xii83.26 (6)
O5v—Sr2—Si3iii97.35 (4)Si3—O9—O10ii32.41 (5)
O5—Sr2—Si3iii90.13 (4)Na3iv—O9—O10ii116.52 (8)
O11v—Sr2—Si3iii119.27 (3)Na4iv—O9—O10ii87.45 (6)
O11—Sr2—Si3iii27.30 (3)Sr2iv—O9—O10ii140.77 (8)
Na4ii—Sr2—Si3iii123.286 (11)O11xii—O9—O10ii58.86 (6)
Si3iv—Sr2—Si3iii113.43 (2)Si3—O9—O733.07 (5)
O15iii—Sr2—Na4136.47 (4)Na3iv—O9—O791.40 (7)
O15iv—Sr2—Na4136.47 (4)Na4iv—O9—O7143.96 (8)
O9iii—Sr2—Na442.94 (4)Sr2iv—O9—O7113.50 (7)
O9iv—Sr2—Na442.94 (4)O11xii—O9—O758.24 (6)
O5v—Sr2—Na496.81 (4)O10ii—O9—O756.67 (6)
O5—Sr2—Na496.81 (4)Si3—O9—OW2iv137.88 (9)
O11v—Sr2—Na468.65 (3)Na3iv—O9—OW2iv59.89 (6)
O11—Sr2—Na468.65 (3)Na4iv—O9—OW2iv49.89 (5)
Na4ii—Sr2—Na4180.0Sr2iv—O9—OW2iv102.88 (6)
Si3iv—Sr2—Na456.714 (11)O11xii—O9—OW2iv151.23 (8)
Si3iii—Sr2—Na456.714 (11)O10ii—O9—OW2iv106.14 (7)
O12vi—Na1—O17vii161.65 (7)O7—O9—OW2iv137.51 (7)
O12vi—Na1—O19viii103.38 (7)Si3—O9—O5iv139.32 (9)
O17vii—Na1—O19viii94.19 (7)Na3iv—O9—O5iv49.42 (5)
O12vi—Na1—O19ix78.44 (7)Na4iv—O9—O5iv106.53 (6)
O17vii—Na1—O19ix95.21 (7)Sr2iv—O9—O5iv51.27 (4)
O19viii—Na1—O19ix94.33 (7)O11xii—O9—O5iv125.49 (7)
O12vi—Na1—OW193.28 (8)O10ii—O9—O5iv162.56 (7)
O17vii—Na1—OW188.97 (8)O7—O9—O5iv109.35 (7)
O19viii—Na1—OW199.35 (7)OW2iv—O9—O5iv76.73 (6)
O19ix—Na1—OW1165.37 (8)Si3—O9—O15ii82.76 (7)
O12vi—Na1—OW1ix64.38 (7)Na3iv—O9—O15ii101.21 (7)
O17vii—Na1—OW1ix97.30 (8)Na4iv—O9—O15ii44.83 (4)
O19viii—Na1—OW1ix162.58 (8)Sr2iv—O9—O15ii135.81 (6)
O19ix—Na1—OW1ix71.67 (6)O11xii—O9—O15ii97.74 (6)
OW1—Na1—OW1ix93.91 (8)O10ii—O9—O15ii50.63 (5)
O12vi—Na1—O14vi58.33 (5)O7—O9—O15ii103.82 (6)
O17vii—Na1—O14vi138.67 (6)OW2iv—O9—O15ii58.18 (6)
O19viii—Na1—O14vi57.06 (6)O5iv—O9—O15ii134.90 (6)
O19ix—Na1—O14vi114.30 (7)Si3—O9—O9xv127.16 (11)
OW1—Na1—O14vi69.88 (7)Na3iv—O9—O9xv112.14 (9)
OW1ix—Na1—O14vi118.53 (7)Na4iv—O9—O9xv44.50 (4)
O12vi—Na1—Si4vi28.53 (4)Sr2iv—O9—O9xv47.06 (4)
O17vii—Na1—Si4vi164.86 (6)O11xii—O9—O9xv94.34 (7)
O19viii—Na1—Si4vi83.19 (6)O10ii—O9—O9xv120.70 (7)
O19ix—Na1—Si4vi99.85 (6)O7—O9—O9xv150.66 (8)
OW1—Na1—Si4vi76.82 (6)OW2iv—O9—O9xv71.61 (6)
OW1ix—Na1—Si4vi88.94 (6)O5iv—O9—O9xv76.68 (5)
O14vi—Na1—Si4vi30.45 (3)O15ii—O9—O9xv89.05 (3)
O12vi—Na1—Si8viii80.31 (5)Si3viii—O10—Si5140.80 (13)
O17vii—Na1—Si8viii118.03 (6)Si3viii—O10—O16xii153.11 (11)
O19viii—Na1—Si8viii27.36 (5)Si5—O10—O16xii38.13 (6)
O19ix—Na1—Si8viii103.98 (6)Si3viii—O10—O7viii38.18 (5)
OW1—Na1—Si8viii86.24 (6)Si5—O10—O7viii150.13 (12)
OW1ix—Na1—Si8viii144.65 (7)O16xii—O10—O7viii163.86 (10)
O14vi—Na1—Si8viii29.80 (3)Si3viii—O10—O6138.79 (12)
Si4vi—Na1—Si8viii56.63 (2)Si5—O10—O637.28 (6)
O12vi—Na1—Si6vii137.08 (6)O16xii—O10—O661.30 (6)
O17vii—Na1—Si6vii25.33 (4)O7viii—O10—O6117.76 (8)
O19viii—Na1—Si6vii113.78 (6)Si3viii—O10—O11xiii36.85 (6)
O19ix—Na1—Si6vii78.11 (5)Si5—O10—O11xiii143.16 (10)
OW1—Na1—Si6vii100.82 (7)O16xii—O10—O11xiii122.12 (9)
OW1ix—Na1—Si6vii74.30 (6)O7viii—O10—O11xiii59.97 (6)
O14vi—Na1—Si6vii163.84 (5)O6—O10—O11xiii175.40 (10)
Si4vi—Na1—Si6vii162.95 (4)Si3viii—O10—O15109.31 (10)
Si8viii—Na1—Si6vii140.41 (4)Si5—O10—O1531.86 (6)
O12vi—Na1—Na1x90.94 (6)O16xii—O10—O1561.34 (6)
O17vii—Na1—Na1x96.94 (6)O7viii—O10—O15133.62 (10)
O19viii—Na1—Na1x48.41 (5)O6—O10—O1559.51 (6)
O19ix—Na1—Na1x45.92 (5)O11xiii—O10—O15118.61 (8)
OW1—Na1—Na1x147.44 (7)Si3viii—O10—O9viii31.37 (6)
OW1ix—Na1—Na1x116.84 (7)Si5—O10—O9viii109.45 (10)
O14vi—Na1—Na1x85.23 (5)O16xii—O10—O9viii133.99 (9)
Si4vi—Na1—Na1x92.46 (4)O7viii—O10—O9viii61.87 (6)
Si8viii—Na1—Na1x62.71 (4)O6—O10—O9viii116.88 (9)
Si6vii—Na1—Na1x97.82 (5)O11xiii—O10—O9viii58.61 (6)
O12vi—Na1—Si8ix100.11 (6)O15—O10—O9viii78.30 (8)
O17vii—Na1—Si8ix70.88 (5)Si3viii—O10—Na5xiii82.45 (6)
O19viii—Na1—Si8ix101.25 (6)Si5—O10—Na5xiii129.42 (9)
O19ix—Na1—Si8ix24.97 (5)O16xii—O10—Na5xiii117.81 (8)
OW1—Na1—Si8ix152.02 (7)O7viii—O10—Na5xiii46.42 (5)
OW1ix—Na1—Si8ix70.54 (6)O6—O10—Na5xiii95.04 (6)
O14vi—Na1—Si8ix137.84 (5)O11xiii—O10—Na5xiii85.93 (5)
Si4vi—Na1—Si8ix124.26 (4)O15—O10—Na5xiii152.56 (8)
Si8viii—Na1—Si8ix120.06 (4)O9viii—O10—Na5xiii108.20 (6)
Si6vii—Na1—Si8ix53.29 (2)Si3viii—O10—Na4xi69.77 (7)
Na1x—Na1—Si8ix57.35 (3)Si5—O10—Na4xi73.80 (7)
O17viii—Na2—O17vii90.88 (9)O16xii—O10—Na4xi91.32 (6)
O17viii—Na2—O1290.41 (6)O7viii—O10—Na4xi104.47 (7)
O17vii—Na2—O12167.97 (6)O6—O10—Na4xi100.05 (7)
O17viii—Na2—O12i167.97 (6)O11xiii—O10—Na4xi77.21 (6)
O17vii—Na2—O12i90.41 (6)O15—O10—Na4xi42.76 (5)
O12—Na2—O12i90.82 (9)O9viii—O10—Na4xi42.66 (5)
O17viii—Na2—OW198.42 (7)Na5xiii—O10—Na4xi150.86 (5)
O17vii—Na2—OW192.13 (7)Si7—O11—Si3iii135.83 (11)
