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In the title compound, [CoCl2(C24H20N2)2], CoII is coordinated in an approximately tetra­hedral geometry by two Cl atoms and two N atoms of the pyridine rings from two 2-[(triphenyl­meth­yl)imino]pyridyl ligands.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536806045764/bi2085sup1.cif
Contains datablocks I, global

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S1600536806045764/bi2085Isup2.hkl
Contains datablock I

CCDC reference: 629436

Key indicators

  • Single-crystal X-ray study
  • T = 150 K
  • Mean [sigma](C-C) = 0.003 Å
  • R factor = 0.039
  • wR factor = 0.097
  • Data-to-parameter ratio = 13.8

checkCIF/PLATON results

No syntax errors found



Alert level C PLAT318_ALERT_2_C Check Hybridisation of N2 in Main Residue . ?
0 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 1 ALERT level C = Check and explain 0 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 0 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check

Computing details top

Data collection: APEX2 (Bruker, 2005); cell refinement: SAINT (Bruker, 2005); data reduction: SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: SHELXTL (Bruker, 1997); software used to prepare material for publication: SHELXTL.

Dichlorobis{2-[(triphenylmethyl)imino]pyridyl}cobalt(II) top
Crystal data top
[CoCl2(C24H20N2)2]F(000) = 1668
Mr = 802.67Dx = 1.372 Mg m3
Monoclinic, P21/nMo Kα radiation, λ = 0.71073 Å
Hall symbol: -P 2ynCell parameters from 19035 reflections
a = 9.920 (2) Åθ = 1.0–30.0°
b = 22.620 (5) ŵ = 0.62 mm1
c = 17.460 (4) ÅT = 150 K
β = 97.36 (3)°Block, blue
V = 3885.6 (15) Å30.35 × 0.34 × 0.30 mm
Z = 4
Data collection top
Bruker APEXII CCD
diffractometer
6823 independent reflections
Radiation source: fine-focus sealed tube5433 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.081
ω scansθmax = 25.0°, θmin = 2.7°
Absorption correction: multi-scan
(SADABS; Sheldrick, 2003)
h = 1111
Tmin = 0.812, Tmax = 0.836k = 2626
25600 measured reflectionsl = 2020
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.039Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.098H-atom parameters constrained
S = 1.02 w = 1/[σ2(Fo2) + (0.039P)2 + 2.5598P]
where P = (Fo2 + 2Fc2)/3
6823 reflections(Δ/σ)max = 0.001
496 parametersΔρmax = 0.69 e Å3
0 restraintsΔρmin = 0.52 e Å3
Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
Co10.70721 (3)0.186000 (14)0.673481 (17)0.02327 (10)
