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The flux synthesis of single crystals of the isostructural compounds tristrontium zinc platinum hexaoxide, Sr3ZnPtO6, and tristrontium cadmium platinum hexaoxide, Sr3CdPtO6, is reported. The compounds adopt the pseudo-one-dimensional rhombohedral K4CdCl6 structure type, and feature chains of face-shared distorted ZnO6 or CdO6 trigonal prisms and PtO6 octahedra, surrounded by columns of Sr2+ ions. All transition metals are located on the threefold axis of symmetry, while the Sr2+ cations lie on twofold axes.
Supporting information
For both compounds, data collection: SMART (Bruker, 1999); cell refinement: SMART; data reduction: SHELXTL (Bruker, 1999); program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: SHELXTL; software used to prepare material for publication: SHELXTL.
(I) Tristrontium zinc platinum hexaoxide
top
Crystal data top
Sr3ZnPtO6 | Dx = 6.847 Mg m−3 |
Mr = 619.32 | Mo Kα radiation, λ = 0.71073 Å |
Trigonal, R3c | Cell parameters from 823 reflections |
Hall symbol: -R 3 2"c | θ = 4.2–36.2° |
a = 9.6267 (7) Å | µ = 53.56 mm−1 |
c = 11.2292 (11) Å | T = 293 K |
V = 901.23 (13) Å3 | Fragment, brown |
Z = 6 | 0.11 × 0.05 × 0.03 mm |
F(000) = 1620 | |
Data collection top
Bruker SMART APEX CCD diffractometer | 493 independent reflections |
Radiation source: fine-focus sealed tube | 405 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.045 |
ω scans | θmax = 36.3°, θmin = 4.2° |
Absorption correction: multi-scan (SADABS; Bruker, 1999) | h = −13→15 |
Tmin = 0.054, Tmax = 0.211 | k = −13→15 |
2881 measured reflections | l = −18→17 |
Refinement top
Refinement on F2 | Primary atom site location: structure-invariant direct methods |
Least-squares matrix: full | Secondary atom site location: difference Fourier map |
R[F2 > 2σ(F2)] = 0.029 | w = 1/[σ2(Fo2) + (0.0272P)2] where P = (Fo2 + 2Fc2)/3 |
wR(F2) = 0.059 | (Δ/σ)max < 0.001 |
S = 0.98 | Δρmax = 6.49 e Å−3 |
493 reflections | Δρmin = −4.57 e Å−3 |
20 parameters | Extinction correction: SHELXL97 (Sheldrick, 1997), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
0 restraints | Extinction coefficient: 0.00027 (5) |
Special details top
Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell e.s.d.'s are taken
into account individually in the estimation of e.s.d.'s in distances, angles
and torsion angles; correlations between e.s.d.'s in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s.
planes. |
Refinement. Refinement of F2 against ALL reflections. The weighted R-factor