O12—Na2—OW199.52 (7)Si7—O11—O7iii98.00 (8)
O12i—Na2—OW169.57 (7)Si3iii—O11—O7iii37.85 (5)
O17viii—Na2—OW1i92.13 (7)Si7—O11—O235.89 (6)
O17vii—Na2—OW1i98.42 (7)Si3iii—O11—O2116.62 (9)
O12—Na2—OW1i69.57 (7)O7iii—O11—O284.92 (7)
O12i—Na2—OW1i99.52 (7)Si7—O11—O836.36 (6)
OW1—Na2—OW1i164.97 (11)Si3iii—O11—O8170.67 (10)
O17viii—Na2—Si6vii110.85 (6)O7iii—O11—O8134.04 (8)
O17vii—Na2—Si6vii24.94 (4)O2—O11—O860.32 (6)
O12—Na2—Si6vii145.91 (5)Si7—O11—O9iii142.93 (10)
O12i—Na2—Si6vii73.92 (4)Si3iii—O11—O9iii34.86 (6)
OW1—Na2—Si6vii103.12 (6)O7iii—O11—O9iii63.06 (6)
OW1i—Na2—Si6vii82.86 (6)O2—O11—O9iii147.98 (8)
O17viii—Na2—Si6viii24.94 (4)O8—O11—O9iii144.30 (9)
O17vii—Na2—Si6viii110.85 (6)Si7—O11—O10vi137.21 (10)
O12—Na2—Si6viii73.92 (4)Si3iii—O11—O10vi36.37 (6)
O12i—Na2—Si6viii145.91 (5)O7iii—O11—O10vi59.31 (6)
OW1—Na2—Si6viii82.86 (6)O2—O11—O10vi102.35 (8)
OW1i—Na2—Si6viii103.12 (6)O8—O11—O10vi150.56 (9)
Si6vii—Na2—Si6viii133.78 (5)O9iii—O11—O10vi62.53 (7)
O17viii—Na2—Si475.58 (4)Si7—O11—O1633.41 (6)
O17vii—Na2—Si4163.96 (6)Si3iii—O11—O16110.66 (8)
O12—Na2—Si425.26 (4)O7iii—O11—O1677.07 (6)
O12i—Na2—Si4101.06 (6)O2—O11—O1659.38 (6)
OW1—Na2—Si481.60 (6)O8—O11—O1660.02 (6)
OW1i—Na2—Si490.76 (6)O9iii—O11—O16109.56 (8)
Si6vii—Na2—Si4171.01 (4)O10vi—O11—O16134.70 (8)
Si6viii—Na2—Si453.887 (16)Si7—O11—OW496.77 (10)
O17viii—Na2—Si4i163.96 (6)Si3iii—O11—OW4110.00 (10)
O17vii—Na2—Si4i75.58 (4)O7iii—O11—OW4124.92 (9)
O12—Na2—Si4i101.06 (6)O2—O11—OW477.23 (9)
O12i—Na2—Si4i25.26 (4)O8—O11—OW478.42 (8)
OW1—Na2—Si4i90.76 (6)O9iii—O11—OW4120.29 (9)
OW1i—Na2—Si4i81.60 (6)O10vi—O11—OW474.30 (8)
Si6vii—Na2—Si4i53.887 (16)O16—O11—OW4130.15 (9)
Si6viii—Na2—Si4i171.01 (4)Si7—O11—O579.99 (7)
Si4—Na2—Si4i119.01 (5)Si3iii—O11—O5126.20 (9)
O17viii—Na2—Na193.52 (6)O7iii—O11—O5134.60 (8)
O17vii—Na2—Na142.48 (5)O2—O11—O5112.80 (7)
O12—Na2—Na1149.30 (5)O8—O11—O553.73 (6)
O12i—Na2—Na179.44 (4)O9iii—O11—O591.46 (7)
OW1—Na2—Na149.79 (6)O10vi—O11—O5142.37 (8)
OW1i—Na2—Na1140.51 (6)O16—O11—O577.59 (6)
Si6vii—Na2—Na158.68 (2)OW4—O11—O5100.17 (9)
Si6viii—Na2—Na198.14 (3)Si7—O11—Sr2107.72 (8)
Si4—Na2—Na1128.45 (2)Si3iii—O11—Sr280.28 (7)
Si4i—Na2—Na182.37 (2)O7iii—O11—Sr292.80 (6)
O17viii—Na2—Na1i42.48 (5)O2—O11—Sr2141.87 (7)
O17vii—Na2—Na1i93.52 (6)O8—O11—Sr297.23 (6)
O12—Na2—Na1i79.44 (4)O9iii—O11—Sr247.20 (4)
O12i—Na2—Na1i149.30 (5)O10vi—O11—Sr2109.05 (7)
OW1—Na2—Na1i140.51 (6)O16—O11—Sr282.97 (6)
OW1i—Na2—Na1i49.79 (6)OW4—O11—Sr2131.56 (8)
Si6vii—Na2—Na1i98.14 (3)O5—O11—Sr247.06 (4)
Si6viii—Na2—Na1i58.68 (2)Si4—O12—Na1xiii106.62 (8)
Si4—Na2—Na1i82.37 (2)Si4—O12—Na2114.05 (9)
Si4i—Na2—Na1i128.45 (2)Na1xiii—O12—Na2123.88 (8)
Na1—Na2—Na1i122.38 (6)Si4—O12—Sr1111.86 (8)
O9iv—Na3—O15170.25 (8)Na1xiii—O12—Sr1107.72 (7)
O9iv—Na3—O5iv94.99 (7)Na2—O12—Sr191.49 (6)
O15—Na3—O5iv82.61 (7)Si4—O12—O137.35 (6)
O9iv—Na3—O588.52 (7)Na1xiii—O12—O1129.72 (8)
O15—Na3—O5101.09 (7)Na2—O12—O1105.74 (7)
O5iv—Na3—O595.54 (7)Sr1—O12—O176.07 (6)
O9iv—Na3—OW2xi92.05 (7)Si4—O12—O1333.13 (5)
O15—Na3—OW2xi78.27 (7)Na1xiii—O12—O13112.11 (8)
O5iv—Na3—OW2xi68.54 (6)Na2—O12—O1386.20 (6)
O5—Na3—OW2xi164.07 (8)Sr1—O12—O13133.23 (8)
O9iv—Na3—O6128.58 (7)O1—O12—O1359.93 (6)
O15—Na3—O659.31 (5)Si4—O12—O1433.47 (6)
O5iv—Na3—O6124.48 (7)Na1xiii—O12—O1474.52 (6)
O5—Na3—O659.12 (6)Na2—O12—O14143.58 (8)
OW2xi—Na3—O6130.12 (7)Sr1—O12—O14113.85 (7)
O9iv—Na3—OW277.40 (7)O1—O12—O1459.64 (6)
O15—Na3—OW2102.56 (7)O13—O12—O1457.42 (6)
O5iv—Na3—OW2164.30 (8)Si4—O12—OW1i148.47 (10)
O5—Na3—OW297.94 (6)Na1xiii—O12—OW1i67.59 (7)
OW2xi—Na3—OW297.72 (7)Na2—O12—OW1i57.36 (6)
O6—Na3—OW269.94 (6)Sr1—O12—OW1i99.09 (7)
O9iv—Na3—Si5155.51 (6)O1—O12—OW1i162.68 (9)
O15—Na3—Si529.64 (4)O13—O12—OW1i117.97 (8)
O5iv—Na3—Si5109.22 (6)O14—O12—OW1i135.75 (8)
O5—Na3—Si585.59 (6)Si4—O12—O19i137.86 (9)
OW2xi—Na3—Si5100.04 (6)Na1xiii—O12—O19i53.44 (6)
O6—Na3—Si531.58 (3)Na2—O12—O19i107.03 (7)
OW2—Na3—Si579.91 (6)Sr1—O12—O19i56.78 (5)
O9iv—Na3—Si2112.56 (6)O1—O12—O19i122.05 (7)
O15—Na3—Si277.11 (5)O13—O12—O19i164.19 (8)
O5iv—Na3—Si2108.30 (6)O14—O12—O19i108.71 (7)
O5—Na3—Si229.06 (5)OW1i—O12—O19i65.26 (7)
OW2xi—Na3—Si2155.38 (6)Si4—O12—O17viii85.11 (7)
O6—Na3—Si230.62 (4)Na1xiii—O12—O17viii107.20 (7)
OW2—Na3—Si287.36 (6)Na2—O12—O17viii43.89 (4)
Si5—Na3—Si256.98 (3)Sr1—O12—O17viii134.16 (6)
O9iv—Na3—Si3iv23.86 (4)O1—O12—O17viii102.70 (7)
O15—Na3—Si3iv148.09 (6)O13—O12—O17viii51.99 (5)
O5iv—Na3—Si3iv75.57 (5)O14—O12—O17viii103.41 (6)
O5—Na3—Si3iv103.91 (6)OW1i—O12—O17viii68.46 (6)
OW2xi—Na3—Si3iv72.23 (6)O19i—O12—O17viii133.71 (7)