Cl10.68790 (6)0.10025 (3)0.60866 (3)0.02932 (15)
Cl20.88192 (7)0.24252 (3)0.64883 (4)0.03773 (17)
N10.52808 (19)0.23246 (9)0.65478 (10)0.0236 (4)
N20.62268 (18)0.31205 (8)0.72491 (10)0.0222 (4)
H2A0.70050.29630.71650.027*
N30.72435 (18)0.16938 (8)0.78980 (10)0.0218 (4)
N40.53460 (18)0.10888 (9)0.77534 (10)0.0231 (4)
H4A0.55010.10590.72700.028*
C10.5085 (2)0.28445 (10)0.69112 (12)0.0225 (5)
C20.3755 (2)0.30661 (11)0.69188 (13)0.0244 (5)
H2B0.36120.34190.71930.029*
C30.2672 (2)0.27700 (11)0.65295 (13)0.0275 (5)
H3A0.17750.29160.65360.033*
C40.2887 (2)0.22557 (11)0.61244 (13)0.0302 (6)
H4B0.21510.20530.58370.036*
C50.4189 (2)0.20507 (11)0.61526 (13)0.0279 (5)
H5A0.43370.16970.58810.033*
C60.6313 (2)0.36542 (10)0.77415 (12)0.0209 (5)
C70.5425 (2)0.35682 (10)0.83968 (12)0.0214 (5)
C80.4647 (2)0.40136 (11)0.86690 (13)0.0237 (5)
H8A0.45230.43770.83970.028*
C90.4050 (2)0.39288 (11)0.93402 (13)0.0263 (5)
H9A0.35350.42390.95280.032*
C100.4195 (2)0.34000 (11)0.97362 (13)0.0267 (5)
H10A0.37940.33471.01970.032*
C110.4934 (2)0.29468 (11)0.94530 (13)0.0280 (5)
H11A0.50220.25780.97150.034*
C120.5542 (2)0.30301 (11)0.87923 (13)0.0251 (5)
H12A0.60470.27170.86040.030*
C130.5995 (2)0.42206 (11)0.72563 (13)0.0228 (5)
C140.6281 (2)0.47723 (11)0.75930 (14)0.0271 (5)
H14A0.66570.47950.81210.033*
C150.6028 (2)0.52896 (11)0.71702 (15)0.0317 (6)
H15A0.62100.56620.74120.038*
C160.5509 (3)0.52626 (12)0.63960 (15)0.0359 (6)
H16A0.53350.56150.61050.043*
C170.5247 (3)0.47197 (12)0.60522 (15)0.0351 (6)
H17A0.48950.46980.55210.042*
C180.5493 (2)0.42024 (11)0.64772 (13)0.0269 (5)
H18A0.53160.38310.62310.032*
C190.7815 (2)0.36978 (10)0.81091 (12)0.0226 (5)
C200.8833 (2)0.36785 (11)0.76339 (14)0.0277 (5)
H20A0.85950.36400.70920.033*
C211.0189 (3)0.37151 (12)0.79374 (16)0.0369 (6)
H21A1.08750.36920.76050.044*
C221.0544 (3)0.37847 (13)0.87202 (16)0.0413 (7)
H22A1.14750.38030.89310.050*
C230.9545 (3)0.38270 (13)0.91973 (15)0.0416 (7)
H23A0.97890.38870.97360.050*
C240.8187 (3)0.37825 (12)0.88975 (14)0.0327 (6)
H24A0.75060.38100.92320.039*
C250.6301 (2)0.13826 (10)0.82401 (12)0.0218 (5)
C260.6359 (2)0.13716 (11)0.90486 (12)0.0247 (5)
H26A0.56950.11610.92850.030*
C270.7383 (2)0.16684 (11)0.94924 (13)0.0290 (6)
H27A0.74210.16681.00390.035*
C280.8367 (2)0.19697 (11)0.91444 (14)0.0295 (6)
H28A0.90910.21700.94460.035*
C290.8263 (2)0.19690 (11)0.83554 (13)0.0263 (5)
H29A0.89380.21710.81160.032*
C300.4072 (2)0.08126 (11)0.79455 (12)0.0227 (5)
C310.3339 (2)0.12535 (11)0.84251 (13)0.0244 (5)
