Buy article online - an online subscription or single-article purchase is required to access this article.
The title compound was obtained by reaction of pyrido[2,1-c][1,4]benzodiazepine in boiling phosphorus oxychloride with a catalytic amount of pyridine under microwave heating. Its structure determination establishes the mechanism of the reaction, which was otherwise uncertain.
Supporting information
| Crystallographic Information File (CIF) Contains datablocks QA0102, global |
| Structure factor file (CIF format) Supplementary material |
CCDC reference: 131209
Subscribe to Acta Crystallographica Section C: Structural Chemistry
The full text of this article is available to subscribers to the journal.
If you have already registered and are using a computer listed in your registration details, please email
support@iucr.org for assistance.