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Single crystals of Lu5Ba6B9O27 were obtained by cooling from a melt and polycrystals of the borate were prepared using a multi-step solid-state synthesis. The crystal structure was determined from single-crystal X-ray diffraction data. The borate crystallizes in a new structure type in the monoclinic crystal system in space group C2/c, with cell parameters a = 13.0927 (3), b = 9.9970 (2) and c = 20.4884 (4) Å, β = 106.827 (1)°, V = 2566.86 (9) Å3 and Z = 4. It is described as a framework composed of rings consisting of vertex-sharing [BO3] triangles and [LuO6] octahedra. The Ba atoms are in the cavities of the framework. The structure is disordered: one of the B atoms is surrounded by six O atoms with partial occupancies of 0.5. The thermal properties of Lu5Ba6B9O27 were investigated by thermal analysis and high-temperature X-ray powder diffraction. Its thermal expansion is highly anisotropic. The negative expansion (contraction) is along the b axis, i.e. parallel to the planes of the largest number of [BO3] triangles. The coefficient of negative linear expansion ranges from −1.42 (at 20°C) to −5.57 × 10–6 °C–1 (at 1000°C). Thermal deformation of the ac plane is described in terms of the theory of shear deformation of monoclinic crystals. The Lu5Ba6B9O27 sample melts at 1170°C.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S2052520619007443/ra5058sup1.cif
Contains datablocks global, I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S2052520619007443/ra5058Isup2.hkl
Contains datablock I

pdf

Portable Document Format (PDF) file https://doi.org/10.1107/S2052520619007443/ra5058sup3.pdf
Additional tables and figures

CCDC reference: 1917796

Computing details top

(I) top
Crystal data top
B9Ba6Lu5O27F(000) = 3808
Mr = 2244.2Dx = 5.807 Mg m3
Monoclinic, C2/cMo Kα radiation, λ = 0.71069 Å
Hall symbol: -C 2ycCell parameters from 13445 reflections
a = 13.0927 (3) Åθ = 2.1–33.4°
b = 9.9970 (2) ŵ = 28.19 mm1
c = 20.4884 (4) ÅT = 293 K
β = 106.827 (1)°Table, white
V = 2566.86 (9) Å30.08 × 0.06 × 0.05 mm
Z = 4
Data collection top
Bruker Smart APEX II
diffractometer
3199 reflections with I > 3σ(I)
Radiation source: X-ray tubeRint = 0.035
Absorption correction: multi-scan
(Krause et al., 2015)
θmax = 33.4°, θmin = 2.1°
Tmin = 0.820, Tmax = 0.870h = 2018
13445 measured reflectionsk = 1114
4428 independent reflectionsl = 3127
Refinement top
Refinement on F12 constraints
R[F2 > 2σ(F2)] = 0.028Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0001F2)
wR(F2) = 0.030(Δ/σ)max = 0.028
S = 1.18Δρmax = 1.18 e Å3
4428 reflectionsΔρmin = 1.50 e Å3
204 parametersExtinction correction: B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)
0 restraintsExtinction coefficient: 550 (20)
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Lu10.5000.00822 (11)
Lu20.26103 (2)0.00756 (3)0.066162 (14)0.00822 (8)
Lu30.36450 (2)0.24784 (3)0.212196 (14)0.00974 (8)
Ba10.48188 (3)0.37268 (4)0.07664 (2)0.01094 (11)
Ba20.74687 (3)0.11058 (4)0.14021 (2)0.01546 (13)
Ba30.56852 (3)0.25023 (5)0.15923 (3)0.02098 (14)
O10.5840 (4)0.1921 (4)0.0196 (2)0.0131 (15)
O20.2920 (4)0.3363 (5)0.1078 (2)0.0168 (16)
O30.5376 (4)0.0040 (5)0.1119 (2)0.0164 (16)
O40.8365 (4)0.2913 (5)0.0714 (2)0.0167 (9)
O50.6869 (4)0.4256 (5)0.1427 (2)0.0201 (17)
O60.5036 (8)0.3968 (9)0.2771 (5)0.016 (2)*0.5
O70.4537 (7)0.6346 (9)0.2168 (5)0.017 (3)0.5
O80.5466 (4)0.1841 (5)0.1846 (2)0.0167 (9)
O90.3432 (3)0.0938 (4)0.0073 (2)0.0119 (14)
O100.7513 (4)0.1127 (5)0.2366 (2)0.0155 (16)
O110.7363 (4)0.3916 (5)0.2203 (3)0.0162 (16)
O120.4546 (7)0.5346 (10)0.1764 (5)0.016 (3)0.5
O130.1607 (4)0.1799 (5)0.0485 (3)0.0165 (16)
O140.3924 (4)0.0599 (5)0.1533 (3)0.0198 (17)
O150.1249 (4)0.0937 (5)0.0155 (2)0.0167 (9)
B10.50.5202 (11)0.250.012 (2)*
B20.2062 (6)0.3058 (7)0.0547 (4)0.009 (2)
B30.4938 (6)0.0752 (8)0.1502 (4)0.014 (2)
B40.8724 (5)0.2318 (7)0.0222 (4)0.0092 (13)*
B50.7750 (6)0.0274 (8)0.2921 (4)0.012 (2)
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Lu10.00680 (16)0.00809 (17)0.00940 (18)0.00033 (14)0.00176 (14)0.00171 (15)
Lu20.00879 (12)0.00692 (12)0.00902 (13)0.00089 (10)0.00269 (10)0.00025 (10)
Lu30.00939 (12)0.00834 (13)0.01087 (13)0.00005 (10)0.00196 (10)0.00119 (10)
Ba10.01000 (17)0.01309 (19)0.00999 (18)0.00075 (15)0.00330 (15)0.00045 (15)
Ba20.00929 (18)0.0210 (2)0.0145 (2)0.00102 (16)0.00082 (16)0.00691 (17)
Ba30.01235 (19)0.0164 (2)0.0304 (3)0.00111 (17)0.00027 (18)0.00768 (19)
O10.018 (2)0.007 (2)0.016 (3)0.0030 (18)0.007 (2)0.0008 (19)
O20.018 (2)0.022 (3)0.009 (2)0.001 (2)0.002 (2)0.001 (2)
O30.012 (2)0.025 (3)0.012 (2)0.003 (2)0.005 (2)0.009 (2)
O40.0210 (15)0.0136 (14)0.0128 (15)0.0043 (12)0.0004 (12)0.0017 (11)
O50.017 (3)0.033 (3)0.010 (2)0.013 (2)0.005 (2)0.002 (2)
O70.016 (5)0.017 (5)0.019 (5)0.002 (4)0.007 (4)0.009 (4)
O80.0210 (15)0.0136 (14)0.0128 (15)0.0043 (12)0.0004 (12)0.0017 (11)
O90.013 (2)0.013 (2)0.011 (2)0.0040 (18)0.0059 (19)0.0044 (19)
O100.019 (2)0.012 (2)0.015 (2)0.003 (2)0.004 (2)0.005 (2)
O110.016 (2)0.013 (2)0.019 (3)0.001 (2)0.005 (2)0.005 (2)
O120.012 (5)0.025 (5)0.009 (5)0.004 (4)0.001 (4)0.000 (4)
O130.014 (2)0.010 (2)0.023 (3)0.0025 (19)0.000 (2)0.002 (2)
O140.009 (2)0.027 (3)0.021 (3)0.001 (2)0.000 (2)0.007 (2)
O150.0210 (15)0.0136 (14)0.0128 (15)0.0043 (12)0.0004 (12)0.0017 (11)
B20.015 (3)0.005 (3)0.009 (3)0.003 (3)0.007 (3)0.000 (3)
B30.018 (4)0.010 (3)0.013 (4)0.002 (3)0.001 (3)0.002 (3)
B50.009 (3)0.016 (4)0.011 (4)0.003 (3)0.002 (3)0.006 (3)
Geometric parameters (Å, º) top
Lu1—O12.192 (4)O1—B4v1.385 (9)
Lu1—O1i2.192 (4)O2—O9iii2.398 (6)
Lu1—O32.201 (5)O2—O10vii2.885 (8)
Lu1—O3i2.201 (5)O2—O132.380 (6)
Lu1—O92.222 (5)O2—O143.086 (7)
Lu1—O9i2.222 (5)O2—B21.353 (8)
Lu1—B2ii3.250 (7)O2—O6vi3.071 (9)
Lu1—B2iii3.250 (7)O2—O122.950 (10)
Lu1—B33.191 (9)O3—O4iv3.248 (7)
Lu1—B3i3.191 (9)O3—O82.380 (7)
Lu1—B4iv3.259 (7)O3—O93.130 (6)
