Penta­cyclo­hexyl­oxy­phospho­rane

The crystal structure of penta­cyclo­hexyl­oxy­phospho­rane, C₃₀H₅₅O₅P, has been determined at 180 (2) K. In space group P1, there are four independent mol­ecules in the unit cell, each displaying trigonal bipyramidal geometry at the P atom.

Key indicators

• Single-crystal X-ray study
• T = 180 K
• Mean [sigma](C-C) = 0.006 Å
• R factor = 0.043
• wR factor = 0.108
• Data-to-parameter ratio = 10.6

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



PLAT_320  Alert C Check Hybridisation of  P1_1   in main residue          ?

PLAT_320  Alert C Check Hybridisation of  P1_2   in main residue          ?

PLAT_320  Alert C Check Hybridisation of  P1_3   in main residue          ?

PLAT_320  Alert C Check Hybridisation of  P1_4   in main residue          ?

General Notes



REFLT_03
         From the CIF: _diffrn_reflns_theta_max           25.02
         From the CIF: _reflns_number_total              13809
         Count of symmetry unique reflns        10753
         Completeness (_total/calc)            128.42%
         TEST3: Check Friedels for noncentro structure
         Estimate of Friedel pairs measured      3056
         Fraction of Friedel pairs measured     0.284
         Are heavy atom types Z>Si present          yes
          WARNING: Large fraction of Friedel related reflns may
                   be needed to determine absolute structure


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 4 Alert Level C = Please check

---

S1. Comment

Pentaoxyphosphoranes (RO)₅P, where two or three of the OR groups are OH, or ionized to O^-, are of interest as potential intermediates in the hydrolysis reactions of phosphodiesters. Their lifetimes and protonation states are of paramount importance in, for example, understanding the mechanisms of action of nuclease enzymes (Perreault & Anslyn, 1997). However, such species are too short-lived for them to be isolated, so that the pK_a values of the OH groups cannot be measured directly.

A possible solution to this problem lies in the simple linear relationship (Kirby, 1994) between the length of a C—OX bond and the pK_a of the acid HOX: the stronger the acid, the longer the bond. The sensitivity of this bond length to the pK_a depends on the substituents on C (Kirby, 1994); a good correlation has been established for derivatives of cyclohexanol (Jones et al., 1992), and this correlation can in principle be used to estimate pK_a values of compounds HOX too unstable to exist as the free acid or anion. For example, the method has been used recently to estimate the pK_a of 2,4-dinitrobenzenesulfenic acid (Green et al., 2000). As a first step, we have prepared the title compound, pentacyclohexyloxyphosphorane (CyO)₅P, with the maximum number of cyclohexyl–OX bonds.

S2. Experimental

The title compound was prepared using the method of Chang et al. (1977). It is liquid at room temperature, melting just above 273 K. The crystal was obtained by slow cooling in a freezer and transferred to the diffractometer with the aid of a microscope equipped with a cold stage.

S3. Refinement

Despite the suspicious cell dimensions (a approximately equal to b, α approximately equal to β), many strenuous efforts to locate extra symmetry all failed conspicuously. There is a pseudo-C-centred monoclinic cell, but R_int for this setting is ca 0.26. The refinement shows no anomalies: with anisotropic displacement parameters for all non-H atoms, all H atoms placed geometrically, and no constraints on other atoms, there are no unusual bond distances, displacement parameters or correlation coefficients. Furthermore, and perhaps most significantly, the orientation of the cyclohexyl groups in one of the four independent molecules in the asymmetric unit (with atom labels ending in _4) is noticeably different from that observed for the other three molecules. From this we conclude that the spacegroup really is P1, as described.

Computing details

Data collection: COLLECT (Nonius, 1998); cell refinement: HKL SCALEPACK (Otwinowski & Minor, 1997); data reduction: HKL DENZO (Otwinowski & Minor, 1997) and SCALEPACK; program(s) used to solve structure: SHELXS97 (Sheldrick 1997); program(s) used to refine structure: SHELXL97 (Sheldrick 1997); molecular graphics: XP (Sheldrick, 1993); software used to prepare material for publication: SHELXL97.

Figures

Fig. 1. One of the four independent molecules in the asymmetric unit of (I) with displacement ellipsoids at the 50% probability level. In the deposited tables, independent molecules are distinguished by _n (n = 1–4).

Pentacyclohexyloxyphosphorane

Crystal data

C30H55O5P	Z = 4
Mr = 526.71	F(000) = 1160
Triclinic, P1	Dx = 1.143 Mg m^−3
a = 10.0853 (2) Å	Mo Kα radiation, λ = 0.71073 Å
b = 10.0892 (2) Å	Cell parameters from 37465 reflections
c = 30.1129 (7) Å	θ = 1.0–25.0°
α = 88.403 (2)°	µ = 0.12 mm^−1
β = 88.589 (9)°	T = 180 K
γ = 90.021 (1)°	Block, colourless
V = 3061.95 (11) Å^3	0.37 × 0.32 × 0.32 mm

Data collection

Nonius KappaCCD diffractometer	12562 reflections with I > 2σ(I)
Radiation source: fine-focus sealed tube	Rint = 0.042
Graphite monochromator	θmax = 25.0°, θmin = 3.6°
Thin–slice ω and ϕ scans	h = −11→9
22250 measured reflections	k = −11→8
13809 independent reflections	l = −35→33

Refinement

Refinement on F^2	Secondary atom site location: difference Fourier map
Least-squares matrix: full	Hydrogen site location: inferred from neighbouring sites
R[F^2 > 2σ(F^2)] = 0.044	H-atom parameters constrained
wR(F^2) = 0.108	w = 1/[σ^2(Fo^2) + (0.0381P)^2 + 1.8978P] where P = (Fo^2 + 2Fc^2)/3
S = 1.06	(Δ/σ)max = 0.001
13809 reflections	Δρmax = 0.21 e Å^−3
1297 parameters	Δρmin = −0.28 e Å^−3
3 restraints	Absolute structure: Flack (1983), 3513 Friedel pairs
Primary atom site location: structure-invariant direct methods	Absolute structure parameter: −0.01 (7)

Special details

Experimental. Crystals are VERY prone to split: many crystals from several different samples were examined before a suitable crystal was obtained.

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F² against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F², conventional R-factors R are based on F, with F set to zero for negative F². The threshold expression of F² > σ(F²) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F² are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Ų)

