research papers
Aluminium indium tungstate (AlInW3O12) and aluminium indium molybdate (Al0.84In1.16Mo3O12) were synthesized by non-hydrolytic sol–gel chemistry, and their crystal structures, phase transition and thermal expansion behavior were studied using variable-temperature synchrotron powder diffraction. AlInW3O12 adopts an orthorhombic phase above 260 K and gradually transitions to a monoclinic polymorph below this temperature. Al0.84In1.16Mo3O12 also shows a gradual transition between the monoclinic and orthorhombic structures between 330 and 445 K. Both materials display much lower phase-transition temperatures than predicted on the basis of the parent compounds and Vegard's law. This suppression is attributed to the large size difference between Al3+ and In3+. Interestingly, both samples display positive thermal expansion along all unit-cell axes instead of the typically observed negative expansion of orthorhombic A2M3O12 compositions.
Keywords: negative thermal expansion materials; scandium tungstate family; expansion behavior; phase-transition temperature; powder diffraction.
Supporting information
Portable Document Format (PDF) file https://doi.org/10.1107/S1600576722005751/ap5044sup1.pdf | |
Crystallographic Information File (CIF) https://doi.org/10.1107/S1600576722005751/ap5044sup2.cif |
Computing details top
(AlInW3O12_mono_1) top
Crystal data top
Mr = 1770.63 | β = 125.634 (7)° |
Monoclinic, P121/a1 | V = 2252.1 (3) Å3 |
a = 15.9295 (15) Å | Z = 4 |
b = 9.3851 (2) Å | Dx = 5.222 (1) Mg m−3 |
c = 18.5351 (5) Å | T = 80 K |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
x | y | z | Biso*/Beq | Occ. (<1) | |
W1 | 0.0033 (9) | 0.2390 (12) | 0.4891 (7) | 1.11 (4) | |
W2 | 0.3625 (7) | 0.1272 (16) | 0.1332 (7) | 1.11 (4) | |
W3 | 0.1466 (7) | 0.1171 (12) | 0.2594 (5) | 1.11 (4) | |
W4 | 0.1483 (9) | 0.6118 (13) | 0.3747 (7) | 1.11 (4) | |
W5 | 0.3562 (9) | 0.6233 (15) | 0.2249 (7) | 1.11 (4) | |
W6 | −0.0096 (8) | 0.7471 (12) | 0.0095 (7) | 1.11 (4) | |
In1 | 0.382 (3) | 0.970 (3) | 0.318 (2) | 1.11 (4) | 0.5 |
In2 | 0.373 (2) | 0.463 (3) | 0.059 (2) | 1.11 (4) | 0.5 |
In3 | 0.122 (3) | 0.469 (3) | 0.186 (2) | 1.11 (4) | 0.5 |
In4 | 0.115 (3) | 0.971 (3) | 0.4308 (19) | 1.11 (4) | 0.5 |
Al1 | 0.382 (3) | 0.970 (3) | 0.318 (2) | 1.11 (4) | 0.5 |
Al2 | 0.373 (2) | 0.463 (3) | 0.059 (2) | 1.11 (4) | 0.5 |
Al3 | 0.122 (3) | 0.469 (3) | 0.186 (2) | 1.11 (4) | 0.5 |
Al4 | 0.115 (3) | 0.971 (3) | 0.4308 (19) | 1.11 (4) | 0.5 |
O1 | 0.578 (6) | 0.418 (7) | −0.029 (7) | 1.11 (4) | |
O2 | 0.972 (13) | 0.423 (17) | 0.146 (11) | 1.11 (4) | |
O3 | 0.819 (6) | 0.199 (11) | 0.069 (5) | 1.11 (4) | |
O4 | 0.787 (8) | 0.512 (13) | 0.057 (6) | 1.11 (4) | |