Lu1—B4v3.259 (7)O3—O9i3.126 (8)
Lu2—O4iv2.230 (5)O3—O103.376 (6)
Lu2—O5iv2.174 (6)O3—O142.383 (8)
Lu2—O92.321 (5)O3—B2ii3.370 (10)
Lu2—O132.257 (5)O3—B31.354 (10)
Lu2—O142.196 (4)O4—O4v3.245 (6)
Lu2—O152.235 (4)O4—O53.071 (8)
Lu2—B23.207 (7)O4—O14viii3.139 (7)
Lu2—B2iii3.316 (8)O4—O15viii3.052 (6)
Lu2—B33.146 (7)O4—O15i2.408 (7)
Lu2—B4iv3.239 (8)O4—B41.365 (10)
Lu2—B4i3.086 (7)O4—B4v2.860 (8)
Lu2—B5vi3.080 (9)O4—O7ii3.322 (10)
Lu3—O22.255 (5)O5—O83.295 (7)
Lu3—O82.682 (5)O5—O10ix2.401 (7)
Lu3—O8vi2.193 (4)O5—O11xii2.387 (7)
Lu3—O10vii2.195 (5)O5—O13viii3.150 (7)
Lu3—O11vii2.225 (5)O5—O14viii2.958 (7)
Lu3—O142.319 (5)O5—O15viii3.111 (7)
Lu3—B13.220 (9)O5—B5ix1.368 (9)
Lu3—B23.343 (7)O5—O6vi3.374 (13)
Lu3—B32.950 (9)O8—O8vi3.251 (8)
Lu3—B3vi3.368 (7)O8—O10ix3.356 (6)
Lu3—B5vii3.196 (8)O8—O11ix3.041 (6)
Lu3—B5vi3.290 (8)O8—O142.297 (7)
Lu3—O62.429 (9)O8—B31.370 (9)
Lu3—O6vi2.242 (10)O8—O63.008 (11)
Lu3—O123.263 (10)O8—O6vi2.423 (11)
Ba1—O12.705 (5)O9—O133.056 (8)
Ba1—O22.763 (5)O9—O13iii2.410 (6)
Ba1—O52.686 (5)O9—O143.182 (7)
Ba1—O82.842 (5)O9—O153.382 (7)
Ba1—O13iii2.751 (4)O9—B23.262 (9)
Ba1—O15viii3.038 (6)O9—B2iii1.416 (8)
Ba1—O15iii2.719 (5)O9—B33.263 (8)
Ba1—B33.317 (8)O10—O112.808 (6)
Ba1—B4v3.326 (8)O10—O11ix2.369 (7)
Ba1—O6vi2.957 (10)O10—B51.383 (9)
Ba1—O122.711 (10)O10—O6ii3.166 (11)
Ba2—O12.875 (4)O10—O6xiii3.302 (12)
Ba2—O2ii2.921 (5)O11—O14ii2.815 (8)
Ba2—O32.869 (5)O11—B5xiii1.381 (9)
Ba2—O42.755 (5)O11—O7xi3.125 (12)
Ba2—O53.249 (5)O13—O143.388 (6)
Ba2—O83.102 (5)O13—O153.011 (7)
Ba2—O9i3.335 (4)O13—B21.382 (8)
Ba2—O102.970 (5)O13—B2iii3.108 (10)
Ba2—O11ix2.801 (5)O14—B31.356 (10)
Ba2—B33.397 (9)O14—B5vi2.870 (10)
Ba2—B53.325 (8)O15—B4i1.389 (9)
Ba2—O7ii2.718 (8)O15—O12iii3.212 (11)
Ba2—O12ii2.712 (9)B1—B5vii3.334 (9)
Ba3—O32.634 (5)B1—B5ix3.334 (9)
Ba3—O4iv3.078 (4)B1—O61.348 (14)
Ba3—O102.816 (4)B1—O6vi1.348 (14)
Ba3—O112.607 (4)B1—O71.378 (13)
Ba3—O13ii2.946 (6)B1—O7vi1.378 (13)
Ba3—B1x3.240 (8)B1—O121.458 (9)
Ba3—B2ii3.223 (9)B1—O12vi1.458 (9)
Ba3—B33.387 (8)B2—B2iii3.011 (12)
Ba3—B4iv3.215 (6)B4—B4v3.091 (10)
Ba3—O7x2.451 (11)B5—O6ii3.188 (13)
Ba3—O7xi2.879 (10)O6—O6vi1.086 (14)
Ba3—O12x2.698 (10)O6—O72.671 (13)
O1—O32.907 (7)O6—O7vi2.437 (13)
O1—O3i3.293 (6)O6—O122.407 (13)
O1—O43.318 (7)O6—O12vi1.674 (13)
O1—O4v2.389 (8)O7—O7vi1.539 (12)
O1—O93.195 (6)O7—O121.299 (14)
O1—O9i3.046 (6)O7—O12vi2.389 (13)
O1—O13iii3.356 (6)O12—O12vi2.902 (13)
O1—O15viii2.369 (7)
O1—Lu1—O1i180.0 (5)Ba2i—O9—O3i52.61 (11)
O1—Lu1—O382.87 (18)Ba2i—O9—O13110.38 (15)
O1—Lu1—O3i97.13 (18)Ba2i—O9—O13iii108.79 (19)
O1—Lu1—O992.72 (17)Ba2i—O9—O14134.18 (18)
O1—Lu1—O9i87.28 (17)Ba2i—O9—O1561.69 (11)
O1—Lu1—B2ii97.90 (17)Ba2i—O9—B2127.71 (17)
O1—Lu1—B2iii82.10 (17)Ba2i—O9—B2iii83.7 (3)
O1—Lu1—B376.6 (2)Ba2i—O9—B3137.9 (2)
O1—Lu1—B3i103.4 (2)O1—O9—O1i89.20 (17)
O1—Lu1—B4iv161.00 (19)O1—O9—O2iii120.3 (2)
O1—Lu1—B4v19.00 (19)O1—O9—O354.71 (14)
O1i—Lu1—O397.13 (18)O1—O9—O3i62.80 (15)
O1i—Lu1—O3i82.87 (18)O1—O9—O13133.51 (19)
O1i—Lu1—O987.28 (17)O1—O9—O13iii72.02 (18)
O1i—Lu1—O9i92.72 (17)O1—O9—O1487.73 (16)
O1i—Lu1—B2ii82.10 (17)O1—O9—O15163.15 (18)
O1i—Lu1—B2iii97.90 (17)O1—O9—B2111.1 (2)
O1i—Lu1—B3103.4 (2)O1—O9—B2iii97.6 (4)
O1i—Lu1—B3i76.6 (2)O1—O9—B364.1 (2)
O1i—Lu1—B4iv19.00 (19)O1i—O9—O2iii111.9 (2)
O1i—Lu1—B4v161.00 (19)O1i—O9—O364.43 (15)
O3—Lu1—O3i180.0 (5)O1i—O9—O3i56.18 (16)
O3—Lu1—O990.08 (17)O1i—O9—O13126.3 (2)
O3—Lu1—O9i89.92 (17)O1i—O9—O13iii145.8 (3)
O3—Lu1—B2ii73.56 (19)O1i—O9—O1490.64 (17)
O3—Lu1—B2iii106.44 (19)O1i—O9—O1575.87 (16)
O3—Lu1—B320.05 (18)O1i—O9—B2149.6 (2)
O3—Lu1—B3i159.95 (18)O1i—O9—B2iii134.4 (4)
O3—Lu1—B4iv79.01 (18)O1i—O9—B385.09 (19)
O3—Lu1—B4v100.99 (18)O2iii—O9—O3172.8 (3)
O3i—Lu1—O989.92 (17)O2iii—O9—O3i83.4 (2)
O3i—Lu1—O9i90.08 (17)O2iii—O9—O1377.1 (2)
O3i—Lu1—B2ii106.44 (19)O2iii—O9—O13iii59.35 (19)
O3i—Lu1—B2iii73.56 (19)O2iii—O9—O14142.8 (3)
O3i—Lu1—B3159.95 (18)O2iii—O9—O1573.46 (18)
O3i—Lu1—B3i20.05 (18)O2iii—O9—B278.0 (2)
O3i—Lu1—B4iv100.99 (18)O2iii—O9—B2iii29.3 (3)
O3i—Lu1—B4v79.01 (18)O2iii—O9—B3161.8 (3)
O9—Lu1—O9i180.0 (5)O3—O9—O3i89.44 (17)
O9—Lu1—B2ii159.11 (19)O3—O9—O13110.1 (2)
O9—Lu1—B2iii20.89 (19)O3—O9—O13iii119.8 (2)
O9—Lu1—B371.60 (18)O3—O9—O1444.35 (15)
O9—Lu1—B3i108.40 (18)O3—O9—O15110.54 (18)
O9—Lu1—B4iv81.71 (17)O3—O9—B2108.3 (2)
O9—Lu1—B4v98.29 (17)O3—O9—B2iii149.7 (4)
O9i—Lu1—B2ii20.89 (19)O3—O9—B324.34 (18)
O9i—Lu1—B2iii159.11 (19)O3i—O9—O13159.55 (18)
O9i—Lu1—B3108.40 (18)O3i—O9—O13iii89.6 (2)
O9i—Lu1—B3i71.60 (18)O3i—O9—O14133.35 (18)
O9i—Lu1—B4iv98.29 (17)O3i—O9—O15112.89 (18)
O9i—Lu1—B4v81.71 (17)O3i—O9—B2153.3 (2)
B2ii—Lu1—B2iii180.0 (5)O3i—O9—B2iii87.3 (4)
B2ii—Lu1—B393.37 (19)O3i—O9—B3112.5 (2)
B2ii—Lu1—B3i86.63 (19)O13—O9—O13iii85.8 (2)
B2ii—Lu1—B4iv82.46 (18)O13—O9—O1465.76 (16)
B2ii—Lu1—B4v97.54 (18)O13—O9—O1555.51 (15)
B2iii—Lu1—B386.63 (19)O13—O9—B225.01 (16)
B2iii—Lu1—B3i93.37 (19)O13—O9—B2iii78.8 (4)
B2iii—Lu1—B4iv97.54 (18)O13—O9—B387.7 (2)
B2iii—Lu1—B4v82.46 (18)O13iii—O9—O14116.1 (2)
B3—Lu1—B3i180.0 (5)O13iii—O9—O15124.8 (2)
B3—Lu1—B4iv84.4 (2)O13iii—O9—B264.4 (2)
B3—Lu1—B4v95.6 (2)O13iii—O9—B2iii30.2 (3)
B3i—Lu1—B4iv95.6 (2)O13iii—O9—B3110.2 (2)
B3i—Lu1—B4v84.4 (2)O14—O9—O1584.71 (17)
B4iv—Lu1—B4v180.0 (5)O14—O9—B268.68 (18)
O4iv—Lu2—O5iv88.4 (2)O14—O9—B2iii134.4 (4)
O4iv—Lu2—O998.20 (18)O14—O9—B324.25 (19)
O4iv—Lu2—O13170.41 (16)O15—O9—B280.07 (19)
O4iv—Lu2—O1490.35 (17)O15—O9—B2iii98.4 (4)
O4iv—Lu2—O1586.26 (17)O15—O9—B3106.1 (2)
O4iv—Lu2—B2166.2 (2)B2—O9—B2iii67.2 (4)
O4iv—Lu2—B2iii115.7 (2)B2—O9—B384.0 (2)
O4iv—Lu2—B382.25 (18)B2iii—O9—B3138.1 (4)
O4iv—Lu2—B4iv19.72 (19)Lu3ii—O10—Ba2102.2 (2)
O4iv—Lu2—B4i62.66 (17)Lu3ii—O10—Ba394.69 (16)
O4iv—Lu2—B5vi94.8 (2)Lu3ii—O10—O2ii50.50 (14)
O5iv—Lu2—O9171.59 (18)Lu3ii—O10—O3119.9 (2)
O5iv—Lu2—O1390.6 (2)Lu3ii—O10—O5xiii106.7 (2)
O5iv—Lu2—O1485.20 (19)Lu3ii—O10—O8xiii40.09 (12)
O5iv—Lu2—O1589.75 (18)Lu3ii—O10—O1151.05 (14)
O5iv—Lu2—B2102.5 (2)Lu3ii—O10—O11ix134.4 (3)