O6—Na3—Si3iv152.41 (5)Si4—O12—O12i124.00 (10)
OW2—Na3—Si3iv93.34 (6)Na1xiii—O12—O12i128.38 (9)
Si5—Na3—Si3iv169.12 (5)Na2—O12—O12i44.59 (4)
Si2—Na3—Si3iv131.75 (4)Sr1—O12—O12i46.89 (4)
O9iv—Na3—Na3iv92.55 (6)O1—O12—O12i91.66 (7)
O15—Na3—Na3iv92.90 (6)O13—O12—O12i115.63 (8)
O5iv—Na3—Na3iv48.59 (5)O14—O12—O12i150.66 (9)
O5—Na3—Na3iv46.95 (5)OW1i—O12—O12i73.57 (7)
OW2xi—Na3—Na3iv117.13 (7)O19i—O12—O12i80.17 (6)
O6—Na3—Na3iv91.66 (6)O17viii—O12—O12i87.87 (4)
OW2—Na3—Na3iv144.18 (7)Si4—O12—Na1i104.61 (7)
Si5—Na3—Na3iv100.59 (5)Na1xiii—O12—Na1i71.30 (5)
Si2—Na3—Na3iv64.65 (4)Na2—O12—Na1i62.40 (4)
Si3iv—Na3—Na3iv89.89 (4)Sr1—O12—Na1i141.68 (6)
O9iv—Na3—O7iv49.51 (5)O1—O12—Na1i135.34 (7)
O15—Na3—O7iv124.63 (6)O13—O12—Na1i75.90 (5)
O5iv—Na3—O7iv48.75 (5)O14—O12—Na1i102.92 (6)
O5—Na3—O7iv107.41 (6)OW1i—O12—Na1i43.86 (5)
OW2xi—Na3—O7iv61.95 (6)O19i—O12—Na1i102.20 (6)
O6—Na3—O7iv165.95 (6)O17viii—O12—Na1i37.28 (4)
OW2—Na3—O7iv118.73 (6)O12i—O12—Na1i102.28 (4)
Si5—Na3—O7iv154.27 (4)Si4—O13—Si6viii139.85 (14)
Si2—Na3—O7iv135.45 (5)Si4—O13—O3viii152.07 (11)
Si3iv—Na3—O7iv27.23 (3)Si6viii—O13—O3viii38.87 (6)
Na3iv—Na3—O7iv75.01 (5)Si4—O13—O1437.54 (6)
O9iii—Na4—O9iv91.00 (8)Si6viii—O13—O14145.00 (12)
O9iii—Na4—O15xi171.79 (5)O3viii—O13—O14168.19 (10)
O9iv—Na4—O15xi90.43 (6)Si4—O13—O18viii140.93 (12)
O9iii—Na4—O15vi90.43 (6)Si6viii—O13—O18viii37.10 (5)
O9iv—Na4—O15vi171.79 (5)O3viii—O13—O18viii60.21 (6)
O15xi—Na4—O15vi89.30 (9)O14—O13—O18viii116.19 (9)
O9iii—Na4—OW2v82.88 (6)Si4—O13—O136.08 (6)
O9iv—Na4—OW2v105.59 (7)Si6viii—O13—O1145.56 (10)
O15xi—Na4—OW2v88.95 (7)O3viii—O13—O1123.24 (9)
O15vi—Na4—OW2v82.61 (7)O14—O13—O160.38 (6)
O9iii—Na4—OW2105.59 (7)O18viii—O13—O1176.54 (9)
O9iv—Na4—OW282.88 (6)Si4—O13—O1232.17 (6)
O15xi—Na4—OW282.61 (7)Si6viii—O13—O12107.73 (10)
O15vi—Na4—OW288.95 (7)O3viii—O13—O12130.27 (9)
OW2v—Na4—OW2168.15 (11)O14—O13—O1261.53 (6)
O9iii—Na4—Si3iv103.54 (5)O18viii—O13—O12120.62 (9)
O9iv—Na4—Si3iv25.64 (4)O1—O13—O1257.85 (6)
O15xi—Na4—Si3iv74.82 (4)Si4—O13—O17viii109.02 (10)
O15vi—Na4—Si3iv159.95 (5)Si6viii—O13—O17viii31.17 (6)
OW2v—Na4—Si3iv84.90 (5)O3viii—O13—O17viii61.26 (6)
OW2—Na4—Si3iv100.79 (5)O14—O13—O17viii128.19 (10)
O9iii—Na4—Si3iii25.64 (4)O18viii—O13—O17viii60.09 (6)
O9iv—Na4—Si3iii103.54 (5)O1—O13—O17viii121.19 (8)
O15xi—Na4—Si3iii159.95 (5)O12—O13—O17viii76.87 (7)
O15vi—Na4—Si3iii74.82 (4)Si4—O13—OW4115.46 (9)
OW2v—Na4—Si3iii100.79 (5)Si6viii—O13—OW4103.46 (9)
OW2—Na4—Si3iii84.90 (5)O3viii—O13—OW482.23 (8)
Si3iv—Na4—Si3iii123.13 (4)O14—O13—OW486.04 (8)
O9iii—Na4—Si5vi73.08 (4)O18viii—O13—OW479.15 (7)
O9iv—Na4—Si5vi151.58 (5)O1—O13—OW4100.73 (8)
O15xi—Na4—Si5vi108.72 (5)O12—O13—OW4146.64 (8)
O15vi—Na4—Si5vi23.34 (4)O17viii—O13—OW4134.56 (7)
OW2v—Na4—Si5vi95.82 (6)Si4—O13—Na272.39 (7)
OW2—Na4—Si5vi79.16 (5)Si6viii—O13—Na271.40 (7)
Si3iv—Na4—Si5vi176.38 (4)O3viii—O13—Na286.77 (6)
Si3iii—Na4—Si5vi53.256 (16)O14—O13—Na2105.03 (7)
O9iii—Na4—Si5xi151.58 (5)O18viii—O13—Na2101.31 (7)
O9iv—Na4—Si5xi73.08 (4)O1—O13—Na279.61 (6)
O15xi—Na4—Si5xi23.34 (4)O12—O13—Na243.52 (5)
O15vi—Na4—Si5xi108.72 (5)O17viii—O13—Na241.87 (5)
OW2v—Na4—Si5xi79.16 (5)OW4—O13—Na2167.03 (9)
OW2—Na4—Si5xi95.82 (6)Si4—O13—OW3xiii94.27 (8)
Si3iv—Na4—Si5xi53.256 (16)Si6viii—O13—OW3xiii100.42 (8)
Si3iii—Na4—Si5xi176.39 (4)O3viii—O13—OW3xiii113.65 (7)
Si5vi—Na4—Si5xi130.36 (4)O14—O13—OW3xiii57.52 (6)
O9iii—Na4—Sr2viii134.50 (4)O18viii—O13—OW3xiii63.52 (6)
O9iv—Na4—Sr2viii134.50 (4)O1—O13—OW3xiii113.54 (7)
O15xi—Na4—Sr2viii44.65 (4)O12—O13—OW3xiii107.07 (8)
O15vi—Na4—Sr2viii44.65 (4)O17viii—O13—OW3xiii114.29 (8)
OW2v—Na4—Sr2viii84.08 (6)OW4—O13—OW3xiii54.94 (8)
OW2—Na4—Sr2viii84.08 (6)Na2—O13—OW3xiii136.94 (8)
Si3iv—Na4—Sr2viii118.43 (2)Si4—O13—Na5xiii131.39 (8)
Si3iii—Na4—Sr2viii118.43 (2)Si6viii—O13—Na5xiii75.92 (6)
Si5vi—Na4—Sr2viii65.18 (2)O3viii—O13—Na5xiii76.02 (6)
Si5xi—Na4—Sr2viii65.18 (2)O14—O13—Na5xiii93.86 (6)
O9iii—Na4—Sr245.50 (4)O18viii—O13—Na5xiii43.26 (5)
O9iv—Na4—Sr245.50 (4)O1—O13—Na5xiii135.67 (7)
O15xi—Na4—Sr2135.35 (4)O12—O13—Na5xiii143.05 (8)
O15vi—Na4—Sr2135.35 (4)O17viii—O13—Na5xiii103.13 (5)
OW2v—Na4—Sr295.92 (6)OW4—O13—Na5xiii37.92 (5)
OW2—Na4—Sr295.92 (6)Na2—O13—Na5xiii144.55 (5)
Si3iv—Na4—Sr261.57 (2)OW3xiii—O13—Na5xiii38.43 (5)
Si3iii—Na4—Sr261.57 (2)Si8xii—O14—Si4137.10 (11)
Si5vi—Na4—Sr2114.82 (2)Si8xii—O14—O13174.04 (10)
Si5xi—Na4—Sr2114.82 (2)Si4—O14—O1337.02 (6)
Sr2viii—Na4—Sr2180.0Si8xii—O14—O4xii37.75 (6)
OW4vi—Na5—OW385.48 (10)Si4—O14—O4xii169.87 (10)
OW4vi—Na5—O7iii92.14 (11)O13—O14—O4xii148.19 (9)