	x	y	z	Uiso*/Ueq
P1_1	0.66801 (9)	−0.06476 (9)	0.78644 (3)	0.0234 (2)
O1_1	0.5051 (2)	−0.0463 (2)	0.78810 (8)	0.0251 (6)
O2_1	0.8317 (2)	−0.0928 (2)	0.78532 (8)	0.0244 (6)
O3_1	0.6643 (2)	−0.0421 (2)	0.73331 (8)	0.0275 (6)
O4_1	0.6842 (2)	0.0664 (2)	0.81462 (8)	0.0274 (6)
O5_1	0.6491 (2)	−0.2066 (2)	0.81147 (9)	0.0276 (6)
C1_1	0.4377 (4)	0.0694 (3)	0.77073 (12)	0.0265 (8)
H1_1	0.5048	0.1366	0.7600	0.032*
C2_1	0.3547 (4)	0.0284 (4)	0.73217 (14)	0.0355 (10)
H2A_1	0.2976	−0.0475	0.7418	0.043*
H2B_1	0.4140	−0.0010	0.7077	0.043*
C3_1	0.2680 (5)	0.1414 (5)	0.71522 (15)	0.0472 (12)
H3A_1	0.3251	0.2129	0.7021	0.057*
H3B_1	0.2107	0.1089	0.6916	0.057*
C4_1	0.1820 (4)	0.1968 (4)	0.75243 (16)	0.0456 (11)
H4A_1	0.1183	0.1281	0.7635	0.055*
H4B_1	0.1308	0.2734	0.7409	0.055*
C5_1	0.2674 (4)	0.2402 (4)	0.79043 (14)	0.0378 (10)
H5A_1	0.3248	0.3150	0.7800	0.045*
H5B_1	0.2095	0.2717	0.8150	0.045*
C6_1	0.3536 (4)	0.1269 (4)	0.80760 (13)	0.0342 (9)
H6A_1	0.4120	0.1599	0.8309	0.041*
H6B_1	0.2962	0.0565	0.8213	0.041*
C7_1	0.8975 (4)	−0.2194 (3)	0.78534 (12)	0.0259 (8)
H7_1	0.8694	−0.2710	0.8128	0.031*
C8_1	1.0441 (4)	−0.1904 (4)	0.78742 (14)	0.0333 (9)
H8A_1	1.0615	−0.1393	0.8143	0.040*
H8B_1	1.0723	−0.1357	0.7611	0.040*
C9_1	1.1243 (4)	−0.3187 (4)	0.78882 (14)	0.0395 (10)
H9A_1	1.2200	−0.2971	0.7885	0.047*
H9B_1	1.1028	−0.3688	0.8168	0.047*
C10_1	1.0950 (4)	−0.4041 (4)	0.74975 (15)	0.0459 (12)
H10A_1	1.1428	−0.4894	0.7529	0.055*
H10B_1	1.1271	−0.3589	0.7219	0.055*
C11_1	0.9469 (4)	−0.4305 (4)	0.74702 (16)	0.0440 (11)
H11A_1	0.9296	−0.4813	0.7201	0.053*
H11B_1	0.9168	−0.4848	0.7733	0.053*
C12_1	0.8692 (4)	−0.3014 (4)	0.74530 (14)	0.0333 (9)
H12A_1	0.8940	−0.2503	0.7178	0.040*
H12B_1	0.7731	−0.3212	0.7446	0.040*
C13_1	0.7684 (4)	0.0083 (4)	0.70340 (12)	0.0282 (9)
H13_1	0.8549	−0.0314	0.7124	0.034*
C14_1	0.7779 (5)	0.1572 (4)	0.70549 (14)	0.0405 (11)
H14A_1	0.8068	0.1817	0.7354	0.049*
H14B_1	0.6892	0.1965	0.7008	0.049*
C15_1	0.8759 (5)	0.2135 (4)	0.67034 (14)	0.0417 (11)
H15A_1	0.8748	0.3115	0.6711	0.050*
H15B_1	0.9665	0.1833	0.6775	0.050*
C16_1	0.8437 (4)	0.1714 (4)	0.62431 (13)	0.0408 (11)
H16A_1	0.9131	0.2044	0.6029	0.049*
H16B_1	0.7579	0.2105	0.6155	0.049*
C17_1	0.8357 (5)	0.0216 (5)	0.62278 (14)	0.0497 (12)
H17A_1	0.9247	−0.0166	0.6278	0.060*
H17B_1	0.8077	−0.0041	0.5929	0.060*
C18_1	0.7378 (5)	−0.0352 (4)	0.65784 (14)	0.0429 (11)
H18A_1	0.6470	−0.0063	0.6504	0.051*
H18B_1	0.7403	−0.1332	0.6573	0.051*
C19_1	0.5302 (4)	−0.2685 (3)	0.82986 (12)	0.0247 (8)
H19_1	0.4572	−0.2578	0.8082	0.030*
C20_1	0.5609 (4)	−0.4149 (3)	0.83658 (13)	0.0311 (9)
H20A_1	0.6342	−0.4263	0.8576	0.037*
H20B_1	0.5890	−0.4530	0.8079	0.037*
C21_1	0.4372 (4)	−0.4868 (4)	0.85499 (14)	0.0363 (10)
H21A_1	0.3671	−0.4823	0.8326	0.044*
H21B_1	0.4585	−0.5814	0.8608	0.044*
C22_1	0.3860 (5)	−0.4263 (4)	0.89760 (14)	0.0400 (10)
H22A_1	0.3012	−0.4696	0.9069	0.048*
H22B_1	0.4504	−0.4436	0.9213	0.048*
C23_1	0.3642 (4)	−0.2785 (4)	0.89249 (13)	0.0351 (9)
H23A_1	0.3408	−0.2420	0.9218	0.042*
H23B_1	0.2890	−0.2615	0.8726	0.042*
C24_1	0.4878 (4)	−0.2085 (4)	0.87334 (12)	0.0298 (9)
H24A_1	0.4689	−0.1130	0.8685	0.036*
H24B_1	0.5606	−0.2170	0.8947	0.036*
C25_1	0.8056 (4)	0.1224 (4)	0.83106 (12)	0.0269 (8)
H25_1	0.8786	0.1142	0.8082	0.032*
C26_1	0.7782 (4)	0.2675 (4)	0.83901 (13)	0.0303 (9)
H26A_1	0.7040	0.2758	0.8609	0.036*
H26B_1	0.7524	0.3125	0.8109	0.036*
C27_1	0.9030 (4)	0.3334 (4)	0.85659 (14)	0.0367 (10)
H27A_1	0.9746	0.3319	0.8335	0.044*
H27B_1	0.8835	0.4271	0.8631	0.044*
C28_1	0.9494 (5)	0.2622 (4)	0.89849 (15)	0.0435 (11)
H28A_1	0.8826	0.2741	0.9227	0.052*
H28B_1	1.0336	0.3024	0.9077	0.052*
C29_1	0.9704 (4)	0.1151 (4)	0.89163 (15)	0.0414 (10)
H29A_1	0.9939	0.0711	0.9202	0.050*
H29B_1	1.0449	0.1025	0.8701	0.050*
C30_1	0.8448 (4)	0.0514 (4)	0.87416 (13)	0.0332 (9)
H30A_1	0.8612	−0.0436	0.8687	0.040*
H30B_1	0.7718	0.0577	0.8966	0.040*
P1_2	0.62711 (9)	0.45500 (9)	0.54386 (3)	0.0239 (2)
O1_2	0.7896 (2)	0.4771 (2)	0.54091 (8)	0.0257 (6)
O2_2	0.4643 (2)	0.4245 (2)	0.54571 (8)	0.0269 (6)
O3_2	0.6331 (2)	0.4715 (2)	0.59667 (8)	0.0295 (6)
O4_2	0.6069 (2)	0.5901 (2)	0.51544 (8)	0.0281 (6)
O5_2	0.6472 (2)	0.3162 (2)	0.51989 (8)	0.0282 (6)
C1_2	0.8578 (4)	0.5892 (3)	0.55785 (12)	0.0263 (8)
H1_2	0.7912	0.6552	0.5685	0.032*
C2_2	0.9421 (4)	0.5441 (4)	0.59637 (14)	0.0335 (9)
H2A_2	0.9986	0.4692	0.5870	0.040*
H2B_2	0.8835	0.5120	0.6212	0.040*
C3_2	1.0296 (5)	0.6542 (4)	0.61247 (15)	0.0465 (11)
H3A_2	0.9734	0.7242	0.6255	0.056*
H3B_2	1.0876	0.6184	0.6360	0.056*
C4_2	1.1144 (4)	0.7139 (4)	0.57495 (16)	0.0446 (11)
H4A_2	1.1769	0.6462	0.5637	0.054*
H4B_2	1.1669	0.7883	0.5861	0.054*
C5_2	1.0281 (4)	0.7639 (4)	0.53721 (15)	0.0408 (10)
H5A_2	1.0852	0.7990	0.5124	0.049*
H5B_2	0.9710	0.8370	0.5477	0.049*
C6_2	0.9416 (4)	0.6519 (4)	0.52083 (13)	0.0347 (9)
H6A_2	0.8830	0.6874	0.4974	0.042*
H6B_2	0.9990	0.5834	0.5075	0.042*
C7_2	0.3972 (4)	0.2993 (3)	0.54413 (13)	0.0269 (8)
H7_2	0.4263	0.2538	0.5165	0.032*
C8_2	0.2512 (4)	0.3307 (4)	0.54147 (14)	0.0356 (10)
H8A_2	0.2357	0.3881	0.5149	0.043*
H8B_2	0.2223	0.3796	0.5681	0.043*
C9_2	0.1691 (4)	0.2029 (5)	0.53870 (15)	0.0455 (11)
H9A_2	0.0736	0.2252	0.5380	0.055*
H9B_2	0.1931	0.1572	0.5110	0.055*
C10_2	0.1950 (4)	0.1121 (4)	0.57825 (16)	0.0473 (12)
H10A_2	0.1444	0.0288	0.5755	0.057*
H10B_2	0.1640	0.1551	0.6058	0.057*
C11_2	0.3437 (5)	0.0801 (4)	0.58140 (17)	0.0464 (11)
H11A_2	0.3589	0.0232	0.6081	0.056*
H11B_2	0.3736	0.0310	0.5550	0.056*
C12_2	0.4232 (4)	0.2083 (4)	0.58411 (14)	0.0341 (9)
H12A_2	0.3979	0.2539	0.6117	0.041*
H12B_2	0.5190	0.1873	0.5851	0.041*
C13_2	0.5284 (4)	0.5148 (4)	0.62727 (12)	0.0291 (9)
H13_2	0.4436	0.4695	0.6202	0.035*
C14_2	0.5090 (5)	0.6630 (4)	0.62323 (14)	0.0440 (11)
H14A_2	0.4753	0.6865	0.5934	0.053*
H14B_2	0.5953	0.7081	0.6264	0.053*
C15_2	0.4118 (5)	0.7102 (5)	0.65865 (15)	0.0499 (12)
H15A_2	0.4062	0.8082	0.6566	0.060*
H15B_2	0.3227	0.6743	0.6528	0.060*
C16_2	0.4503 (5)	0.6686 (4)	0.70472 (14)	0.0429 (11)
H16A_2	0.3806	0.6959	0.7263	0.051*
H16B_2	0.5341	0.7130	0.7122	0.051*
C17_2	0.4680 (6)	0.5206 (5)	0.70785 (15)	0.0608 (15)
H17A_2	0.3816	0.4768	0.7035	0.073*
H17B_2	0.4985	0.4950	0.7379	0.073*
C18_2	0.5683 (5)	0.4727 (5)	0.67313 (14)	0.0561 (14)
H18A_2	0.6569	0.5095	0.6791	0.067*
H18B_2	0.5744	0.3747	0.6752	0.067*
C19_2	0.7661 (4)	0.2589 (3)	0.50051 (12)	0.0260 (8)
H19_2	0.8416	0.2705	0.5210	0.031*
C20_2	0.7381 (4)	0.1122 (4)	0.49606 (13)	0.0297 (9)
H20A_2	0.6595	0.1004	0.4775	0.036*
H20B_2	0.7185	0.0713	0.5258	0.036*
C21_2	0.8575 (4)	0.0448 (4)	0.47488 (13)	0.0357 (10)
H21A_2	0.8371	−0.0502	0.4712	0.043*
H21B_2	0.9336	0.0505	0.4949	0.043*
C22_2	0.8956 (5)	0.1080 (4)	0.42975 (14)	0.0411 (11)
H22A_2	0.8240	0.0928	0.4086	0.049*
H22B_2	0.9775	0.0659	0.4181	0.049*
C23_2	0.9186 (4)	0.2571 (4)	0.43374 (13)	0.0368 (10)
H23A_2	0.9983	0.2717	0.4515	0.044*
H23B_2	0.9352	0.2974	0.4038	0.044*
C24_2	0.8002 (4)	0.3247 (4)	0.45561 (12)	0.0291 (9)
H24A_2	0.7228	0.3197	0.4361	0.035*
H24B_2	0.8209	0.4195	0.4596	0.035*
C25_2	0.4856 (4)	0.6449 (3)	0.49835 (12)	0.0262 (8)
H25_2	0.4111	0.6283	0.5204	0.031*
C26_2	0.5091 (4)	0.7937 (4)	0.49231 (13)	0.0329 (9)
H26A_2	0.5874	0.8099	0.4724	0.040*
H26B_2	0.5271	0.8324	0.5214	0.040*
C27_2	0.3867 (4)	0.8598 (4)	0.47225 (14)	0.0389 (10)
H27A_2	0.3106	0.8500	0.4935	0.047*
H27B_2	0.4041	0.9557	0.4673	0.047*
C28_2	0.3513 (5)	0.7993 (4)	0.42859 (16)	0.0504 (12)
H28A_2	0.4233	0.8173	0.4063	0.060*
H28B_2	0.2691	0.8406	0.4175	0.060*
C29_2	0.3309 (5)	0.6490 (4)	0.43440 (16)	0.0453 (11)
H29A_2	0.2523	0.6311	0.4540	0.054*
H29B_2	0.3142	0.6106	0.4052	0.054*
C30_2	0.4532 (4)	0.5837 (4)	0.45458 (13)	0.0326 (9)
H30A_2	0.4366	0.4876	0.4594	0.039*
H30B_2	0.5298	0.5945	0.4336	0.039*