wR and goodness of fit S are based on F2, conventional
R-factors R are based on F, with F set to zero for
negative F2. The threshold expression of F2 >
σ(F2) is used only for calculating R-factors(gt) etc.
and is not relevant to the choice of reflections for refinement.
R-factors based on F2 are statistically about twice as large
as those based on F, and R- factors based on ALL data will be
even larger. |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | |
Sr | 0.36425 (7) | 0 | 1/4 | 0.00588 (16) | |
Zn | 0 | 0 | 1/4 | 0.0087 (3) | |
Pt | 0 | 0 | 0 | 0.00336 (12) | |
O | −0.0203 (5) | 0.1528 (5) | 0.1135 (3) | 0.0092 (7) | |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
Sr | 0.0053 (2) | 0.0055 (3) | 0.0069 (3) | 0.00276 (15) | −0.00037 (11) | −0.0007 (2) |
Zn | 0.0106 (4) | 0.0106 (4) | 0.0051 (6) | 0.0053 (2) | 0 | 0 |
Pt | 0.00297 (15) | 0.00297 (15) | 0.00413 (19) | 0.00149 (7) | 0 | 0 |
O | 0.0099 (19) | 0.0083 (18) | 0.0103 (17) | 0.0053 (16) | −0.0005 (14) | −0.0030 (14) |
Geometric parameters (Å, º) top
Sr—Oi | 2.476 (4) | Zn—Ptii | 2.8073 (3) |
Sr—Oii | 2.476 (4) | Zn—Sri | 3.5066 (8) |
Sr—Oiii | 2.645 (4) | Zn—Srxii | 3.5066 (8) |
Sr—Oiv | 2.645 (4) | Zn—Srxv | 3.5962 (3) |
Sr—Ov | 2.668 (4) | Pt—Oxvi | 2.029 (4) |
Sr—Ovi | 2.668 (4) | Pt—Oxvii | 2.029 (4) |
Sr—Ovii | 2.718 (4) | Pt—Oi | 2.029 (4) |
Sr—Oviii | 2.718 (4) | Pt—O | 2.029 (4) |
Sr—Ptix | 3.2103 (4) | Pt—Oxviii | 2.029 (4) |
Sr—Ptx | 3.2104 (4) | Pt—Oxii | 2.029 (4) |
Sr—Zn | 3.5066 (8) | Pt—Znxvi | 2.8073 (3) |
Sr—Srxi | 3.5962 (3) | Pt—Srxix | 3.2103 (4) |
Zn—Oxii | 2.200 (4) | Pt—Srxv | 3.2103 (4) |
Zn—Oxiii | 2.200 (4) | Pt—Srvii | 3.2103 (4) |
Zn—Oii | 2.200 (4) | Pt—Srxx | 3.2103 (4) |
Zn—Oxiv | 2.200 (4) | O—Srxii | 2.476 (4) |
Zn—Oi | 2.200 (4) | O—Srxxi | 2.645 (4) |
Zn—O | 2.200 (4) | O—Srxix | 2.668 (4) |
Zn—Pt | 2.8073 (3) | O—Srvii | 2.718 (4) |
| | | |
Oi—Sr—Oii | 77.04 (19) | O—Zn—Srxii | 44.50 (10) |
Oi—Sr—Oiii | 93.97 (12) | Pt—Zn—Srxii | 90.0 |
Oii—Sr—Oiii | 77.03 (14) | Ptii—Zn—Srxii | 90.0 |
Oi—Sr—Oiv | 77.03 (14) | Sri—Zn—Srxii | 120.0 |
Oii—Sr—Oiv | 93.97 (12) | Oxii—Zn—Sr | 106.85 (11) |
Oiii—Sr—Oiv | 168.62 (18) | Oxiii—Zn—Sr | 106.85 (11) |
Oi—Sr—Ov | 132.44 (7) | Oii—Zn—Sr | 44.50 (10) |
Oii—Sr—Ov | 73.60 (16) | Oxiv—Zn—Sr | 115.04 (10) |
Oiii—Sr—Ov | 114.38 (14) | Oi—Zn—Sr | 44.50 (10) |
Oiv—Sr—Ov | 68.71 (15) | O—Zn—Sr | 115.04 (10) |
Oi—Sr—Ovi | 73.60 (16) | Pt—Zn—Sr | 90.0 |
Oii—Sr—Ovi | 132.44 (7) | Ptii—Zn—Sr | 90.0 |
Oiii—Sr—Ovi | 68.71 (16) | Sri—Zn—Sr | 120.0 |
Oiv—Sr—Ovi | 114.38 (14) | Srxii—Zn—Sr | 120.0 |
