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For the title compound, (OC-6-22)-[Co(CN5O2)2(NH3)4]ClO4, the structure determination confirms the cis relationship of the two ring ligands deduced from NMR and shows that these ligands involve N-2 bonding to the Co atom. The accompanying low temperature study suggests several O atoms of the ClO4- ion are slightly disordered rather than having large thermal displacements.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablocks 1, 2, default

fcf

Structure factor file (CIF format)
Contains datablock 1

fcf

Structure factor file (CIF format)
Contains datablock 2

CCDC references: 129267; 129268

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