O5iv—Lu2—B2iii155.04 (19)Lu3ii—O10—B5125.0 (4)
O5iv—Lu2—B3104.5 (2)Lu3ii—O10—O6ii50.0 (2)
O5iv—Lu2—B4iv106.5 (2)Lu3ii—O10—O6xiii42.46 (18)
O5iv—Lu2—B4i84.5 (2)Ba2—O10—Ba398.22 (13)
O5iv—Lu2—B5vi22.83 (18)Ba2—O10—O2ii59.85 (14)
O9—Lu2—O1383.74 (18)Ba2—O10—O353.29 (11)
O9—Lu2—O1489.54 (18)Ba2—O10—O5xiii120.1 (2)
O9—Lu2—O1595.84 (17)Ba2—O10—O8xiii129.5 (2)
O9—Lu2—B270.23 (19)Ba2—O10—O11132.9 (2)
O9—Lu2—B2iii20.92 (17)Ba2—O10—O11ix62.10 (17)
O9—Lu2—B371.49 (19)Ba2—O10—B592.3 (4)
O9—Lu2—B4iv80.80 (18)Ba2—O10—O6ii88.3 (2)
O9—Lu2—B4i103.12 (18)Ba2—O10—O6xiii75.8 (2)
O9—Lu2—B5vi149.96 (17)Ba3—O10—O2ii75.59 (15)
O13—Lu2—O1499.08 (17)Ba3—O10—O349.34 (11)
O13—Lu2—O1584.20 (17)Ba3—O10—O5xiii129.5 (3)
O13—Lu2—B221.51 (18)Ba3—O10—O8xiii113.49 (16)
O13—Lu2—B2iii64.5 (2)Ba3—O10—O1155.23 (12)
O13—Lu2—B3107.21 (18)Ba3—O10—O11ix128.4 (2)
O13—Lu2—B4iv155.72 (18)Ba3—O10—B5135.7 (5)
O13—Lu2—B4i107.75 (17)Ba3—O10—O6ii144.5 (3)
O13—Lu2—B5vi87.9 (2)Ba3—O10—O6xiii130.9 (2)
O14—Lu2—O15173.99 (19)O2ii—O10—O372.34 (16)
O14—Lu2—B282.28 (18)O2ii—O10—O5xiii151.0 (3)
O14—Lu2—B2iii100.38 (18)O2ii—O10—O8xiii90.27 (19)
O14—Lu2—B321.2 (2)O2ii—O10—O1175.02 (19)
O14—Lu2—B4iv99.40 (17)O2ii—O10—O11ix119.6 (3)
O14—Lu2—B4i151.29 (18)O2ii—O10—B5143.5 (5)
O14—Lu2—B5vi63.3 (2)O2ii—O10—O6ii77.9 (2)
O15—Lu2—B2102.04 (17)O2ii—O10—O6xiii59.1 (2)
O15—Lu2—B2iii85.57 (18)O3—O10—O5xiii133.4 (2)
O15—Lu2—B3161.4 (2)O3—O10—O8xiii157.6 (2)
O15—Lu2—B4iv78.90 (17)O3—O10—O11102.47 (17)
O15—Lu2—B4i24.12 (17)O3—O10—O11ix86.21 (18)
O15—Lu2—B5vi111.99 (19)O3—O10—B5111.3 (4)
B2—Lu2—B2iii54.9 (2)O3—O10—O6ii139.6 (3)
B2—Lu2—B386.79 (18)O3—O10—O6xiii122.6 (2)
B2—Lu2—B4iv151.0 (2)O5xiii—O10—O8xiii67.48 (18)
B2—Lu2—B4i126.15 (17)O5xiii—O10—O11105.8 (2)
B2—Lu2—B5vi92.3 (2)O5xiii—O10—O11ix60.1 (2)
B2iii—Lu2—B386.25 (19)O5xiii—O10—B529.1 (4)
B2iii—Lu2—B4iv96.63 (19)O5xiii—O10—O6ii73.2 (2)
B2iii—Lu2—B4i100.23 (18)O5xiii—O10—O6xiii92.1 (2)
B2iii—Lu2—B5vi146.23 (19)O8xiii—O10—O1158.30 (14)
B3—Lu2—B4iv85.46 (19)O8xiii—O10—O11ix115.21 (19)
B3—Lu2—B4i143.7 (2)O8xiii—O10—B591.1 (4)
B3—Lu2—B5vi83.7 (2)O8xiii—O10—O6ii43.5 (2)
B4iv—Lu2—B4i58.44 (18)O8xiii—O10—O6xiii53.7 (2)
B4iv—Lu2—B5vi114.5 (2)O11—O10—O11ix165.0 (3)
B4i—Lu2—B5vi106.9 (2)O11—O10—B5134.5 (4)
O2—Lu3—O892.79 (17)O11—O10—O6ii95.3 (2)
O2—Lu3—O8vi171.56 (18)O11—O10—O6xiii93.2 (2)
O2—Lu3—O10vii80.81 (18)O11ix—O10—B531.0 (4)
O2—Lu3—O11vii101.39 (17)O11ix—O10—O6ii85.4 (2)
O2—Lu3—O1484.86 (18)O11ix—O10—O6xiii92.3 (2)
O2—Lu3—B187.00 (14)B5—O10—O6ii78.3 (4)
O2—Lu3—B216.86 (18)B5—O10—O6xiii93.4 (4)
O2—Lu3—B387.6 (2)O6ii—O10—O6xiii19.2 (2)
O2—Lu3—B3vi166.9 (2)Lu3ii—O11—Ba2xiii103.49 (16)
O2—Lu3—B5vii95.40 (19)Lu3ii—O11—Ba399.99 (17)
O2—Lu3—B5vi103.00 (17)Lu3ii—O11—O5x119.6 (3)
O2—Lu3—O6108.8 (3)Lu3ii—O11—O8xiii46.08 (13)
O2—Lu3—O6vi86.2 (3)Lu3ii—O11—O1050.09 (14)
O2—Lu3—O1261.48 (19)Lu3ii—O11—O10xiii129.8 (2)
O8—Lu3—O8vi83.01 (17)Lu3ii—O11—O14ii53.22 (16)
O8—Lu3—O10vii154.05 (16)Lu3ii—O11—B5xiii130.1 (5)
O8—Lu3—O11vii127.08 (16)Lu3ii—O11—O7xi133.3 (3)
O8—Lu3—O1454.12 (15)Ba2xiii—O11—Ba3107.00 (19)
O8—Lu3—B177.90 (13)Ba2xiii—O11—O5x127.8 (2)
O8—Lu3—B2100.25 (18)Ba2xiii—O11—O8xiii63.99 (14)
O8—Lu3—B327.63 (18)Ba2xiii—O11—O1083.65 (17)
O8—Lu3—B3vi75.34 (19)Ba2xiii—O11—O10xiii69.55 (18)
O8—Lu3—B5vii139.07 (16)Ba2xiii—O11—O14ii130.17 (18)
O8—Lu3—B5vi108.43 (18)Ba2xiii—O11—B5xiii99.7 (4)
O8—Lu3—O671.9 (3)Ba2xiii—O11—O7xi54.28 (19)
O8—Lu3—O6vi58.1 (3)Ba3—O11—O5x93.85 (18)
O8—Lu3—O1276.1 (2)Ba3—O11—O8xiii132.41 (19)
O8vi—Lu3—O10vii99.79 (18)Ba3—O11—O1062.55 (13)
O8vi—Lu3—O11vii86.96 (18)Ba3—O11—O10xiii130.0 (2)
O8vi—Lu3—O1498.44 (17)Ba3—O11—O14ii119.3 (2)
O8vi—Lu3—B184.96 (14)Ba3—O11—B5xiii114.5 (4)
O8vi—Lu3—B2171.56 (18)Ba3—O11—O7xi59.49 (19)
O8vi—Lu3—B392.0 (2)O5x—O11—O8xiii129.8 (2)
O8vi—Lu3—B3vi14.90 (19)O5x—O11—O10146.7 (3)
O8vi—Lu3—B5vii83.19 (18)O5x—O11—O10xiii60.6 (2)
O8vi—Lu3—B5vi85.31 (17)O5x—O11—O14ii68.7 (2)
O8vi—Lu3—O663.0 (2)O5x—O11—B5xiii29.6 (4)
O8vi—Lu3—O6vi85.4 (3)O5x—O11—O7xi104.2 (3)
O8vi—Lu3—O12110.27 (19)O8xiii—O11—O1069.92 (16)
O10vii—Lu3—O11vii78.86 (18)O8xiii—O11—O10xiii92.44 (19)
O10vii—Lu3—O14148.38 (16)O8xiii—O11—O14ii71.29 (18)
O10vii—Lu3—B176.68 (15)O8xiii—O11—B5xiii113.1 (4)
O10vii—Lu3—B280.73 (18)O8xiii—O11—O7xi115.0 (2)
O10vii—Lu3—B3168.23 (19)O10—O11—O10xiii152.6 (3)
O10vii—Lu3—B3vi112.3 (2)O10—O11—O14ii101.1 (2)
O10vii—Lu3—B5vii20.78 (16)O10—O11—B5xiii176.2 (4)
O10vii—Lu3—B5vi97.52 (19)O10—O11—O7xi84.5 (2)
O10vii—Lu3—O686.3 (3)O10xiii—O11—O14ii92.3 (2)
O10vii—Lu3—O6vi96.2 (3)O10xiii—O11—B5xiii31.1 (4)
O10vii—Lu3—O1278.8 (2)O10xiii—O11—O7xi84.4 (3)
O11vii—Lu3—O1476.54 (19)O14ii—O11—B5xiii78.1 (4)
O11vii—Lu3—B1152.48 (15)O14ii—O11—O7xi172.9 (3)
O11vii—Lu3—B284.88 (18)B5xiii—O11—O7xi95.9 (5)
O11vii—Lu3—B3101.8 (2)Lu2—O13—Ba1iii101.36 (17)
O11vii—Lu3—B3vi82.01 (18)Lu2—O13—Ba3vii115.0 (2)
O11vii—Lu3—B5vii90.3 (2)Lu2—O13—O1iii145.53 (19)
O11vii—Lu3—B5vi18.7 (2)Lu2—O13—O299.4 (2)
O11vii—Lu3—O6143.7 (3)Lu2—O13—O5iv43.63 (13)
O11vii—Lu3—O6vi170.1 (3)Lu2—O13—O949.02 (13)
O11vii—Lu3—O12153.7 (2)Lu2—O13—O9iii142.0 (3)
O14—Lu3—B1130.68 (15)Lu2—O13—O1439.79 (11)
O14—Lu3—B277.58 (17)Lu2—O13—O1547.58 (12)
O14—Lu3—B326.52 (19)Lu2—O13—B2121.7 (4)
O14—Lu3—B3vi83.62 (18)Lu2—O13—B2iii74.5 (2)
O14—Lu3—B5vii166.61 (19)Ba1iii—O13—Ba3vii116.38 (17)
O14—Lu3—B5vi58.5 (2)Ba1iii—O13—O1iii51.43 (11)
O14—Lu3—O6125.1 (3)Ba1iii—O13—O2142.8 (2)
O14—Lu3—O6vi110.9 (3)Ba1iii—O13—O5iv109.92 (17)
O14—Lu3—O12118.3 (2)Ba1iii—O13—O989.46 (17)
B1—Lu3—B2103.30 (14)Ba1iii—O13—O9iii85.00 (17)
B1—Lu3—B3104.69 (17)Ba1iii—O13—O14139.9 (2)
B1—Lu3—B3vi95.76 (15)Ba1iii—O13—O1556.08 (12)
B1—Lu3—B5vii62.63 (16)Ba1iii—O13—B2114.7 (4)
B1—Lu3—B5vi167.64 (14)Ba1iii—O13—B2iii74.78 (18)
B1—Lu3—O622.5 (2)Ba3vii—O13—O1iii71.04 (14)
B1—Lu3—O6vi19.9 (3)Ba3vii—O13—O281.3 (2)
B1—Lu3—O1225.99 (16)Ba3vii—O13—O5iv73.50 (16)
B2—Lu3—B387.6 (2)Ba3vii—O13—O9153.38 (18)
B2—Lu3—B3vi159.14 (17)Ba3vii—O13—O9iii94.3 (2)