Ov—Sr—Ovi | 150.95 (18) | Oxii—Zn—Srxv | 47.06 (11) |
Oi—Sr—Ovii | 121.95 (6) | Oxiii—Zn—Srxv | 164.56 (10) |
Oii—Sr—Ovii | 139.40 (13) | Oii—Zn—Srxv | 87.76 (10) |
Oiii—Sr—Ovii | 130.09 (3) | Oxiv—Zn—Srxv | 99.38 (10) |
Oiv—Sr—Ovii | 61.27 (17) | Oi—Zn—Srxv | 48.98 (11) |
Ov—Sr—Ovii | 67.64 (15) | O—Zn—Srxv | 104.47 (10) |
Ovi—Sr—Ovii | 88.13 (12) | Pt—Zn—Srxv | 58.640 (4) |
Oi—Sr—Oviii | 139.40 (13) | Ptii—Zn—Srxv | 121.360 (4) |
Oii—Sr—Oviii | 121.95 (6) | Sri—Zn—Srxv | 68.692 (11) |
Oiii—Sr—Oviii | 61.27 (17) | Srxii—Zn—Srxv | 148.310 (5) |
Oiv—Sr—Oviii | 130.09 (3) | Sr—Zn—Srxv | 60.822 (9) |
Ov—Sr—Oviii | 88.13 (12) | Oxvi—Pt—Oxvii | 84.72 (17) |
Ovi—Sr—Oviii | 67.64 (15) | Oxvi—Pt—Oi | 95.28 (17) |
Ovii—Sr—Oviii | 69.15 (17) | Oxvii—Pt—Oi | 180.0 (3) |
Oi—Sr—Ptix | 116.08 (9) | Oxvi—Pt—O | 180.0 (3) |
Oii—Sr—Ptix | 101.38 (10) | Oxvii—Pt—O | 95.28 (17) |
Oiii—Sr—Ptix | 149.01 (9) | Oi—Pt—O | 84.72 (17) |
Oiv—Sr—Ptix | 39.06 (8) | Oxvi—Pt—Oxviii | 84.72 (17) |
Ov—Sr—Ptix | 39.02 (8) | Oxvii—Pt—Oxviii | 84.72 (17) |
Ovi—Sr—Ptix | 124.94 (9) | Oi—Pt—Oxviii | 95.28 (17) |
Ovii—Sr—Ptix | 38.91 (8) | O—Pt—Oxviii | 95.28 (17) |
Oviii—Sr—Ptix | 96.19 (9) | Oxvi—Pt—Oxii | 95.28 (17) |
Oi—Sr—Ptx | 101.38 (10) | Oxvii—Pt—Oxii | 95.28 (17) |
Oii—Sr—Ptx | 116.08 (9) | Oi—Pt—Oxii | 84.72 (17) |
Oiii—Sr—Ptx | 39.06 (8) | O—Pt—Oxii | 84.72 (17) |
Oiv—Sr—Ptx | 149.01 (9) | Oxviii—Pt—Oxii | 180.0 (3) |
Ov—Sr—Ptx | 124.95 (9) | Oxvi—Pt—Zn | 128.92 (11) |
Ovi—Sr—Ptx | 39.02 (8) | Oxvii—Pt—Zn | 128.92 (11) |
Ovii—Sr—Ptx | 96.19 (9) | Oi—Pt—Zn | 51.08 (11) |
Oviii—Sr—Ptx | 38.91 (8) | O—Pt—Zn | 51.08 (11) |
Ptix—Sr—Ptx | 131.96 (2) | Oxviii—Pt—Zn | 128.92 (11) |
Oi—Sr—Zn | 38.52 (9) | Oxii—Pt—Zn | 51.08 (11) |
Oii—Sr—Zn | 38.52 (9) | Oxvi—Pt—Znxvi | 51.08 (11) |
Oiii—Sr—Zn | 84.31 (9) | Oxvii—Pt—Znxvi | 51.08 (11) |
Oiv—Sr—Zn | 84.31 (9) | Oi—Pt—Znxvi | 128.92 (11) |
Ov—Sr—Zn | 104.52 (9) | O—Pt—Znxvi | 128.92 (11) |
Ovi—Sr—Zn | 104.52 (9) | Oxviii—Pt—Znxvi | 51.08 (11) |
Ovii—Sr—Zn | 145.42 (9) | Oxii—Pt—Znxvi | 128.92 (11) |
Oviii—Sr—Zn | 145.42 (9) | Zn—Pt—Znxvi | 180.0 |
Ptix—Sr—Zn | 114.019 (12) | Oxvi—Pt—Srxix | 124.11 (11) |
Ptx—Sr—Zn | 114.020 (12) | Oxvii—Pt—Srxix | 57.32 (12) |
Oi—Sr—Srxi | 83.84 (10) | Oi—Pt—Srxix | 122.68 (12) |
Oii—Sr—Srxi | 49.03 (9) | O—Pt—Srxix | 55.89 (11) |
Oiii—Sr—Srxi | 125.23 (9) | Oxviii—Pt—Srxix | 55.23 (11) |
Oiv—Sr—Srxi | 47.66 (9) | Oxii—Pt—Srxix | 124.77 (11) |
Ov—Sr—Srxi | 48.71 (9) | Zn—Pt—Srxix | 106.948 (2) |
Ovi—Sr—Srxi | 154.74 (9) | Znxvi—Pt—Srxix | 73.052 (2) |
Ovii—Sr—Srxi | 94.48 (8) | Oxvi—Pt—Srxv | 55.89 (11) |