P1_3	1.12986 (9)	0.45739 (9)	0.28611 (3)	0.0241 (2)
O1_3	1.1097 (2)	0.2949 (2)	0.28792 (8)	0.0271 (6)
O2_3	1.1587 (2)	0.6208 (2)	0.28475 (8)	0.0257 (6)
O3_3	1.1155 (3)	0.4539 (2)	0.23313 (8)	0.0274 (6)
O4_3	0.9940 (2)	0.4741 (2)	0.31442 (8)	0.0274 (6)
O5_3	1.2676 (2)	0.4393 (2)	0.31096 (9)	0.0290 (6)
C1_3	0.9982 (4)	0.2272 (3)	0.27011 (12)	0.0256 (8)
H1_3	0.9325	0.2940	0.2592	0.031*
C2_3	1.0452 (4)	0.1444 (4)	0.23187 (13)	0.0334 (9)
H2A_3	1.1189	0.0867	0.2417	0.040*
H2B_3	1.0793	0.2034	0.2074	0.040*
C3_3	0.9337 (5)	0.0584 (5)	0.21476 (15)	0.0459 (11)
H3A_3	0.8646	0.1160	0.2017	0.055*
H3B_3	0.9695	0.0012	0.1911	0.055*
C4_3	0.8719 (5)	−0.0283 (4)	0.25212 (16)	0.0445 (11)
H4A_3	0.7967	−0.0791	0.2406	0.053*
H4B_3	0.9385	−0.0922	0.2633	0.053*
C5_3	0.8233 (4)	0.0573 (4)	0.28965 (14)	0.0394 (10)
H5A_3	0.7867	−0.0002	0.3142	0.047*
H5B_3	0.7511	0.1155	0.2790	0.047*
C6_3	0.9344 (4)	0.1420 (4)	0.30699 (13)	0.0311 (9)
H6A_3	0.8984	0.1998	0.3304	0.037*
H6B_3	1.0025	0.0838	0.3204	0.037*
C7_3	1.2844 (4)	0.6868 (3)	0.28534 (12)	0.0265 (8)
H7_3	1.3318	0.6579	0.3127	0.032*
C8_3	1.2542 (4)	0.8350 (3)	0.28755 (14)	0.0338 (9)
H8A_3	1.2042	0.8637	0.2611	0.041*
H8B_3	1.1984	0.8519	0.3143	0.041*
C9_3	1.3828 (5)	0.9145 (4)	0.28932 (14)	0.0405 (10)
H9A_3	1.3618	1.0104	0.2897	0.049*
H9B_3	1.4292	0.8907	0.3170	0.049*
C10_3	1.4722 (4)	0.8873 (4)	0.24981 (15)	0.0431 (11)
H10A_3	1.5565	0.9365	0.2525	0.052*
H10B_3	1.4292	0.9193	0.2223	0.052*
C11_3	1.5016 (4)	0.7403 (4)	0.24652 (16)	0.0441 (11)
H11A_3	1.5530	0.7100	0.2725	0.053*
H11B_3	1.5560	0.7248	0.2193	0.053*
C12_3	1.3722 (4)	0.6609 (4)	0.24503 (13)	0.0329 (9)
H12A_3	1.3245	0.6860	0.2177	0.039*
H12B_3	1.3928	0.5651	0.2441	0.039*
C13_3	1.0693 (4)	0.5585 (4)	0.20282 (12)	0.0281 (8)
H13_3	1.1084	0.6451	0.2113	0.034*
C14_3	0.9200 (4)	0.5681 (4)	0.20509 (13)	0.0381 (10)
H14A_3	0.8910	0.5970	0.2349	0.046*
H14B_3	0.8809	0.4798	0.2003	0.046*
C15_3	0.8713 (5)	0.6665 (5)	0.16996 (14)	0.0452 (11)
H15A_3	0.7732	0.6676	0.1709	0.054*
H15B_3	0.9027	0.7564	0.1769	0.054*
C16_3	0.9190 (4)	0.6332 (4)	0.12393 (13)	0.0398 (10)
H16A_3	0.8893	0.7023	0.1024	0.048*
H16B_3	0.8809	0.5473	0.1155	0.048*
C17_3	1.0694 (5)	0.6250 (5)	0.12253 (14)	0.0494 (12)
H17A_3	1.1070	0.7134	0.1281	0.059*
H17B_3	1.1001	0.5986	0.0926	0.059*
C18_3	1.1191 (5)	0.5250 (5)	0.15713 (13)	0.0447 (12)
H18A_3	1.0884	0.4351	0.1499	0.054*
H18B_3	1.2173	0.5248	0.1564	0.054*
C19_3	1.3258 (4)	0.3203 (3)	0.33041 (12)	0.0261 (8)
H19_3	1.3190	0.2464	0.3091	0.031*
C20_3	1.4709 (4)	0.3513 (4)	0.33728 (13)	0.0319 (9)
H20A_3	1.4784	0.4258	0.3578	0.038*
H20B_3	1.5139	0.3783	0.3085	0.038*
C21_3	1.5403 (4)	0.2300 (4)	0.35653 (14)	0.0393 (10)
H21A_3	1.6339	0.2522	0.3621	0.047*
H21B_3	1.5395	0.1583	0.3347	0.047*
C22_3	1.4728 (4)	0.1811 (4)	0.39987 (15)	0.0431 (11)
H22A_3	1.5147	0.0972	0.4100	0.052*
H22B_3	1.4856	0.2474	0.4230	0.052*
C23_3	1.3256 (4)	0.1584 (4)	0.39423 (14)	0.0386 (10)
H23A_3	1.2836	0.1367	0.4236	0.046*
H23B_3	1.3130	0.0816	0.3750	0.046*
C24_3	1.2573 (4)	0.2799 (4)	0.37368 (12)	0.0305 (9)
H24A_3	1.1631	0.2590	0.3684	0.037*
H24B_3	1.2600	0.3542	0.3945	0.037*
C25_3	0.9357 (4)	0.5950 (4)	0.33073 (12)	0.0253 (8)
H25_3	0.9480	0.6673	0.3076	0.030*
C26_3	0.7888 (4)	0.5688 (4)	0.33811 (13)	0.0306 (9)
H26A_3	0.7756	0.4955	0.3603	0.037*
H26B_3	0.7493	0.5421	0.3099	0.037*
C27_3	0.7210 (4)	0.6933 (4)	0.35447 (13)	0.0346 (9)
H27A_3	0.6259	0.6742	0.3606	0.042*
H27B_3	0.7272	0.7635	0.3309	0.042*
C28_3	0.7835 (4)	0.7433 (4)	0.39659 (14)	0.0390 (10)
H28A_3	0.7430	0.8291	0.4044	0.047*
H28B_3	0.7654	0.6792	0.4215	0.047*
C29_3	0.9331 (4)	0.7609 (4)	0.39000 (14)	0.0366 (10)
H29A_3	0.9506	0.8352	0.3685	0.044*
H29B_3	0.9720	0.7843	0.4186	0.044*
C30_3	0.9996 (4)	0.6363 (4)	0.37310 (12)	0.0297 (9)
H30A_3	1.0953	0.6533	0.3674	0.036*
H30B_3	0.9908	0.5640	0.3959	0.036*
P1_4	0.64770 (9)	0.42034 (8)	0.04390 (3)	0.0238 (2)
O1_4	0.6262 (2)	0.5826 (2)	0.04113 (8)	0.0259 (6)
O2_4	0.6781 (2)	0.2573 (2)	0.04599 (9)	0.0283 (6)
O3_4	0.7900 (2)	0.4404 (2)	0.01966 (9)	0.0281 (6)
O4_4	0.6239 (3)	0.4254 (2)	0.09703 (8)	0.0290 (6)
O5_4	0.5167 (2)	0.4004 (2)	0.01584 (8)	0.0272 (6)
C1_4	0.5109 (4)	0.6487 (4)	0.05789 (12)	0.0268 (8)
H1_4	0.4440	0.5814	0.0688	0.032*
C2_4	0.4528 (4)	0.7327 (4)	0.02046 (13)	0.0339 (9)
H2A_4	0.4203	0.6739	−0.0027	0.041*
H2B_4	0.5230	0.7902	0.0068	0.041*
C3_4	0.3386 (4)	0.8187 (4)	0.03727 (15)	0.0386 (10)
H3A_4	0.3063	0.8755	0.0125	0.046*
H3B_4	0.2644	0.7612	0.0481	0.046*
C4_4	0.3821 (4)	0.9051 (4)	0.07448 (15)	0.0442 (11)
H4A_4	0.3057	0.9576	0.0854	0.053*
H4B_4	0.4514	0.9677	0.0631	0.053*
C5_4	0.4367 (5)	0.8204 (5)	0.11287 (15)	0.0468 (12)
H5A_4	0.4681	0.8788	0.1363	0.056*
H5B_4	0.3653	0.7632	0.1259	0.056*
C6_4	0.5515 (4)	0.7340 (4)	0.09638 (13)	0.0328 (9)
H6A_4	0.6268	0.7916	0.0866	0.039*
H6B_4	0.5816	0.6758	0.1212	0.039*
C7_4	0.8036 (4)	0.1908 (3)	0.04427 (13)	0.0271 (8)
H7_4	0.8539	0.2213	0.0168	0.033*
C8_4	0.8867 (4)	0.2142 (4)	0.08411 (13)	0.0326 (9)
H8A_4	0.8360	0.1878	0.1115	0.039*
H8B_4	0.9079	0.3097	0.0856	0.039*
C9_4	1.0155 (4)	0.1344 (4)	0.08149 (16)	0.0424 (11)
H9A_4	1.0695	0.1656	0.0554	0.051*
H9B_4	1.0673	0.1485	0.1085	0.051*
C10_4	0.9856 (5)	−0.0128 (4)	0.07766 (16)	0.0491 (12)
H10A_4	1.0699	−0.0622	0.0743	0.059*
H10B_4	0.9399	−0.0458	0.1052	0.059*
C11_4	0.8992 (5)	−0.0380 (4)	0.03828 (16)	0.0450 (12)
H11A_4	0.8763	−0.1333	0.0378	0.054*
H11B_4	0.9489	−0.0147	0.0104	0.054*
C12_4	0.7716 (4)	0.0445 (4)	0.04089 (14)	0.0350 (10)
H12A_4	0.7191	0.0306	0.0141	0.042*
H12B_4	0.7174	0.0148	0.0672	0.042*
C13_4	0.8489 (4)	0.5587 (3)	−0.00105 (12)	0.0253 (8)
H13_4	0.8341	0.6354	0.0188	0.030*
C14_4	0.9959 (4)	0.5322 (4)	−0.00574 (13)	0.0314 (9)
H14A_4	1.0107	0.4528	−0.0238	0.038*
H14B_4	1.0329	0.5144	0.0240	0.038*
C15_4	1.0666 (4)	0.6513 (4)	−0.02803 (14)	0.0379 (10)
H15A_4	1.1621	0.6311	−0.0321	0.045*
H15B_4	1.0582	0.7289	−0.0088	0.045*
C16_4	1.0065 (4)	0.6843 (5)	−0.07334 (14)	0.0441 (11)
H16A_4	1.0496	0.7650	−0.0865	0.053*
H16B_4	1.0240	0.6105	−0.0936	0.053*
C17_4	0.8581 (4)	0.7071 (4)	−0.06915 (14)	0.0389 (10)
H17A_4	0.8215	0.7208	−0.0991	0.047*
H17B_4	0.8410	0.7883	−0.0522	0.047*
C18_4	0.7881 (4)	0.5892 (4)	−0.04553 (12)	0.0309 (9)
H18A_4	0.6928	0.6098	−0.0411	0.037*
H18B_4	0.7954	0.5104	−0.0643	0.037*
C19_4	0.4622 (4)	0.2782 (3)	−0.00060 (12)	0.0245 (8)
H19_4	0.4761	0.2050	0.0219	0.029*
C20_4	0.5301 (4)	0.2424 (4)	−0.04413 (12)	0.0320 (9)
H20A_4	0.6253	0.2250	−0.0391	0.038*
H20B_4	0.5236	0.3179	−0.0657	0.038*
C21_4	0.4666 (4)	0.1200 (4)	−0.06321 (14)	0.0388 (10)
H21A_4	0.5080	0.1025	−0.0926	0.047*
H21B_4	0.4831	0.0422	−0.0434	0.047*
C22_4	0.3176 (4)	0.1381 (5)	−0.06818 (15)	0.0443 (11)
H22A_4	0.2784	0.0545	−0.0783	0.053*
H22B_4	0.3014	0.2081	−0.0911	0.053*
C23_4	0.2502 (4)	0.1764 (4)	−0.02440 (13)	0.0364 (10)
H23A_4	0.1550	0.1939	−0.0293	0.044*
H23B_4	0.2569	0.1019	−0.0025	0.044*
C24_4	0.3146 (4)	0.2994 (4)	−0.00608 (12)	0.0278 (8)
H24A_4	0.3001	0.3761	−0.0266	0.033*
H24B_4	0.2727	0.3194	0.0230	0.033*
C25_4	0.5764 (4)	0.3212 (4)	0.12723 (12)	0.0263 (8)
H25_4	0.6221	0.2365	0.1197	0.032*
C26_4	0.4298 (4)	0.3024 (5)	0.12387 (14)	0.0399 (10)
H26A_4	0.4099	0.2697	0.0941	0.048*
H26B_4	0.3849	0.3890	0.1272	0.048*
C27_4	0.3755 (5)	0.2046 (5)	0.15918 (15)	0.0494 (12)
H27A_4	0.2777	0.2003	0.1571	0.059*
H27B_4	0.4113	0.1153	0.1533	0.059*
C28_4	0.4103 (4)	0.2419 (4)	0.20519 (14)	0.0412 (11)
H28A_4	0.3795	0.1721	0.2268	0.049*
H28B_4	0.3658	0.3260	0.2128	0.049*
C29_4	0.5582 (5)	0.2582 (5)	0.20774 (15)	0.0596 (14)
H29A_4	0.6014	0.1713	0.2032	0.072*
H29B_4	0.5803	0.2875	0.2378	0.072*
C30_4	0.6129 (5)	0.3588 (5)	0.17307 (14)	0.0587 (15)
H30A_4	0.5768	0.4478	0.1793	0.070*
H30B_4	0.7107	0.3631	0.1749	0.070*