C320.3114 (2)0.18246 (11)0.81394 (14)0.0301 (6)
H32A0.34320.19300.76670.036*
C330.2440 (3)0.22403 (12)0.85273 (15)0.0336 (6)
H33A0.22780.26240.83150.040*
C340.2000 (2)0.20986 (12)0.92262 (15)0.0342 (6)
H34A0.15490.23850.95000.041*
C350.2227 (2)0.15351 (12)0.95189 (14)0.0343 (6)
H35A0.19270.14340.99970.041*
C360.2886 (2)0.11150 (12)0.91248 (13)0.0287 (5)
H36A0.30290.07290.93340.034*
C370.4344 (2)0.02124 (11)0.83545 (12)0.0233 (5)
C380.3239 (2)0.01469 (11)0.84641 (13)0.0273 (5)
H38A0.23450.00230.82720.033*
C390.3430 (3)0.06814 (11)0.88491 (13)0.0299 (6)
H39A0.26660.09150.89330.036*
C400.4729 (3)0.08767 (11)0.91121 (13)0.0300 (6)
H40A0.48620.12460.93710.036*
C410.5831 (2)0.05303 (11)0.89949 (13)0.0288 (6)
H41A0.67250.06610.91770.035*
C420.5640 (2)0.00078 (11)0.86119 (12)0.0256 (5)
H42A0.64070.02380.85250.031*
C430.3218 (2)0.06899 (10)0.71549 (13)0.0249 (5)
C440.3816 (2)0.03749 (11)0.65995 (13)0.0292 (6)
H44A0.47130.02250.67210.035*
C450.3111 (3)0.02787 (12)0.58710 (14)0.0336 (6)
H45A0.35380.00770.54900.040*
C460.1783 (3)0.04760 (12)0.56981 (15)0.0355 (6)
H46A0.13040.04150.51970.043*
C470.1165 (3)0.07601 (12)0.62565 (15)0.0357 (6)
H47A0.02440.08820.61460.043*
C480.1876 (2)0.08709 (11)0.69828 (14)0.0293 (6)
H48A0.14410.10710.73620.035*
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Co10.02553 (18)0.02205 (19)0.02354 (17)0.00188 (14)0.00817 (12)0.00120 (13)
Cl10.0348 (3)0.0258 (3)0.0285 (3)0.0020 (3)0.0083 (2)0.0045 (2)
Cl20.0391 (4)0.0352 (4)0.0436 (4)0.0125 (3)0.0234 (3)0.0099 (3)
N10.0285 (10)0.0217 (11)0.0206 (9)0.0029 (9)0.0036 (8)0.0002 (8)
N20.0198 (9)0.0210 (10)0.0264 (10)0.0012 (8)0.0050 (7)0.0023 (8)
N30.0194 (10)0.0207 (10)0.0261 (10)0.0009 (8)0.0058 (8)0.0000 (8)
N40.0242 (10)0.0261 (11)0.0199 (9)0.0066 (9)0.0060 (7)0.0010 (8)
C10.0281 (12)0.0202 (13)0.0194 (11)0.0012 (10)0.0039 (9)0.0042 (9)
C20.0266 (12)0.0219 (13)0.0247 (12)0.0005 (10)0.0031 (9)0.0051 (10)
C30.0243 (12)0.0287 (14)0.0290 (12)0.0010 (11)0.0009 (9)0.0091 (11)
C40.0304 (13)0.0282 (14)0.0300 (13)0.0070 (11)0.0038 (10)0.0055 (11)
C50.0347 (14)0.0241 (13)0.0238 (12)0.0043 (11)0.0001 (10)0.0003 (10)
C60.0228 (11)0.0176 (12)0.0228 (11)0.0006 (10)0.0052 (9)0.0012 (9)
C70.0199 (11)0.0220 (13)0.0226 (11)0.0014 (10)0.0037 (8)0.0005 (9)
C80.0217 (12)0.0223 (13)0.0271 (12)0.0010 (10)0.0031 (9)0.0022 (10)
C90.0201 (12)0.0285 (14)0.0309 (12)0.0003 (10)0.0063 (9)0.0047 (11)
C100.0245 (12)0.0329 (14)0.0239 (12)0.0059 (11)0.0072 (9)0.0019 (11)