Oviii—Sr—Srxi | 136.45 (8) | Oxvii—Pt—Srxv | 122.68 (12) |
Ptix—Sr—Srxi | 55.935 (1) | Oi—Pt—Srxv | 57.32 (12) |
Ptx—Sr—Srxi | 163.141 (12) | O—Pt—Srxv | 124.11 (11) |
Zn—Sr—Srxi | 60.822 (9) | Oxviii—Pt—Srxv | 124.77 (11) |
Oxii—Zn—Oxiii | 146.3 (2) | Oxii—Pt—Srxv | 55.23 (11) |
Oxii—Zn—Oii | 129.9 (2) | Zn—Pt—Srxv | 73.052 (2) |
Oxiii—Zn—Oii | 76.81 (16) | Znxvi—Pt—Srxv | 106.948 (2) |
Oxii—Zn—Oxiv | 89.0 (2) | Srxix—Pt—Srxv | 180.00 (2) |
Oxiii—Zn—Oxiv | 76.81 (16) | Oxvi—Pt—Srvii | 122.68 (12) |
Oii—Zn—Oxiv | 76.81 (16) | Oxvii—Pt—Srvii | 124.77 (11) |
Oxii—Zn—Oi | 76.81 (16) | Oi—Pt—Srvii | 55.23 (11) |
Oxiii—Zn—Oi | 129.9 (2) | O—Pt—Srvii | 57.32 (12) |
Oii—Zn—Oi | 89.0 (2) | Oxviii—Pt—Srvii | 55.88 (11) |
Oxiv—Zn—Oi | 146.3 (2) | Oxii—Pt—Srvii | 124.12 (11) |
Oxii—Zn—O | 76.81 (16) | Zn—Pt—Srvii | 73.052 (2) |
Oxiii—Zn—O | 89.0 (2) | Znxvi—Pt—Srvii | 106.948 (3) |
Oii—Zn—O | 146.3 (2) | Srxix—Pt—Srvii | 68.126 (2) |
Oxiv—Zn—O | 129.9 (2) | Srxv—Pt—Srvii | 111.874 (2) |
Oi—Zn—O | 76.81 (16) | Oxvi—Pt—Srxx | 57.32 (12) |
Oxii—Zn—Pt | 45.84 (10) | Oxvii—Pt—Srxx | 55.23 (11) |
Oxiii—Zn—Pt | 134.16 (10) | Oi—Pt—Srxx | 124.77 (11) |
Oii—Zn—Pt | 134.16 (10) | O—Pt—Srxx | 122.68 (12) |
Oxiv—Zn—Pt | 134.16 (10) | Oxviii—Pt—Srxx | 124.12 (11) |
Oi—Zn—Pt | 45.84 (10) | Oxii—Pt—Srxx | 55.88 (11) |
O—Zn—Pt | 45.84 (10) | Zn—Pt—Srxx | 106.948 (2) |
Oxii—Zn—Ptii | 134.16 (10) | Znxvi—Pt—Srxx | 73.052 (2) |
Oxiii—Zn—Ptii | 45.84 (10) | Srxix—Pt—Srxx | 111.874 (2) |
Oii—Zn—Ptii | 45.84 (10) | Srxv—Pt—Srxx | 68.126 (2) |
Oxiv—Zn—Ptii | 45.84 (10) | Srvii—Pt—Srxx | 180.00 (2) |
Oi—Zn—Ptii | 134.16 (10) | Pt—O—Zn | 83.09 (15) |
O—Zn—Ptii | 134.16 (10) | Pt—O—Srxii | 171.3 (2) |
Pt—Zn—Ptii | 180.0 | Zn—O—Srxii | 96.98 (14) |
Oxii—Zn—Sri | 44.50 (10) | Pt—O—Srxxi | 85.71 (14) |
Oxiii—Zn—Sri | 115.04 (10) | Zn—O—Srxxi | 95.42 (15) |
Oii—Zn—Sri | 106.85 (11) | Srxii—O—Srxxi | 102.97 (14) |
Oxiv—Zn—Sri | 44.50 (10) | Pt—O—Srxix | 85.10 (13) |
Oi—Zn—Sri | 115.04 (10) | Zn—O—Srxix | 168.08 (18) |
O—Zn—Sri | 106.85 (11) | Srxii—O—Srxix | 94.46 (14) |
Pt—Zn—Sri | 90.0 | Srxxi—O—Srxix | 85.22 (11) |
Ptii—Zn—Sri | 90.0 | Pt—O—Srvii | 83.77 (13) |
Oxii—Zn—Srxii | 115.04 (10) | Zn—O—Srvii | 93.38 (13) |
Oxiii—Zn—Srxii | 44.50 (10) | Srxii—O—Srvii | 87.50 (12) |
Oii—Zn—Srxii | 115.04 (10) | Srxxi—O—Srvii | 165.37 (16) |
Oxiv—Zn—Srxii | 106.85 (11) | Srxix—O—Srvii | 83.78 (12) |
Oi—Zn—Srxii | 106.85 (11) | | |