B2—Lu3—B5vii98.97 (18)Ba3vii—O13—O1495.01 (16)
B2—Lu3—B5vi86.27 (17)Ba3vii—O13—O15120.3 (2)
B2—Lu3—O6125.4 (2)Ba3vii—O13—B288.6 (4)
B2—Lu3—O6vi102.9 (3)Ba3vii—O13—B2iii161.5 (2)
B2—Lu3—O1278.13 (19)O1iii—O13—O2115.1 (2)
B3—Lu3—B3vi79.3 (2)O1iii—O13—O5iv118.9 (2)
B3—Lu3—B5vii166.7 (2)O1iii—O13—O9135.1 (2)
B3—Lu3—B5vi83.2 (2)O1iii—O13—O9iii64.89 (16)
B3—Lu3—O699.3 (3)O1iii—O13—O14166.0 (2)
B3—Lu3—O6vi84.8 (3)O1iii—O13—O1598.94 (16)
B3—Lu3—O1297.3 (2)O1iii—O13—B291.5 (4)
B3vi—Lu3—B5vii97.3 (2)O1iii—O13—B2iii110.8 (2)
B3vi—Lu3—B5vi76.16 (18)O2—O13—O5iv106.5 (2)
B3vi—Lu3—O673.3 (2)O2—O13—O981.3 (2)
B3vi—Lu3—O6vi92.1 (3)O2—O13—O9iii60.09 (18)
B3vi—Lu3—O12119.4 (2)O2—O13—O1461.80 (17)
B5vii—Lu3—B5vi108.6 (2)O2—O13—O15144.8 (2)
B5vii—Lu3—O667.5 (3)O2—O13—B229.2 (3)
B5vii—Lu3—O6vi82.5 (3)O2—O13—B2iii81.5 (2)
B5vii—Lu3—O1273.0 (2)O5iv—O13—O992.47 (18)
B5vi—Lu3—O6148.2 (3)O5iv—O13—O9iii163.7 (2)
B5vi—Lu3—O6vi164.6 (3)O5iv—O13—O1453.64 (14)
B5vi—Lu3—O12164.34 (19)O5iv—O13—O1560.59 (16)
O6—Lu3—O6vi26.5 (3)O5iv—O13—B2135.3 (4)
O6—Lu3—O1247.3 (3)O5iv—O13—B2iii118.1 (2)
O6vi—Lu3—O1228.4 (3)O9—O13—O9iii94.2 (2)
O1—Ba1—O2127.03 (14)O9—O13—O1458.91 (15)
O1—Ba1—O578.58 (15)O9—O13—O1567.74 (17)
O1—Ba1—O879.64 (15)O9—O13—B285.9 (4)
O1—Ba1—O13iii75.91 (14)O9—O13—B2iii26.55 (16)
O1—Ba1—O15viii48.29 (14)O9iii—O13—O14118.6 (2)
O1—Ba1—O15iii126.57 (15)O9iii—O13—O15135.7 (3)
O1—Ba1—B368.53 (19)O9iii—O13—B231.0 (3)
O1—Ba1—B4v23.81 (16)O9iii—O13—B2iii71.2 (2)
O1—Ba1—O6vi126.7 (2)O14—O13—O1587.26 (16)
O1—Ba1—O12156.0 (2)O14—O13—B288.9 (3)
O2—Ba1—O5138.10 (15)O14—O13—B2iii82.6 (2)
O2—Ba1—O879.54 (14)O15—O13—B2151.1 (5)
O2—Ba1—O13iii77.11 (15)O15—O13—B2iii78.0 (2)
O2—Ba1—O15viii156.26 (12)B2—O13—B2iii73.1 (4)
O2—Ba1—O15iii80.59 (15)Lu2—O14—Lu3117.9 (2)
O2—Ba1—B372.80 (18)Lu2—O14—O282.22 (16)
O2—Ba1—B4v144.28 (15)Lu2—O14—O398.4 (2)
O2—Ba1—O6vi64.8 (2)Lu2—O14—O4iv45.27 (12)
O2—Ba1—O1265.2 (2)Lu2—O14—O5iv47.09 (13)
O5—Ba1—O873.11 (15)Lu2—O14—O8144.2 (3)
O5—Ba1—O13iii144.78 (17)Lu2—O14—O946.83 (13)
O5—Ba1—O15viii65.50 (14)Lu2—O14—O11vii86.63 (18)
O5—Ba1—O15iii112.19 (15)Lu2—O14—O1341.14 (11)
O5—Ba1—B392.24 (17)Lu2—O14—B3122.9 (5)
O5—Ba1—B4v72.71 (16)Lu2—O14—B5vi73.6 (2)
O5—Ba1—O6vi73.3 (2)Lu3—O14—O246.69 (13)
O5—Ba1—O1280.4 (2)Lu3—O14—O3131.6 (2)
O8—Ba1—O13iii124.56 (13)Lu3—O14—O4iv157.6 (2)
O8—Ba1—O15viii117.29 (14)Lu3—O14—O5iv97.4 (2)
O8—Ba1—O15iii153.55 (16)Lu3—O14—O871.03 (19)
O8—Ba1—B324.15 (15)Lu3—O14—O9115.9 (2)
O8—Ba1—B4v99.84 (16)Lu3—O14—O11vii50.24 (14)
O8—Ba1—O6vi49.3 (2)Lu3—O14—O1378.22 (15)
O8—Ba1—O1283.3 (2)Lu3—O14—B3103.7 (4)
O13iii—Ba1—O15viii79.39 (14)Lu3—O14—B5vi77.9 (2)
O13iii—Ba1—O15iii66.82 (13)O2—O14—O3116.5 (3)
O13iii—Ba1—B3100.48 (16)O2—O14—O4iv126.28 (18)
O13iii—Ba1—B4v74.13 (16)O2—O14—O5iv94.92 (19)
O13iii—Ba1—O6vi141.9 (2)O2—O14—O882.1 (2)
O13iii—Ba1—O12128.0 (2)O2—O14—O969.59 (16)
O15viii—Ba1—O15iii87.18 (15)O2—O14—O11vii71.78 (18)
O15viii—Ba1—B3115.16 (18)O2—O14—O1342.83 (13)
O15viii—Ba1—B4v24.68 (16)O2—O14—B3102.8 (4)
O15viii—Ba1—O6vi138.6 (2)O2—O14—B5vi94.8 (2)
O15viii—Ba1—O12130.0 (2)O3—O14—O4iv70.5 (2)
O15iii—Ba1—B3152.65 (18)O3—O14—O5iv130.9 (3)
O15iii—Ba1—B4v106.49 (17)O3—O14—O861.1 (2)
O15iii—Ba1—O6vi105.9 (2)O3—O14—O966.67 (19)
O15iii—Ba1—O1272.5 (2)O3—O14—O11vii170.7 (3)
B3—Ba1—B4v92.0 (2)O3—O14—O13122.0 (2)
B3—Ba1—O6vi68.4 (2)O3—O14—B328.4 (4)
B3—Ba1—O12101.1 (3)O3—O14—B5vi146.7 (3)
B4v—Ba1—O6vi139.7 (2)O4iv—O14—O5iv60.40 (17)
B4v—Ba1—O12150.5 (2)O4iv—O14—O8131.4 (3)
O6vi—Ba1—O1234.0 (3)O4iv—O14—O965.94 (16)
O1—Ba2—O2ii102.66 (12)O4iv—O14—O11vii108.6 (2)
O1—Ba2—O360.80 (14)O4iv—O14—O1386.39 (15)
O1—Ba2—O472.18 (13)O4iv—O14—B398.7 (4)
O1—Ba2—O567.43 (12)O4iv—O14—B5vi82.1 (2)
O1—Ba2—O872.85 (14)O5iv—O14—O8166.6 (3)
O1—Ba2—O9i58.19 (12)O5iv—O14—O993.71 (17)
O1—Ba2—O10130.65 (13)O5iv—O14—O11vii48.76 (16)
O1—Ba2—O11ix134.33 (15)O5iv—O14—O1359.06 (15)
O1—Ba2—B365.65 (17)O5iv—O14—B3158.4 (5)
O1—Ba2—B5140.86 (17)O5iv—O14—B5vi27.09 (18)
O1—Ba2—O7ii146.9 (2)O8—O14—O997.4 (2)
O1—Ba2—O12ii138.6 (2)O8—O14—O11vii118.3 (3)
O2ii—Ba2—O379.85 (14)O8—O14—O13122.6 (2)
O2ii—Ba2—O4110.77 (15)O8—O14—B332.7 (4)
O2ii—Ba2—O5168.15 (13)O8—O14—B5vi139.8 (3)
O2ii—Ba2—O8122.19 (14)O9—O14—O11vii121.86 (19)
O2ii—Ba2—O9i44.47 (11)O9—O14—O1355.32 (15)
O2ii—Ba2—O1058.63 (14)O9—O14—B381.2 (4)
O2ii—Ba2—O11ix105.27 (13)O9—O14—B5vi119.1 (2)
O2ii—Ba2—B3100.43 (16)O11vii—O14—O1366.73 (16)
O2ii—Ba2—B581.29 (17)O11vii—O14—B3149.6 (5)
O2ii—Ba2—O7ii88.9 (2)O11vii—O14—B5vi28.10 (19)
O2ii—Ba2—O12ii63.0 (2)O13—O14—B3129.8 (4)
O3—Ba2—O4132.96 (13)O13—O14—B5vi73.2 (2)
O3—Ba2—O599.74 (13)B3—O14—B5vi157.1 (5)
O3—Ba2—O846.78 (13)Lu2—O15—Ba1iv94.51 (17)
O3—Ba2—O9i59.94 (13)Lu2—O15—Ba1iii102.94 (18)
O3—Ba2—O1070.62 (13)Lu2—O15—O1iv108.8 (2)
O3—Ba2—O11ix89.55 (14)Lu2—O15—O4iv46.80 (12)
O3—Ba2—B323.04 (17)Lu2—O15—O4i116.1 (2)
O3—Ba2—B582.21 (16)Lu2—O15—O5iv44.33 (13)
O3—Ba2—O7ii152.3 (2)Lu2—O15—O943.05 (12)
O3—Ba2—O12ii140.1 (2)Lu2—O15—O1348.22 (12)
O4—Ba2—O560.86 (15)Lu2—O15—B4i114.8 (4)
O4—Ba2—O8121.09 (14)Lu2—O15—O12iii130.5 (3)
O4—Ba2—O9i94.93 (13)Ba1iv—O15—Ba1iii92.82 (15)
O4—Ba2—O10154.71 (13)Ba1iv—O15—O1iv58.49 (17)
O4—Ba2—O11ix127.43 (13)Ba1iv—O15—O4iv102.39 (18)
O4—Ba2—B3131.82 (16)Ba1iv—O15—O4i117.2 (2)
O4—Ba2—B5143.41 (15)Ba1iv—O15—O5iv51.78 (13)
O4—Ba2—O7ii74.7 (2)Ba1iv—O15—O9133.97 (18)
O4—Ba2—O12ii77.4 (2)Ba1iv—O15—O1382.88 (17)
O5—Ba2—O862.45 (13)Ba1iv—O15—B4i89.4 (4)
O5—Ba2—O9i125.20 (11)Ba1iv—O15—O12iii125.7 (2)
O5—Ba2—O10132.58 (14)Ba1iii—O15—O1iv138.0 (2)
O5—Ba2—O11ix86.55 (13)Ba1iii—O15—O4iv146.5 (2)
O5—Ba2—B381.71 (16)Ba1iii—O15—O4i126.7 (2)
O5—Ba2—B5110.45 (17)Ba1iii—O15—O5iv111.96 (19)
O5—Ba2—O7ii96.3 (2)Ba1iii—O15—O983.50 (15)
O5—Ba2—O12ii119.7 (2)Ba1iii—O15—O1357.10 (13)
O8—Ba2—O9i104.79 (12)Ba1iii—O15—B4i141.9 (4)
O8—Ba2—O1080.72 (13)Ba1iii—O15—O12iii53.6 (2)
O8—Ba2—O11ix61.76 (13)O1iv—O15—O4iv74.28 (18)
O8—Ba2—B323.78 (16)O1iv—O15—O4i60.0 (2)
O8—Ba2—B572.43 (16)O1iv—O15—O5iv75.7 (2)
O8—Ba2—O7ii126.5 (2)O1iv—O15—O9138.4 (2)