Atomic displacement parameters (Ų)

	U^11	U^22	U^33	U^12	U^13	U^23
P1_1	0.0183 (5)	0.0247 (5)	0.0271 (5)	0.0011 (4)	0.0008 (4)	0.0009 (4)
O1_1	0.0169 (14)	0.0258 (14)	0.0323 (14)	0.0002 (10)	0.0005 (11)	0.0064 (11)
O2_1	0.0162 (13)	0.0242 (13)	0.0327 (14)	0.0029 (10)	0.0012 (11)	−0.0002 (11)
O3_1	0.0216 (14)	0.0334 (15)	0.0273 (14)	−0.0032 (11)	0.0002 (11)	0.0013 (11)
O4_1	0.0213 (14)	0.0283 (14)	0.0329 (14)	0.0045 (11)	−0.0034 (11)	−0.0032 (11)
O5_1	0.0204 (14)	0.0230 (13)	0.0388 (15)	0.0012 (10)	0.0028 (11)	0.0065 (11)
C1_1	0.027 (2)	0.0213 (19)	0.031 (2)	0.0064 (15)	0.0021 (16)	0.0011 (15)
C2_1	0.034 (2)	0.032 (2)	0.041 (2)	0.0075 (17)	−0.0081 (19)	−0.0070 (18)
C3_1	0.047 (3)	0.051 (3)	0.045 (3)	0.013 (2)	−0.019 (2)	−0.004 (2)
C4_1	0.035 (3)	0.042 (3)	0.061 (3)	0.014 (2)	−0.014 (2)	−0.001 (2)
C5_1	0.035 (2)	0.032 (2)	0.047 (3)	0.0099 (18)	−0.0011 (19)	−0.0072 (19)
C6_1	0.032 (2)	0.036 (2)	0.034 (2)	0.0094 (18)	0.0009 (18)	−0.0013 (18)
C7_1	0.025 (2)	0.0219 (19)	0.030 (2)	0.0039 (15)	−0.0022 (16)	0.0003 (15)
C8_1	0.018 (2)	0.042 (2)	0.040 (2)	0.0044 (17)	−0.0030 (17)	−0.0054 (18)
C9_1	0.025 (2)	0.053 (3)	0.040 (2)	0.0116 (19)	−0.0019 (18)	0.001 (2)
C10_1	0.037 (3)	0.047 (3)	0.053 (3)	0.022 (2)	0.003 (2)	−0.004 (2)
C11_1	0.046 (3)	0.031 (2)	0.055 (3)	0.0094 (19)	−0.001 (2)	−0.008 (2)
C12_1	0.025 (2)	0.035 (2)	0.040 (2)	0.0010 (17)	−0.0032 (18)	−0.0042 (18)
C13_1	0.021 (2)	0.032 (2)	0.032 (2)	0.0019 (16)	0.0037 (16)	0.0042 (16)
C14_1	0.058 (3)	0.031 (2)	0.033 (2)	0.002 (2)	0.004 (2)	0.0037 (18)
C15_1	0.046 (3)	0.034 (2)	0.045 (3)	−0.0098 (19)	0.002 (2)	0.0097 (19)
C16_1	0.038 (3)	0.049 (3)	0.033 (2)	0.007 (2)	0.0067 (19)	0.016 (2)
C17_1	0.061 (3)	0.058 (3)	0.030 (2)	0.000 (2)	0.011 (2)	−0.003 (2)
C18_1	0.046 (3)	0.046 (3)	0.037 (2)	−0.008 (2)	0.001 (2)	−0.002 (2)
C19_1	0.020 (2)	0.027 (2)	0.0263 (19)	−0.0004 (15)	−0.0005 (15)	0.0005 (15)
C20_1	0.034 (2)	0.026 (2)	0.034 (2)	0.0031 (17)	0.0001 (18)	0.0021 (16)
C21_1	0.038 (3)	0.026 (2)	0.044 (2)	−0.0034 (17)	−0.0001 (19)	0.0029 (18)
C22_1	0.044 (3)	0.034 (2)	0.041 (2)	−0.0053 (19)	0.007 (2)	0.0114 (19)
C23_1	0.033 (2)	0.043 (2)	0.030 (2)	−0.0005 (18)	0.0053 (18)	0.0037 (18)
C24_1	0.034 (2)	0.029 (2)	0.026 (2)	−0.0003 (17)	−0.0004 (17)	0.0010 (16)
C25_1	0.026 (2)	0.027 (2)	0.027 (2)	0.0033 (16)	−0.0020 (16)	−0.0012 (16)
C26_1	0.030 (2)	0.027 (2)	0.034 (2)	0.0081 (16)	−0.0029 (17)	−0.0016 (16)
C27_1	0.039 (3)	0.027 (2)	0.045 (2)	−0.0003 (18)	−0.0037 (19)	−0.0078 (18)
C28_1	0.045 (3)	0.044 (3)	0.043 (3)	−0.001 (2)	−0.014 (2)	−0.010 (2)
C29_1	0.043 (3)	0.041 (3)	0.041 (2)	0.006 (2)	−0.017 (2)	−0.0028 (19)
C30_1	0.035 (2)	0.033 (2)	0.031 (2)	0.0035 (17)	−0.0040 (18)	0.0000 (17)
P1_2	0.0197 (5)	0.0234 (5)	0.0285 (5)	0.0008 (4)	0.0008 (4)	−0.0006 (4)
O1_2	0.0184 (14)	0.0274 (14)	0.0317 (14)	0.0006 (10)	−0.0027 (11)	−0.0077 (11)
O2_2	0.0187 (14)	0.0212 (13)	0.0404 (15)	−0.0032 (10)	0.0009 (11)	0.0029 (11)
O3_2	0.0209 (14)	0.0366 (15)	0.0309 (15)	0.0044 (11)	0.0028 (11)	−0.0006 (12)
O4_2	0.0230 (14)	0.0261 (14)	0.0350 (15)	−0.0043 (11)	−0.0017 (11)	0.0050 (11)
O5_2	0.0211 (14)	0.0261 (14)	0.0375 (15)	−0.0016 (10)	0.0021 (11)	−0.0063 (11)
C1_2	0.024 (2)	0.0217 (19)	0.034 (2)	−0.0006 (15)	−0.0004 (16)	−0.0051 (15)
C2_2	0.030 (2)	0.031 (2)	0.040 (2)	−0.0071 (17)	−0.0076 (18)	0.0041 (17)
C3_2	0.050 (3)	0.045 (3)	0.046 (3)	−0.006 (2)	−0.019 (2)	−0.001 (2)
C4_2	0.030 (2)	0.036 (2)	0.069 (3)	−0.0121 (18)	−0.011 (2)	0.000 (2)
C5_2	0.036 (3)	0.038 (2)	0.047 (3)	−0.0118 (19)	0.002 (2)	0.005 (2)
C6_2	0.029 (2)	0.040 (2)	0.035 (2)	−0.0045 (18)	−0.0001 (18)	−0.0006 (18)
C7_2	0.023 (2)	0.024 (2)	0.034 (2)	−0.0033 (15)	−0.0019 (16)	−0.0012 (16)
C8_2	0.019 (2)	0.042 (2)	0.046 (2)	0.0002 (17)	−0.0030 (18)	0.0054 (19)
C9_2	0.029 (2)	0.059 (3)	0.049 (3)	−0.013 (2)	0.000 (2)	−0.006 (2)
C10_2	0.036 (3)	0.044 (3)	0.062 (3)	−0.020 (2)	0.001 (2)	−0.001 (2)
C11_2	0.047 (3)	0.032 (2)	0.060 (3)	−0.006 (2)	0.002 (2)	0.005 (2)
C12_2	0.031 (2)	0.029 (2)	0.042 (2)	−0.0031 (17)	−0.0056 (18)	0.0052 (18)
C13_2	0.028 (2)	0.032 (2)	0.028 (2)	−0.0024 (16)	0.0049 (16)	−0.0049 (16)
C14_2	0.064 (3)	0.036 (2)	0.032 (2)	0.009 (2)	0.004 (2)	−0.0030 (18)
C15_2	0.061 (3)	0.046 (3)	0.044 (3)	0.015 (2)	0.000 (2)	−0.011 (2)
C16_2	0.040 (3)	0.054 (3)	0.034 (2)	−0.004 (2)	0.003 (2)	−0.011 (2)
C17_2	0.080 (4)	0.066 (4)	0.035 (3)	0.014 (3)	0.019 (3)	0.004 (2)
C18_2	0.078 (4)	0.056 (3)	0.033 (3)	0.030 (3)	0.007 (2)	0.008 (2)
C19_2	0.021 (2)	0.028 (2)	0.030 (2)	0.0019 (15)	0.0002 (16)	−0.0039 (16)
C20_2	0.032 (2)	0.027 (2)	0.031 (2)	0.0022 (16)	−0.0043 (17)	0.0001 (16)
C21_2	0.043 (3)	0.025 (2)	0.039 (2)	0.0056 (18)	−0.0030 (19)	−0.0050 (17)
C22_2	0.048 (3)	0.035 (2)	0.040 (2)	0.007 (2)	0.009 (2)	−0.0100 (19)
C23_2	0.038 (3)	0.038 (2)	0.034 (2)	−0.0032 (19)	0.0116 (19)	−0.0005 (18)
C24_2	0.032 (2)	0.025 (2)	0.031 (2)	−0.0002 (16)	−0.0013 (17)	−0.0009 (16)
C25_2	0.021 (2)	0.024 (2)	0.033 (2)	0.0037 (15)	−0.0001 (16)	0.0038 (16)
C26_2	0.035 (2)	0.028 (2)	0.035 (2)	−0.0044 (17)	0.0022 (18)	0.0016 (17)
C27_2	0.038 (3)	0.027 (2)	0.051 (3)	0.0030 (18)	0.002 (2)	0.0087 (19)
C28_2	0.051 (3)	0.047 (3)	0.053 (3)	0.007 (2)	−0.012 (2)	0.012 (2)
C29_2	0.045 (3)	0.045 (3)	0.046 (3)	0.004 (2)	−0.020 (2)	0.000 (2)
C30_2	0.033 (2)	0.033 (2)	0.032 (2)	−0.0001 (17)	−0.0045 (17)	0.0019 (17)
P1_3	0.0237 (5)	0.0198 (5)	0.0288 (5)	−0.0003 (4)	−0.0026 (4)	0.0014 (4)
O1_3	0.0250 (15)	0.0213 (13)	0.0355 (15)	−0.0014 (10)	−0.0090 (11)	0.0004 (11)
O2_3	0.0225 (14)	0.0203 (13)	0.0342 (14)	−0.0029 (10)	−0.0006 (11)	0.0010 (11)
O3_3	0.0358 (16)	0.0187 (13)	0.0277 (14)	0.0051 (11)	−0.0022 (12)	0.0010 (10)
O4_3	0.0287 (15)	0.0206 (13)	0.0325 (14)	−0.0029 (10)	0.0043 (11)	−0.0004 (11)
O5_3	0.0272 (15)	0.0179 (13)	0.0422 (16)	−0.0023 (10)	−0.0123 (12)	0.0053 (11)
C1_3	0.024 (2)	0.025 (2)	0.028 (2)	0.0000 (15)	−0.0044 (16)	−0.0017 (15)
C2_3	0.034 (2)	0.030 (2)	0.036 (2)	−0.0047 (17)	0.0049 (18)	−0.0048 (17)
C3_3	0.047 (3)	0.051 (3)	0.041 (3)	−0.009 (2)	0.003 (2)	−0.020 (2)
C4_3	0.037 (3)	0.035 (2)	0.062 (3)	−0.0140 (19)	0.001 (2)	−0.014 (2)
C5_3	0.035 (3)	0.038 (2)	0.045 (3)	−0.0108 (19)	0.001 (2)	0.0014 (19)
C6_3	0.034 (2)	0.029 (2)	0.031 (2)	−0.0045 (17)	−0.0019 (17)	−0.0013 (16)
C7_3	0.029 (2)	0.0210 (19)	0.030 (2)	−0.0029 (15)	−0.0034 (16)	−0.0014 (15)
C8_3	0.037 (2)	0.020 (2)	0.044 (2)	−0.0011 (17)	0.0074 (19)	−0.0034 (17)
C9_3	0.055 (3)	0.024 (2)	0.042 (2)	−0.0147 (19)	−0.006 (2)	−0.0017 (18)
C10_3	0.038 (3)	0.035 (2)	0.056 (3)	−0.0161 (19)	−0.003 (2)	0.004 (2)
C11_3	0.026 (2)	0.050 (3)	0.057 (3)	−0.0097 (19)	0.001 (2)	−0.002 (2)
C12_3	0.031 (2)	0.028 (2)	0.040 (2)	−0.0036 (17)	0.0036 (18)	−0.0054 (17)
C13_3	0.035 (2)	0.0203 (19)	0.029 (2)	−0.0031 (16)	−0.0056 (17)	0.0050 (15)
C14_3	0.031 (2)	0.052 (3)	0.031 (2)	0.0033 (19)	−0.0023 (18)	0.0048 (19)
C15_3	0.041 (3)	0.055 (3)	0.040 (2)	0.012 (2)	−0.014 (2)	0.000 (2)
C16_3	0.051 (3)	0.035 (2)	0.033 (2)	−0.008 (2)	−0.013 (2)	0.0077 (18)
C17_3	0.056 (3)	0.062 (3)	0.029 (2)	0.003 (2)	0.001 (2)	0.013 (2)
C18_3	0.047 (3)	0.054 (3)	0.033 (2)	0.018 (2)	0.007 (2)	0.005 (2)
C19_3	0.028 (2)	0.0200 (19)	0.031 (2)	−0.0002 (15)	−0.0048 (16)	0.0010 (15)
C20_3	0.026 (2)	0.037 (2)	0.033 (2)	−0.0027 (17)	−0.0034 (17)	0.0019 (17)
C21_3	0.033 (3)	0.039 (2)	0.046 (3)	0.0032 (18)	−0.006 (2)	−0.0017 (19)
C22_3	0.038 (3)	0.044 (3)	0.047 (3)	0.006 (2)	−0.013 (2)	0.010 (2)
C23_3	0.041 (3)	0.040 (2)	0.034 (2)	−0.0008 (19)	−0.0050 (19)	0.0112 (18)
C24_3	0.025 (2)	0.034 (2)	0.032 (2)	0.0021 (16)	−0.0014 (17)	0.0019 (17)
C25_3	0.027 (2)	0.025 (2)	0.0236 (19)	0.0016 (15)	−0.0023 (15)	−0.0003 (15)
C26_3	0.027 (2)	0.034 (2)	0.031 (2)	−0.0083 (17)	−0.0025 (17)	−0.0013 (17)
C27_3	0.027 (2)	0.041 (2)	0.035 (2)	−0.0006 (18)	0.0041 (18)	0.0018 (18)
C28_3	0.041 (3)	0.040 (2)	0.036 (2)	0.0019 (19)	0.0087 (19)	−0.0074 (19)
C29_3	0.041 (3)	0.034 (2)	0.035 (2)	−0.0037 (18)	0.0004 (19)	−0.0095 (18)
C30_3	0.032 (2)	0.027 (2)	0.030 (2)	−0.0035 (16)	−0.0036 (17)	0.0001 (16)
P1_4	0.0226 (5)	0.0201 (5)	0.0285 (5)	0.0015 (4)	0.0008 (4)	0.0022 (4)
O1_4	0.0236 (14)	0.0191 (13)	0.0344 (14)	0.0024 (10)	0.0069 (11)	0.0024 (11)
O2_4	0.0234 (15)	0.0225 (14)	0.0389 (15)	0.0036 (11)	−0.0028 (11)	0.0027 (11)
O3_4	0.0234 (15)	0.0215 (13)	0.0387 (15)	0.0005 (10)	0.0074 (12)	0.0025 (11)
O4_4	0.0374 (16)	0.0201 (13)	0.0293 (14)	−0.0031 (11)	0.0004 (12)	0.0009 (11)
O5_4	0.0256 (15)	0.0226 (13)	0.0336 (14)	0.0041 (11)	−0.0055 (11)	−0.0021 (11)
C1_4	0.026 (2)	0.026 (2)	0.0282 (19)	0.0058 (15)	0.0019 (16)	0.0007 (15)
C2_4	0.038 (2)	0.028 (2)	0.036 (2)	0.0079 (17)	−0.0014 (18)	0.0002 (17)
C3_4	0.032 (2)	0.032 (2)	0.051 (3)	0.0100 (18)	−0.006 (2)	0.000 (2)
C4_4	0.037 (3)	0.037 (2)	0.059 (3)	0.0152 (19)	−0.002 (2)	−0.010 (2)
C5_4	0.046 (3)	0.050 (3)	0.046 (3)	0.012 (2)	−0.003 (2)	−0.021 (2)
C6_4	0.029 (2)	0.033 (2)	0.036 (2)	0.0052 (17)	−0.0037 (17)	−0.0046 (17)
C7_4	0.025 (2)	0.022 (2)	0.035 (2)	0.0054 (15)	0.0000 (16)	0.0019 (16)
C8_4	0.035 (2)	0.027 (2)	0.036 (2)	0.0042 (17)	−0.0027 (18)	−0.0006 (17)
C9_4	0.025 (2)	0.044 (3)	0.058 (3)	0.0064 (19)	−0.005 (2)	−0.001 (2)
C10_4	0.041 (3)	0.043 (3)	0.063 (3)	0.022 (2)	−0.002 (2)	0.003 (2)
C11_4	0.053 (3)	0.027 (2)	0.056 (3)	0.016 (2)	0.003 (2)	−0.006 (2)
C12_4	0.044 (3)	0.022 (2)	0.039 (2)	0.0068 (18)	−0.0081 (19)	−0.0027 (17)
C13_4	0.027 (2)	0.0198 (19)	0.029 (2)	0.0001 (15)	0.0027 (16)	0.0001 (15)
C14_4	0.022 (2)	0.035 (2)	0.037 (2)	−0.0015 (16)	0.0055 (17)	−0.0055 (18)
C15_4	0.028 (2)	0.041 (2)	0.045 (3)	−0.0056 (18)	0.0075 (19)	−0.0051 (19)
C16_4	0.034 (3)	0.052 (3)	0.045 (3)	−0.010 (2)	0.012 (2)	0.007 (2)
C17_4	0.043 (3)	0.040 (2)	0.033 (2)	−0.0076 (19)	0.0042 (19)	0.0090 (19)
C18_4	0.027 (2)	0.037 (2)	0.029 (2)	−0.0011 (17)	0.0005 (17)	−0.0012 (17)
C19_4	0.026 (2)	0.0208 (19)	0.027 (2)	−0.0015 (15)	−0.0039 (16)	0.0000 (15)
C20_4	0.030 (2)	0.035 (2)	0.031 (2)	0.0009 (17)	0.0004 (17)	−0.0011 (17)
C21_4	0.039 (3)	0.044 (3)	0.034 (2)	0.0054 (19)	−0.0039 (19)	−0.0143 (19)
C22_4	0.042 (3)	0.050 (3)	0.042 (3)	−0.002 (2)	−0.010 (2)	−0.015 (2)
C23_4	0.027 (2)	0.043 (3)	0.039 (2)	−0.0019 (18)	−0.0075 (18)	0.0033 (19)
C24_4	0.024 (2)	0.029 (2)	0.030 (2)	0.0034 (16)	−0.0014 (16)	0.0023 (16)
C25_4	0.029 (2)	0.0236 (19)	0.0252 (19)	0.0020 (15)	0.0016 (16)	0.0059 (15)
C26_4	0.030 (2)	0.057 (3)	0.032 (2)	−0.005 (2)	0.0006 (18)	0.002 (2)
C27_4	0.043 (3)	0.064 (3)	0.041 (3)	−0.017 (2)	0.015 (2)	−0.002 (2)
C28_4	0.045 (3)	0.043 (3)	0.035 (2)	0.003 (2)	0.012 (2)	0.0031 (19)
C29_4	0.068 (4)	0.078 (4)	0.032 (3)	−0.014 (3)	−0.003 (2)	0.017 (2)
C30_4	0.061 (3)	0.083 (4)	0.032 (3)	−0.038 (3)	−0.010 (2)	0.012 (2)