C110.0298 (13)0.0269 (14)0.0276 (12)0.0044 (11)0.0053 (10)0.0065 (10)
C120.0278 (12)0.0206 (13)0.0281 (12)0.0014 (10)0.0078 (9)0.0003 (10)
C130.0170 (11)0.0248 (13)0.0285 (12)0.0002 (10)0.0101 (9)0.0045 (10)
C140.0286 (12)0.0238 (13)0.0299 (12)0.0011 (11)0.0080 (10)0.0002 (10)
C150.0275 (13)0.0215 (13)0.0488 (16)0.0002 (11)0.0149 (11)0.0049 (12)
C160.0308 (13)0.0315 (16)0.0469 (16)0.0043 (12)0.0104 (11)0.0179 (13)
C170.0326 (14)0.0395 (17)0.0331 (14)0.0029 (12)0.0038 (11)0.0125 (12)
C180.0263 (12)0.0259 (14)0.0297 (13)0.0044 (11)0.0079 (10)0.0038 (10)
C190.0236 (12)0.0160 (12)0.0283 (12)0.0011 (9)0.0038 (9)0.0019 (10)
C200.0271 (13)0.0253 (14)0.0317 (13)0.0030 (11)0.0074 (10)0.0016 (11)
C210.0251 (13)0.0341 (16)0.0533 (17)0.0032 (12)0.0115 (11)0.0071 (13)
C220.0251 (13)0.0406 (17)0.0555 (18)0.0045 (12)0.0055 (12)0.0026 (14)
C230.0384 (16)0.0490 (18)0.0339 (14)0.0097 (14)0.0085 (12)0.0043 (13)
C240.0311 (13)0.0382 (16)0.0286 (13)0.0050 (12)0.0033 (10)0.0008 (11)
C250.0209 (11)0.0195 (12)0.0256 (11)0.0012 (10)0.0050 (9)0.0005 (10)
C260.0229 (12)0.0256 (13)0.0263 (12)0.0004 (10)0.0056 (9)0.0016 (10)
C270.0317 (13)0.0321 (14)0.0233 (12)0.0031 (11)0.0035 (10)0.0009 (10)
C280.0236 (12)0.0322 (15)0.0321 (13)0.0051 (11)0.0008 (10)0.0033 (11)
C290.0208 (12)0.0274 (14)0.0311 (13)0.0016 (10)0.0047 (9)0.0013 (10)
C300.0208 (11)0.0232 (13)0.0246 (12)0.0026 (10)0.0043 (9)0.0036 (10)
C310.0202 (11)0.0252 (13)0.0276 (12)0.0043 (10)0.0025 (9)0.0000 (10)
C320.0304 (13)0.0278 (14)0.0327 (13)0.0023 (11)0.0064 (10)0.0047 (11)
C330.0327 (14)0.0254 (14)0.0427 (15)0.0015 (11)0.0052 (11)0.0016 (12)
C340.0272 (13)0.0326 (15)0.0445 (15)0.0012 (12)0.0110 (11)0.0076 (12)
C350.0302 (13)0.0394 (16)0.0358 (14)0.0005 (12)0.0137 (11)0.0008 (12)
C360.0280 (13)0.0287 (14)0.0302 (13)0.0004 (11)0.0069 (10)0.0036 (11)
C370.0259 (12)0.0233 (13)0.0210 (11)0.0007 (10)0.0049 (9)0.0014 (10)
C380.0258 (12)0.0272 (14)0.0291 (12)0.0036 (11)0.0039 (9)0.0043 (10)
C390.0326 (14)0.0269 (14)0.0315 (13)0.0056 (11)0.0085 (10)0.0045 (11)
C400.0393 (14)0.0241 (13)0.0275 (12)0.0032 (11)0.0076 (10)0.0055 (10)
C410.0295 (13)0.0308 (14)0.0266 (12)0.0052 (11)0.0051 (10)0.0037 (11)
C420.0275 (13)0.0261 (13)0.0244 (12)0.0016 (11)0.0082 (9)0.0001 (10)
C430.0271 (12)0.0211 (13)0.0262 (12)0.0072 (10)0.0026 (9)0.0058 (10)
C440.0298 (13)0.0253 (14)0.0323 (13)0.0034 (11)0.0030 (10)0.0002 (11)
C450.0430 (15)0.0284 (15)0.0290 (13)0.0050 (12)0.0033 (11)0.0007 (11)