OW3—Na5—O7iii120.48 (9)Si8xii—O14—O1115.36 (9)
OW4vi—Na5—O18iii106.46 (11)Si4—O14—O136.44 (6)
OW3—Na5—O18iii84.04 (8)O13—O14—O160.58 (6)
O7iii—Na5—O18iii150.77 (7)O4xii—O14—O1133.62 (9)
OW4vi—Na5—O4165.05 (12)Si8xii—O14—O1836.07 (6)
OW3—Na5—O493.26 (9)Si4—O14—O18113.65 (8)
O7iii—Na5—O4101.27 (6)O13—O14—O18141.57 (8)
O18iii—Na5—O458.62 (6)O4xii—O14—O1856.89 (6)
OW4vi—Na5—O8iii86.08 (10)O1—O14—O1882.07 (6)
OW3—Na5—O8iii171.52 (10)Si8xii—O14—O19xii32.77 (6)
O7iii—Na5—O8iii59.10 (6)Si4—O14—O19xii118.47 (10)
O18iii—Na5—O8iii99.10 (7)O13—O14—O19xii143.84 (9)
O4—Na5—O8iii95.10 (6)O4xii—O14—O19xii61.87 (7)
OW4vi—Na5—Si2iii90.86 (10)O1—O14—O19xii119.06 (8)
OW3—Na5—Si2iii149.49 (8)O18—O14—O19xii61.47 (6)
O7iii—Na5—Si2iii29.27 (4)Si8xii—O14—O12113.30 (9)
O18iii—Na5—Si2iii125.80 (5)Si4—O14—O1232.07 (6)
O4—Na5—Si2iii97.59 (5)O13—O14—O1261.05 (6)
O8iii—Na5—Si2iii29.93 (4)O4xii—O14—O12149.29 (9)
OW4vi—Na5—Si8135.41 (11)O1—O14—O1257.75 (6)
OW3—Na5—Si890.65 (8)O18—O14—O12107.76 (7)
O7iii—Na5—Si8126.87 (5)O19xii—O14—O1287.53 (7)
O18iii—Na5—Si829.13 (4)Si8xii—O14—OW3xiii109.13 (8)
O4—Na5—Si829.65 (4)Si4—O14—OW3xiii112.39 (9)
O8iii—Na5—Si895.91 (5)O13—O14—OW3xiii76.33 (7)
Si2iii—Na5—Si8112.45 (3)O4xii—O14—OW3xiii75.60 (7)
OW4vi—Na5—O10vi76.37 (11)O1—O14—OW3xiii130.63 (9)
OW3—Na5—O10vi74.22 (8)O18—O14—OW3xiii130.38 (8)
O7iii—Na5—O10vi47.86 (5)O19xii—O14—OW3xiii109.83 (8)
O18iii—Na5—O10vi157.87 (6)O12—O14—OW3xiii121.04 (8)
O4—Na5—O10vi117.65 (6)Si8xii—O14—Na1xiii81.79 (8)
O8iii—Na5—O10vi103.00 (6)Si4—O14—Na1xiii78.24 (7)
Si2iii—Na5—O10vi75.48 (4)O13—O14—Na1xiii94.68 (7)
Si8—Na5—O10vi144.45 (5)O4xii—O14—Na1xiii106.42 (7)
OW4vi—Na5—O2146.82 (11)O1—O14—Na1xiii102.36 (7)
OW3—Na5—O282.76 (8)O18—O14—Na1xiii102.31 (7)
O7iii—Na5—O267.96 (5)O19xii—O14—Na1xiii49.18 (6)
O18iii—Na5—O2103.04 (6)O12—O14—Na1xiii47.15 (5)
O4—Na5—O247.11 (5)OW3xiii—O14—Na1xiii104.12 (8)
O8iii—Na5—O2104.04 (5)Si8xii—O14—OW1xiii106.32 (9)
Si2iii—Na5—O283.97 (4)Si4—O14—OW1xiii88.49 (8)
Si8—Na5—O275.78 (4)O13—O14—OW1xiii74.51 (7)
O10vi—Na5—O270.59 (4)O4xii—O14—OW1xiii101.37 (7)
OW4vi—Na5—O13vi65.01 (10)O1—O14—OW1xiii124.93 (8)
OW3—Na5—O13vi65.85 (7)O18—O14—OW1xiii141.15 (8)
O7iii—Na5—O13vi156.47 (6)O19xii—O14—OW1xiii80.09 (7)
O18iii—Na5—O13vi44.64 (5)O12—O14—OW1xiii73.84 (7)
O4—Na5—O13vi100.88 (6)OW3xiii—O14—OW1xiii55.99 (8)
O8iii—Na5—O13vi110.99 (6)Na1xiii—O14—OW1xiii49.28 (6)
Si2iii—Na5—O13vi138.41 (5)Si5—O15—Na4xi119.33 (9)
Si8—Na5—O13vi72.93 (4)Si5—O15—Na3100.66 (8)
O10vi—Na5—O13vi125.29 (4)Na4xi—O15—Na3103.18 (7)
O2—Na5—O13vi134.69 (5)Si5—O15—Sr2iv135.65 (10)
O1—Si1—O2108.38 (9)Na4xi—O15—Sr2iv91.82 (6)
O1—Si1—O3110.90 (10)Na3—O15—Sr2iv101.78 (7)
O2—Si1—O3111.39 (9)Si5—O15—O636.00 (6)
O1—Si1—O4109.52 (9)Na4xi—O15—O6141.03 (8)
O2—Si1—O4108.89 (10)Na3—O15—O668.38 (6)
O3—Si1—O4107.73 (9)Sr2iv—O15—O6126.93 (8)
O5—Si2—O6113.50 (10)Si5—O15—O16xii33.70 (6)
O5—Si2—O7114.36 (9)Na4xi—O15—O16xii120.35 (8)
O6—Si2—O7107.70 (9)Na3—O15—O16xii127.49 (8)
O5—Si2—O8114.19 (10)Sr2iv—O15—O16xii104.48 (7)
O6—Si2—O8105.41 (9)O6—O15—O16xii59.43 (6)
O7—Si2—O8100.53 (9)Si5—O15—O1032.96 (5)
O5—Si2—Na352.29 (7)Na4xi—O15—O1087.75 (6)
O6—Si2—Na362.72 (7)Na3—O15—O10100.84 (8)
O7—Si2—Na3119.55 (6)Sr2iv—O15—O10156.86 (9)
O8—Si2—Na3139.88 (7)O6—O15—O1058.65 (6)
O5—Si2—Na5xii133.96 (7)O16xii—O15—O1056.82 (6)
O6—Si2—Na5xii112.55 (8)Si5—O15—OW2xi133.48 (9)
O7—Si2—Na5xii48.95 (6)Na4xi—O15—OW2xi49.98 (5)
O8—Si2—Na5xii51.81 (7)Na3—O15—OW2xi54.67 (6)
Na3—Si2—Na5xii167.16 (4)Sr2iv—O15—OW2xi90.43 (6)
O9—Si3—O10ii116.22 (9)O6—O15—OW2xi117.43 (8)
O9—Si3—O11xii108.61 (9)O16xii—O15—OW2xi163.12 (8)
O10ii—Si3—O11xii106.78 (10)O10—O15—OW2xi106.71 (8)
O9—Si3—O7115.48 (9)Si5—O15—O5iv142.46 (9)
O10ii—Si3—O7104.33 (9)Na4xi—O15—O5iv92.69 (6)
O11xii—Si3—O7104.49 (9)Na3—O15—O5iv49.62 (5)
O9—Si3—Na3iv35.46 (6)Sr2iv—O15—O5iv53.43 (4)
O10ii—Si3—Na3iv112.18 (8)O6—O15—O5iv106.62 (7)
O11xii—Si3—Na3iv136.44 (7)O16xii—O15—O5iv142.51 (8)
O7—Si3—Na3iv84.28 (7)O10—O15—O5iv149.71 (8)
O9—Si3—Na4iv41.37 (6)OW2xi—O15—O5iv53.70 (6)
O10ii—Si3—Na4iv83.22 (7)Si5—O15—O15xv149.81 (12)
O11xii—Si3—Na4iv97.32 (6)Na4xi—O15—O15xv45.35 (4)
O7—Si3—Na4iv153.45 (7)Na3—O15—O15xv108.10 (9)
Na3iv—Si3—Na4iv69.42 (3)Sr2iv—O15—O15xv46.47 (4)
O9—Si3—Sr2iv39.56 (6)O6—O15—O15xv172.59 (7)
O10ii—Si3—Sr2iv144.02 (7)O16xii—O15—O15xv122.99 (9)
O11xii—Si3—Sr2iv72.42 (6)O10—O15—O15xv128.76 (6)
O7—Si3—Sr2iv110.71 (6)OW2xi—O15—O15xv62.54 (6)
Na3iv—Si3—Sr2iv64.72 (2)O5iv—O15—O15xv67.05 (6)
Na4iv—Si3—Sr2iv61.72 (2)Si5—O15—O9viii83.47 (7)
O12—Si4—O13114.71 (9)Na4xi—O15—O9viii44.74 (4)