Symmetry codes: (i) −x+y, −x, z; (ii) y, x, −z+1/2; (iii) −y+1/3, −x−1/3, z+1/6; (iv) x−y+2/3, x+1/3, −z+1/3; (v) −y+2/3, x−y+1/3, z+1/3; (vi) −x+1/3, −x+y−1/3, −z+1/6; (vii) −x+2/3, −y+1/3, −z+1/3; (viii) −x+y+1/3, y−1/3, z+1/6; (ix) x+2/3, y+1/3, z+1/3; (x) y+1/3, x−1/3, −z+1/6; (xi) y+1/3, −x+y+2/3, −z+2/3; (xii) −y, x−y, z; (xiii) −x, −x+y, −z+1/2; (xiv) x−y, −y, −z+1/2; (xv) x−y−1/3, x−2/3, −z+1/3; (xvi) −x, −y, −z; (xvii) x−y, x, −z; (xviii) y, −x+y, −z; (xix) −x+y+1/3, −x+2/3, z−1/3; (xx) x−2/3, y−1/3, z−1/3; (xxi) y−1/3, −x+y+1/3, −z+1/3. |
(II) Tristrontium cadmium platinum hexaoxide
top
Crystal data top
Sr3CdPtO6 | Dx = 7.114 Mg m−3 |
Mr = 666.35 | Mo Kα radiation, λ = 0.71073 Å |
Trigonal, R3c | Cell parameters from 1517 reflections |
Hall symbol: -R 3 2"c | θ = 4.2–36.2° |
a = 9.6413 (4) Å | µ = 51.29 mm−1 |
c = 11.5935 (7) Å | T = 293 K |
V = 933.29 (8) Å3 | Chunk, brown |
Z = 6 | 0.09 × 0.04 × 0.03 mm |
F(000) = 1728 | |
Data collection top
Bruker SMART APEX CCD diffractometer | 505 independent reflections |
Radiation source: fine-focus sealed tube | 465 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.036 |
ω scans | θmax = 36.4°, θmin = 4.2° |
Absorption correction: multi-scan (SADABS; Bruker, 1999) | h = −15→8 |
Tmin = 0.091, Tmax = 0.360 | k = −16→15 |
2632 measured reflections | l = −19→9 |
Refinement top
Refinement on F2 | 0 restraints |
Least-squares matrix: full | Primary atom site location: structure-invariant direct methods |
R[F2 > 2σ(F2)] = 0.030 | Secondary atom site location: difference Fourier map |
wR(F2) = 0.072 | w = 1/[σ2(Fo2) + (0.0463P)2 + 3.1434P] where P = (Fo2 + 2Fc2)/3 |
S = 1.09 | (Δ/σ)max < 0.001 |
505 reflections | Δρmax = 5.05 e Å−3 |
19 parameters | Δρmin = −3.56 e Å−3 |
Special details top
Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell e.s.d.'s are taken
into account individually in the estimation of e.s.d.'s in distances, angles
and torsion angles; correlations between e.s.d.'s in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s.
planes. |
Refinement. Refinement of F2 against ALL reflections. The weighted R-factor
wR and goodness of fit S are based on F2, conventional
R-factors R are based on F, with F set to zero for
negative F2. The threshold expression of F2 >
σ(F2) is used only for calculating R-factors(gt) etc.
and is not relevant to the choice of reflections for refinement.
R-factors based on F2 are statistically about twice as large
as those based on F, and R- factors based on ALL data will be
even larger. |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | |
Sr | 0.36366 (6) | 0 | 1/4 | 0.00457 (14) | |
Cd | 0 | 0 | 1/4 | 0.00566 (17) | |
Pt | 0 | 0 | 0 | 0.00178 (12) | |