O8—Ba2—O12ii148.4 (2)O1iv—O15—O13135.2 (3)
O9i—Ba2—O1090.95 (12)O1iv—O15—B4i31.3 (4)
O9i—Ba2—O11ix137.14 (13)O1iv—O15—O12iii116.3 (3)
O9i—Ba2—B382.23 (16)O4iv—O15—O4i71.83 (18)
O9i—Ba2—B5115.30 (15)O4iv—O15—O5iv59.76 (16)
O9i—Ba2—O7ii125.7 (2)O4iv—O15—O964.40 (15)
O9i—Ba2—O12ii98.1 (2)O4iv—O15—O1395.02 (17)
O10—Ba2—O11ix48.36 (13)O4iv—O15—B4i68.8 (3)
O10—Ba2—B373.34 (16)O4iv—O15—O12iii129.6 (3)
O10—Ba2—B524.56 (16)O4i—O15—O5iv121.2 (2)
O10—Ba2—O7ii81.8 (2)O4i—O15—O9100.8 (2)
O10—Ba2—O12ii77.4 (2)O4i—O15—O13157.5 (3)
O11ix—Ba2—B374.22 (17)O4i—O15—B4i28.8 (4)
O11ix—Ba2—B524.17 (16)O4i—O15—O12iii73.3 (2)
O11ix—Ba2—O7ii68.9 (2)O5iv—O15—O987.22 (16)
O11ix—Ba2—O12ii86.7 (2)O5iv—O15—O1361.91 (17)
B3—Ba2—B575.30 (18)O5iv—O15—B4i99.1 (4)
B3—Ba2—O7ii143.2 (3)O5iv—O15—O12iii165.3 (3)
B3—Ba2—O12ii150.8 (3)O9—O15—O1356.75 (15)
B5—Ba2—O7ii71.0 (3)O9—O15—B4i120.7 (4)
B5—Ba2—O12ii78.3 (3)O9—O15—O12iii88.1 (2)
O7ii—Ba2—O12ii27.7 (3)O13—O15—B4i160.2 (4)
O3—Ba3—O4iv68.80 (13)O13—O15—O12iii104.1 (2)
O3—Ba3—O1076.46 (13)B4i—O15—O12iii95.3 (4)
O3—Ba3—O11134.56 (14)Lu3—B1—Lu3vi64.5 (2)
O3—Ba3—O13ii89.50 (15)Lu3—B1—Ba3xii133.30 (6)
O3—Ba3—B1x146.62 (17)Lu3—B1—Ba3xiv120.82 (5)
O3—Ba3—B2ii69.42 (17)Lu3—B1—B5vii58.33 (17)
O3—Ba3—B321.7 (2)Lu3—B1—B5ix106.5 (3)
O3—Ba3—B4iv74.44 (16)Lu3—B1—O643.6 (4)
O3—Ba3—O7x124.5 (2)Lu3—B1—O6vi34.5 (5)
O3—Ba3—O7xi130.9 (2)Lu3—B1—O7116.7 (4)
O3—Ba3—O12x139.6 (2)Lu3—B1—O7vi162.5 (5)
O4iv—Ba3—O10142.87 (13)Lu3—B1—O1278.7 (5)
O4iv—Ba3—O11154.90 (13)Lu3—B1—O12vi111.3 (6)
O4iv—Ba3—O13ii97.85 (13)Lu3vi—B1—Ba3xii120.82 (5)
O4iv—Ba3—B1x92.34 (10)Lu3vi—B1—Ba3xiv133.30 (6)
O4iv—Ba3—B2ii103.60 (16)Lu3vi—B1—B5vii106.5 (3)
O4iv—Ba3—B367.54 (15)Lu3vi—B1—B5ix58.33 (17)
O4iv—Ba3—B4iv24.94 (17)Lu3vi—B1—O634.5 (5)
O4iv—Ba3—O7x72.9 (2)Lu3vi—B1—O6vi43.6 (4)
O4iv—Ba3—O7xi103.6 (2)Lu3vi—B1—O7162.5 (5)
O4iv—Ba3—O12x72.2 (2)Lu3vi—B1—O7vi116.7 (4)
O10—Ba3—O1162.21 (13)Lu3vi—B1—O12111.3 (6)
O10—Ba3—O13ii94.48 (14)Lu3vi—B1—O12vi78.7 (5)
O10—Ba3—B1x110.74 (11)Ba3xii—B1—Ba3xiv89.8 (3)
O10—Ba3—B2ii75.02 (16)Ba3xii—B1—B5vii131.4 (3)
O10—Ba3—B375.34 (16)Ba3xii—B1—B5ix62.64 (15)
O10—Ba3—B4iv148.47 (17)Ba3xii—B1—O6154.4 (5)
O10—Ba3—O7x119.9 (2)Ba3xii—B1—O6vi113.2 (4)
O10—Ba3—O7xi89.1 (2)Ba3xii—B1—O744.3 (5)
O10—Ba3—O12x136.7 (2)Ba3xii—B1—O7vi62.6 (5)
O11—Ba3—O13ii76.43 (15)Ba3xii—B1—O1255.6 (5)
O11—Ba3—B1x71.04 (13)Ba3xii—B1—O12vi115.2 (6)
O11—Ba3—B2ii81.83 (17)Ba3xiv—B1—B5vii62.64 (15)
O11—Ba3—B3137.46 (16)Ba3xiv—B1—B5ix131.4 (3)
O11—Ba3—B4iv137.56 (17)Ba3xiv—B1—O6113.2 (4)
O11—Ba3—O7x93.6 (2)Ba3xiv—B1—O6vi154.4 (5)
O11—Ba3—O7xi69.2 (2)Ba3xiv—B1—O762.6 (5)
O11—Ba3—O12x85.7 (2)Ba3xiv—B1—O7vi44.3 (5)
O13ii—Ba3—B1x121.17 (16)Ba3xiv—B1—O12115.2 (6)
O13ii—Ba3—B2ii25.39 (15)Ba3xiv—B1—O12vi55.6 (5)
O13ii—Ba3—B3111.21 (18)B5vii—B1—B5ix163.6 (4)
O13ii—Ba3—B4iv73.48 (17)B5vii—B1—O672.0 (5)
O13ii—Ba3—O7x134.8 (2)B5vii—B1—O6vi92.7 (5)
O13ii—Ba3—O7xi138.9 (2)B5vii—B1—O787.2 (5)
O13ii—Ba3—O12x106.1 (2)B5vii—B1—O7vi106.6 (5)
B1x—Ba3—B2ii143.68 (18)B5vii—B1—O1298.9 (4)
B1x—Ba3—B3126.0 (2)B5vii—B1—O12vi82.7 (4)
B1x—Ba3—B4iv100.26 (14)B5ix—B1—O692.7 (5)
B1x—Ba3—O7x23.1 (2)B5ix—B1—O6vi72.0 (5)
B1x—Ba3—O7xi25.2 (2)B5ix—B1—O7106.6 (5)
B1x—Ba3—O12x26.5 (2)B5ix—B1—O7vi87.2 (5)
B2ii—Ba3—B390.3 (2)B5ix—B1—O1282.7 (4)
B2ii—Ba3—B4iv83.57 (19)B5ix—B1—O12vi98.9 (4)
B2ii—Ba3—O7x160.2 (3)O6—B1—O6vi47.5 (7)
B2ii—Ba3—O7xi151.0 (2)O6—B1—O7157.0 (6)
B2ii—Ba3—O12x131.5 (3)O6—B1—O7vi126.7 (5)
B3—Ba3—B4iv82.00 (18)O6—B1—O12118.1 (8)
B3—Ba3—O7x105.7 (3)O6—B1—O12vi73.1 (6)
B3—Ba3—O7xi109.3 (2)O6vi—B1—O7126.7 (5)
B3—Ba3—O12x127.7 (3)O6vi—B1—O7vi157.0 (6)
B4iv—Ba3—O7x87.0 (2)O6vi—B1—O1273.1 (6)
B4iv—Ba3—O7xi119.3 (2)O6vi—B1—O12vi118.1 (8)
B4iv—Ba3—O12x74.8 (2)O7—B1—O7vi67.9 (7)
O7x—Ba3—O7xi32.3 (3)O7—B1—O1254.4 (6)
O7x—Ba3—O12x28.7 (3)O7—B1—O12vi114.7 (8)
O7xi—Ba3—O12x50.6 (3)O7vi—B1—O12114.7 (8)
Lu1—O1—Ba1112.3 (2)O7vi—B1—O12vi54.4 (6)
Lu1—O1—Ba296.72 (15)O12—B1—O12vi168.7 (10)
Lu1—O1—O348.70 (13)Lu1vii—B2—Lu2139.0 (2)
Lu1—O1—O3i41.54 (12)Lu1vii—B2—Lu2iii69.72 (14)
Lu1—O1—O4136.2 (2)Lu1vii—B2—Lu3131.1 (3)
Lu1—O1—O4v103.1 (2)Lu1vii—B2—Ba3vii76.36 (18)
Lu1—O1—O944.02 (12)Lu1vii—B2—O2123.8 (4)
Lu1—O1—O9i46.78 (12)Lu1vii—B2—O3vii38.78 (12)
Lu1—O1—O13iii83.67 (15)Lu1vii—B2—O9138.5 (2)
Lu1—O1—O15viii151.9 (2)Lu1vii—B2—O9iii34.0 (3)
Lu1—O1—B4v130.0 (4)Lu1vii—B2—O13102.7 (4)
Ba1—O1—Ba298.86 (15)Lu1vii—B2—O13iii108.2 (2)
Ba1—O1—O386.93 (18)Lu1vii—B2—B2iii115.0 (3)
Ba1—O1—O3i123.50 (17)Lu2—B2—Lu2iii125.1 (3)
Ba1—O1—O4103.53 (16)Lu2—B2—Lu372.35 (14)
Ba1—O1—O4v132.2 (2)Lu2—B2—Ba3vii86.43 (19)
Ba1—O1—O972.13 (15)Lu2—B2—O292.6 (4)
Ba1—O1—O9i150.2 (2)Lu2—B2—O3vii132.9 (3)
Ba1—O1—O13iii52.65 (12)Lu2—B2—O942.03 (13)
Ba1—O1—O15viii73.22 (18)Lu2—B2—O9iii142.2 (4)
Ba1—O1—B4v104.1 (4)Lu2—B2—O1336.8 (3)
Ba2—O1—O359.49 (12)Lu2—B2—O13iii86.4 (2)
Ba2—O1—O3i127.14 (17)Lu2—B2—B2iii64.4 (2)
Ba2—O1—O452.23 (11)Lu2iii—B2—Lu3130.4 (2)
Ba2—O1—O4v108.0 (2)Lu2iii—B2—Ba3vii145.1 (2)
Ba2—O1—O9120.68 (19)Lu2iii—B2—O2101.9 (4)
Ba2—O1—O9i68.49 (12)Lu2iii—B2—O3vii99.0 (2)
Ba2—O1—O13iii147.8 (2)Lu2iii—B2—O984.3 (2)
Ba2—O1—O15viii109.93 (18)Lu2iii—B2—O9iii35.8 (3)
Ba2—O1—B4v110.6 (3)Lu2iii—B2—O13129.1 (5)
O3—O1—O3i90.24 (17)Lu2iii—B2—O13iii40.98 (13)
O3—O1—O4111.71 (17)Lu2iii—B2—B2iii60.7 (2)
O3—O1—O4v140.8 (2)Lu3—B2—Ba3vii68.77 (15)
O3—O1—O961.51 (15)Lu3—B2—O228.9 (3)
O3—O1—O9i63.29 (17)Lu3—B2—O3vii92.7 (2)
O3—O1—O13iii99.98 (19)Lu3—B2—O990.35 (19)
O3—O1—O15viii156.2 (3)Lu3—B2—O9iii144.8 (4)
O3—O1—B4v166.7 (4)Lu3—B2—O1393.5 (4)
O3i—O1—O4129.3 (2)Lu3—B2—O13iii110.6 (2)
O3i—O1—O4v67.57 (18)Lu3—B2—B2iii113.0 (3)
O3i—O1—O957.58 (14)Ba3vii—B2—O289.9 (5)
O3i—O1—O9i59.02 (14)Ba3vii—B2—O3vii47.03 (15)
O3i—O1—O13iii72.55 (14)Ba3vii—B2—O9128.5 (2)
O3i—O1—O15viii111.5 (2)Ba3vii—B2—O9iii110.3 (5)
O3i—O1—B4v89.8 (4)Ba3vii—B2—O1366.0 (4)
O4—O1—O4v67.04 (18)Ba3vii—B2—O13iii172.6 (3)
O4—O1—O9171.7 (2)Ba3vii—B2—B2iii146.8 (3)
O4—O1—O9i90.01 (17)O2—B2—O3vii93.9 (4)
O4—O1—O13iii139.66 (18)O2—B2—O992.1 (4)