O12—Si4—O1106.74 (9)Na3—O15—O9viii85.36 (6)
O13—Si4—O1108.17 (10)Sr2iv—O15—O9viii135.97 (6)
O12—Si4—O14114.46 (10)O6—O15—O9viii96.31 (6)
O13—Si4—O14105.44 (9)O16xii—O15—O9viii104.83 (6)
O1—Si4—O14106.95 (9)O10—O15—O9viii51.06 (5)
O12—Si4—Na1xiii44.85 (6)OW2xi—O15—O9viii58.35 (5)
O13—Si4—Na1xiii117.62 (8)O5iv—O15—O9viii111.53 (6)
O1—Si4—Na1xiii133.03 (7)O15xv—O15—O9viii89.80 (3)
O14—Si4—Na1xiii71.30 (7)Si5—O15—OW2xiii93.54 (8)
O12—Si4—Na240.69 (6)Na4xi—O15—OW2xiii46.67 (5)
O13—Si4—Na280.40 (7)Na3—O15—OW2xiii149.53 (8)
O1—Si4—Na299.15 (6)Sr2iv—O15—OW2xiii85.90 (6)
O14—Si4—Na2149.49 (7)O6—O15—OW2xiii129.53 (8)
Na1xiii—Si4—Na279.43 (3)O16xii—O15—OW2xiii77.25 (7)
O12—Si4—Sr142.85 (6)O10—O15—OW2xiii77.02 (7)
O13—Si4—Sr1139.54 (7)OW2xi—O15—OW2xiii96.31 (7)
O1—Si4—Sr165.82 (6)O5iv—O15—OW2xiii123.77 (7)
O14—Si4—Sr1114.64 (6)O15xv—O15—OW2xiii56.73 (6)
Na1xiii—Si4—Sr172.65 (3)O9viii—O15—OW2xiii69.52 (5)
Na2—Si4—Sr162.42 (2)Si7—O16—Si5iii145.32 (12)
O15—Si5—O10115.18 (10)Si7—O16—O10iii173.78 (11)
O15—Si5—O16xii113.91 (10)Si5iii—O16—O10iii37.92 (6)
O10—Si5—O16xii103.94 (10)Si7—O16—O235.40 (6)
O15—Si5—O6109.86 (10)Si5iii—O16—O2148.90 (10)
O10—Si5—O6106.12 (9)O10iii—O16—O2147.11 (9)
O16xii—Si5—O6107.21 (9)Si7—O16—O6iii125.64 (9)
O15—Si5—Na349.70 (7)Si5iii—O16—O6iii36.63 (5)
O10—Si5—Na3108.51 (8)O10iii—O16—O6iii60.33 (6)
O16xii—Si5—Na3147.52 (7)O2—O16—O6iii112.50 (8)
O6—Si5—Na364.93 (7)Si7—O16—O835.07 (5)
O15—Si5—Na4xi37.33 (7)Si5iii—O16—O8145.00 (11)
O10—Si5—Na4xi79.47 (7)O10iii—O16—O8138.71 (9)
O16xii—Si5—Na4xi115.74 (7)O2—O16—O859.66 (6)
O6—Si5—Na4xi133.98 (7)O6iii—O16—O8157.15 (8)
Na3—Si5—Na4xi69.98 (3)Si7—O16—O1133.56 (6)
O15—Si5—Sr2iv27.28 (6)Si5iii—O16—O11111.80 (9)
O10—Si5—Sr2iv136.61 (7)O10iii—O16—O11149.29 (9)
O16xii—Si5—Sr2iv89.28 (6)O2—O16—O1158.88 (6)
O6—Si5—Sr2iv108.98 (6)O6iii—O16—O1198.67 (7)
Na3—Si5—Sr2iv66.19 (3)O8—O16—O1158.58 (6)
Na4xi—Si5—Sr2iv57.84 (2)Si7—O16—O15iii118.58 (9)
O17—Si6—O13ii116.59 (10)Si5iii—O16—O15iii32.40 (6)
O17—Si6—O18112.39 (10)O10iii—O16—O15iii61.84 (7)
O13ii—Si6—O18106.15 (9)O2—O16—O15iii146.08 (9)
O17—Si6—O3113.45 (9)O6iii—O16—O15iii59.38 (6)
O13ii—Si6—O3102.84 (10)O8—O16—O15iii113.62 (8)
O18—Si6—O3104.21 (9)O11—O16—O15iii88.60 (7)
O17—Si6—Na1xiv39.50 (6)Si7—O16—O7iii74.20 (7)
O13ii—Si6—Na1xiv106.93 (8)Si5iii—O16—O7iii79.97 (7)
O18—Si6—Na1xiv80.37 (7)O10iii—O16—O7iii111.67 (7)
O3—Si6—Na1xiv147.27 (7)O2—O16—O7iii71.98 (6)
O17—Si6—Na2ii38.61 (6)O6iii—O16—O7iii51.49 (5)
O13ii—Si6—Na2ii81.22 (7)O8—O16—O7iii107.23 (7)
O18—Si6—Na2ii142.23 (7)O11—O16—O7iii50.40 (5)
O3—Si6—Na2ii110.19 (6)O15iii—O16—O7iii79.95 (6)
Na1xiv—Si6—Na2ii62.28 (2)Si7—O16—OW4ii100.22 (9)
O17—Si6—Sr128.05 (6)Si5iii—O16—OW4ii106.85 (9)
O13ii—Si6—Sr1139.58 (7)O10iii—O16—OW4ii74.08 (7)
O18—Si6—Sr1108.07 (6)O2—O16—OW4ii100.96 (9)
O3—Si6—Sr189.02 (6)O6iii—O16—OW4ii133.69 (8)
Na1xiv—Si6—Sr159.34 (2)O8—O16—OW4ii68.34 (7)
Na2ii—Si6—Sr158.52 (2)O11—O16—OW4ii126.39 (8)
O16—Si7—O2109.30 (9)O15iii—O16—OW4ii106.76 (9)
O16—Si7—O11113.03 (11)O7iii—O16—OW4ii172.93 (9)
O2—Si7—O11108.15 (9)Si7—O16—Sr283.06 (7)
O16—Si7—O8110.26 (9)Si5iii—O16—Sr267.12 (6)
O2—Si7—O8108.45 (10)O10iii—O16—Sr296.63 (7)
O11—Si7—O8107.54 (9)O2—O16—Sr2114.87 (6)
O19—Si8—O18iii115.89 (10)O6iii—O16—Sr282.70 (6)
O19—Si8—O14iii112.97 (10)O8—O16—Sr282.23 (6)
O18iii—Si8—O14iii107.77 (10)O11—O16—Sr256.26 (5)
O19—Si8—O4114.77 (10)O15iii—O16—Sr235.81 (4)
O18iii—Si8—O499.13 (9)O7iii—O16—Sr272.33 (4)
O14iii—Si8—O4104.92 (9)OW4ii—O16—Sr2111.72 (8)
O19—Si8—Na1ii44.83 (7)Si6—O17—Na2ii116.45 (9)
O18iii—Si8—Na1ii127.70 (7)Si6—O17—Na1xiv115.17 (9)
O14iii—Si8—Na1ii68.41 (7)Na2ii—O17—Na1xiv95.27 (7)
O4—Si8—Na1ii132.94 (7)Si6—O17—Sr1134.69 (9)
O19—Si8—Na5136.01 (7)Na2ii—O17—Sr192.85 (6)
O18iii—Si8—Na549.31 (6)Na1xiv—O17—Sr193.96 (6)
O14iii—Si8—Na5110.99 (8)Si6—O17—O1834.53 (6)
O4—Si8—Na550.15 (7)Na2ii—O17—O18143.17 (8)
Na1ii—Si8—Na5176.87 (4)Na1xiv—O17—O1887.02 (7)
O19—Si8—Na1ix42.41 (7)Sr1—O17—O18123.73 (7)
O18iii—Si8—Na1ix77.04 (7)Si6—O17—O334.07 (6)
O14iii—Si8—Na1ix112.92 (7)Na2ii—O17—O3113.50 (7)
O4—Si8—Na1ix141.36 (7)Na1xiv—O17—O3144.73 (8)
Na1ii—Si8—Na1ix59.94 (4)Sr1—O17—O3104.04 (7)
Na5—Si8—Na1ix118.28 (3)O18—O17—O357.74 (6)
Si1—O1—Si4146.18 (11)Si6—O17—O13ii32.23 (5)
Si1—O1—O12161.15 (10)Na2ii—O17—O13ii86.96 (6)
Si4—O1—O1235.91 (6)Na1xiv—O17—O13ii108.28 (8)
Si1—O1—O235.81 (6)Sr1—O17—O13ii157.69 (8)
Si4—O1—O2114.92 (9)O18—O17—O13ii57.80 (6)
O12—O1—O2150.06 (8)O3—O17—O13ii56.30 (6)
Si1—O1—O435.33 (6)Si6—O17—O17i145.79 (11)
Si4—O1—O4167.41 (11)Na2ii—O17—O17i44.56 (5)