O | −0.0230 (4) | 0.1559 (4) | 0.1062 (3) | 0.0067 (6) | |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
Sr | 0.0044 (2) | 0.0042 (2) | 0.0050 (3) | 0.00208 (12) | −0.00029 (9) | −0.00057 (17) |
Cd | 0.0069 (2) | 0.0069 (2) | 0.0032 (4) | 0.00344 (11) | 0 | 0 |
Pt | 0.00179 (13) | 0.00179 (13) | 0.00177 (19) | 0.00089 (7) | 0 | 0 |
O | 0.0083 (15) | 0.0069 (14) | 0.0064 (14) | 0.0050 (13) | 0.0005 (10) | −0.0015 (11) |
Geometric parameters (Å, º) top
Sr—Oi | 2.529 (4) | Cd—Ptii | 2.8984 (2) |
Sr—Oii | 2.529 (4) | Cd—Sri | 3.5061 (6) |
Sr—Oiii | 2.622 (4) | Cd—Srxii | 3.5061 (6) |
Sr—Oiv | 2.622 (4) | Cd—Srxv | 3.6342 (2) |
Sr—Ov | 2.635 (4) | Pt—O | 2.039 (4) |
Sr—Ovi | 2.635 (4) | Pt—Oxvi | 2.039 (4) |
Sr—Ovii | 2.739 (4) | Pt—Oi | 2.039 (4) |
Sr—Oviii | 2.739 (4) | Pt—Oxii | 2.039 (4) |
Sr—Ptix | 3.2261 (3) | Pt—Oxvii | 2.039 (4) |
Sr—Ptx | 3.2261 (3) | Pt—Oxviii | 2.039 (4) |
Sr—Cd | 3.5061 (6) | Pt—Cdxviii | 2.8984 (2) |
Sr—Srxi | 3.6342 (2) | Pt—Srxix | 3.2260 (3) |
Cd—Oxii | 2.328 (4) | Pt—Srxx | 3.2260 (3) |
Cd—Oxiii | 2.328 (4) | Pt—Srxxi | 3.2261 (3) |
Cd—Oii | 2.328 (4) | Pt—Srvii | 3.2261 (3) |
Cd—Oxiv | 2.328 (4) | O—Srxii | 2.529 (4) |
Cd—O | 2.328 (4) | O—Srxxii | 2.622 (4) |
Cd—Oi | 2.328 (4) | O—Srxix | 2.635 (4) |
Cd—Pt | 2.8984 (2) | O—Srvii | 2.739 (4) |
| | | |
Oi—Sr—Oii | 83.14 (17) | Oi—Cd—Srxii | 105.97 (9) |
Oi—Sr—Oiii | 93.23 (10) | Pt—Cd—Srxii | 90.0 |
Oii—Sr—Oiii | 76.86 (12) | Ptii—Cd—Srxii | 90.0 |
Oi—Sr—Oiv | 76.86 (12) | Sri—Cd—Srxii | 120.0 |
Oii—Sr—Oiv | 93.22 (10) | Oxii—Cd—Sr | 105.97 (9) |
Oiii—Sr—Oiv | 166.87 (16) | Oxiii—Cd—Sr | 105.97 (9) |
Oi—Sr—Ov | 134.73 (6) | Oii—Cd—Sr | 46.11 (9) |
Oii—Sr—Ov | 71.26 (14) | Oxiv—Cd—Sr | 114.72 (9) |
Oiii—Sr—Ov | 115.36 (13) | O—Cd—Sr | 114.72 (9) |
Oiv—Sr—Ov | 68.29 (14) | Oi—Cd—Sr | 46.11 (9) |
Oi—Sr—Ovi | 71.26 (13) | Pt—Cd—Sr | 90.0 |
Oii—Sr—Ovi | 134.73 (6) | Ptii—Cd—Sr | 90.0 |
Oiii—Sr—Ovi | 68.29 (14) | Sri—Cd—Sr | 120.0 |
Oiv—Sr—Ovi | 115.36 (13) | Srxii—Cd—Sr | 120.0 |
Ov—Sr—Ovi | 150.37 (16) | Oxii—Cd—Srxv | 101.13 (9) |
Oi—Sr—Ovii | 121.34 (5) | Oxiii—Cd—Srxv | 48.88 (9) |
Oii—Sr—Ovii | 136.88 (12) | Oii—Cd—Srxv | 102.14 (9) |
Oiii—Sr—Ovii | 129.78 (2) | Oxiv—Cd—Srxv | 46.00 (9) |
Oiv—Sr—Ovii | 63.33 (15) | O—Cd—Srxv | 89.36 (9) |
Ov—Sr—Ovii | 66.58 (14) | Oi—Cd—Srxv | 163.75 (9) |
Ovi—Sr—Ovii | 88.29 (11) | Pt—Cd—Srxv | 122.119 (3) |
Oi—Sr—Oviii | 136.88 (12) | Ptii—Cd—Srxv | 57.881 (3) |
Oii—Sr—Oviii | 121.34 (5) | Sri—Cd—Srxv | 68.795 (9) |
Oiii—Sr—Oviii | 63.33 (15) | Srxii—Cd—Srxv | 61.160 (7) |