Geometric parameters (Å, º)

P1_1—O4_1	1.602 (3)	P1_3—O5_3	1.602 (3)
P1_1—O5_1	1.607 (2)	P1_3—O3_3	1.607 (3)
P1_1—O3_1	1.611 (3)	P1_3—O4_3	1.607 (3)
P1_1—O1_1	1.653 (2)	P1_3—O1_3	1.651 (2)
P1_1—O2_1	1.675 (2)	P1_3—O2_3	1.673 (2)
O1_1—C1_1	1.443 (4)	O1_3—C1_3	1.438 (4)
O2_1—C7_1	1.440 (4)	O2_3—C7_3	1.433 (4)
O3_1—C13_1	1.449 (4)	O3_3—C13_3	1.460 (4)
O4_1—C25_1	1.452 (4)	O4_3—C25_3	1.447 (4)
O5_1—C19_1	1.443 (4)	O5_3—C19_3	1.452 (4)
C1_1—C6_1	1.510 (5)	C1_3—C2_3	1.509 (5)
C1_1—C2_1	1.514 (5)	C1_3—C6_3	1.516 (5)
C1_1—H1_1	1.000	C1_3—H1_3	1.000
C2_1—C3_1	1.521 (5)	C2_3—C3_3	1.528 (6)
C2_1—H2A_1	0.990	C2_3—H2A_3	0.990
C2_1—H2B_1	0.990	C2_3—H2B_3	0.990
C3_1—C4_1	1.519 (6)	C3_3—C4_3	1.526 (6)
C3_1—H3A_1	0.990	C3_3—H3A_3	0.990
C3_1—H3B_1	0.990	C3_3—H3B_3	0.990
C4_1—C5_1	1.523 (6)	C4_3—C5_3	1.513 (6)
C4_1—H4A_1	0.990	C4_3—H4A_3	0.990
C4_1—H4B_1	0.990	C4_3—H4B_3	0.990
C5_1—C6_1	1.523 (5)	C5_3—C6_3	1.521 (5)
C5_1—H5A_1	0.990	C5_3—H5A_3	0.990
C5_1—H5B_1	0.990	C5_3—H5B_3	0.990
C6_1—H6A_1	0.990	C6_3—H6A_3	0.990
C6_1—H6B_1	0.990	C6_3—H6B_3	0.990
C7_1—C8_1	1.510 (5)	C7_3—C12_3	1.514 (5)
C7_1—C12_1	1.514 (5)	C7_3—C8_3	1.528 (5)
C7_1—H7_1	1.000	C7_3—H7_3	1.000
C8_1—C9_1	1.527 (5)	C8_3—C9_3	1.528 (6)
C8_1—H8A_1	0.990	C8_3—H8A_3	0.990
C8_1—H8B_1	0.990	C8_3—H8B_3	0.990
C9_1—C10_1	1.512 (6)	C9_3—C10_3	1.507 (6)
C9_1—H9A_1	0.990	C9_3—H9A_3	0.990
C9_1—H9B_1	0.990	C9_3—H9B_3	0.990
C10_1—C11_1	1.521 (6)	C10_3—C11_3	1.517 (6)
C10_1—H10A_1	0.990	C10_3—H10A_3	0.990
C10_1—H10B_1	0.990	C10_3—H10B_3	0.990
C11_1—C12_1	1.521 (5)	C11_3—C12_3	1.534 (5)
C11_1—H11A_1	0.990	C11_3—H11A_3	0.990
C11_1—H11B_1	0.990	C11_3—H11B_3	0.990
C12_1—H12A_1	0.990	C12_3—H12A_3	0.990
C12_1—H12B_1	0.990	C12_3—H12B_3	0.990
C13_1—C18_1	1.491 (6)	C13_3—C18_3	1.501 (5)
C13_1—C14_1	1.509 (5)	C13_3—C14_3	1.509 (5)
C13_1—H13_1	1.000	C13_3—H13_3	1.000
C14_1—C15_1	1.528 (6)	C14_3—C15_3	1.521 (6)
C14_1—H14A_1	0.990	C14_3—H14A_3	0.990
C14_1—H14B_1	0.990	C14_3—H14B_3	0.990
C15_1—C16_1	1.504 (6)	C15_3—C16_3	1.503 (6)
C15_1—H15A_1	0.990	C15_3—H15A_3	0.990
C15_1—H15B_1	0.990	C15_3—H15B_3	0.990
C16_1—C17_1	1.515 (6)	C16_3—C17_3	1.519 (6)
C16_1—H16A_1	0.990	C16_3—H16A_3	0.990
C16_1—H16B_1	0.990	C16_3—H16B_3	0.990
C17_1—C18_1	1.527 (6)	C17_3—C18_3	1.524 (6)
C17_1—H17A_1	0.990	C17_3—H17A_3	0.990
C17_1—H17B_1	0.990	C17_3—H17B_3	0.990
C18_1—H18A_1	0.990	C18_3—H18A_3	0.990
C18_1—H18B_1	0.990	C18_3—H18B_3	0.990
C19_1—C24_1	1.510 (5)	C19_3—C24_3	1.506 (5)
C19_1—C20_1	1.519 (5)	C19_3—C20_3	1.516 (5)
C19_1—H19_1	1.000	C19_3—H19_3	1.000
C20_1—C21_1	1.527 (5)	C20_3—C21_3	1.518 (6)
C20_1—H20A_1	0.990	C20_3—H20A_3	0.990
C20_1—H20B_1	0.990	C20_3—H20B_3	0.990
C21_1—C22_1	1.516 (6)	C21_3—C22_3	1.526 (6)
C21_1—H21A_1	0.990	C21_3—H21A_3	0.990
C21_1—H21B_1	0.990	C21_3—H21B_3	0.990
C22_1—C23_1	1.511 (5)	C22_3—C23_3	1.517 (6)
C22_1—H22A_1	0.990	C22_3—H22A_3	0.990
C22_1—H22B_1	0.990	C22_3—H22B_3	0.990
C23_1—C24_1	1.526 (5)	C23_3—C24_3	1.530 (5)
C23_1—H23A_1	0.990	C23_3—H23A_3	0.990
C23_1—H23B_1	0.990	C23_3—H23B_3	0.990
C24_1—H24A_1	0.990	C24_3—H24A_3	0.990
C24_1—H24B_1	0.990	C24_3—H24B_3	0.990
C25_1—C26_1	1.514 (5)	C25_3—C30_3	1.512 (5)
C25_1—C30_1	1.526 (5)	C25_3—C26_3	1.515 (5)
C25_1—H25_1	1.000	C25_3—H25_3	1.000
C26_1—C27_1	1.536 (6)	C26_3—C27_3	1.518 (5)
C26_1—H26A_1	0.990	C26_3—H26A_3	0.990
C26_1—H26B_1	0.990	C26_3—H26B_3	0.990
C27_1—C28_1	1.518 (6)	C27_3—C28_3	1.528 (6)
C27_1—H27A_1	0.990	C27_3—H27A_3	0.990
C27_1—H27B_1	0.990	C27_3—H27B_3	0.990
C28_1—C29_1	1.519 (6)	C28_3—C29_3	1.526 (6)
C28_1—H28A_1	0.990	C28_3—H28A_3	0.990
C28_1—H28B_1	0.990	C28_3—H28B_3	0.990
C29_1—C30_1	1.531 (6)	C29_3—C30_3	1.520 (5)
C29_1—H29A_1	0.990	C29_3—H29A_3	0.990
C29_1—H29B_1	0.990	C29_3—H29B_3	0.990
C30_1—H30A_1	0.990	C30_3—H30A_3	0.990
C30_1—H30B_1	0.990	C30_3—H30B_3	0.990
P1_2—O5_2	1.603 (3)	P1_4—O5_4	1.602 (3)
P1_2—O4_2	1.605 (3)	P1_4—O3_4	1.604 (3)
P1_2—O3_2	1.606 (3)	P1_4—O4_4	1.614 (3)
P1_2—O1_2	1.654 (3)	P1_4—O1_4	1.652 (2)
P1_2—O2_2	1.669 (3)	P1_4—O2_4	1.673 (2)
O1_2—C1_2	1.435 (4)	O1_4—C1_4	1.429 (4)
O2_2—C7_2	1.435 (4)	O2_4—C7_4	1.433 (4)
O3_2—C13_2	1.459 (4)	O3_4—C13_4	1.451 (4)
O4_2—C25_2	1.444 (4)	O4_4—C25_4	1.445 (4)
O5_2—C19_2	1.449 (4)	O5_4—C19_4	1.454 (4)
C1_2—C6_2	1.507 (5)	C1_4—C2_4	1.520 (5)
C1_2—C2_2	1.515 (5)	C1_4—C6_4	1.526 (5)
C1_2—H1_2	1.000	C1_4—H1_4	1.000
C2_2—C3_2	1.516 (6)	C2_4—C3_4	1.527 (5)
C2_2—H2A_2	0.990	C2_4—H2A_4	0.990
C2_2—H2B_2	0.990	C2_4—H2B_4	0.990
C3_2—C4_2	1.511 (6)	C3_4—C4_4	1.512 (6)
C3_2—H3A_2	0.990	C3_4—H3A_4	0.990
C3_2—H3B_2	0.990	C3_4—H3B_4	0.990
C4_2—C5_2	1.523 (6)	C4_4—C5_4	1.532 (6)
C4_2—H4A_2	0.990	C4_4—H4A_4	0.990
C4_2—H4B_2	0.990	C4_4—H4B_4	0.990
C5_2—C6_2	1.528 (6)	C5_4—C6_4	1.531 (5)
C5_2—H5A_2	0.990	C5_4—H5A_4	0.990
C5_2—H5B_2	0.990	C5_4—H5B_4	0.990
C6_2—H6A_2	0.990	C6_4—H6A_4	0.990
C6_2—H6B_2	0.990	C6_4—H6B_4	0.990
C7_2—C8_2	1.509 (5)	C7_4—C8_4	1.504 (5)
C7_2—C12_2	1.522 (5)	C7_4—C12_4	1.518 (5)
C7_2—H7_2	1.000	C7_4—H7_4	1.000
C8_2—C9_2	1.537 (6)	C8_4—C9_4	1.529 (5)
C8_2—H8A_2	0.990	C8_4—H8A_4	0.990
C8_2—H8B_2	0.990	C8_4—H8B_4	0.990
C9_2—C10_2	1.510 (6)	C9_4—C10_4	1.523 (6)
C9_2—H9A_2	0.990	C9_4—H9A_4	0.990
C9_2—H9B_2	0.990	C9_4—H9B_4	0.990
C10_2—C11_2	1.539 (6)	C10_4—C11_4	1.516 (6)
C10_2—H10A_2	0.990	C10_4—H10A_4	0.990
C10_2—H10B_2	0.990	C10_4—H10B_4	0.990
C11_2—C12_2	1.526 (6)	C11_4—C12_4	1.535 (5)
C11_2—H11A_2	0.990	C11_4—H11A_4	0.990
C11_2—H11B_2	0.990	C11_4—H11B_4	0.990
C12_2—H12A_2	0.990	C12_4—H12A_4	0.990
C12_2—H12B_2	0.990	C12_4—H12B_4	0.990
C13_2—C18_2	1.498 (5)	C13_4—C14_4	1.510 (5)
C13_2—C14_2	1.509 (5)	C13_4—C18_4	1.511 (5)
C13_2—H13_2	1.000	C13_4—H13_4	1.000
C14_2—C15_2	1.518 (6)	C14_4—C15_4	1.528 (5)
C14_2—H14A_2	0.990	C14_4—H14A_4	0.990
C14_2—H14B_2	0.990	C14_4—H14B_4	0.990
C15_2—C16_2	1.499 (6)	C15_4—C16_4	1.535 (6)
C15_2—H15A_2	0.990	C15_4—H15A_4	0.990
C15_2—H15B_2	0.990	C15_4—H15B_4	0.990
C16_2—C17_2	1.505 (6)	C16_4—C17_4	1.516 (6)
C16_2—H16A_2	0.990	C16_4—H16A_4	0.990
C16_2—H16B_2	0.990	C16_4—H16B_4	0.990
C17_2—C18_2	1.525 (6)	C17_4—C18_4	1.532 (5)
C17_2—H17A_2	0.990	C17_4—H17A_4	0.990
C17_2—H17B_2	0.990	C17_4—H17B_4	0.990
C18_2—H18A_2	0.990	C18_4—H18A_4	0.990
C18_2—H18B_2	0.990	C18_4—H18B_4	0.990
C19_2—C20_2	1.517 (5)	C19_4—C20_4	1.517 (5)
C19_2—C24_2	1.521 (5)	C19_4—C24_4	1.517 (5)
C19_2—H19_2	1.000	C19_4—H19_4	1.000
C20_2—C21_2	1.519 (5)	C20_4—C21_4	1.524 (5)
C20_2—H20A_2	0.990	C20_4—H20A_4	0.990
C20_2—H20B_2	0.990	C20_4—H20B_4	0.990
C21_2—C22_2	1.526 (6)	C21_4—C22_4	1.524 (6)
C21_2—H21A_2	0.990	C21_4—H21A_4	0.990
C21_2—H21B_2	0.990	C21_4—H21B_4	0.990
C22_2—C23_2	1.531 (5)	C22_4—C23_4	1.528 (6)
C22_2—H22A_2	0.990	C22_4—H22A_4	0.990
C22_2—H22B_2	0.990	C22_4—H22B_4	0.990
C23_2—C24_2	1.521 (5)	C23_4—C24_4	1.523 (5)
C23_2—H23A_2	0.990	C23_4—H23A_4	0.990
C23_2—H23B_2	0.990	C23_4—H23B_4	0.990
C24_2—H24A_2	0.990	C24_4—H24A_4	0.990
C24_2—H24B_2	0.990	C24_4—H24B_4	0.990
C25_2—C30_2	1.514 (5)	C25_4—C30_4	1.496 (6)
C25_2—C26_2	1.525 (5)	C25_4—C26_4	1.497 (5)
C25_2—H25_2	1.000	C25_4—H25_4	1.000
C26_2—C27_2	1.533 (6)	C26_4—C27_4	1.522 (6)
C26_2—H26A_2	0.990	C26_4—H26A_4	0.990
C26_2—H26B_2	0.990	C26_4—H26B_4	0.990
C27_2—C28_2	1.515 (6)	C27_4—C28_4	1.496 (6)
C27_2—H27A_2	0.990	C27_4—H27A_4	0.990
C27_2—H27B_2	0.990	C27_4—H27B_4	0.990
C28_2—C29_2	1.534 (6)	C28_4—C29_4	1.504 (6)
C28_2—H28A_2	0.990	C28_4—H28A_4	0.990
C28_2—H28B_2	0.990	C28_4—H28B_4	0.990
C29_2—C30_2	1.530 (6)	C29_4—C30_4	1.529 (6)
C29_2—H29A_2	0.990	C29_4—H29A_4	0.990
C29_2—H29B_2	0.990	C29_4—H29B_4	0.990
C30_2—H30A_2	0.990	C30_4—H30A_4	0.990
C30_2—H30B_2	0.990	C30_4—H30B_4	0.990
O4_1—P1_1—O5_1	120.09 (14)	O5_3—P1_3—O3_3	123.95 (15)
O4_1—P1_1—O3_1	115.78 (14)	O5_3—P1_3—O4_3	120.15 (15)
O5_1—P1_1—O3_1	124.04 (14)	O3_3—P1_3—O4_3	115.84 (14)
O4_1—P1_1—O1_1	90.17 (13)	O5_3—P1_3—O1_3	89.53 (13)
O5_1—P1_1—O1_1	88.78 (12)	O3_3—P1_3—O1_3	88.24 (13)
O3_1—P1_1—O1_1	88.27 (13)	O4_3—P1_3—O1_3	89.96 (13)
O4_1—P1_1—O2_1	92.28 (13)	O5_3—P1_3—O2_3	87.64 (12)
O5_1—P1_1—O2_1	88.07 (13)	O3_3—P1_3—O2_3	92.56 (13)
O3_1—P1_1—O2_1	92.66 (13)	O4_3—P1_3—O2_3	92.28 (13)
O1_1—P1_1—O2_1	176.70 (13)	O1_3—P1_3—O2_3	177.02 (14)
C1_1—O1_1—P1_1	123.8 (2)	C1_3—O1_3—P1_3	124.4 (2)
C7_1—O2_1—P1_1	127.2 (2)	C7_3—O2_3—P1_3	127.7 (2)
C13_1—O3_1—P1_1	128.4 (2)	C13_3—O3_3—P1_3	128.5 (2)
C25_1—O4_1—P1_1	127.8 (2)	C25_3—O4_3—P1_3	128.0 (2)
C19_1—O5_1—P1_1	129.6 (2)	C19_3—O5_3—P1_3	129.4 (2)
O1_1—C1_1—C6_1	108.6 (3)	O1_3—C1_3—C2_3	109.3 (3)
O1_1—C1_1—C2_1	108.5 (3)	O1_3—C1_3—C6_3	108.3 (3)
C6_1—C1_1—C2_1	111.8 (3)	C2_3—C1_3—C6_3	111.3 (3)
O1_1—C1_1—H1_1	109.3	O1_3—C1_3—H1_3	109.3
C6_1—C1_1—H1_1	109.3	C2_3—C1_3—H1_3	109.3
C2_1—C1_1—H1_1	109.3	C6_3—C1_3—H1_3	109.3
C1_1—C2_1—C3_1	111.9 (3)	C1_3—C2_3—C3_3	111.7 (3)
C1_1—C2_1—H2A_1	109.2	C1_3—C2_3—H2A_3	109.3
C3_1—C2_1—H2A_1	109.2	C3_3—C2_3—H2A_3	109.3
C1_1—C2_1—H2B_1	109.2	C1_3—C2_3—H2B_3	109.3
C3_1—C2_1—H2B_1	109.2	C3_3—C2_3—H2B_3	109.3
H2A_1—C2_1—H2B_1	107.9	H2A_3—C2_3—H2B_3	107.9
C4_1—C3_1—C2_1	111.2 (4)	C4_3—C3_3—C2_3	111.2 (4)
C4_1—C3_1—H3A_1	109.4	C4_3—C3_3—H3A_3	109.4