O12—O1—O4149.84 (8)Na1xiv—O17—O17i96.73 (8)
O2—O1—O460.05 (6)Sr1—O17—O17i48.29 (4)
Si1—O1—O14111.32 (9)O18—O17—O17i171.25 (6)
Si4—O1—O1436.61 (6)O3—O17—O17i117.94 (8)
O12—O1—O1462.61 (6)O13ii—O17—O17i127.61 (6)
O2—O1—O1488.66 (7)Si6—O17—O12ii83.12 (7)
O4—O1—O14146.23 (8)Na2ii—O17—O12ii45.70 (4)
Si1—O1—O13132.02 (10)Na1xiv—O17—O12ii82.26 (6)
Si4—O1—O1335.76 (6)Sr1—O17—O12ii137.22 (6)
O12—O1—O1362.22 (7)O18—O17—O12ii98.72 (6)
O2—O1—O1396.82 (8)O3—O17—O12ii103.00 (6)
O4—O1—O13131.65 (9)O13ii—O17—O12ii51.13 (5)
O14—O1—O1359.04 (6)O17i—O17—O12ii89.64 (4)
Si1—O1—O334.61 (6)Si6—O17—O173.14 (7)
Si4—O1—O3130.33 (9)Na2ii—O17—O1137.24 (7)
O12—O1—O3126.55 (9)Na1xiv—O17—O1119.09 (7)
O2—O1—O360.75 (6)Sr1—O17—O162.25 (4)
O4—O1—O359.11 (6)O18—O17—O168.51 (6)
O14—O1—O395.94 (7)O3—O17—O150.07 (5)
O13—O1—O3148.27 (8)O13ii—O17—O1103.67 (7)
Si1—O1—O1983.37 (7)O17i—O17—O1102.80 (5)
Si4—O1—O19129.37 (9)O12ii—O17—O1153.07 (7)
O12—O1—O1994.49 (7)Si6—O17—O19i143.28 (9)
O2—O1—O19115.37 (7)Na2ii—O17—O19i97.45 (6)
O4—O1—O1955.72 (6)Na1xiv—O17—O19i43.68 (5)
O14—O1—O19149.01 (9)Sr1—O17—O19i50.31 (4)
O13—O1—O19130.78 (8)O18—O17—O19i108.89 (7)
O3—O1—O1980.84 (6)O3—O17—O19i141.73 (7)
Si1—O1—Sr1116.45 (8)O13ii—O17—O19i151.79 (8)
Si4—O1—Sr185.83 (7)O17i—O17—O19i69.41 (5)
O12—O1—Sr151.04 (5)O12ii—O17—O19i114.87 (6)
O2—O1—Sr1150.36 (7)O1—O17—O19i91.95 (6)
O4—O1—Sr1103.51 (6)Si8xii—O18—Si6136.70 (11)
O14—O1—Sr198.31 (7)Si8xii—O18—O4xii40.72 (6)
O13—O1—Sr1111.52 (7)Si6—O18—O4xii176.78 (10)
O3—O1—Sr189.78 (6)Si8xii—O18—Na5xii101.56 (8)
O19—O1—Sr151.12 (4)Si6—O18—Na5xii121.18 (9)
Si1—O1—O1785.28 (7)O4xii—O18—Na5xii61.09 (6)
Si4—O1—O1795.73 (8)Si8xii—O18—O3132.38 (9)
O12—O1—O1776.21 (6)Si6—O18—O337.99 (6)
O2—O1—O17109.08 (7)O4xii—O18—O3140.73 (9)
O4—O1—O1796.85 (7)Na5xii—O18—O3101.07 (8)
O14—O1—O1780.77 (6)Si8xii—O18—O13ii158.64 (11)
O13—O1—O17131.48 (8)Si6—O18—O13ii36.75 (5)
O3—O1—O1751.29 (6)O4xii—O18—O13ii146.46 (8)
O19—O1—O1773.20 (6)Na5xii—O18—O13ii92.10 (7)
Sr1—O1—O1744.89 (4)O3—O18—O13ii58.90 (6)
Si1—O1—O1874.14 (7)Si8xii—O18—O1436.16 (6)
Si4—O1—O1882.39 (7)Si6—O18—O14115.92 (8)
O12—O1—O1890.16 (6)O4xii—O18—O1460.87 (6)
O2—O1—O1875.49 (6)Na5xii—O18—O14106.81 (7)
O4—O1—O18106.16 (7)O3—O18—O1496.99 (7)
O14—O1—O1849.14 (5)O13ii—O18—O14152.36 (8)
O13—O1—O18107.66 (7)Si8xii—O18—O17104.89 (9)
O3—O1—O1847.97 (5)Si6—O18—O1733.08 (6)
O19—O1—O18115.58 (6)O4xii—O18—O17144.98 (9)
Sr1—O1—O1887.37 (5)Na5xii—O18—O17153.50 (8)
O17—O1—O1845.93 (4)O3—O18—O1761.57 (6)
Si1—O2—Si7145.98 (10)O13ii—O18—O1762.11 (6)
Si1—O2—O11161.40 (11)O14—O18—O1795.67 (7)
Si7—O2—O1135.97 (6)Si8xii—O18—O19xii31.38 (6)
Si1—O2—O135.81 (6)Si6—O18—O19xii116.11 (9)
Si7—O2—O1164.76 (11)O4xii—O18—O19xii62.59 (7)
O11—O2—O1150.90 (8)Na5xii—O18—O19xii119.75 (7)
Si1—O2—O8134.97 (10)O3—O18—O19xii136.81 (8)
Si7—O2—O835.94 (6)O13ii—O18—O19xii127.26 (9)
O11—O2—O859.84 (6)O14—O18—O19xii59.90 (6)
O1—O2—O8129.02 (9)O17—O18—O19xii83.50 (7)
Si1—O2—O16112.40 (8)Si8xii—O18—OW3xii106.71 (9)
Si7—O2—O1635.31 (5)Si6—O18—OW3xii107.97 (8)
O11—O2—O1661.74 (7)O4xii—O18—OW3xii75.24 (7)
O1—O2—O16146.97 (8)Na5xii—O18—OW3xii45.85 (6)
O8—O2—O1660.66 (6)O3—O18—OW3xii119.08 (8)
Si1—O2—O435.65 (6)O13ii—O18—OW3xii71.43 (7)
Si7—O2—O4131.27 (10)O14—O18—OW3xii136.11 (7)
O11—O2—O4125.81 (9)O17—O18—OW3xii122.37 (8)
O1—O2—O460.44 (7)O19xii—O18—OW3xii100.39 (8)
O8—O2—O4154.69 (8)Si8xii—O18—OW1xii88.45 (8)
O16—O2—O498.65 (7)Si6—O18—OW1xii92.03 (8)
Si1—O2—O334.36 (5)O4xii—O18—OW1xii89.82 (7)
Si7—O2—O3114.45 (8)Na5xii—O18—OW1xii97.94 (7)
O11—O2—O3148.65 (8)O3—O18—OW1xii128.73 (8)
O1—O2—O360.45 (6)O13ii—O18—OW1xii73.31 (7)
O8—O2—O3102.70 (7)O14—O18—OW1xii122.04 (8)
O16—O2—O387.19 (7)O17—O18—OW1xii81.19 (7)
O4—O2—O359.13 (6)O19xii—O18—OW1xii62.26 (6)
Si1—O2—Na578.83 (6)OW3xii—O18—OW1xii53.22 (7)
Si7—O2—Na5108.75 (9)Si8xii—O18—O183.05 (7)
O11—O2—Na584.22 (6)Si6—O18—O170.39 (6)
O1—O2—Na586.47 (6)O4xii—O18—O1106.59 (7)
O8—O2—Na5143.05 (8)Na5xii—O18—O1120.09 (7)
O16—O2—Na596.33 (7)O3—O18—O149.38 (5)
O4—O2—Na545.87 (5)O13ii—O18—O1104.33 (6)
O3—O2—Na5104.63 (6)O14—O18—O148.79 (5)
Si1—O3—Si6130.68 (11)O17—O18—O165.56 (5)
Si1—O3—O13ii166.22 (10)O19xii—O18—O194.72 (6)
Si6—O3—O13ii38.30 (6)OW3xii—O18—O1163.56 (9)
Si1—O3—O18105.34 (8)OW1xii—O18—O1141.96 (8)
Si6—O3—O1837.79 (6)Si8—O19—Na1ii107.80 (9)
O13ii—O3—O1860.89 (6)Si8—O19—Na1ix112.62 (10)
Si1—O3—O436.17 (5)Na1ii—O19—Na1ix85.67 (7)
Si6—O3—O4149.30 (10)Si8—O19—O14iii34.26 (6)
O13ii—O3—O4157.35 (9)Na1ii—O19—O14iii73.76 (6)
O18—O3—O4140.80 (8)Na1ix—O19—O14iii113.74 (8)
Si1—O3—O134.49 (6)Si8—O19—Sr1146.93 (10)
