Bis[di(2-aminoethyl)amine-N,N',N'']nickel(II) Chloride Monohydrate, a Redetermination

Hynes, R.C.; Willis, C.J.; Vittal, J.J.

doi:10.1107/S0108270196005835

Bis[di(2-aminoethyl)amine-N,N',N'']nickel(II) Chloride Monohydrate, a Redetermination

R. C. Hynes, C. J. Willis and J. J. Vittal

A redetermination of the structure of the title compound, [Ni(C₄H₁₃N₃)₂]Cl².H₂O, from diffractometer data leads to considerably more accurate geometric parameters than those obtained in a previous determination using film data. The coordination geometry around the Ni^II atom in the [Ni(C₄H₁₃N₃)₂]²⁺ cation is distorted octahedron, with the Ni-N distances in the range 2.083 (4)-2.166 (4) Å and the trans- N-Ni-N 161.9 (2)-177.5 (2)°

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Bis[di(2-aminoethyl)amine-N,N',N'']nickel(II) Chloride Monohydrate, a Redetermination

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	Crystallographic Information File (CIF) Contains datablocks hynes1, global
	Structure factor file (CIF format) Supplementary material