C460.0406 (15)0.0318 (15)0.0313 (14)0.0101 (12)0.0067 (11)0.0043 (12)
C470.0299 (13)0.0343 (16)0.0405 (15)0.0043 (12)0.0046 (11)0.0064 (12)
C480.0270 (13)0.0266 (14)0.0342 (13)0.0024 (11)0.0035 (10)0.0038 (11)
Geometric parameters (Å, º) top
Co1—Cl12.2415 (8)C21—C221.376 (4)
Co1—Cl22.2394 (8)C21—H21A0.950
Co1—N12.054 (2)C22—C231.378 (4)
Co1—N32.0510 (18)C22—H22A0.950
N1—C51.357 (3)C23—C241.385 (4)
N1—C11.362 (3)C23—H23A0.950
N2—C11.360 (3)C24—H24A0.950
N2—C61.478 (3)C25—C261.406 (3)
N2—H2A0.880C26—C271.372 (3)
N3—C291.357 (3)C26—H26A0.950
N3—C251.367 (3)C27—C281.392 (4)
N4—C251.362 (3)C27—H27A0.950
N4—C301.486 (3)C28—C291.368 (3)
N4—H4A0.880C28—H28A0.950
C1—C21.414 (3)C29—H29A0.950
C2—C31.370 (3)C30—C371.542 (3)
C2—H2B0.950C30—C311.543 (3)
C3—C41.392 (4)C30—C431.550 (3)
C3—H3A0.950C31—C361.391 (3)
C4—C51.367 (4)C31—C321.392 (3)
C4—H4B0.950C32—C331.381 (4)
C5—H5A0.950C32—H32A0.950
C6—C71.543 (3)C33—C341.385 (4)
C6—C131.546 (3)C33—H33A0.950
C6—C191.548 (3)C34—C351.381 (4)
C7—C81.389 (3)C34—H34A0.950
C7—C121.397 (3)C35—C361.385 (4)
C8—C91.393 (3)C35—H35A0.950
C8—H8A0.950C36—H36A0.950
C9—C101.380 (4)C37—C421.386 (3)
C9—H9A0.950C37—C381.398 (3)
C10—C111.388 (4)C38—C391.385 (3)
C10—H10A0.950C38—H38A0.950
C11—C121.381 (3)C39—C401.384 (3)
C11—H11A0.950C39—H39A0.950
C12—H12A0.950C40—C411.381 (4)
C13—C181.388 (3)C40—H40A0.950
C13—C141.393 (3)C41—C421.390 (3)
C14—C151.389 (3)C41—H41A0.950
C14—H14A0.950C42—H42A0.950
C15—C161.385 (4)C43—C481.388 (3)
C15—H15A0.950C43—C441.396 (3)
C16—C171.377 (4)C44—C451.388 (3)
C16—H16A0.950C44—H44A0.950
C17—C181.390 (4)C45—C461.387 (4)
C17—H17A0.950C45—H45A0.950
C18—H18A0.950C46—C471.376 (4)
C19—C201.387 (3)C46—H46A0.950
C19—C241.392 (3)C47—C481.393 (3)
C20—C211.384 (3)C47—H47A0.950
C20—H20A0.950C48—H48A0.950
Cl1—Co1—Cl2114.53 (3)C21—C22—C23119.7 (2)
Cl1—Co1—N1110.26 (6)C21—C22—H22A120.1
Cl1—Co1—N3109.41 (6)C23—C22—H22A120.1
Cl2—Co1—N1110.63 (6)C22—C23—C24120.5 (2)
Cl2—Co1—N3109.08 (6)C22—C23—H23A119.8
N1—Co1—N3102.21 (8)C24—C23—H23A119.8
C5—N1—C1118.6 (2)C23—C24—C19120.4 (2)
C5—N1—Co1117.71 (16)C23—C24—H24A119.8
C1—N1—Co1122.66 (14)C19—C24—H24A119.8
C1—N2—C6127.61 (19)N4—C25—N3116.01 (19)
C1—N2—H2A116.2N4—C25—C26123.6 (2)
C6—N2—H2A116.2N3—C25—C26120.4 (2)
C29—N3—C25118.62 (19)C27—C26—C25119.4 (2)
C29—N3—Co1117.36 (16)C27—C26—H26A120.3
C25—N3—Co1123.53 (14)C25—C26—H26A120.3
C25—N4—C30127.44 (18)C26—C27—C28120.2 (2)
C25—N4—H4A116.3C26—C27—H27A119.9
C30—N4—H4A116.3C28—C27—H27A119.9
N2—C1—N1116.0 (2)C29—C28—C27118.2 (2)