C2_1—C3_1—H3A_1	109.4	C2_3—C3_3—H3A_3	109.4
C4_1—C3_1—H3B_1	109.4	C4_3—C3_3—H3B_3	109.4
C2_1—C3_1—H3B_1	109.4	C2_3—C3_3—H3B_3	109.4
H3A_1—C3_1—H3B_1	108.0	H3A_3—C3_3—H3B_3	108.0
C3_1—C4_1—C5_1	110.5 (4)	C5_3—C4_3—C3_3	110.0 (4)
C3_1—C4_1—H4A_1	109.5	C5_3—C4_3—H4A_3	109.7
C5_1—C4_1—H4A_1	109.5	C3_3—C4_3—H4A_3	109.7
C3_1—C4_1—H4B_1	109.5	C5_3—C4_3—H4B_3	109.7
C5_1—C4_1—H4B_1	109.5	C3_3—C4_3—H4B_3	109.7
H4A_1—C4_1—H4B_1	108.1	H4A_3—C4_3—H4B_3	108.2
C6_1—C5_1—C4_1	111.4 (3)	C4_3—C5_3—C6_3	111.5 (4)
C6_1—C5_1—H5A_1	109.4	C4_3—C5_3—H5A_3	109.3
C4_1—C5_1—H5A_1	109.4	C6_3—C5_3—H5A_3	109.3
C6_1—C5_1—H5B_1	109.4	C4_3—C5_3—H5B_3	109.3
C4_1—C5_1—H5B_1	109.4	C6_3—C5_3—H5B_3	109.3
H5A_1—C5_1—H5B_1	108.0	H5A_3—C5_3—H5B_3	108.0
C1_1—C6_1—C5_1	111.5 (3)	C1_3—C6_3—C5_3	111.3 (3)
C1_1—C6_1—H6A_1	109.3	C1_3—C6_3—H6A_3	109.4
C5_1—C6_1—H6A_1	109.3	C5_3—C6_3—H6A_3	109.4
C1_1—C6_1—H6B_1	109.3	C1_3—C6_3—H6B_3	109.4
C5_1—C6_1—H6B_1	109.3	C5_3—C6_3—H6B_3	109.4
H6A_1—C6_1—H6B_1	108.0	H6A_3—C6_3—H6B_3	108.0
O2_1—C7_1—C8_1	106.2 (3)	O2_3—C7_3—C12_3	113.5 (3)
O2_1—C7_1—C12_1	114.1 (3)	O2_3—C7_3—C8_3	106.3 (3)
C8_1—C7_1—C12_1	110.4 (3)	C12_3—C7_3—C8_3	109.8 (3)
O2_1—C7_1—H7_1	108.7	O2_3—C7_3—H7_3	109.0
C8_1—C7_1—H7_1	108.7	C12_3—C7_3—H7_3	109.0
C12_1—C7_1—H7_1	108.7	C8_3—C7_3—H7_3	109.0
C7_1—C8_1—C9_1	110.8 (3)	C9_3—C8_3—C7_3	110.4 (3)
C7_1—C8_1—H8A_1	109.5	C9_3—C8_3—H8A_3	109.6
C9_1—C8_1—H8A_1	109.5	C7_3—C8_3—H8A_3	109.6
C7_1—C8_1—H8B_1	109.5	C9_3—C8_3—H8B_3	109.6
C9_1—C8_1—H8B_1	109.5	C7_3—C8_3—H8B_3	109.6
H8A_1—C8_1—H8B_1	108.1	H8A_3—C8_3—H8B_3	108.1
C10_1—C9_1—C8_1	111.5 (3)	C10_3—C9_3—C8_3	110.9 (3)
C10_1—C9_1—H9A_1	109.3	C10_3—C9_3—H9A_3	109.5
C8_1—C9_1—H9A_1	109.3	C8_3—C9_3—H9A_3	109.5
C10_1—C9_1—H9B_1	109.3	C10_3—C9_3—H9B_3	109.5
C8_1—C9_1—H9B_1	109.3	C8_3—C9_3—H9B_3	109.5
H9A_1—C9_1—H9B_1	108.0	H9A_3—C9_3—H9B_3	108.0
C9_1—C10_1—C11_1	110.9 (3)	C9_3—C10_3—C11_3	111.4 (3)
C9_1—C10_1—H10A_1	109.5	C9_3—C10_3—H10A_3	109.4
C11_1—C10_1—H10A_1	109.5	C11_3—C10_3—H10A_3	109.4
C9_1—C10_1—H10B_1	109.5	C9_3—C10_3—H10B_3	109.4
C11_1—C10_1—H10B_1	109.5	C11_3—C10_3—H10B_3	109.4
H10A_1—C10_1—H10B_1	108.0	H10A_3—C10_3—H10B_3	108.0
C12_1—C11_1—C10_1	111.0 (4)	C10_3—C11_3—C12_3	110.4 (4)
C12_1—C11_1—H11A_1	109.4	C10_3—C11_3—H11A_3	109.6
C10_1—C11_1—H11A_1	109.4	C12_3—C11_3—H11A_3	109.6
C12_1—C11_1—H11B_1	109.4	C10_3—C11_3—H11B_3	109.6
C10_1—C11_1—H11B_1	109.4	C12_3—C11_3—H11B_3	109.6
H11A_1—C11_1—H11B_1	108.0	H11A_3—C11_3—H11B_3	108.1
C7_1—C12_1—C11_1	110.6 (3)	C7_3—C12_3—C11_3	110.8 (3)
C7_1—C12_1—H12A_1	109.5	C7_3—C12_3—H12A_3	109.5
C11_1—C12_1—H12A_1	109.5	C11_3—C12_3—H12A_3	109.5
C7_1—C12_1—H12B_1	109.5	C7_3—C12_3—H12B_3	109.5
C11_1—C12_1—H12B_1	109.5	C11_3—C12_3—H12B_3	109.5
H12A_1—C12_1—H12B_1	108.1	H12A_3—C12_3—H12B_3	108.1
O3_1—C13_1—C18_1	107.5 (3)	O3_3—C13_3—C18_3	106.9 (3)
O3_1—C13_1—C14_1	110.6 (3)	O3_3—C13_3—C14_3	110.6 (3)
C18_1—C13_1—C14_1	111.8 (3)	C18_3—C13_3—C14_3	111.6 (3)
O3_1—C13_1—H13_1	108.9	O3_3—C13_3—H13_3	109.2
C18_1—C13_1—H13_1	108.9	C18_3—C13_3—H13_3	109.2
C14_1—C13_1—H13_1	108.9	C14_3—C13_3—H13_3	109.2
C13_1—C14_1—C15_1	111.3 (3)	C13_3—C14_3—C15_3	110.4 (3)
C13_1—C14_1—H14A_1	109.4	C13_3—C14_3—H14A_3	109.6
C15_1—C14_1—H14A_1	109.4	C15_3—C14_3—H14A_3	109.6
C13_1—C14_1—H14B_1	109.4	C13_3—C14_3—H14B_3	109.6
C15_1—C14_1—H14B_1	109.4	C15_3—C14_3—H14B_3	109.6
H14A_1—C14_1—H14B_1	108.0	H14A_3—C14_3—H14B_3	108.1
C16_1—C15_1—C14_1	112.2 (4)	C16_3—C15_3—C14_3	112.4 (4)
C16_1—C15_1—H15A_1	109.2	C16_3—C15_3—H15A_3	109.1
C14_1—C15_1—H15A_1	109.2	C14_3—C15_3—H15A_3	109.1
C16_1—C15_1—H15B_1	109.2	C16_3—C15_3—H15B_3	109.1
C14_1—C15_1—H15B_1	109.2	C14_3—C15_3—H15B_3	109.1
H15A_1—C15_1—H15B_1	107.9	H15A_3—C15_3—H15B_3	107.8
C15_1—C16_1—C17_1	110.4 (3)	C15_3—C16_3—C17_3	109.6 (4)
C15_1—C16_1—H16A_1	109.6	C15_3—C16_3—H16A_3	109.7
C17_1—C16_1—H16A_1	109.6	C17_3—C16_3—H16A_3	109.7
C15_1—C16_1—H16B_1	109.6	C15_3—C16_3—H16B_3	109.7
C17_1—C16_1—H16B_1	109.6	C17_3—C16_3—H16B_3	109.7
H16A_1—C16_1—H16B_1	108.1	H16A_3—C16_3—H16B_3	108.2
C16_1—C17_1—C18_1	111.6 (4)	C16_3—C17_3—C18_3	111.2 (4)
C16_1—C17_1—H17A_1	109.3	C16_3—C17_3—H17A_3	109.4
C18_1—C17_1—H17A_1	109.3	C18_3—C17_3—H17A_3	109.4
C16_1—C17_1—H17B_1	109.3	C16_3—C17_3—H17B_3	109.4
C18_1—C17_1—H17B_1	109.3	C18_3—C17_3—H17B_3	109.4
H17A_1—C17_1—H17B_1	108.0	H17A_3—C17_3—H17B_3	108.0
C13_1—C18_1—C17_1	112.1 (4)	C13_3—C18_3—C17_3	110.9 (3)
C13_1—C18_1—H18A_1	109.2	C13_3—C18_3—H18A_3	109.5
C17_1—C18_1—H18A_1	109.2	C17_3—C18_3—H18A_3	109.5
C13_1—C18_1—H18B_1	109.2	C13_3—C18_3—H18B_3	109.5
C17_1—C18_1—H18B_1	109.2	C17_3—C18_3—H18B_3	109.5
H18A_1—C18_1—H18B_1	107.9	H18A_3—C18_3—H18B_3	108.0
O5_1—C19_1—C24_1	111.6 (3)	O5_3—C19_3—C24_3	111.6 (3)
O5_1—C19_1—C20_1	106.9 (3)	O5_3—C19_3—C20_3	106.5 (3)
C24_1—C19_1—C20_1	110.5 (3)	C24_3—C19_3—C20_3	111.0 (3)
O5_1—C19_1—H19_1	109.3	O5_3—C19_3—H19_3	109.2
C24_1—C19_1—H19_1	109.3	C24_3—C19_3—H19_3	109.2
C20_1—C19_1—H19_1	109.3	C20_3—C19_3—H19_3	109.2
C19_1—C20_1—C21_1	109.4 (3)	C19_3—C20_3—C21_3	109.9 (3)
C19_1—C20_1—H20A_1	109.8	C19_3—C20_3—H20A_3	109.7
C21_1—C20_1—H20A_1	109.8	C21_3—C20_3—H20A_3	109.7
C19_1—C20_1—H20B_1	109.8	C19_3—C20_3—H20B_3	109.7
C21_1—C20_1—H20B_1	109.8	C21_3—C20_3—H20B_3	109.7
H20A_1—C20_1—H20B_1	108.2	H20A_3—C20_3—H20B_3	108.2
C22_1—C21_1—C20_1	111.5 (3)	C20_3—C21_3—C22_3	111.3 (3)
C22_1—C21_1—H21A_1	109.3	C20_3—C21_3—H21A_3	109.4
C20_1—C21_1—H21A_1	109.3	C22_3—C21_3—H21A_3	109.4
C22_1—C21_1—H21B_1	109.3	C20_3—C21_3—H21B_3	109.4
C20_1—C21_1—H21B_1	109.3	C22_3—C21_3—H21B_3	109.4
H21A_1—C21_1—H21B_1	108.0	H21A_3—C21_3—H21B_3	108.0
C23_1—C22_1—C21_1	112.4 (3)	C23_3—C22_3—C21_3	111.6 (4)
C23_1—C22_1—H22A_1	109.1	C23_3—C22_3—H22A_3	109.3
C21_1—C22_1—H22A_1	109.1	C21_3—C22_3—H22A_3	109.3
C23_1—C22_1—H22B_1	109.1	C23_3—C22_3—H22B_3	109.3
C21_1—C22_1—H22B_1	109.1	C21_3—C22_3—H22B_3	109.3
H22A_1—C22_1—H22B_1	107.9	H22A_3—C22_3—H22B_3	108.0
C22_1—C23_1—C24_1	111.3 (3)	C22_3—C23_3—C24_3	112.1 (3)
C22_1—C23_1—H23A_1	109.4	C22_3—C23_3—H23A_3	109.2
C24_1—C23_1—H23A_1	109.4	C24_3—C23_3—H23A_3	109.2
C22_1—C23_1—H23B_1	109.4	C22_3—C23_3—H23B_3	109.2
C24_1—C23_1—H23B_1	109.4	C24_3—C23_3—H23B_3	109.2
H23A_1—C23_1—H23B_1	108.0	H23A_3—C23_3—H23B_3	107.9
C19_1—C24_1—C23_1	110.3 (3)	C19_3—C24_3—C23_3	110.0 (3)
C19_1—C24_1—H24A_1	109.6	C19_3—C24_3—H24A_3	109.7
C23_1—C24_1—H24A_1	109.6	C23_3—C24_3—H24A_3	109.7
C19_1—C24_1—H24B_1	109.6	C19_3—C24_3—H24B_3	109.7
C23_1—C24_1—H24B_1	109.6	C23_3—C24_3—H24B_3	109.7
H24A_1—C24_1—H24B_1	108.1	H24A_3—C24_3—H24B_3	108.2
O4_1—C25_1—C26_1	106.8 (3)	O4_3—C25_3—C30_3	111.3 (3)
O4_1—C25_1—C30_1	110.5 (3)	O4_3—C25_3—C26_3	107.0 (3)
C26_1—C25_1—C30_1	110.4 (3)	C30_3—C25_3—C26_3	111.3 (3)
O4_1—C25_1—H25_1	109.7	O4_3—C25_3—H25_3	109.1
C26_1—C25_1—H25_1	109.7	C30_3—C25_3—H25_3	109.1
C30_1—C25_1—H25_1	109.7	C26_3—C25_3—H25_3	109.1
C25_1—C26_1—C27_1	109.6 (3)	C25_3—C26_3—C27_3	109.7 (3)
C25_1—C26_1—H26A_1	109.7	C25_3—C26_3—H26A_3	109.7
C27_1—C26_1—H26A_1	109.7	C27_3—C26_3—H26A_3	109.7
C25_1—C26_1—H26B_1	109.7	C25_3—C26_3—H26B_3	109.7
C27_1—C26_1—H26B_1	109.7	C27_3—C26_3—H26B_3	109.7
H26A_1—C26_1—H26B_1	108.2	H26A_3—C26_3—H26B_3	108.2
C28_1—C27_1—C26_1	111.1 (3)	C26_3—C27_3—C28_3	111.9 (3)
C28_1—C27_1—H27A_1	109.4	C26_3—C27_3—H27A_3	109.2
C26_1—C27_1—H27A_1	109.4	C28_3—C27_3—H27A_3	109.2
C28_1—C27_1—H27B_1	109.4	C26_3—C27_3—H27B_3	109.2
C26_1—C27_1—H27B_1	109.4	C28_3—C27_3—H27B_3	109.2
H27A_1—C27_1—H27B_1	108.0	H27A_3—C27_3—H27B_3	107.9
C27_1—C28_1—C29_1	111.9 (3)	C29_3—C28_3—C27_3	111.0 (3)
C27_1—C28_1—H28A_1	109.2	C29_3—C28_3—H28A_3	109.4
C29_1—C28_1—H28A_1	109.2	C27_3—C28_3—H28A_3	109.4
C27_1—C28_1—H28B_1	109.2	C29_3—C28_3—H28B_3	109.4
C29_1—C28_1—H28B_1	109.2	C27_3—C28_3—H28B_3	109.4
H28A_1—C28_1—H28B_1	107.9	H28A_3—C28_3—H28B_3	108.0
C28_1—C29_1—C30_1	110.7 (3)	C30_3—C29_3—C28_3	112.1 (3)
C28_1—C29_1—H29A_1	109.5	C30_3—C29_3—H29A_3	109.2
C30_1—C29_1—H29A_1	109.5	C28_3—C29_3—H29A_3	109.2
C28_1—C29_1—H29B_1	109.5	C30_3—C29_3—H29B_3	109.2
C30_1—C29_1—H29B_1	109.5	C28_3—C29_3—H29B_3	109.2
H29A_1—C29_1—H29B_1	108.1	H29A_3—C29_3—H29B_3	107.9
C25_1—C30_1—C29_1	109.5 (3)	C25_3—C30_3—C29_3	109.8 (3)
C25_1—C30_1—H30A_1	109.8	C25_3—C30_3—H30A_3	109.7
C29_1—C30_1—H30A_1	109.8	C29_3—C30_3—H30A_3	109.7
C25_1—C30_1—H30B_1	109.8	C25_3—C30_3—H30B_3	109.7
C29_1—C30_1—H30B_1	109.8	C29_3—C30_3—H30B_3	109.7
H30A_1—C30_1—H30B_1	108.2	H30A_3—C30_3—H30B_3	108.2
O5_2—P1_2—O4_2	121.04 (14)	O5_4—P1_4—O3_4	121.10 (15)
O5_2—P1_2—O3_2	123.66 (14)	O5_4—P1_4—O4_4	115.23 (14)
O4_2—P1_2—O3_2	115.23 (14)	O3_4—P1_4—O4_4	123.60 (15)
O5_2—P1_2—O1_2	88.85 (13)	O5_4—P1_4—O1_4	90.05 (13)
O4_2—P1_2—O1_2	89.93 (13)	O3_4—P1_4—O1_4	88.96 (12)
O3_2—P1_2—O1_2	88.53 (13)	O4_4—P1_4—O1_4	88.54 (13)
O5_2—P1_2—O2_2	88.05 (13)	O5_4—P1_4—O2_4	92.11 (13)
O4_2—P1_2—O2_2	91.89 (13)	O3_4—P1_4—O2_4	88.03 (13)
O3_2—P1_2—O2_2	92.96 (13)	O4_4—P1_4—O2_4	92.53 (13)
O1_2—P1_2—O2_2	176.89 (13)	O1_4—P1_4—O2_4	176.91 (14)
C1_2—O1_2—P1_2	124.8 (2)	C1_4—O1_4—P1_4	124.1 (2)