O4—O1—O15viii62.31 (17)O2—B2—O9iii120.0 (6)
O4—O1—B4v58.9 (3)O2—B2—O13120.9 (6)
O4v—O1—O9121.2 (2)O2—B2—O13iii92.2 (5)
O4v—O1—O9i77.5 (2)O2—B2—B2iii106.0 (5)
O4v—O1—O13iii103.2 (2)O3vii—B2—O9172.4 (3)
O4v—O1—O15viii60.8 (2)O3vii—B2—O9iii67.9 (4)
O4v—O1—B4v29.5 (4)O3vii—B2—O13103.7 (5)
O9—O1—O9i90.80 (16)O3vii—B2—O13iii139.8 (3)
O9—O1—O13iii43.08 (13)O3vii—B2—B2iii153.7 (3)
O9—O1—O15viii121.6 (2)O9—B2—O9iii112.8 (5)
O9—O1—B4v128.7 (3)O9—B2—O1369.1 (4)
O9i—O1—O13iii127.38 (17)O9—B2—O13iii44.38 (17)
O9i—O1—O15viii136.0 (3)O9—B2—B2iii25.70 (17)
O9i—O1—B4v105.6 (4)O9iii—B2—O13118.9 (5)
O13iii—O1—O15viii78.55 (18)O9iii—B2—O13iii74.7 (4)
O13iii—O1—B4v92.8 (3)O9iii—B2—B2iii87.1 (4)
O15viii—O1—B4v31.4 (4)O13—B2—O13iii106.9 (5)
Lu3—O2—Ba196.38 (16)O13—B2—B2iii80.9 (4)
Lu3—O2—Ba2vii102.11 (17)O13iii—B2—B2iii26.05 (18)
Lu3—O2—O9iii158.8 (3)Lu1—B3—Lu272.63 (16)
Lu3—O2—O10vii48.69 (13)Lu1—B3—Lu3137.0 (2)
Lu3—O2—O13105.7 (2)Lu1—B3—Lu3vi140.0 (3)
Lu3—O2—O1448.44 (13)Lu1—B3—Ba177.53 (19)
Lu3—O2—B2134.3 (5)Lu1—B3—Ba270.67 (19)
Lu3—O2—O6vi46.8 (2)Lu1—B3—Ba374.87 (18)
Lu3—O2—O1276.3 (2)Lu1—B3—O333.9 (3)
Ba1—O2—Ba2vii100.60 (16)Lu1—B3—O8122.2 (5)
Ba1—O2—O9iii104.7 (2)Lu1—B3—O940.26 (13)
Ba1—O2—O10vii127.22 (18)Lu1—B3—O14108.5 (4)
Ba1—O2—O13122.3 (2)Lu2—B3—Lu378.7 (2)
Ba1—O2—O1481.65 (16)Lu2—B3—Lu3vi143.6 (3)
Ba1—O2—B2115.9 (5)Lu2—B3—Ba194.39 (19)
Ba1—O2—O6vi60.6 (2)Lu2—B3—Ba2143.3 (3)
Ba1—O2—O1256.5 (2)Lu2—B3—Ba389.78 (19)
Ba2vii—O2—O9iii76.95 (17)Lu2—B3—O392.0 (4)
Ba2vii—O2—O10vii61.52 (14)Lu2—B3—O8139.0 (5)
Ba2vii—O2—O13124.6 (2)Lu2—B3—O942.41 (13)
Ba2vii—O2—O14150.25 (19)Lu2—B3—O1435.9 (3)
Ba2vii—O2—B2102.6 (4)Lu3—B3—Lu3vi65.50 (16)
Ba2vii—O2—O6vi80.2 (2)Lu3—B3—Ba173.36 (17)
Ba2vii—O2—O1255.0 (2)Lu3—B3—Ba2131.0 (2)
O9iii—O2—O10vii116.6 (2)Lu3—B3—Ba3137.0 (3)
O9iii—O2—O1360.56 (18)Lu3—B3—O3169.8 (5)
O9iii—O2—O14131.6 (2)Lu3—B3—O865.2 (4)
O9iii—O2—B230.8 (3)Lu3—B3—O997.7 (2)
O9iii—O2—O6vi149.8 (3)Lu3—B3—O1449.8 (4)
O9iii—O2—O12117.7 (3)Lu3vi—B3—Ba182.11 (17)
O10vii—O2—O13106.6 (3)Lu3vi—B3—Ba271.72 (15)
O10vii—O2—O1493.27 (19)Lu3vi—B3—Ba3111.5 (2)
O10vii—O2—B2116.4 (5)Lu3vi—B3—O3124.2 (4)
O10vii—O2—O6vi67.3 (2)Lu3vi—B3—O824.3 (3)
O10vii—O2—O1275.2 (3)Lu3vi—B3—O9145.8 (3)
O13—O2—O1475.37 (19)Lu3vi—B3—O14109.2 (5)
O13—O2—B229.9 (3)Ba1—B3—Ba278.32 (19)
O13—O2—O6vi149.4 (3)Ba1—B3—Ba3149.4 (3)
O13—O2—O12177.9 (3)Ba1—B3—O3103.4 (5)
O14—O2—B2102.9 (4)Ba1—B3—O858.1 (3)
O14—O2—O6vi75.2 (2)Ba1—B3—O964.17 (16)
O14—O2—O12105.8 (2)Ba1—B3—O14101.8 (4)
B2—O2—O6vi176.1 (5)Ba2—B3—Ba380.33 (18)
B2—O2—O12148.3 (5)Ba2—B3—O356.0 (4)
O6vi—O2—O1232.2 (3)Ba2—B3—O865.9 (4)
Lu1—O3—Ba296.69 (18)Ba2—B3—O9104.8 (3)
Lu1—O3—Ba3111.4 (2)Ba2—B3—O14179.1 (5)
Lu1—O3—O148.43 (13)Ba3—B3—O346.1 (3)
Lu1—O3—O1i41.33 (12)Ba3—B3—O8129.8 (4)
Lu1—O3—O4iv79.90 (15)Ba3—B3—O9101.0 (2)
Lu1—O3—O8126.4 (2)Ba3—B3—O1499.2 (4)
Lu1—O3—O945.24 (12)O3—B3—O8121.8 (7)
Lu1—O3—O9i45.32 (12)O3—B3—O972.3 (4)
Lu1—O3—O10132.9 (2)O3—B3—O14123.1 (6)
Lu1—O3—O14113.9 (2)O8—B3—O9122.2 (5)
Lu1—O3—B2ii67.65 (18)O8—B3—O14114.9 (7)
Lu1—O3—B3126.1 (4)O9—B3—O1474.5 (4)
Ba2—O3—Ba3105.23 (14)Lu1viii—B4—Lu2viii70.57 (15)
Ba2—O3—O159.71 (13)Lu1viii—B4—Lu2i137.9 (3)
Ba2—O3—O1i126.9 (2)Lu1viii—B4—Ba1v76.48 (17)
Ba2—O3—O4iv163.6 (2)Lu1viii—B4—Ba3viii76.35 (15)
Ba2—O3—O871.77 (17)Lu1viii—B4—O1v31.0 (3)
Ba2—O3—O9123.13 (19)Lu1viii—B4—O492.6 (4)
Ba2—O3—O9i67.45 (14)Lu1viii—B4—O4v113.7 (2)
Ba2—O3—O1056.08 (11)Lu1viii—B4—O15i140.8 (5)
Ba2—O3—O14129.4 (2)Lu1viii—B4—B4v113.1 (3)
Ba2—O3—B2ii67.20 (16)Lu2viii—B4—Lu2i121.6 (2)
Ba2—O3—B3100.9 (4)Lu2viii—B4—Ba1v143.7 (3)
Ba3—O3—O1146.2 (2)Lu2viii—B4—Ba3viii91.27 (18)
Ba3—O3—O1i75.74 (14)Lu2viii—B4—O1v91.7 (4)
Ba3—O3—O4iv62.07 (13)Lu2viii—B4—O433.4 (3)
Ba3—O3—O8122.2 (2)Lu2viii—B4—O4v80.3 (2)
Ba3—O3—O9125.63 (18)Lu2viii—B4—O15i148.6 (5)
Ba3—O3—O9i85.99 (16)Lu2viii—B4—B4v58.32 (19)
Ba3—O3—O1054.20 (11)Lu2i—B4—Ba1v75.05 (17)
Ba3—O3—O1499.9 (2)Lu2i—B4—Ba3viii136.6 (2)
Ba3—O3—B2ii63.55 (17)Lu2i—B4—O1v107.5 (4)
Ba3—O3—B3112.2 (4)Lu2i—B4—O4119.4 (4)
O1—O3—O1i89.76 (17)Lu2i—B4—O4v43.84 (13)
O1—O3—O4iv124.43 (18)Lu2i—B4—O15i41.1 (3)
O1—O3—O883.8 (2)Lu2i—B4—B4v63.24 (18)
O1—O3—O963.77 (15)Ba1v—B4—Ba3viii95.49 (18)
O1—O3—O9i60.53 (16)Ba1v—B4—O1v52.1 (3)
O1—O3—O10115.22 (19)Ba1v—B4—O4165.2 (4)
O1—O3—O14112.9 (2)Ba1v—B4—O4v99.9 (2)
O1—O3—B2ii82.7 (2)Ba1v—B4—O15i66.0 (4)
O1—O3—B3100.8 (4)Ba1v—B4—B4v125.9 (3)
O1i—O3—O4iv42.83 (14)Ba3viii—B4—O1v98.1 (3)
O1i—O3—O8152.6 (2)Ba3viii—B4—O471.9 (3)
O1i—O3—O956.56 (13)Ba3viii—B4—O4v163.2 (3)
O1i—O3—O9i59.63 (15)Ba3viii—B4—O15i96.0 (3)
O1i—O3—O10122.25 (18)Ba3viii—B4—B4v138.5 (3)
O1i—O3—O14101.4 (2)O1v—B4—O4120.6 (6)
O1i—O3—B2ii66.66 (17)O1v—B4—O4v96.6 (4)
O1i—O3—B3128.5 (4)O1v—B4—O15i117.3 (6)
O4iv—O3—O8123.2 (2)O1v—B4—B4v109.4 (4)
O4iv—O3—O965.25 (14)O4—B4—O4v93.6 (4)
O4iv—O3—O9i99.93 (18)O4—B4—O15i121.9 (7)
O4iv—O3—O10115.03 (18)O4—B4—B4v67.4 (4)
O4iv—O3—O1465.68 (19)O4v—B4—O15i84.3 (3)
O4iv—O3—B2ii96.9 (2)O4v—B4—B4v26.16 (19)
O4iv—O3—B393.9 (4)O15i—B4—B4v98.1 (4)
O8—O3—O997.1 (2)Lu2vi—B5—Lu3ii135.0 (3)
O8—O3—O9i135.4 (2)Lu2vi—B5—Lu3vi74.69 (19)
O8—O3—O1084.32 (18)Lu2vi—B5—Ba2148.2 (3)
O8—O3—O1457.7 (2)Lu2vi—B5—O5xiii38.1 (3)
O8—O3—B2ii138.1 (2)Lu2vi—B5—O10139.1 (5)
O8—O3—B329.3 (4)Lu2vi—B5—O11ix94.2 (5)
O9—O3—O9i90.56 (17)Lu2vi—B5—O14vi43.13 (16)
O9—O3—O10178.1 (2)Lu2vi—B5—B1ii128.5 (2)
O9—O3—O1468.98 (18)Lu2vi—B5—O6ii120.7 (3)
O9—O3—B2ii111.8 (2)Lu3ii—B5—Lu3vi149.0 (3)
O9—O3—B383.3 (4)Lu3ii—B5—Ba276.70 (19)
O9i—O3—O1087.57 (17)Lu3ii—B5—O5xiii100.1 (4)
O9i—O3—O14158.3 (2)Lu3ii—B5—O1034.3 (3)
O9i—O3—B2ii24.82 (15)Lu3ii—B5—O11ix129.2 (5)
O9i—O3—B3160.9 (5)Lu3ii—B5—O14vi148.0 (3)
O10—O3—O14112.9 (2)Lu3ii—B5—B1ii59.0 (2)
O10—O3—B2ii66.35 (17)Lu3ii—B5—O6ii44.7 (2)
O10—O3—B398.4 (4)Lu3vi—B5—Ba273.61 (15)
O14—O3—B2ii161.0 (3)Lu3vi—B5—O5xiii110.9 (5)
O14—O3—B328.5 (4)Lu3vi—B5—O10120.2 (4)
B2ii—O3—B3164.1 (4)Lu3vi—B5—O11ix31.1 (3)
Lu2viii—O4—Ba2111.5 (2)Lu3vi—B5—O14vi43.56 (15)