Oiv—Sr—Oviii | 129.78 (2) | Sr—Cd—Srxv | 147.573 (4) |
Ov—Sr—Oviii | 88.30 (11) | O—Pt—Oxvi | 92.69 (15) |
Ovi—Sr—Oviii | 66.58 (14) | O—Pt—Oi | 87.31 (15) |
Ovii—Sr—Oviii | 66.67 (15) | Oxvi—Pt—Oi | 180.0 (3) |
Oi—Sr—Ptix | 115.89 (8) | O—Pt—Oxii | 87.31 (15) |
Oii—Sr—Ptix | 99.96 (8) | Oxvi—Pt—Oxii | 92.69 (15) |
Oiii—Sr—Ptix | 150.33 (8) | Oi—Pt—Oxii | 87.31 (15) |
Oiv—Sr—Ptix | 39.13 (8) | O—Pt—Oxvii | 92.69 (15) |
Ov—Sr—Ptix | 39.11 (8) | Oxvi—Pt—Oxvii | 87.31 (15) |
Ovi—Sr—Ptix | 124.58 (8) | Oi—Pt—Oxvii | 92.69 (15) |
Ovii—Sr—Ptix | 38.91 (7) | Oxii—Pt—Oxvii | 180.0 (3) |
Oviii—Sr—Ptix | 95.58 (8) | O—Pt—Oxviii | 180.0 (2) |
Oi—Sr—Ptx | 99.96 (8) | Oxvi—Pt—Oxviii | 87.31 (15) |
Oii—Sr—Ptx | 115.89 (8) | Oi—Pt—Oxviii | 92.69 (15) |
Oiii—Sr—Ptx | 39.13 (8) | Oxii—Pt—Oxviii | 92.69 (15) |
Oiv—Sr—Ptx | 150.33 (8) | Oxvii—Pt—Oxviii | 87.31 (15) |
Ov—Sr—Ptx | 124.58 (8) | O—Pt—Cd | 52.86 (10) |
Ovi—Sr—Ptx | 39.11 (8) | Oxvi—Pt—Cd | 127.14 (10) |
Ovii—Sr—Ptx | 95.58 (8) | Oi—Pt—Cd | 52.86 (10) |
Oviii—Sr—Ptx | 38.91 (7) | Oxii—Pt—Cd | 52.86 (10) |
Ptix—Sr—Ptx | 131.909 (19) | Oxvii—Pt—Cd | 127.14 (10) |
Oi—Sr—Cd | 41.57 (8) | Oxviii—Pt—Cd | 127.14 (10) |
Oii—Sr—Cd | 41.57 (8) | O—Pt—Cdxviii | 127.14 (10) |
Oiii—Sr—Cd | 83.44 (8) | Oxvi—Pt—Cdxviii | 52.86 (10) |
Oiv—Sr—Cd | 83.43 (8) | Oi—Pt—Cdxviii | 127.14 (10) |
Ov—Sr—Cd | 104.81 (8) | Oxii—Pt—Cdxviii | 127.14 (10) |
Ovi—Sr—Cd | 104.82 (8) | Oxvii—Pt—Cdxviii | 52.86 (10) |
Ovii—Sr—Cd | 146.67 (8) | Oxviii—Pt—Cdxviii | 52.86 (10) |
Oviii—Sr—Cd | 146.67 (8) | Cd—Pt—Cdxviii | 180.0 |
Ptix—Sr—Cd | 114.045 (10) | O—Pt—Srxix | 54.60 (10) |
Ptx—Sr—Cd | 114.046 (10) | Oxvi—Pt—Srxix | 57.52 (10) |
Oi—Sr—Srxi | 86.37 (8) | Oi—Pt—Srxix | 122.48 (10) |
Oii—Sr—Srxi | 48.82 (8) | Oxii—Pt—Srxix | 125.78 (10) |
Oiii—Sr—Srxi | 125.39 (8) | Oxvii—Pt—Srxix | 54.22 (10) |
Oiv—Sr—Srxi | 46.42 (8) | Oxviii—Pt—Srxix | 125.40 (10) |
Ov—Sr—Srxi | 48.66 (8) | Cd—Pt—Srxix | 107.427 (2) |
Ovi—Sr—Srxi | 155.13 (8) | Cdxviii—Pt—Srxix | 72.573 (2) |
Ovii—Sr—Srxi | 94.47 (7) | O—Pt—Srxx | 125.40 (10) |
Oviii—Sr—Srxi | 136.73 (8) | Oxvi—Pt—Srxx | 122.48 (10) |
Ptix—Sr—Srxi | 55.717 (1) | Oi—Pt—Srxx | 57.52 (10) |
Ptx—Sr—Srxi | 163.012 (10) | Oxii—Pt—Srxx | 54.22 (10) |
Cd—Sr—Srxi | 61.160 (7) | Oxvii—Pt—Srxx | 125.78 (10) |
Oxii—Cd—Oxiii | 148.06 (18) | Oxviii—Pt—Srxx | 54.60 (10) |
Oxii—Cd—Oii | 130.57 (18) | Cd—Pt—Srxx | 72.573 (2) |
Oxiii—Cd—Oii | 74.40 (14) | Cdxviii—Pt—Srxx | 107.427 (2) |
Oxii—Cd—Oxiv | 92.22 (18) | Srxix—Pt—Srxx | 180.000 (7) |
Oxiii—Cd—Oxiv | 74.40 (14) | O—Pt—Srxxi | 122.48 (10) |