Si6—O3—O197.45 (9)Na1ii—O19—Sr187.61 (6)
O13ii—O3—O1135.73 (9)Na1ix—O19—Sr197.24 (7)
O18—O3—O182.65 (7)O14iii—O19—Sr1141.83 (8)
O4—O3—O160.06 (6)Si8—O19—O433.51 (6)
Si1—O3—O234.25 (6)Na1ii—O19—O4124.77 (8)
Si6—O3—O2129.11 (9)Na1ix—O19—O4135.50 (9)
O13ii—O3—O2139.12 (8)O14iii—O19—O457.82 (6)
O18—O3—O291.94 (7)Sr1—O19—O4113.87 (7)
O4—O3—O259.71 (6)Si8—O19—O18iii32.72 (6)
O1—O3—O258.80 (6)Na1ii—O19—O18iii120.14 (8)
Si1—O3—O17112.28 (9)Na1ix—O19—O18iii82.75 (6)
Si6—O3—O1732.48 (5)O14iii—O19—O18iii58.63 (7)
O13ii—O3—O1762.44 (7)Sr1—O19—O18iii152.05 (8)
O18—O3—O1760.69 (6)O4—O19—O18iii54.78 (6)
O4—O3—O17117.41 (8)Si8—O19—O12i148.24 (10)
O1—O3—O1778.63 (7)Na1ii—O19—O12i96.54 (7)
O2—O3—O17132.59 (8)Na1ix—O19—O12i48.12 (5)
Si1—O3—OW3ii110.27 (10)O14iii—O19—O12i160.92 (8)
Si6—O3—OW3ii116.60 (9)Sr1—O19—O12i51.19 (4)
O13ii—O3—OW3ii83.12 (8)O4—O19—O12i137.20 (8)
O18—O3—OW3ii141.99 (8)O18iii—O19—O12i116.59 (7)
O4—O3—OW3ii76.71 (7)Si8—O19—O185.52 (8)
O1—O3—OW3ii135.15 (8)Na1ii—O19—O1138.66 (8)
O2—O3—OW3ii110.15 (9)Na1ix—O19—O1125.98 (7)
O17—O3—OW3ii114.83 (9)O14iii—O19—O1108.70 (8)
Si1—O3—Sr179.15 (7)Sr1—O19—O164.84 (5)
Si6—O3—Sr167.30 (6)O4—O19—O153.04 (6)
O13ii—O3—Sr198.13 (7)O18iii—O19—O192.45 (7)
O18—O3—Sr182.73 (6)O12i—O19—O189.51 (6)
O4—O3—Sr182.00 (6)Si8—O19—OW195.63 (9)
O1—O3—Sr149.94 (5)Na1ii—O19—OW1143.97 (9)
O2—O3—Sr1108.66 (6)Na1ix—O19—OW159.77 (6)
O17—O3—Sr136.31 (4)O14iii—O19—OW1127.14 (9)
OW3ii—O3—Sr1116.38 (7)Sr1—O19—OW187.11 (7)
Si1—O4—Si8128.83 (13)O4—O19—OW189.68 (8)
Si1—O4—O18iii145.59 (10)O18iii—O19—OW168.64 (7)
Si8—O4—O18iii40.16 (6)O12i—O19—OW153.73 (7)
Si1—O4—Na5118.25 (9)O1—O19—OW168.41 (6)
Si8—O4—Na5100.21 (8)Si8—O19—O17i142.27 (9)
O18iii—O4—Na560.29 (6)Na1ii—O19—O17i42.12 (5)
Si1—O4—O336.10 (5)Na1ix—O19—O17i90.50 (6)
Si8—O4—O3112.46 (10)O14iii—O19—O17i109.86 (7)
O18iii—O4—O3151.78 (10)Sr1—O19—O17i45.51 (4)
Na5—O4—O3147.25 (8)O4—O19—O17i133.99 (7)
Si1—O4—O14iii134.43 (10)O18iii—O19—O17i161.79 (7)
Si8—O4—O14iii37.34 (5)O12i—O19—O17i69.14 (6)
O18iii—O4—O14iii62.24 (7)O1—O19—O17i105.14 (7)
Na5—O4—O14iii107.24 (8)OW1—O19—O17i122.04 (8)
O3—O4—O14iii100.45 (7)Na2—OW1—Na183.36 (8)
Si1—O4—O235.46 (6)Na2—OW1—O12i53.07 (7)
Si8—O4—O2161.25 (12)Na1—OW1—O12i88.70 (9)
O18iii—O4—O2141.11 (8)Na2—OW1—Na1ix100.41 (9)
Na5—O4—O287.02 (7)Na1—OW1—Na1ix86.09 (8)
O3—O4—O261.16 (6)O12i—OW1—Na1ix48.03 (5)
O14iii—O4—O2155.43 (8)Na2—OW1—OW3125.43 (10)
Si1—O4—O135.15 (6)Na1—OW1—OW3116.94 (9)
Si8—O4—O1101.76 (10)O12i—OW1—OW3154.35 (10)
O18iii—O4—O1110.71 (8)Na1ix—OW1—OW3129.17 (10)
Na5—O4—O1111.25 (7)Na2—OW1—O19100.54 (9)
O3—O4—O160.83 (6)Na1—OW1—O19134.59 (10)
O14iii—O4—O1128.32 (9)O12i—OW1—O1961.01 (6)
O2—O4—O159.51 (7)Na1ix—OW1—O1948.56 (5)
Si1—O4—O1997.43 (10)OW3—OW1—O1997.59 (9)
Si8—O4—O1931.72 (6)Na2—OW1—O14vi127.48 (9)
O18iii—O4—O1962.63 (7)Na1—OW1—O14vi60.84 (6)
Na5—O4—O19119.05 (7)O12i—OW1—O14vi147.10 (10)
O3—O4—O1989.70 (8)Na1ix—OW1—O14vi112.90 (8)
O14iii—O4—O1960.31 (6)OW3—OW1—O14vi57.57 (7)
O2—O4—O19130.20 (9)O19—OW1—O14vi131.97 (10)
O1—O4—O1971.23 (7)Na2—OW1—O18iii148.69 (9)
Si1—O4—OW3ii90.50 (8)Na1—OW1—O18iii122.10 (9)
Si8—O4—OW3ii91.68 (8)O12i—OW1—O18iii105.47 (7)
O18iii—O4—OW3ii118.32 (8)Na1ix—OW1—O18iii66.86 (6)
Na5—O4—OW3ii127.24 (9)OW3—OW1—O18iii62.51 (8)
O3—O4—OW3ii56.47 (7)O19—OW1—O18iii49.10 (6)
O14iii—O4—OW3ii57.74 (6)O14vi—OW1—O18iii83.32 (8)
O2—O4—OW3ii97.69 (7)Na2—OW1—Sr159.27 (5)
O1—O4—OW3ii116.21 (8)Na1—OW1—Sr1125.43 (9)
O19—O4—OW3ii97.37 (8)O12i—OW1—Sr137.58 (4)
Si2—O5—Na3iv118.80 (10)Na1ix—OW1—Sr165.87 (5)
Si2—O5—Na398.65 (9)OW3—OW1—Sr1117.05 (8)
Na3iv—O5—Na384.46 (7)O19—OW1—Sr141.47 (4)
Si2—O5—Sr2146.19 (10)O14vi—OW1—Sr1172.68 (9)
Na3iv—O5—Sr294.51 (7)O18iii—OW1—Sr189.70 (5)
Na3—O5—Sr289.61 (6)Na4—OW2—Na3xi93.24 (8)
Si2—O5—O633.96 (6)Na4—OW2—Na389.87 (7)
Na3iv—O5—O6120.63 (8)Na3xi—OW2—Na382.28 (7)
Na3—O5—O665.81 (6)Na4—OW2—O5viii98.68 (9)
Sr2—O5—O6132.64 (7)Na3xi—OW2—O5viii52.38 (6)
Si2—O5—O733.54 (6)Na3—OW2—O5viii134.06 (9)
Na3iv—O5—O787.13 (7)Na4—OW2—OW4123.27 (10)
Na3—O5—O7107.94 (7)Na3xi—OW2—OW4137.77 (10)
Sr2—O5—O7162.45 (8)Na3—OW2—OW4114.94 (10)
O6—O5—O758.78 (6)O5viii—OW2—OW497.64 (9)
Si2—O5—O833.80 (6)Na4—OW2—O15xi47.41 (5)
Na3iv—O5—O8138.76 (8)Na3xi—OW2—O15xi47.06 (5)
Na3—O5—O8121.12 (8)Na3—OW2—O15xi92.90 (7)
Sr2—O5—O8115.52 (7)O5viii—OW2—O15xi63.24 (7)
O6—O5—O858.01 (6)OW4—OW2—O15xi151.65 (10)
O7—O5—O855.76 (6)Na4—OW2—O9iv47.23 (5)
Si2—O5—OW2ii98.52 (10)Na3xi—OW2—O9iv84.59 (7)
Na3iv—O5—OW2ii59.07 (6)Na3—OW2—O9iv42.71 (5)
Na3—O5—OW2ii143.52 (9)O5viii—OW2—O9iv126.01 (10)