Lu2viii—O4—Ba3viii119.89 (17)Lu3vi—B5—B1ii113.5 (3)
Lu2viii—O4—O182.37 (16)Lu3vi—B5—O6ii136.5 (3)
Lu2viii—O4—O1v100.8 (2)Ba2—B5—O5xiii165.4 (5)
Lu2viii—O4—O3viii76.06 (15)Ba2—B5—O1063.2 (4)
Lu2viii—O4—O4v90.11 (16)Ba2—B5—O11ix56.1 (4)
Lu2viii—O4—O545.05 (14)Ba2—B5—O14vi110.4 (2)
Lu2viii—O4—O14viii44.39 (12)Ba2—B5—B1ii64.25 (18)
Lu2viii—O4—O15viii46.94 (12)Ba2—B5—O6ii82.0 (3)
Lu2viii—O4—O15i150.2 (2)O5xiii—B5—O10121.5 (6)
Lu2viii—O4—B4126.9 (4)O5xiii—B5—O11ix120.5 (6)
Lu2viii—O4—B4v73.49 (19)O5xiii—B5—O14vi80.0 (5)
Lu2viii—O4—O7ii123.5 (3)O5xiii—B5—B1ii101.7 (4)
Ba2—O4—Ba3viii96.13 (13)O5xiii—B5—O6ii85.7 (4)
Ba2—O4—O155.59 (12)O10—B5—O11ix117.9 (6)
Ba2—O4—O1v142.3 (2)O10—B5—O14vi119.5 (5)
Ba2—O4—O3viii135.78 (18)O10—B5—B1ii83.1 (5)
Ba2—O4—O4v90.28 (16)O10—B5—O6ii76.6 (4)
Ba2—O4—O567.55 (16)O11ix—B5—O14vi73.8 (4)
Ba2—O4—O14viii110.8 (2)O11ix—B5—B1ii82.4 (5)
Ba2—O4—O15viii95.52 (18)O11ix—B5—O6ii105.6 (5)
Ba2—O4—O15i83.38 (19)O14vi—B5—B1ii152.7 (3)
Ba2—O4—B4112.4 (4)O14vi—B5—O6ii162.6 (3)
Ba2—O4—B4v79.8 (2)B1ii—B5—O6ii23.7 (2)
Ba2—O4—O7ii52.13 (19)Lu3—O6—Lu3vi94.6 (3)
Ba3viii—O4—O1150.47 (18)Lu3—O6—Ba1vi108.8 (4)
Ba3viii—O4—O1v83.50 (18)Lu3—O6—O2vi130.4 (4)
Ba3viii—O4—O3viii49.13 (11)Lu3—O6—O5vi77.0 (3)
Ba3viii—O4—O4v143.7 (2)Lu3—O6—O857.9 (2)
Ba3viii—O4—O5115.98 (17)Lu3—O6—O8vi53.7 (2)
Ba3viii—O4—O14viii76.40 (13)Lu3—O6—O10vii43.77 (18)
Ba3viii—O4—O15viii165.4 (2)Lu3—O6—O10ix121.9 (4)
Ba3viii—O4—O15i81.95 (17)Lu3—O6—B1113.8 (5)
Ba3viii—O4—B483.1 (3)Lu3—O6—B5vii67.8 (3)
Ba3viii—O4—B4v166.4 (2)Lu3—O6—O6vi67.1 (7)
Ba3viii—O4—O7ii44.83 (18)Lu3—O6—O7104.4 (3)
O1—O4—O1v113.0 (2)Lu3—O6—O7vi138.6 (4)
O1—O4—O3viii158.31 (19)Lu3—O6—O1284.8 (3)
O1—O4—O4v42.67 (15)Lu3—O6—O12vi152.3 (7)
O1—O4—O564.46 (16)Lu3vi—O6—Ba1vi91.4 (3)
O1—O4—O14viii118.9 (2)Lu3vi—O6—O2vi47.09 (19)
O1—O4—O15viii43.41 (14)Lu3vi—O6—O5vi131.7 (4)
O1—O4—O15i85.98 (19)Lu3vi—O6—O846.6 (2)
O1—O4—B499.1 (4)Lu3vi—O6—O8vi70.0 (3)
O1—O4—B4v24.49 (18)Lu3vi—O6—O10vii136.1 (4)
O1—O4—O7ii107.7 (2)Lu3vi—O6—O10ix41.4 (2)
O1v—O4—O3viii69.60 (19)Lu3vi—O6—B1125.6 (7)
O1v—O4—O4v70.29 (18)Lu3vi—O6—B5vii150.0 (4)
O1v—O4—O5145.3 (2)Lu3vi—O6—O6vi86.4 (8)
O1v—O4—O14viii105.7 (2)Lu3vi—O6—O7135.6 (5)
O1v—O4—O15viii92.6 (2)Lu3vi—O6—O7vi119.0 (5)
O1v—O4—O15i59.2 (2)Lu3vi—O6—O12118.1 (5)
O1v—O4—B429.9 (4)Lu3vi—O6—O12vi112.0 (5)
O1v—O4—B4v91.8 (2)Ba1vi—O6—O2vi54.52 (18)
O1v—O4—O7ii122.7 (3)Ba1vi—O6—O5vi49.66 (19)
O3viii—O4—O4v133.9 (2)Ba1vi—O6—O8127.7 (3)
O3viii—O4—O5100.63 (19)Ba1vi—O6—O8vi62.9 (3)
O3viii—O4—O14viii43.77 (15)Ba1vi—O6—O10vii91.1 (3)
O3viii—O4—O15viii116.34 (19)Ba1vi—O6—O10ix107.7 (3)
O3viii—O4—O15i111.8 (2)Ba1vi—O6—B1118.4 (6)
O3viii—O4—B492.1 (4)Ba1vi—O6—B5vii73.0 (3)
O3viii—O4—B4v140.3 (2)Ba1vi—O6—O6vi175.2 (8)
O3viii—O4—O7ii86.5 (2)Ba1vi—O6—O7118.5 (4)
O4v—O4—O599.48 (18)Ba1vi—O6—O7vi94.6 (4)
O4v—O4—O14viii133.88 (19)Ba1vi—O6—O12146.9 (5)
O4v—O4—O15viii44.84 (14)Ba1vi—O6—O12vi64.9 (5)
O4v—O4—O15i63.33 (17)O2vi—O6—O5vi104.2 (3)
O4v—O4—B461.6 (3)O2vi—O6—O893.7 (3)
O4v—O4—B4v24.83 (19)O2vi—O6—O8vi80.6 (3)
O4v—O4—O7ii135.1 (2)O2vi—O6—O10vii143.7 (4)
O5—O4—O14viii56.88 (16)O2vi—O6—O10ix53.7 (2)
O5—O4—O15viii61.07 (16)O2vi—O6—B1114.5 (5)
O5—O4—O15i146.6 (3)O2vi—O6—B5vii127.3 (4)
O5—O4—B4160.9 (4)O2vi—O6—O6vi125.7 (9)
O5—O4—B4v74.7 (2)O2vi—O6—O7124.9 (4)
O5—O4—O7ii88.4 (2)O2vi—O6—O7vi90.9 (3)
O14viii—O4—O15viii91.21 (17)O2vi—O6—O12136.7 (5)
O14viii—O4—O15i155.1 (3)O2vi—O6—O12vi69.9 (4)
O14viii—O4—B4133.6 (4)O5vi—O6—O8131.8 (3)
O14viii—O4—B4v117.2 (2)O5vi—O6—O8vi67.0 (3)
O14viii—O4—O7ii87.0 (2)O5vi—O6—O10vii42.92 (18)
O15viii—O4—O15i108.2 (2)O5vi—O6—O10ix156.6 (3)
O15viii—O4—B4100.5 (4)O5vi—O6—B1100.4 (5)
O15viii—O4—B4v26.92 (18)O5vi—O6—B5vii23.84 (18)
O15viii—O4—O7ii143.7 (3)O5vi—O6—O6vi129.8 (8)
O15i—O4—B429.3 (4)O5vi—O6—O791.9 (4)
O15i—O4—B4v84.7 (2)O5vi—O6—O7vi94.8 (4)
O15i—O4—O7ii86.2 (2)O5vi—O6—O12108.5 (4)
B4—O4—B4v86.4 (4)O5vi—O6—O12vi79.6 (5)
B4—O4—O7ii106.8 (4)O8—O6—O8vi72.6 (3)
B4v—O4—O7ii131.8 (3)O8—O6—O10vii100.6 (3)
Lu2viii—O5—Ba1106.68 (17)O8—O6—O10ix64.1 (2)
Lu2viii—O5—Ba297.28 (19)O8—O6—B1112.2 (6)
Lu2viii—O5—O446.54 (14)O8—O6—B5vii125.5 (3)
Lu2viii—O5—O8144.3 (2)O8—O6—O6vi48.2 (6)
Lu2viii—O5—O10ix134.8 (2)O8—O6—O7113.8 (4)
Lu2viii—O5—O11xii98.9 (2)O8—O6—O7vi129.8 (5)
Lu2viii—O5—O13viii45.76 (14)O8—O6—O1285.2 (4)
Lu2viii—O5—O14viii47.71 (14)O8—O6—O12vi148.3 (7)
Lu2viii—O5—O15viii45.92 (13)O8vi—O6—O10vii72.4 (3)
Lu2viii—O5—B5ix119.1 (5)O8vi—O6—O10ix111.3 (4)
Lu2viii—O5—O6vi157.6 (2)O8vi—O6—B1163.0 (6)
Ba1—O5—Ba290.70 (14)O8vi—O6—B5vii80.0 (3)
Ba1—O5—O4110.89 (18)O8vi—O6—O6vi112.3 (8)
Ba1—O5—O855.63 (12)O8vi—O6—O7151.4 (5)
Ba1—O5—O10ix118.5 (2)O8vi—O6—O7vi156.8 (5)
Ba1—O5—O11xii121.6 (2)O8vi—O6—O12138.6 (4)
Ba1—O5—O13viii86.25 (15)O8vi—O6—O12vi127.8 (6)
Ba1—O5—O14viii151.8 (2)O10vii—O6—O10ix160.5 (3)
Ba1—O5—O15viii62.71 (13)O10vii—O6—B190.6 (4)
Ba1—O5—B5ix126.0 (5)O10vii—O6—B5vii25.15 (18)
Ba1—O5—O6vi57.07 (17)O10vii—O6—O6vi87.5 (7)
Ba2—O5—O451.59 (13)O10vii—O6—O778.9 (3)
Ba2—O5—O856.59 (13)O10vii—O6—O7vi104.4 (4)
Ba2—O5—O10ix81.40 (18)O10vii—O6—O1278.1 (3)
Ba2—O5—O11xii137.1 (2)O10vii—O6—O12vi108.6 (6)
Ba2—O5—O13viii139.2 (2)O10ix—O6—B184.9 (5)
Ba2—O5—O14viii102.86 (18)O10ix—O6—B5vii167.9 (4)
Ba2—O5—O15viii85.14 (16)O10ix—O6—O6vi73.3 (8)
Ba2—O5—B5ix109.1 (4)O10ix—O6—O795.8 (4)
Ba2—O5—O6vi98.1 (2)O10ix—O6—O7vi79.5 (4)
O4—O5—O8106.5 (2)O10ix—O6—O1288.2 (4)
O4—O5—O10ix110.5 (2)O10ix—O6—O12vi84.6 (5)
O4—O5—O11xii124.4 (2)B1—O6—B5vii84.3 (5)
O4—O5—O13viii91.9 (2)B1—O6—O6vi66.2 (7)
O4—O5—O14viii62.72 (17)B1—O6—O711.6 (3)
O4—O5—O15viii59.17 (16)B1—O6—O7vi27.0 (3)
O4—O5—B5ix120.9 (4)B1—O6—O1232.3 (4)
O4—O5—O6vi149.1 (3)B1—O6—O12vi56.5 (5)
O8—O5—O10ix70.22 (19)B5vii—O6—O6vi107.0 (8)
O8—O5—O11xii116.8 (3)B5vii—O6—O773.9 (4)
O8—O5—O13viii141.35 (19)B5vii—O6—O7vi88.3 (4)
O8—O5—O14viii151.3 (2)B5vii—O6—O1285.5 (4)
O8—O5—O15viii103.23 (18)B5vii—O6—O12vi84.9 (5)
O8—O5—B5ix94.0 (4)O6vi—O6—O765.8 (7)
O8—O5—O6vi42.59 (19)O6vi—O6—O7vi90.2 (8)