N2—C1—C2124.0 (2)C29—C28—H28A120.9
N1—C1—C2120.0 (2)C27—C28—H28A120.9
C3—C2—C1119.7 (2)N3—C29—C28123.2 (2)
C3—C2—H2B120.2N3—C29—H29A118.4
C1—C2—H2B120.2C28—C29—H29A118.4
C2—C3—C4119.9 (2)N4—C30—C37111.81 (18)
C2—C3—H3A120.0N4—C30—C31108.93 (18)
C4—C3—H3A120.0C37—C30—C31112.61 (18)
C5—C4—C3118.1 (2)N4—C30—C43104.97 (17)
C5—C4—H4B120.9C37—C30—C43107.35 (18)
C3—C4—H4B120.9C31—C30—C43110.90 (18)
N1—C5—C4123.5 (2)C36—C31—C32118.0 (2)
N1—C5—H5A118.2C36—C31—C30124.0 (2)
C4—C5—H5A118.2C32—C31—C30118.0 (2)
N2—C6—C7109.40 (18)C33—C32—C31121.4 (2)
N2—C6—C13111.44 (17)C33—C32—H32A119.3
C7—C6—C13114.50 (18)C31—C32—H32A119.3
N2—C6—C19105.92 (18)C32—C33—C34120.1 (2)
C7—C6—C19108.13 (17)C32—C33—H33A119.9
C13—C6—C19107.02 (18)C34—C33—H33A119.9
C8—C7—C12118.5 (2)C35—C34—C33119.0 (2)
C8—C7—C6123.8 (2)C35—C34—H34A120.5
C12—C7—C6117.2 (2)C33—C34—H34A120.5
C7—C8—C9120.2 (2)C34—C35—C36120.9 (2)
C7—C8—H8A119.9C34—C35—H35A119.5
C9—C8—H8A119.9C36—C35—H35A119.5
C10—C9—C8120.8 (2)C35—C36—C31120.5 (2)
C10—C9—H9A119.6C35—C36—H36A119.7
C8—C9—H9A119.6C31—C36—H36A119.7
C9—C10—C11119.2 (2)C42—C37—C38118.2 (2)
C9—C10—H10A120.4C42—C37—C30123.0 (2)
C11—C10—H10A120.4C38—C37—C30118.8 (2)
C12—C11—C10120.3 (2)C39—C38—C37120.9 (2)
C12—C11—H11A119.9C39—C38—H38A119.6
C10—C11—H11A119.9C37—C38—H38A119.6
C11—C12—C7120.9 (2)C40—C39—C38120.2 (2)
C11—C12—H12A119.5C40—C39—H39A119.9
C7—C12—H12A119.5C38—C39—H39A119.9
C18—C13—C14117.9 (2)C41—C40—C39119.4 (2)
C18—C13—C6122.3 (2)C41—C40—H40A120.3
C14—C13—C6119.65 (19)C39—C40—H40A120.3
C15—C14—C13121.1 (2)C40—C41—C42120.4 (2)
C15—C14—H14A119.4C40—C41—H41A119.8
C13—C14—H14A119.4C42—C41—H41A119.8
C16—C15—C14120.1 (2)C37—C42—C41120.8 (2)
C16—C15—H15A120.0C37—C42—H42A119.6
C14—C15—H15A120.0C41—C42—H42A119.6
C17—C16—C15119.4 (2)C48—C43—C44118.8 (2)
C17—C16—H16A120.3C48—C43—C30122.7 (2)
C15—C16—H16A120.3C44—C43—C30118.5 (2)
C16—C17—C18120.5 (2)C45—C44—C43120.5 (2)
C16—C17—H17A119.8C45—C44—H44A119.8
C18—C17—H17A119.8C43—C44—H44A119.8
C13—C18—C17121.0 (2)C46—C45—C44120.2 (2)
C13—C18—H18A119.5C46—C45—H45A119.9
C17—C18—H18A119.5C44—C45—H45A119.9
C20—C19—C24118.3 (2)C47—C46—C45119.6 (2)
C20—C19—C6119.04 (19)C47—C46—H46A120.2
C24—C19—C6122.6 (2)C45—C46—H46A120.2
C21—C20—C19121.0 (2)C46—C47—C48120.6 (2)
C21—C20—H20A119.5C46—C47—H47A119.7
C19—C20—H20A119.5C48—C47—H47A119.7
C22—C21—C20120.0 (2)C43—C48—C47120.3 (2)
C22—C21—H21A120.0C43—C48—H48A119.9
C20—C21—H21A120.0C47—C48—H48A119.9
 

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