O5 | 0.522 (11) | 0.425 (15) | 0.167 (9) | 1.11 (4) | |
O6 | 0.767 (10) | 0.511 (13) | 0.297 (8) | 1.11 (4) | |
O7 | 0.429 (8) | 0.145 (11) | 0.420 (6) | 1.11 (4) | |
O8 | 0.168 (9) | 0.297 (17) | 0.266 (7) | 1.11 (4) | |
O9 | 0.554 (6) | 0.370 (9) | 0.424 (4) | 1.11 (4) | |
O10 | 0.394 (8) | 0.331 (11) | 0.969 (5) | 1.11 (4) | |
O11 | 0.082 (9) | 0.367 (12) | 0.090 (8) | 1.11 (4) | |
O12 | 0.388 (8) | 0.313 (10) | 0.485 (7) | 1.11 (4) | |
O13 | 0.876 (6) | 0.374 (11) | 0.225 (6) | 1.11 (4) | |
O14 | 0.281 (9) | −0.004 (10) | 0.526 (7) | 1.11 (4) | |
O15 | 0.140 (8) | 0.109 (12) | 0.346 (7) | 1.11 (4) | |
O16 | 0.534 (12) | 0.939 (14) | 0.363 (9) | 1.11 (4) | |
O17 | 0.758 (12) | 0.977 (10) | 0.218 (9) | 1.11 (4) | |
O18 | 0.651 (12) | 0.913 (15) | 0.273 (8) | 1.11 (4) | |
O19 | 0.965 (9) | 0.932 (14) | 0.317 (9) | 1.11 (4) | |
O20 | 0.078 (9) | 0.382 (11) | 0.586 (8) | 1.11 (4) | |
O21 | 0.166 (6) | 0.804 (11) | 0.370 (5) | 1.11 (4) | |
O22 | 0.061 (9) | 0.641 (13) | 0.094 (8) | 1.11 (4) | |
O23 | 0.353 (12) | 0.572 (13) | 0.123 (8) | 1.11 (4) | |
O24 | 0.333 (9) | 0.817 (13) | 0.231 (7) | 1.11 (4) |
Geometric parameters (Å, º) top
W1—O7i | 1.57 (9) | O8—O18ii | 2.7 (2) |
W1—O12i | 1.86 (15) | O8—O11 | 2.80 (19) |
W1—O20 | 1.99 (11) | O8—O2ix | 2.84 (19) |
W1—O9i | 2.07 (11) | O8—O5i | 2.86 (19) |
W2—O13i | 1.58 (12) | O8—O17ii | 3.0 (2) |
W2—O2i | 1.7 (2) | O8—O6i | 3.2 (2) |
W2—O4i | 1.78 (10) | O9—In4xiv | 1.74 (10) |
W2—O3i | 1.89 (10) | O9—Al4xiv | 1.74 (10) |
W3—O15 | 1.67 (14) | O9—W1xii | 2.07 (11) |
W3—O8 | 1.71 (16) | O9—O19ii | 2.48 (15) |
W3—O5i | 1.76 (11) | O9—O15xii | 2.51 (19) |
W3—O6i | 2.01 (14) | O9—O7 | 2.88 (16) |
W4—O16ii | 1.8 (2) | O10—W6xix | 1.81 (13) |
W4—O21 | 1.83 (11) | O10—In2xx | 2.26 (13) |
W4—O14iii | 1.85 (10) | O10—Al2xx | 2.26 (13) |
W4—O18ii | 1.92 (19) | O10—O22xix | 2.45 (19) |
W5—O19ii | 1.65 (11) | O10—O1xi | 2.53 (13) |
W5—O17ii | 1.77 (19) | O10—O3xxi | 2.74 (19) |
W5—O24 | 1.87 (13) | O10—O1xx | 3.01 (18) |
W5—O23 | 1.93 (19) | O10—O4xi | 3.02 (19) |
W6—O22 | 1.63 (11) | O10—O11xxii | 3.10 (14) |
W6—O10iii | 1.81 (13) | O10—O5xx | 3.11 (16) |
W6—O11iv | 1.84 (12) | O11—Al3 | 1.79 (14) |
W6—O1v | 2.08 (10) | O11—In3 | 1.79 (14) |
In1—Al1 | 0.00000 | O11—W6iv | 1.84 (12) |
In1—O6ii | 1.65 (17) | O11—O2ix | 2.6 (3) |
In1—O20iii | 1.72 (14) | O11—O22 | 2.60 (17) |
In1—O24 | 1.95 (12) | O11—O22iv | 2.78 (16) |
In1—O16 | 2.08 (19) | O11—O8 | 2.80 (19) |
In1—O13ii | 2.22 (12) | O11—O17ii | 2.81 (16) |
In1—O7vi | 2.28 (11) | O11—O10xxiii | 3.10 (14) |
In2—Al2 | 0.00000 | O12—W1xii | 1.86 (15) |
In2—O1vii | 1.64 (12) | O12—Al4xix | 2.18 (13) |
In2—O23 | 1.72 (19) | O12—In4xix | 2.18 (13) |