Oii—Cd—Oxiv | 74.40 (14) | Oxvi—Pt—Srxxi | 54.22 (10) |
Oxii—Cd—O | 74.40 (14) | Oi—Pt—Srxxi | 125.78 (10) |
Oxiii—Cd—O | 92.22 (17) | Oxii—Pt—Srxxi | 54.60 (10) |
Oii—Cd—O | 148.06 (18) | Oxvii—Pt—Srxxi | 125.40 (10) |
Oxiv—Cd—O | 130.57 (18) | Oxviii—Pt—Srxxi | 57.52 (10) |
Oxii—Cd—Oi | 74.40 (14) | Cd—Pt—Srxxi | 107.427 (2) |
Oxiii—Cd—Oi | 130.57 (18) | Cdxviii—Pt—Srxxi | 72.573 (2) |
Oii—Cd—Oi | 92.22 (17) | Srxix—Pt—Srxxi | 111.437 (2) |
Oxiv—Cd—Oi | 148.06 (18) | Srxx—Pt—Srxxi | 68.563 (2) |
O—Cd—Oi | 74.40 (14) | O—Pt—Srvii | 57.52 (10) |
Oxii—Cd—Pt | 44.28 (9) | Oxvi—Pt—Srvii | 125.78 (10) |
Oxiii—Cd—Pt | 135.72 (9) | Oi—Pt—Srvii | 54.22 (10) |
Oii—Cd—Pt | 135.72 (9) | Oxii—Pt—Srvii | 125.40 (10) |
Oxiv—Cd—Pt | 135.72 (9) | Oxvii—Pt—Srvii | 54.60 (10) |
O—Cd—Pt | 44.28 (9) | Oxviii—Pt—Srvii | 122.48 (10) |
Oi—Cd—Pt | 44.28 (9) | Cd—Pt—Srvii | 72.573 (2) |
Oxii—Cd—Ptii | 135.72 (9) | Cdxviii—Pt—Srvii | 107.426 (2) |
Oxiii—Cd—Ptii | 44.28 (9) | Srxix—Pt—Srvii | 68.563 (2) |
Oii—Cd—Ptii | 44.28 (9) | Srxx—Pt—Srvii | 111.437 (2) |
Oxiv—Cd—Ptii | 44.28 (9) | Srxxi—Pt—Srvii | 180.0 |
O—Cd—Ptii | 135.72 (9) | Pt—O—Cd | 82.86 (13) |
Oi—Cd—Ptii | 135.72 (9) | Pt—O—Srxii | 169.43 (19) |
Pt—Cd—Ptii | 180.0 | Cd—O—Srxii | 92.32 (12) |
Oxii—Cd—Sri | 46.11 (9) | Pt—O—Srxxii | 86.65 (13) |
Oxiii—Cd—Sri | 114.72 (9) | Cd—O—Srxxii | 94.29 (12) |
Oii—Cd—Sri | 105.97 (9) | Srxii—O—Srxxii | 103.14 (12) |
Oxiv—Cd—Sri | 46.11 (9) | Pt—O—Srxix | 86.29 (12) |
O—Cd—Sri | 105.97 (9) | Cd—O—Srxix | 168.88 (16) |
Oi—Cd—Sri | 114.72 (9) | Srxii—O—Srxix | 97.98 (12) |
Pt—Cd—Sri | 90.0 | Srxxii—O—Srxix | 87.47 (11) |
Ptii—Cd—Sri | 90.0 | Pt—O—Srvii | 83.57 (12) |
Oxii—Cd—Srxii | 114.72 (9) | Cd—O—Srvii | 91.29 (12) |
Oxiii—Cd—Srxii | 46.11 (9) | Srxii—O—Srvii | 87.15 (11) |
Oii—Cd—Srxii | 114.72 (9) | Srxxii—O—Srvii | 168.06 (15) |
Oxiv—Cd—Srxii | 105.97 (9) | Srxix—O—Srvii | 85.08 (10) |
O—Cd—Srxii | 46.11 (9) | | |
Symmetry codes: (i) −x+y, −x, z; (ii) y, x, −z+1/2; (iii) −y+1/3, −x−1/3, z+1/6; (iv) x−y+2/3, x+1/3, −z+1/3; (v) −y+2/3, x−y+1/3, z+1/3; (vi) −x+1/3, −x+y−1/3, −z+1/6; (vii) −x+2/3, −y+1/3, −z+1/3; (viii) −x+y+1/3, y−1/3, z+1/6; (ix) x+2/3, y+1/3, z+1/3; (x) y+1/3, x−1/3, −z+1/6; (xi) y+1/3, −x+y+2/3, −z+2/3; (xii) −y, x−y, z; (xiii) −x, −x+y, −z+1/2; (xiv) x−y, −y, −z+1/2; (xv) x−y−2/3, x−1/3, −z+2/3; (xvi) x−y, x, −z; (xvii) y, −x+y, −z; (xviii) −x, −y, −z; (xix) −x+y+1/3, −x+2/3, z−1/3; (xx) x−y−1/3, x−2/3, −z+1/3; (xxi) x−2/3, y−1/3, z−1/3; (xxii) y−1/3, −x+y+1/3, −z+1/3. |
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