Sr2—O5—OW2ii93.68 (7)OW4—OW2—O9iv134.89 (9)
O6—O5—OW2ii130.48 (9)O15xi—OW2—O9iv63.47 (6)
O7—O5—OW2ii72.18 (7)Na4—OW2—O6126.29 (9)
O8—O5—OW2ii89.90 (8)Na3xi—OW2—O6116.18 (8)
Si2—O5—O1176.62 (8)Na3—OW2—O654.58 (5)
Na3iv—O5—O11162.81 (8)O5viii—OW2—O6135.01 (9)
Na3—O5—O11101.41 (6)OW4—OW2—O661.03 (8)
Sr2—O5—O1169.60 (5)O15xi—OW2—O6147.26 (8)
O6—O5—O1176.26 (6)O9iv—OW2—O689.73 (7)
O7—O5—O11106.01 (8)Na4—OW2—O7viii148.96 (9)
O8—O5—O1150.80 (5)Na3xi—OW2—O7viii72.13 (6)
OW2ii—O5—O11113.77 (8)Na3—OW2—O7viii114.13 (8)
Si2—O5—O15iv160.58 (10)O5viii—OW2—O7viii50.60 (6)
Na3iv—O5—O15iv47.76 (5)OW4—OW2—O7viii65.65 (7)
Na3—O5—O15iv93.98 (7)O15xi—OW2—O7viii109.04 (7)
Sr2—O5—O15iv47.87 (4)O9iv—OW2—O7viii150.38 (8)
O6—O5—O15iv159.00 (8)O6—OW2—O7viii84.61 (7)
O7—O5—O15iv127.88 (7)Na4—OW2—O15vi44.37 (5)
O8—O5—O15iv142.98 (8)Na3xi—OW2—O15vi100.16 (8)
OW2ii—O5—O15iv63.07 (7)Na3—OW2—O15vi134.14 (8)
O11—O5—O15iv115.29 (7)O5viii—OW2—O15vi69.66 (6)
Si2—O5—O9iv131.74 (9)OW4—OW2—O15vi93.90 (9)
Na3iv—O5—O9iv89.13 (7)O15xi—OW2—O15vi60.73 (6)
Na3—O5—O9iv42.05 (4)O9iv—OW2—O15vi91.60 (7)
Sr2—O5—O9iv47.56 (4)O6—OW2—O15vi143.59 (8)
O6—O5—O9iv98.58 (7)O7viii—OW2—O15vi109.99 (7)
O7—O5—O9iv149.99 (8)Na4—OW2—Sr2viii58.33 (5)
O8—O5—O9iv131.87 (7)Na3xi—OW2—Sr2viii64.14 (5)
OW2ii—O5—O9iv129.68 (9)Na3—OW2—Sr2viii129.88 (8)
O11—O5—O9iv84.80 (6)O5viii—OW2—Sr2viii40.56 (5)
O15iv—O5—O9iv66.70 (6)OW4—OW2—Sr2viii114.93 (8)
Si2—O6—Si5133.86 (10)O15xi—OW2—Sr2viii36.99 (4)
Si2—O6—O837.52 (6)O9iv—OW2—Sr2viii95.47 (6)
Si5—O6—O8154.63 (10)O6—OW2—Sr2viii174.79 (8)
Si2—O6—O10170.34 (10)O7viii—OW2—Sr2viii90.67 (5)
Si5—O6—O1036.60 (5)O15vi—OW2—Sr2viii36.88 (4)
O8—O6—O10148.76 (9)Na5—OW3—O3viii156.99 (12)
Si2—O6—O15110.73 (9)Na5—OW3—OW1112.89 (10)
Si5—O6—O1534.14 (6)O3viii—OW3—OW180.14 (9)
O8—O6—O15147.91 (8)Na5—OW3—O14vi118.65 (11)
O10—O6—O1561.83 (6)O3viii—OW3—O14vi83.60 (7)
Si2—O6—O16xii113.21 (9)OW1—OW3—O14vi66.44 (8)
Si5—O6—O16xii36.16 (6)Na5—OW3—OW4vi46.73 (7)
O8—O6—O16xii118.72 (8)O3viii—OW3—OW4vi139.47 (11)
O10—O6—O16xii58.37 (6)OW1—OW3—OW4vi128.32 (12)
O15—O6—O16xii61.19 (6)O14vi—OW3—OW4vi83.90 (10)
Si2—O6—O736.17 (5)Na5—OW3—O18iii50.10 (6)
Si5—O6—O7102.70 (8)O3viii—OW3—O18iii143.69 (12)
O8—O6—O757.51 (6)OW1—OW3—O18iii64.26 (7)
O10—O6—O7135.18 (8)O14vi—OW3—O18iii88.34 (8)
O15—O6—O794.18 (7)OW4vi—OW3—O18iii74.01 (9)
O16xii—O6—O777.05 (6)Na5—OW3—O4viii145.63 (13)
Si2—O6—O532.54 (6)O3viii—OW3—O4viii46.82 (5)
Si5—O6—O5126.03 (10)OW1—OW3—O4viii90.28 (8)
O8—O6—O561.47 (7)O14vi—OW3—O4viii46.66 (5)
O10—O6—O5147.63 (9)OW4vi—OW3—O4viii99.08 (9)
O15—O6—O592.83 (8)O18iii—OW3—O4viii134.93 (9)
O16xii—O6—O5128.96 (8)Na5—OW3—O13vi75.72 (7)
O7—O6—O560.88 (6)O3viii—OW3—O13vi127.28 (9)
Si2—O6—Na386.65 (8)OW1—OW3—O13vi67.19 (8)
Si5—O6—Na383.49 (7)O14vi—OW3—O13vi46.15 (5)
O8—O6—Na3114.20 (8)OW4vi—OW3—O13vi61.85 (9)
O10—O6—Na392.58 (7)O18iii—OW3—O13vi45.06 (5)
O15—O6—Na352.31 (5)O4viii—OW3—O13vi91.77 (7)
O16xii—O6—Na3113.27 (7)Na5xiii—OW4—OW2105.69 (12)
O7—O6—Na3101.49 (7)Na5xiii—OW4—OW3xiii47.79 (8)
O5—O6—Na355.07 (6)OW2—OW4—OW3xiii125.62 (14)
Si2—O6—OW4112.00 (9)Na5xiii—OW4—O11174.74 (17)
Si5—O6—OW4113.49 (9)OW2—OW4—O1169.71 (9)
O8—O6—OW477.91 (7)OW3xiii—OW4—O11132.51 (10)
O10—O6—OW477.20 (7)Na5xiii—OW4—O6106.64 (13)
O15—O6—OW4132.94 (8)OW2—OW4—O661.80 (9)
O16xii—O6—OW4116.15 (9)OW3xiii—OW4—O680.38 (10)
O7—O6—OW4132.44 (8)O11—OW4—O669.13 (7)
O5—O6—OW4113.45 (8)Na5xiii—OW4—O16viii93.35 (9)
Na3—O6—OW4112.01 (9)OW2—OW4—O16viii74.07 (9)
Si2—O6—OW2113.28 (9)OW3xiii—OW4—O16viii137.74 (11)
Si5—O6—OW297.50 (8)O11—OW4—O16viii87.84 (10)
O8—O6—OW2107.47 (7)O6—OW4—O16viii134.86 (14)
O10—O6—OW273.78 (7)Na5xiii—OW4—O8viii50.21 (6)
O15—O6—OW288.29 (7)OW2—OW4—O8viii75.47 (8)
O16xii—O6—OW2130.94 (7)OW3xiii—OW4—O8viii98.00 (9)
O7—O6—OW2147.34 (8)O11—OW4—O8viii129.01 (13)
O5—O6—OW286.49 (7)O6—OW4—O8viii123.21 (12)
Na3—O6—OW255.48 (6)O16viii—OW4—O8viii46.65 (6)
OW4—O6—OW257.17 (8)Na5xiii—OW4—O1377.07 (11)
Si2—O7—Si3137.95 (11)OW2—OW4—O13170.29 (14)
Si2—O7—Na5xii101.78 (7)OW3xiii—OW4—O1363.21 (9)
Si3—O7—Na5xii119.81 (9)O11—OW4—O13107.90 (9)
Si2—O7—O839.96 (6)O6—OW4—O13126.83 (11)
Si3—O7—O8170.91 (11)O16viii—OW4—O1396.60 (11)
Na5xii—O7—O861.99 (6)O8viii—OW4—O13100.22 (10)
Symmetry codes: (i) x, y, z+1/2; (ii) x, y1, z; (iii) x, y, z+1/2; (iv) x+1, y, z; (v) x+1, y, z+1/2; (vi) x, y+1, z+1/2; (vii) x, y+1, z+1/2; (viii) x, y+1, z; (ix) x, y+1, z+1; (x) x, y+2, z+1; (xi) x+1, y+1, z; (xii) x, y, z1/2; (xiii) x, y+1, z1/2; (xiv) x, y1, z+1/2; (xv) x+1, y, z1/2.
 

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