C7_2—O2_2—P1_2	128.6 (2)	C7_4—O2_4—P1_4	128.5 (2)
C13_2—O3_2—P1_2	128.5 (2)	C13_4—O3_4—P1_4	129.7 (2)
C25_2—O4_2—P1_2	128.4 (2)	C25_4—O4_4—P1_4	128.3 (2)
C19_2—O5_2—P1_2	129.7 (2)	C19_4—O5_4—P1_4	128.5 (2)
O1_2—C1_2—C6_2	108.7 (3)	O1_4—C1_4—C2_4	108.6 (3)
O1_2—C1_2—C2_2	109.4 (3)	O1_4—C1_4—C6_4	108.4 (3)
C6_2—C1_2—C2_2	111.2 (3)	C2_4—C1_4—C6_4	111.3 (3)
O1_2—C1_2—H1_2	109.1	O1_4—C1_4—H1_4	109.5
C6_2—C1_2—H1_2	109.1	C2_4—C1_4—H1_4	109.5
C2_2—C1_2—H1_2	109.1	C6_4—C1_4—H1_4	109.5
C1_2—C2_2—C3_2	112.4 (3)	C1_4—C2_4—C3_4	111.5 (3)
C1_2—C2_2—H2A_2	109.1	C1_4—C2_4—H2A_4	109.3
C3_2—C2_2—H2A_2	109.1	C3_4—C2_4—H2A_4	109.3
C1_2—C2_2—H2B_2	109.1	C1_4—C2_4—H2B_4	109.3
C3_2—C2_2—H2B_2	109.1	C3_4—C2_4—H2B_4	109.3
H2A_2—C2_2—H2B_2	107.9	H2A_4—C2_4—H2B_4	108.0
C4_2—C3_2—C2_2	111.3 (4)	C4_4—C3_4—C2_4	111.1 (4)
C4_2—C3_2—H3A_2	109.4	C4_4—C3_4—H3A_4	109.4
C2_2—C3_2—H3A_2	109.4	C2_4—C3_4—H3A_4	109.4
C4_2—C3_2—H3B_2	109.4	C4_4—C3_4—H3B_4	109.4
C2_2—C3_2—H3B_2	109.4	C2_4—C3_4—H3B_4	109.4
H3A_2—C3_2—H3B_2	108.0	H3A_4—C3_4—H3B_4	108.0
C3_2—C4_2—C5_2	110.6 (4)	C3_4—C4_4—C5_4	110.8 (4)
C3_2—C4_2—H4A_2	109.5	C3_4—C4_4—H4A_4	109.5
C5_2—C4_2—H4A_2	109.5	C5_4—C4_4—H4A_4	109.5
C3_2—C4_2—H4B_2	109.5	C3_4—C4_4—H4B_4	109.5
C5_2—C4_2—H4B_2	109.5	C5_4—C4_4—H4B_4	109.5
H4A_2—C4_2—H4B_2	108.1	H4A_4—C4_4—H4B_4	108.1
C4_2—C5_2—C6_2	110.4 (3)	C6_4—C5_4—C4_4	110.4 (4)
C4_2—C5_2—H5A_2	109.6	C6_4—C5_4—H5A_4	109.6
C6_2—C5_2—H5A_2	109.6	C4_4—C5_4—H5A_4	109.6
C4_2—C5_2—H5B_2	109.6	C6_4—C5_4—H5B_4	109.6
C6_2—C5_2—H5B_2	109.6	C4_4—C5_4—H5B_4	109.6
H5A_2—C5_2—H5B_2	108.1	H5A_4—C5_4—H5B_4	108.1
C1_2—C6_2—C5_2	112.0 (3)	C1_4—C6_4—C5_4	111.7 (3)
C1_2—C6_2—H6A_2	109.2	C1_4—C6_4—H6A_4	109.3
C5_2—C6_2—H6A_2	109.2	C5_4—C6_4—H6A_4	109.3
C1_2—C6_2—H6B_2	109.2	C1_4—C6_4—H6B_4	109.3
C5_2—C6_2—H6B_2	109.2	C5_4—C6_4—H6B_4	109.3
H6A_2—C6_2—H6B_2	107.9	H6A_4—C6_4—H6B_4	107.9
O2_2—C7_2—C8_2	106.3 (3)	O2_4—C7_4—C8_4	113.4 (3)
O2_2—C7_2—C12_2	113.3 (3)	O2_4—C7_4—C12_4	105.7 (3)
C8_2—C7_2—C12_2	110.5 (3)	C8_4—C7_4—C12_4	110.5 (3)
O2_2—C7_2—H7_2	108.9	O2_4—C7_4—H7_4	109.0
C8_2—C7_2—H7_2	108.9	C8_4—C7_4—H7_4	109.0
C12_2—C7_2—H7_2	108.9	C12_4—C7_4—H7_4	109.0
C7_2—C8_2—C9_2	110.8 (3)	C7_4—C8_4—C9_4	110.7 (3)
C7_2—C8_2—H8A_2	109.5	C7_4—C8_4—H8A_4	109.5
C9_2—C8_2—H8A_2	109.5	C9_4—C8_4—H8A_4	109.5
C7_2—C8_2—H8B_2	109.5	C7_4—C8_4—H8B_4	109.5
C9_2—C8_2—H8B_2	109.5	C9_4—C8_4—H8B_4	109.5
H8A_2—C8_2—H8B_2	108.1	H8A_4—C8_4—H8B_4	108.1
C10_2—C9_2—C8_2	110.2 (4)	C10_4—C9_4—C8_4	110.5 (4)
C10_2—C9_2—H9A_2	109.6	C10_4—C9_4—H9A_4	109.5
C8_2—C9_2—H9A_2	109.6	C8_4—C9_4—H9A_4	109.5
C10_2—C9_2—H9B_2	109.6	C10_4—C9_4—H9B_4	109.5
C8_2—C9_2—H9B_2	109.6	C8_4—C9_4—H9B_4	109.5
H9A_2—C9_2—H9B_2	108.1	H9A_4—C9_4—H9B_4	108.1
C9_2—C10_2—C11_2	111.0 (4)	C11_4—C10_4—C9_4	111.3 (4)
C9_2—C10_2—H10A_2	109.4	C11_4—C10_4—H10A_4	109.4
C11_2—C10_2—H10A_2	109.4	C9_4—C10_4—H10A_4	109.4
C9_2—C10_2—H10B_2	109.4	C11_4—C10_4—H10B_4	109.4
C11_2—C10_2—H10B_2	109.4	C9_4—C10_4—H10B_4	109.4
H10A_2—C10_2—H10B_2	108.0	H10A_4—C10_4—H10B_4	108.0
C12_2—C11_2—C10_2	109.9 (3)	C10_4—C11_4—C12_4	110.8 (3)
C12_2—C11_2—H11A_2	109.7	C10_4—C11_4—H11A_4	109.5
C10_2—C11_2—H11A_2	109.7	C12_4—C11_4—H11A_4	109.5
C12_2—C11_2—H11B_2	109.7	C10_4—C11_4—H11B_4	109.5
C10_2—C11_2—H11B_2	109.7	C12_4—C11_4—H11B_4	109.5
H11A_2—C11_2—H11B_2	108.2	H11A_4—C11_4—H11B_4	108.1
C7_2—C12_2—C11_2	110.5 (3)	C7_4—C12_4—C11_4	110.7 (4)
C7_2—C12_2—H12A_2	109.6	C7_4—C12_4—H12A_4	109.5
C11_2—C12_2—H12A_2	109.6	C11_4—C12_4—H12A_4	109.5
C7_2—C12_2—H12B_2	109.6	C7_4—C12_4—H12B_4	109.5
C11_2—C12_2—H12B_2	109.6	C11_4—C12_4—H12B_4	109.5
H12A_2—C12_2—H12B_2	108.1	H12A_4—C12_4—H12B_4	108.1
O3_2—C13_2—C18_2	107.0 (3)	O3_4—C13_4—C14_4	106.5 (3)
O3_2—C13_2—C14_2	110.8 (3)	O3_4—C13_4—C18_4	110.8 (3)
C18_2—C13_2—C14_2	111.6 (3)	C14_4—C13_4—C18_4	111.6 (3)
O3_2—C13_2—H13_2	109.1	O3_4—C13_4—H13_4	109.3
C18_2—C13_2—H13_2	109.1	C14_4—C13_4—H13_4	109.3
C14_2—C13_2—H13_2	109.1	C18_4—C13_4—H13_4	109.3
C13_2—C14_2—C15_2	110.9 (4)	C13_4—C14_4—C15_4	110.4 (3)
C13_2—C14_2—H14A_2	109.5	C13_4—C14_4—H14A_4	109.6
C15_2—C14_2—H14A_2	109.5	C15_4—C14_4—H14A_4	109.6
C13_2—C14_2—H14B_2	109.5	C13_4—C14_4—H14B_4	109.6
C15_2—C14_2—H14B_2	109.5	C15_4—C14_4—H14B_4	109.6
H14A_2—C14_2—H14B_2	108.1	H14A_4—C14_4—H14B_4	108.1
C16_2—C15_2—C14_2	112.8 (4)	C14_4—C15_4—C16_4	110.4 (3)
C16_2—C15_2—H15A_2	109.0	C14_4—C15_4—H15A_4	109.6
C14_2—C15_2—H15A_2	109.0	C16_4—C15_4—H15A_4	109.6
C16_2—C15_2—H15B_2	109.0	C14_4—C15_4—H15B_4	109.6
C14_2—C15_2—H15B_2	109.0	C16_4—C15_4—H15B_4	109.6
H15A_2—C15_2—H15B_2	107.8	H15A_4—C15_4—H15B_4	108.1
C15_2—C16_2—C17_2	110.1 (4)	C17_4—C16_4—C15_4	111.5 (3)
C15_2—C16_2—H16A_2	109.6	C17_4—C16_4—H16A_4	109.3
C17_2—C16_2—H16A_2	109.6	C15_4—C16_4—H16A_4	109.3
C15_2—C16_2—H16B_2	109.6	C17_4—C16_4—H16B_4	109.3
C17_2—C16_2—H16B_2	109.6	C15_4—C16_4—H16B_4	109.3
H16A_2—C16_2—H16B_2	108.2	H16A_4—C16_4—H16B_4	108.0
C16_2—C17_2—C18_2	111.6 (4)	C16_4—C17_4—C18_4	111.3 (3)
C16_2—C17_2—H17A_2	109.3	C16_4—C17_4—H17A_4	109.4
C18_2—C17_2—H17A_2	109.3	C18_4—C17_4—H17A_4	109.4
C16_2—C17_2—H17B_2	109.3	C16_4—C17_4—H17B_4	109.4
C18_2—C17_2—H17B_2	109.3	C18_4—C17_4—H17B_4	109.4
H17A_2—C17_2—H17B_2	108.0	H17A_4—C17_4—H17B_4	108.0
C13_2—C18_2—C17_2	110.8 (4)	C13_4—C18_4—C17_4	110.8 (3)
C13_2—C18_2—H18A_2	109.5	C13_4—C18_4—H18A_4	109.5
C17_2—C18_2—H18A_2	109.5	C17_4—C18_4—H18A_4	109.5
C13_2—C18_2—H18B_2	109.5	C13_4—C18_4—H18B_4	109.5
C17_2—C18_2—H18B_2	109.5	C17_4—C18_4—H18B_4	109.5
H18A_2—C18_2—H18B_2	108.1	H18A_4—C18_4—H18B_4	108.1
O5_2—C19_2—C20_2	106.4 (3)	O5_4—C19_4—C20_4	110.7 (3)
O5_2—C19_2—C24_2	110.8 (3)	O5_4—C19_4—C24_4	107.4 (3)
C20_2—C19_2—C24_2	111.3 (3)	C20_4—C19_4—C24_4	111.5 (3)
O5_2—C19_2—H19_2	109.4	O5_4—C19_4—H19_4	109.1
C20_2—C19_2—H19_2	109.4	C20_4—C19_4—H19_4	109.1
C24_2—C19_2—H19_2	109.4	C24_4—C19_4—H19_4	109.1
C19_2—C20_2—C21_2	109.8 (3)	C19_4—C20_4—C21_4	110.8 (3)
C19_2—C20_2—H20A_2	109.7	C19_4—C20_4—H20A_4	109.5
C21_2—C20_2—H20A_2	109.7	C21_4—C20_4—H20A_4	109.5
C19_2—C20_2—H20B_2	109.7	C19_4—C20_4—H20B_4	109.5
C21_2—C20_2—H20B_2	109.7	C21_4—C20_4—H20B_4	109.5
H20A_2—C20_2—H20B_2	108.2	H20A_4—C20_4—H20B_4	108.1
C20_2—C21_2—C22_2	111.9 (3)	C22_4—C21_4—C20_4	111.4 (3)
C20_2—C21_2—H21A_2	109.2	C22_4—C21_4—H21A_4	109.3
C22_2—C21_2—H21A_2	109.2	C20_4—C21_4—H21A_4	109.3
C20_2—C21_2—H21B_2	109.2	C22_4—C21_4—H21B_4	109.3
C22_2—C21_2—H21B_2	109.2	C20_4—C21_4—H21B_4	109.3
H21A_2—C21_2—H21B_2	107.9	H21A_4—C21_4—H21B_4	108.0
C21_2—C22_2—C23_2	110.6 (3)	C21_4—C22_4—C23_4	111.5 (3)
C21_2—C22_2—H22A_2	109.5	C21_4—C22_4—H22A_4	109.3
C23_2—C22_2—H22A_2	109.5	C23_4—C22_4—H22A_4	109.3
C21_2—C22_2—H22B_2	109.5	C21_4—C22_4—H22B_4	109.3
C23_2—C22_2—H22B_2	109.5	C23_4—C22_4—H22B_4	109.3
H22A_2—C22_2—H22B_2	108.1	H22A_4—C22_4—H22B_4	108.0
C24_2—C23_2—C22_2	111.7 (3)	C24_4—C23_4—C22_4	110.9 (3)
C24_2—C23_2—H23A_2	109.3	C24_4—C23_4—H23A_4	109.5
C22_2—C23_2—H23A_2	109.3	C22_4—C23_4—H23A_4	109.5
C24_2—C23_2—H23B_2	109.3	C24_4—C23_4—H23B_4	109.5
C22_2—C23_2—H23B_2	109.3	C22_4—C23_4—H23B_4	109.5
H23A_2—C23_2—H23B_2	107.9	H23A_4—C23_4—H23B_4	108.1
C23_2—C24_2—C19_2	110.6 (3)	C19_4—C24_4—C23_4	110.7 (3)
C23_2—C24_2—H24A_2	109.5	C19_4—C24_4—H24A_4	109.5
C19_2—C24_2—H24A_2	109.5	C23_4—C24_4—H24A_4	109.5
C23_2—C24_2—H24B_2	109.5	C19_4—C24_4—H24B_4	109.5
C19_2—C24_2—H24B_2	109.5	C23_4—C24_4—H24B_4	109.5
H24A_2—C24_2—H24B_2	108.1	H24A_4—C24_4—H24B_4	108.1
O4_2—C25_2—C30_2	110.6 (3)	O4_4—C25_4—C30_4	107.2 (3)
O4_2—C25_2—C26_2	106.1 (3)	O4_4—C25_4—C26_4	111.2 (3)
C30_2—C25_2—C26_2	110.9 (3)	C30_4—C25_4—C26_4	111.4 (3)
O4_2—C25_2—H25_2	109.7	O4_4—C25_4—H25_4	109.0
C30_2—C25_2—H25_2	109.7	C30_4—C25_4—H25_4	109.0
C26_2—C25_2—H25_2	109.7	C26_4—C25_4—H25_4	109.0
C25_2—C26_2—C27_2	109.8 (3)	C25_4—C26_4—C27_4	111.9 (4)
C25_2—C26_2—H26A_2	109.7	C25_4—C26_4—H26A_4	109.2
C27_2—C26_2—H26A_2	109.7	C27_4—C26_4—H26A_4	109.2
C25_2—C26_2—H26B_2	109.7	C25_4—C26_4—H26B_4	109.2
C27_2—C26_2—H26B_2	109.7	C27_4—C26_4—H26B_4	109.2
H26A_2—C26_2—H26B_2	108.2	H26A_4—C26_4—H26B_4	107.9
C28_2—C27_2—C26_2	111.7 (3)	C28_4—C27_4—C26_4	112.5 (4)
C28_2—C27_2—H27A_2	109.3	C28_4—C27_4—H27A_4	109.1
C26_2—C27_2—H27A_2	109.3	C26_4—C27_4—H27A_4	109.1
C28_2—C27_2—H27B_2	109.3	C28_4—C27_4—H27B_4	109.1
C26_2—C27_2—H27B_2	109.3	C26_4—C27_4—H27B_4	109.1
H27A_2—C27_2—H27B_2	107.9	H27A_4—C27_4—H27B_4	107.8
C27_2—C28_2—C29_2	110.8 (4)	C27_4—C28_4—C29_4	109.5 (4)
C27_2—C28_2—H28A_2	109.5	C27_4—C28_4—H28A_4	109.8
C29_2—C28_2—H28A_2	109.5	C29_4—C28_4—H28A_4	109.8
C27_2—C28_2—H28B_2	109.5	C27_4—C28_4—H28B_4	109.8
C29_2—C28_2—H28B_2	109.5	C29_4—C28_4—H28B_4	109.8
H28A_2—C28_2—H28B_2	108.1	H28A_4—C28_4—H28B_4	108.2
C30_2—C29_2—C28_2	110.6 (4)	C28_4—C29_4—C30_4	112.2 (4)
C30_2—C29_2—H29A_2	109.5	C28_4—C29_4—H29A_4	109.2
C28_2—C29_2—H29A_2	109.5	C30_4—C29_4—H29A_4	109.2
C30_2—C29_2—H29B_2	109.5	C28_4—C29_4—H29B_4	109.2
C28_2—C29_2—H29B_2	109.5	C30_4—C29_4—H29B_4	109.2
H29A_2—C29_2—H29B_2	108.1	H29A_4—C29_4—H29B_4	107.9
C25_2—C30_2—C29_2	110.9 (3)	C25_4—C30_4—C29_4	110.9 (4)