O10ix—O5—O11xii59.31 (19)O6vi—O6—O1237.1 (6)
O10ix—O5—O13viii134.8 (2)O6vi—O6—O12vi119.9 (10)
O10ix—O5—O14viii88.2 (2)O7—O6—O7vi34.7 (3)
O10ix—O5—O15viii166.5 (3)O7—O6—O1229.1 (3)
O10ix—O5—B5ix29.4 (4)O7—O6—O12vi61.8 (5)
O10ix—O5—O6vi63.9 (2)O7vi—O6—O1259.1 (4)
O11xii—O5—O13viii75.6 (2)O7vi—O6—O12vi30.2 (4)
O11xii—O5—O14viii62.5 (2)O12—O6—O12vi88.8 (6)
O11xii—O5—O15viii132.9 (3)Ba2vii—O7—Ba3xii114.3 (3)
O11xii—O5—B5ix29.9 (4)Ba2vii—O7—Ba3xiv101.9 (3)
O11xii—O5—O6vi80.6 (3)Ba2vii—O7—O4vii53.13 (17)
O13viii—O5—O14viii67.29 (17)Ba2vii—O7—O11xiv56.8 (2)
O13viii—O5—O15viii57.50 (15)Ba2vii—O7—B1115.7 (5)
O13viii—O5—B5ix105.4 (4)Ba2vii—O7—O6105.0 (4)
O13viii—O5—O6vi113.7 (2)Ba2vii—O7—O6vi96.8 (4)
O14viii—O5—O15viii93.6 (2)Ba2vii—O7—O7vi155.4 (7)
O14viii—O5—B5ix72.9 (4)Ba2vii—O7—O1275.9 (5)
O14viii—O5—O6vi142.0 (3)Ba2vii—O7—O12vi130.1 (5)
O15viii—O5—B5ix162.0 (5)Ba3xii—O7—Ba3xiv118.0 (3)
O15viii—O5—O6vi119.7 (2)Ba3xii—O7—O4vii62.3 (2)
B5ix—O5—O6vi70.4 (4)Ba3xii—O7—O11xiv155.5 (4)
Lu3—O8—Lu3vi89.05 (18)Ba3xii—O7—B1112.6 (6)
Lu3—O8—Ba185.62 (13)Ba3xii—O7—O6122.6 (5)
Lu3—O8—Ba2175.37 (18)Ba3xii—O7—O6vi108.6 (5)
Lu3—O8—O3115.7 (2)Ba3xii—O7—O7vi89.4 (6)
Lu3—O8—O5118.53 (18)Ba3xii—O7—O1286.3 (7)
Lu3—O8—O8vi42.04 (11)Ba3xii—O7—O12vi114.9 (4)
Lu3—O8—O10ix112.31 (18)Ba3xiv—O7—O4vii117.7 (3)
Lu3—O8—O11ix130.3 (2)Ba3xiv—O7—O11xiv51.3 (2)
Lu3—O8—O1454.85 (18)Ba3xiv—O7—B192.2 (5)
Lu3—O8—B387.2 (4)Ba3xiv—O7—O691.2 (4)
Lu3—O8—O650.1 (2)Ba3xiv—O7—O6vi115.2 (4)
Lu3—O8—O6vi51.8 (3)Ba3xiv—O7—O7vi58.3 (5)
Lu3vi—O8—Ba1120.85 (19)Ba3xiv—O7—O12153.0 (8)
Lu3vi—O8—Ba295.37 (16)Ba3xiv—O7—O12vi60.8 (3)
Lu3vi—O8—O3138.5 (2)O4vii—O7—O11xiv101.1 (3)
Lu3vi—O8—O581.83 (16)O4vii—O7—B1149.0 (6)
Lu3vi—O8—O8vi54.95 (14)O4vii—O7—O6145.3 (4)
Lu3vi—O8—O10ix40.12 (12)O4vii—O7—O6vi123.1 (4)
Lu3vi—O8—O11ix46.96 (13)O4vii—O7—O7vi146.5 (6)
Lu3vi—O8—O14127.2 (3)O4vii—O7—O1283.1 (6)
Lu3vi—O8—B3140.8 (5)O4vii—O7—O12vi176.2 (4)
Lu3vi—O8—O647.98 (19)O11xiv—O7—B190.9 (5)
Lu3vi—O8—O6vi63.3 (2)O11xiv—O7—O681.5 (4)
Ba1—O8—Ba290.92 (15)O11xiv—O7—O6vi95.5 (4)
Ba1—O8—O395.02 (19)O11xiv—O7—O7vi98.8 (6)
Ba1—O8—O551.26 (11)O11xiv—O7—O12110.7 (7)
Ba1—O8—O8vi122.90 (19)O11xiv—O7—O12vi80.6 (4)
Ba1—O8—O10ix89.36 (15)B1—O7—O611.4 (3)
Ba1—O8—O11ix132.6 (2)B1—O7—O6vi26.3 (4)
Ba1—O8—O1495.83 (19)B1—O7—O7vi56.1 (5)
Ba1—O8—B397.8 (4)B1—O7—O1265.9 (6)
Ba1—O8—O687.3 (2)B1—O7—O12vi33.7 (4)
Ba1—O8—O6vi67.8 (2)O6—O7—O6vi24.0 (3)
Ba2—O8—O361.46 (17)O6—O7—O7vi64.3 (5)
Ba2—O8—O560.96 (14)O6—O7—O1264.1 (6)
Ba2—O8—O8vi142.40 (17)O6—O7—O12vi38.1 (3)
Ba2—O8—O10ix70.65 (14)O6vi—O7—O7vi81.0 (5)
Ba2—O8—O11ix54.25 (14)O6vi—O7—O1240.4 (5)
Ba2—O8—O14122.6 (2)O6vi—O7—O12vi59.8 (4)
Ba2—O8—B390.3 (5)O7vi—O7—O12114.4 (8)
Ba2—O8—O6132.8 (2)O7vi—O7—O12vi29.7 (5)
Ba2—O8—O6vi129.4 (3)O12—O7—O12vi99.6 (7)
O3—O8—O5110.2 (2)Lu3—O12—Ba177.3 (2)
O3—O8—O8vi123.6 (2)Lu3—O12—Ba2vii84.8 (3)
O3—O8—O10ix131.9 (2)Lu3—O12—Ba3xii168.3 (3)
O3—O8—O11ix94.1 (2)Lu3—O12—O242.18 (16)
O3—O8—O1461.2 (2)Lu3—O12—O15iii111.2 (3)
O3—O8—B328.9 (4)Lu3—O12—B175.4 (5)
O3—O8—O6165.6 (3)Lu3—O12—O647.9 (3)
O3—O8—O6vi158.0 (3)Lu3—O12—O6vi39.6 (4)
O5—O8—O8vi125.84 (19)Lu3—O12—O7117.5 (8)
O5—O8—O10ix42.30 (13)Lu3—O12—O7vi106.3 (4)
O5—O8—O11ix81.98 (17)Lu3—O12—O12vi80.4 (3)
O5—O8—O14146.6 (2)Ba1—O12—Ba2vii107.5 (3)
O5—O8—B3133.2 (5)Ba1—O12—Ba3xii100.3 (4)
O5—O8—O682.3 (2)Ba1—O12—O258.2 (2)
O5—O8—O6vi70.5 (3)Ba1—O12—O15iii53.8 (2)
O8vi—O8—O10ix91.99 (17)Ba1—O12—B1128.1 (6)
O8vi—O8—O11ix88.62 (18)Ba1—O12—O6104.1 (4)
O8vi—O8—O1473.8 (2)Ba1—O12—O6vi81.1 (5)
O8vi—O8—B399.8 (5)Ba1—O12—O7165.1 (8)
O8vi—O8—O645.3 (2)Ba1—O12—O7vi143.1 (5)
O8vi—O8—O6vi62.0 (3)Ba1—O12—O12vi132.8 (4)
O10ix—O8—O11ix51.78 (13)Ba2vii—O12—Ba3xii106.8 (3)
O10ix—O8—O14165.5 (3)Ba2vii—O12—O262.0 (2)
O10ix—O8—B3159.8 (5)Ba2vii—O12—O15iii70.5 (2)
O10ix—O8—O662.2 (2)Ba2vii—O12—B1112.8 (6)
O10ix—O8—O6vi64.1 (3)Ba2vii—O12—O6113.1 (5)
O11ix—O8—O14128.9 (2)Ba2vii—O12—O6vi121.5 (6)
O11ix—O8—B3111.8 (4)Ba2vii—O12—O776.4 (6)
O11ix—O8—O694.7 (2)Ba2vii—O12—O7vi109.4 (5)
O11ix—O8—O6vi107.6 (3)Ba2vii—O12—O12vi111.2 (4)
O14—O8—B332.4 (4)Ba3xii—O12—O2145.4 (4)
O14—O8—O6104.4 (3)Ba3xii—O12—O15iii75.3 (3)
O14—O8—O6vi105.4 (3)Ba3xii—O12—B197.9 (5)
B3—O8—O6136.7 (5)Ba3xii—O12—O6123.2 (4)
B3—O8—O6vi136.1 (5)Ba3xii—O12—O6vi128.9 (5)
O6—O8—O6vi19.5 (3)Ba3xii—O12—O765.0 (6)
Lu1—O9—Lu2111.40 (18)Ba3xii—O12—O7vi68.6 (3)
Lu1—O9—Ba2i84.13 (14)Ba3xii—O12—O12vi93.4 (3)
Lu1—O9—O143.26 (11)O2—O12—O15iii70.1 (2)
Lu1—O9—O1i45.94 (12)O2—O12—B1116.7 (6)
Lu1—O9—O2iii128.2 (3)O2—O12—O690.0 (4)
Lu1—O9—O344.68 (12)O2—O12—O6vi77.9 (5)
Lu1—O9—O3i44.76 (12)O2—O12—O7133.0 (7)
Lu1—O9—O13154.3 (2)O2—O12—O7vi145.1 (5)
Lu1—O9—O13iii110.2 (2)O2—O12—O12vi121.1 (4)
Lu1—O9—O1488.80 (16)O15iii—O12—B1173.2 (6)
Lu1—O9—O15121.37 (19)O15iii—O12—O6155.7 (5)
Lu1—O9—B2148.1 (2)O15iii—O12—O6vi133.7 (6)
Lu1—O9—B2iii125.1 (5)O15iii—O12—O7116.9 (7)
Lu1—O9—B368.14 (19)O15iii—O12—O7vi142.2 (5)
Lu2—O9—Ba2i98.12 (14)O15iii—O12—O12vi168.4 (4)
Lu2—O9—O1129.96 (18)B1—O12—O629.6 (5)
Lu2—O9—O1i81.89 (17)B1—O12—O6vi50.4 (6)
Lu2—O9—O2iii108.6 (2)B1—O12—O759.6 (7)
Lu2—O9—O377.47 (15)B1—O12—O7vi31.6 (5)
Lu2—O9—O3i137.4 (2)B1—O12—O12vi5.7 (5)
Lu2—O9—O1347.24 (13)O6—O12—O6vi23.0 (4)
Lu2—O9—O13iii132.1 (3)O6—O12—O786.8 (7)
Lu2—O9—O1443.63 (12)O6—O12—O7vi61.1 (4)
Lu2—O9—O1541.10 (11)O6—O12—O12vi35.2 (3)
Lu2—O9—B267.74 (19)O6vi—O12—O7109.4 (8)
Lu2—O9—B2iii123.3 (4)O6vi—O12—O7vi80.1 (5)
Lu2—O9—B366.10 (19)O6vi—O12—O12vi56.0 (5)
Ba2i—O9—O1115.29 (18)O7—O12—O7vi35.9 (5)
Ba2i—O9—O1i53.33 (11)O7—O12—O12vi54.2 (5)
Ba2i—O9—O2iii58.57 (15)O7vi—O12—O12vi26.2 (3)
Ba2i—O9—O3117.46 (17)
Symmetry codes: (i) x+1, y, z; (ii) x+1/2, y1/2, z; (iii) x+1/2, y+1/2, z; (iv) x1/2, y1/2, z; (v) x+3/2, y+1/2, z; (vi) x+1, y, z+1/2; (vii) x1/2, y+1/2, z; (viii) x+1/2, y+1/2, z; (ix) x+3/2, y+1/2, z+1/2; (x) x, y1, z; (xi) x+1, y1, z+1/2; (xii) x, y+1, z; (xiii) x+3/2, y1/2, z+1/2; (xiv) x+1, y+1, z+1/2.
 

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