C25_2—C30_2—H30A_2	109.5	C25_4—C30_4—H30A_4	109.5
C29_2—C30_2—H30A_2	109.5	C29_4—C30_4—H30A_4	109.5
C25_2—C30_2—H30B_2	109.5	C25_4—C30_4—H30B_4	109.5
C29_2—C30_2—H30B_2	109.5	C29_4—C30_4—H30B_4	109.5
H30A_2—C30_2—H30B_2	108.0	H30A_4—C30_4—H30B_4	108.1
O4_1—P1_1—O1_1—C1_1	59.2 (3)	O5_3—P1_3—O1_3—C1_3	−179.5 (3)
O5_1—P1_1—O1_1—C1_1	179.2 (3)	O3_3—P1_3—O1_3—C1_3	−55.5 (3)
O3_1—P1_1—O1_1—C1_1	−56.6 (3)	O4_3—P1_3—O1_3—C1_3	60.4 (3)
O4_1—P1_1—O2_1—C7_1	147.1 (3)	O5_3—P1_3—O2_3—C7_3	25.9 (3)
O5_1—P1_1—O2_1—C7_1	27.1 (3)	O3_3—P1_3—O2_3—C7_3	−98.0 (3)
O3_1—P1_1—O2_1—C7_1	−96.9 (3)	O4_3—P1_3—O2_3—C7_3	146.0 (3)
O4_1—P1_1—O3_1—C13_1	64.6 (3)	O5_3—P1_3—O3_3—C13_3	−118.4 (3)
O5_1—P1_1—O3_1—C13_1	−118.7 (3)	O4_3—P1_3—O3_3—C13_3	64.2 (3)
O1_1—P1_1—O3_1—C13_1	153.9 (3)	O1_3—P1_3—O3_3—C13_3	153.3 (3)
O2_1—P1_1—O3_1—C13_1	−29.2 (3)	O2_3—P1_3—O3_3—C13_3	−29.5 (3)
O5_1—P1_1—O4_1—C25_1	87.8 (3)	O5_3—P1_3—O4_3—C25_3	87.3 (3)
O3_1—P1_1—O4_1—C25_1	−95.3 (3)	O3_3—P1_3—O4_3—C25_3	−95.3 (3)
O1_1—P1_1—O4_1—C25_1	176.5 (3)	O1_3—P1_3—O4_3—C25_3	176.7 (3)
O2_1—P1_1—O4_1—C25_1	−1.3 (3)	O2_3—P1_3—O4_3—C25_3	−1.3 (3)
O4_1—P1_1—O5_1—C19_1	83.7 (3)	O3_3—P1_3—O5_3—C19_3	−94.7 (3)
O3_1—P1_1—O5_1—C19_1	−92.9 (3)	O4_3—P1_3—O5_3—C19_3	82.6 (3)
O1_1—P1_1—O5_1—C19_1	−5.8 (3)	O1_3—P1_3—O5_3—C19_3	−7.1 (3)
O2_1—P1_1—O5_1—C19_1	175.2 (3)	O2_3—P1_3—O5_3—C19_3	173.8 (3)
P1_1—O1_1—C1_1—C6_1	−123.2 (3)	P1_3—O1_3—C1_3—C2_3	114.5 (3)
P1_1—O1_1—C1_1—C2_1	115.1 (3)	P1_3—O1_3—C1_3—C6_3	−124.1 (3)
O1_1—C1_1—C2_1—C3_1	173.5 (3)	O1_3—C1_3—C2_3—C3_3	173.8 (3)
C6_1—C1_1—C2_1—C3_1	53.8 (5)	C6_3—C1_3—C2_3—C3_3	54.3 (5)
C1_1—C2_1—C3_1—C4_1	−54.9 (5)	C1_3—C2_3—C3_3—C4_3	−55.4 (5)
C2_1—C3_1—C4_1—C5_1	55.8 (5)	C2_3—C3_3—C4_3—C5_3	56.1 (5)
C3_1—C4_1—C5_1—C6_1	−56.2 (5)	C3_3—C4_3—C5_3—C6_3	−56.7 (5)
O1_1—C1_1—C6_1—C5_1	−173.6 (3)	O1_3—C1_3—C6_3—C5_3	−174.7 (3)
C2_1—C1_1—C6_1—C5_1	−53.9 (5)	C2_3—C1_3—C6_3—C5_3	−54.5 (4)
C4_1—C5_1—C6_1—C1_1	55.3 (5)	C4_3—C5_3—C6_3—C1_3	56.3 (5)
P1_1—O2_1—C7_1—C8_1	−176.1 (2)	P1_3—O2_3—C7_3—C12_3	63.9 (4)
P1_1—O2_1—C7_1—C12_1	62.2 (4)	P1_3—O2_3—C7_3—C8_3	−175.3 (2)
O2_1—C7_1—C8_1—C9_1	178.5 (3)	O2_3—C7_3—C8_3—C9_3	178.8 (3)
C12_1—C7_1—C8_1—C9_1	−57.3 (4)	C12_3—C7_3—C8_3—C9_3	−58.0 (4)
C7_1—C8_1—C9_1—C10_1	55.9 (5)	C7_3—C8_3—C9_3—C10_3	57.2 (5)
C8_1—C9_1—C10_1—C11_1	−54.6 (5)	C8_3—C9_3—C10_3—C11_3	−56.3 (5)
C9_1—C10_1—C11_1—C12_1	55.3 (5)	C9_3—C10_3—C11_3—C12_3	55.8 (5)
O2_1—C7_1—C12_1—C11_1	177.6 (3)	O2_3—C7_3—C12_3—C11_3	176.9 (3)
C8_1—C7_1—C12_1—C11_1	58.2 (4)	C8_3—C7_3—C12_3—C11_3	58.1 (4)
C10_1—C11_1—C12_1—C7_1	−57.1 (5)	C10_3—C11_3—C12_3—C7_3	−57.0 (5)
P1_1—O3_1—C13_1—C18_1	159.4 (3)	P1_3—O3_3—C13_3—C18_3	160.3 (3)
P1_1—O3_1—C13_1—C14_1	−78.3 (4)	P1_3—O3_3—C13_3—C14_3	−77.9 (4)
O3_1—C13_1—C14_1—C15_1	−173.4 (3)	O3_3—C13_3—C14_3—C15_3	−173.8 (3)
C18_1—C13_1—C14_1—C15_1	−53.6 (5)	C18_3—C13_3—C14_3—C15_3	−54.9 (5)
C13_1—C14_1—C15_1—C16_1	54.7 (5)	C13_3—C14_3—C15_3—C16_3	55.7 (5)
C14_1—C15_1—C16_1—C17_1	−55.1 (5)	C14_3—C15_3—C16_3—C17_3	−56.3 (5)
C15_1—C16_1—C17_1—C18_1	54.6 (5)	C15_3—C16_3—C17_3—C18_3	56.2 (5)
O3_1—C13_1—C18_1—C17_1	175.6 (3)	O3_3—C13_3—C18_3—C17_3	176.9 (4)
C14_1—C13_1—C18_1—C17_1	54.0 (5)	C14_3—C13_3—C18_3—C17_3	55.8 (5)
C16_1—C17_1—C18_1—C13_1	−54.7 (5)	C16_3—C17_3—C18_3—C13_3	−56.6 (5)
P1_1—O5_1—C19_1—C24_1	−76.0 (4)	P1_3—O5_3—C19_3—C24_3	−74.7 (4)
P1_1—O5_1—C19_1—C20_1	163.1 (3)	P1_3—O5_3—C19_3—C20_3	164.1 (3)
O5_1—C19_1—C20_1—C21_1	−178.6 (3)	O5_3—C19_3—C20_3—C21_3	−178.5 (3)
C24_1—C19_1—C20_1—C21_1	59.8 (4)	C24_3—C19_3—C20_3—C21_3	59.8 (4)
C19_1—C20_1—C21_1—C22_1	−56.2 (4)	C19_3—C20_3—C21_3—C22_3	−56.6 (5)
C20_1—C21_1—C22_1—C23_1	53.3 (5)	C20_3—C21_3—C22_3—C23_3	53.4 (5)
C21_1—C22_1—C23_1—C24_1	−52.6 (5)	C21_3—C22_3—C23_3—C24_3	−52.6 (5)
O5_1—C19_1—C24_1—C23_1	−178.5 (3)	O5_3—C19_3—C24_3—C23_3	−177.2 (3)
C20_1—C19_1—C24_1—C23_1	−59.7 (4)	C20_3—C19_3—C24_3—C23_3	−58.6 (4)
C22_1—C23_1—C24_1—C19_1	55.5 (4)	C22_3—C23_3—C24_3—C19_3	55.0 (5)
P1_1—O4_1—C25_1—C26_1	158.2 (2)	P1_3—O4_3—C25_3—C30_3	−80.9 (4)
P1_1—O4_1—C25_1—C30_1	−81.6 (4)	P1_3—O4_3—C25_3—C26_3	157.3 (2)
O4_1—C25_1—C26_1—C27_1	179.9 (3)	O4_3—C25_3—C26_3—C27_3	−178.9 (3)
C30_1—C25_1—C26_1—C27_1	59.7 (4)	C30_3—C25_3—C26_3—C27_3	59.3 (4)
C25_1—C26_1—C27_1—C28_1	−56.5 (4)	C25_3—C26_3—C27_3—C28_3	−56.2 (4)
C26_1—C27_1—C28_1—C29_1	54.5 (5)	C26_3—C27_3—C28_3—C29_3	53.3 (5)
C27_1—C28_1—C29_1—C30_1	−54.9 (5)	C27_3—C28_3—C29_3—C30_3	−53.0 (5)
O4_1—C25_1—C30_1—C29_1	−178.2 (3)	O4_3—C25_3—C30_3—C29_3	−178.2 (3)
C26_1—C25_1—C30_1—C29_1	−60.3 (4)	C26_3—C25_3—C30_3—C29_3	−59.0 (4)
C28_1—C29_1—C30_1—C25_1	57.1 (5)	C28_3—C29_3—C30_3—C25_3	55.7 (4)
O5_2—P1_2—O1_2—C1_2	−178.7 (3)	O5_4—P1_4—O1_4—C1_4	59.3 (3)
O4_2—P1_2—O1_2—C1_2	60.3 (3)	O3_4—P1_4—O1_4—C1_4	−179.6 (3)
O3_2—P1_2—O1_2—C1_2	−54.9 (3)	O4_4—P1_4—O1_4—C1_4	−55.9 (3)
O5_2—P1_2—O2_2—C7_2	22.8 (3)	O5_4—P1_4—O2_4—C7_4	143.9 (3)
O4_2—P1_2—O2_2—C7_2	143.9 (3)	O3_4—P1_4—O2_4—C7_4	22.8 (3)
O3_2—P1_2—O2_2—C7_2	−100.8 (3)	O4_4—P1_4—O2_4—C7_4	−100.8 (3)
O5_2—P1_2—O3_2—C13_2	−117.6 (3)	O5_4—P1_4—O3_4—C13_4	80.5 (3)
O4_2—P1_2—O3_2—C13_2	65.6 (3)	O4_4—P1_4—O3_4—C13_4	−96.5 (3)
O1_2—P1_2—O3_2—C13_2	154.8 (3)	O1_4—P1_4—O3_4—C13_4	−9.0 (3)
O2_2—P1_2—O3_2—C13_2	−27.9 (3)	O2_4—P1_4—O3_4—C13_4	171.7 (3)
O5_2—P1_2—O4_2—C25_2	85.6 (3)	O5_4—P1_4—O4_4—C25_4	65.3 (3)
O3_2—P1_2—O4_2—C25_2	−97.4 (3)	O3_4—P1_4—O4_4—C25_4	−117.6 (3)
O1_2—P1_2—O4_2—C25_2	174.3 (3)	O1_4—P1_4—O4_4—C25_4	154.6 (3)
O2_2—P1_2—O4_2—C25_2	−3.2 (3)	O2_4—P1_4—O4_4—C25_4	−28.3 (3)
O4_2—P1_2—O5_2—C19_2	82.4 (3)	O3_4—P1_4—O5_4—C19_4	86.7 (3)
O3_2—P1_2—O5_2—C19_2	−94.3 (3)	O4_4—P1_4—O5_4—C19_4	−96.1 (3)
O1_2—P1_2—O5_2—C19_2	−6.8 (3)	O1_4—P1_4—O5_4—C19_4	175.5 (3)
O2_2—P1_2—O5_2—C19_2	173.5 (3)	O2_4—P1_4—O5_4—C19_4	−2.3 (3)
P1_2—O1_2—C1_2—C6_2	−125.0 (3)	P1_4—O1_4—C1_4—C2_4	−124.4 (3)
P1_2—O1_2—C1_2—C2_2	113.3 (3)	P1_4—O1_4—C1_4—C6_4	114.5 (3)
O1_2—C1_2—C2_2—C3_2	173.2 (3)	O1_4—C1_4—C2_4—C3_4	−173.4 (3)
C6_2—C1_2—C2_2—C3_2	53.1 (5)	C6_4—C1_4—C2_4—C3_4	−54.0 (5)
C1_2—C2_2—C3_2—C4_2	−54.7 (5)	C1_4—C2_4—C3_4—C4_4	56.0 (5)
C2_2—C3_2—C4_2—C5_2	56.3 (5)	C2_4—C3_4—C4_4—C5_4	−57.3 (5)
C3_2—C4_2—C5_2—C6_2	−56.7 (5)	C3_4—C4_4—C5_4—C6_4	56.8 (5)
O1_2—C1_2—C6_2—C5_2	−174.4 (3)	O1_4—C1_4—C6_4—C5_4	173.6 (3)
C2_2—C1_2—C6_2—C5_2	−53.8 (4)	C2_4—C1_4—C6_4—C5_4	54.1 (5)
C4_2—C5_2—C6_2—C1_2	56.0 (5)	C4_4—C5_4—C6_4—C1_4	−55.3 (5)
P1_2—O2_2—C7_2—C8_2	−173.4 (2)	P1_4—O2_4—C7_4—C8_4	66.6 (4)
P1_2—O2_2—C7_2—C12_2	65.1 (4)	P1_4—O2_4—C7_4—C12_4	−172.2 (2)
O2_2—C7_2—C8_2—C9_2	178.9 (3)	O2_4—C7_4—C8_4—C9_4	176.8 (3)
C12_2—C7_2—C8_2—C9_2	−57.8 (4)	C12_4—C7_4—C8_4—C9_4	58.3 (4)
C7_2—C8_2—C9_2—C10_2	57.3 (5)	C7_4—C8_4—C9_4—C10_4	−57.2 (5)
C8_2—C9_2—C10_2—C11_2	−56.9 (5)	C8_4—C9_4—C10_4—C11_4	55.8 (5)
C9_2—C10_2—C11_2—C12_2	57.3 (5)	C9_4—C10_4—C11_4—C12_4	−55.2 (5)
O2_2—C7_2—C12_2—C11_2	177.3 (3)	O2_4—C7_4—C12_4—C11_4	179.4 (3)
C8_2—C7_2—C12_2—C11_2	58.2 (4)	C8_4—C7_4—C12_4—C11_4	−57.6 (4)
C10_2—C11_2—C12_2—C7_2	−57.3 (5)	C10_4—C11_4—C12_4—C7_4	55.9 (5)
P1_2—O3_2—C13_2—C18_2	162.3 (3)	P1_4—O3_4—C13_4—C14_4	163.1 (3)
P1_2—O3_2—C13_2—C14_2	−75.8 (4)	P1_4—O3_4—C13_4—C18_4	−75.4 (4)
O3_2—C13_2—C14_2—C15_2	−173.4 (4)	O3_4—C13_4—C14_4—C15_4	179.1 (3)
C18_2—C13_2—C14_2—C15_2	−54.2 (5)	C18_4—C13_4—C14_4—C15_4	58.1 (4)
C13_2—C14_2—C15_2—C16_2	54.5 (6)	C13_4—C14_4—C15_4—C16_4	−56.8 (4)
C14_2—C15_2—C16_2—C17_2	−55.1 (6)	C14_4—C15_4—C16_4—C17_4	55.5 (5)
C15_2—C16_2—C17_2—C18_2	55.7 (6)	C15_4—C16_4—C17_4—C18_4	−54.4 (5)
O3_2—C13_2—C18_2—C17_2	176.9 (4)	O3_4—C13_4—C18_4—C17_4	−175.3 (3)
C14_2—C13_2—C18_2—C17_2	55.4 (6)	C14_4—C13_4—C18_4—C17_4	−56.7 (4)
C16_2—C17_2—C18_2—C13_2	−56.5 (6)	C16_4—C17_4—C18_4—C13_4	54.6 (4)
P1_2—O5_2—C19_2—C20_2	162.5 (2)	P1_4—O5_4—C19_4—C20_4	−83.1 (4)
P1_2—O5_2—C19_2—C24_2	−76.4 (4)	P1_4—O5_4—C19_4—C24_4	155.1 (2)
O5_2—C19_2—C20_2—C21_2	178.7 (3)	O5_4—C19_4—C20_4—C21_4	−175.9 (3)
C24_2—C19_2—C20_2—C21_2	57.9 (4)	C24_4—C19_4—C20_4—C21_4	−56.4 (4)
C19_2—C20_2—C21_2—C22_2	−57.0 (4)	C19_4—C20_4—C21_4—C22_4	54.8 (4)
C20_2—C21_2—C22_2—C23_2	55.0 (5)	C20_4—C21_4—C22_4—C23_4	−54.4 (5)
C21_2—C22_2—C23_2—C24_2	−53.9 (5)	C21_4—C22_4—C23_4—C24_4	55.0 (5)
C22_2—C23_2—C24_2—C19_2	55.1 (5)	O5_4—C19_4—C24_4—C23_4	178.6 (3)
O5_2—C19_2—C24_2—C23_2	−175.5 (3)	C20_4—C19_4—C24_4—C23_4	57.2 (4)
C20_2—C19_2—C24_2—C23_2	−57.3 (4)	C22_4—C23_4—C24_4—C19_4	−56.1 (4)
P1_2—O4_2—C25_2—C30_2	−83.6 (4)	P1_4—O4_4—C25_4—C30_4	161.9 (3)
P1_2—O4_2—C25_2—C26_2	156.1 (3)	P1_4—O4_4—C25_4—C26_4	−76.1 (4)
O4_2—C25_2—C26_2—C27_2	177.6 (3)	O4_4—C25_4—C26_4—C27_4	−173.3 (3)
C30_2—C25_2—C26_2—C27_2	57.4 (4)	C30_4—C25_4—C26_4—C27_4	−53.7 (5)
C25_2—C26_2—C27_2—C28_2	−56.7 (4)	C25_4—C26_4—C27_4—C28_4	54.6 (5)
C26_2—C27_2—C28_2—C29_2	55.9 (5)	C26_4—C27_4—C28_4—C29_4	−54.8 (5)
C27_2—C28_2—C29_2—C30_2	−55.2 (5)	C27_4—C28_4—C29_4—C30_4	55.9 (6)
O4_2—C25_2—C30_2—C29_2	−175.5 (3)	O4_4—C25_4—C30_4—C29_4	176.2 (4)
C26_2—C25_2—C30_2—C29_2	−58.0 (4)	C26_4—C25_4—C30_4—C29_4	54.4 (6)
C28_2—C29_2—C30_2—C25_2	56.4 (5)	C28_4—C29_4—C30_4—C25_4	−56.4 (6)