In2—O3i | 1.81 (11) | O12—O7 | 2.29 (19) |
In2—O5 | 2.05 (12) | O12—O20xii | 3.07 (14) |
In2—O4vii | 2.19 (9) | O12—O14iii | 3.11 (19) |
In2—O10viii | 2.26 (13) | O12—O19xxiv | 3.20 (16) |
In3—Al3 | 0.00000 | O13—W2xii | 1.58 (12) |
In3—O11 | 1.79 (14) | O13—In1xiv | 2.22 (12) |
In3—O18ii | 1.79 (16) | O13—Al1xiv | 2.22 (12) |
In3—O17ii | 1.9 (2) | O13—O2 | 2.7 (3) |
In3—O8 | 2.03 (15) | O13—O4 | 2.86 (15) |
In3—O2ix | 2.1 (2) | O13—O16xiv | 2.92 (15) |
In3—O22 | 2.12 (12) | O13—O3 | 2.97 (14) |
In4—Al4 | 0.00000 | O13—O24xiv | 3.00 (17) |
In4—O9ii | 1.74 (10) | O13—O6 | 3.0 (2) |
In4—O19ix | 2.11 (10) | O14—W4xix | 1.85 (10) |
In4—O14vi | 2.17 (11) | O14—In4xviii | 2.17 (11) |
In4—O12iii | 2.18 (13) | O14—Al4xviii | 2.17 (11) |
In4—O15vi | 2.24 (15) | O14—O16xi | 2.49 (17) |
In4—O21 | 2.33 (12) | O14—O15 | 2.93 (14) |
Al1—In1 | 0.00000 | O14—O21xviii | 2.97 (13) |
Al1—O6ii | 1.65 (17) | O14—O12xix | 3.11 (19) |
Al1—O20iii | 1.72 (14) | O15—W3 | 1.67 (14) |
Al1—O24 | 1.95 (12) | O15—In4xviii | 2.24 (15) |
Al1—O16 | 2.08 (19) | O15—Al4xviii | 2.24 (15) |
Al1—O13ii | 2.22 (12) | O15—O8 | 2.5 (2) |
Al1—O7vi | 2.28 (11) | O15—O9i | 2.51 (19) |
Al2—In2 | 0.00000 | O15—O5i | 2.71 (17) |
Al2—O1vii | 1.64 (12) | O15—O6i | 2.9 (2) |
Al2—O23 | 1.72 (19) | O15—O21xviii | 2.89 (16) |
Al2—O3i | 1.81 (11) | O15—O14 | 2.93 (14) |
Al2—O5 | 2.05 (12) | O15—O19xxv | 3.0 (2) |
Al2—O4vii | 2.19 (9) | O16—W4xiv | 1.8 (2) |
Al2—O10viii | 2.26 (13) | O16—In1 | 2.08 (19) |
Al3—In3 | 0.00000 | O16—Al1 | 2.08 (19) |
Al3—O11 | 1.79 (14) | O16—O14xi | 2.49 (17) |
Al3—O18ii | 1.79 (16) | O16—O20iii | 2.5 (3) |
Al3—O17ii | 1.9 (2) | O16—O24 | 2.91 (17) |
Al3—O8 | 2.03 (15) | O16—O13ii | 2.92 (15) |
Al3—O2ix | 2.1 (2) | O16—O21xiv | 3.0 (2) |
Al3—O22 | 2.12 (12) | O16—O7vi | 3.1 (2) |
Al4—In4 | 0.00000 | O16—O18 | 3.1 (3) |
Al4—O9ii | 1.74 (10) | O17—W5xiv | 1.77 (19) |
Al4—O19ix | 2.11 (10) | O17—Al3xiv | 1.9 (2) |
Al4—O14vi | 2.17 (11) | O17—In3xiv | 1.9 (2) |
Al4—O12iii | 2.18 (13) | O17—O18 | 2.5 (3) |
Al4—O15vi | 2.24 (15) | O17—O19 | 2.7 (2) |
Al4—O21 | 2.33 (12) | O17—O11xiv | 2.81 (16) |
O1—In2vii | 1.64 (12) | O17—O22xiv | 2.82 (17) |
O1—Al2vii | 1.64 (12) | O17—O24xiv | 2.95 (17) |
O1—W6x | 2.08 (10) | O17—O23xiv | 3.0 (3) |
O1—O10xi | 2.53 (13) | O17—O8xiv | 3.0 (2) |
O1—O23vii | 2.5 (3) | O18—Al3xiv | 1.79 (16) |
O1—O5vii | 2.55 (16) | O18—In3xiv | 1.79 (16) |
O1—O4 | 2.86 (15) | O18—W4xiv | 1.92 (19) |
O1—O10viii | 3.01 (18) | O18—O17 | 2.5 (3) |
O1—O22x | 3.16 (14) | O18—O21xiv | 2.63 (19) |
O2—W2xii | 1.7 (2) | O18—O8xiv | 2.7 (2) |
O2—In3xiii | 2.1 (2) | O18—O22xiv | 2.8 (2) |
O2—Al3xiii | 2.1 (2) | O18—O2ii | 2.87 (19) |
O2—O4 | 2.5 (2) | O18—O16 | 3.1 (3) |
O2—O11xiii | 2.6 (3) | O19—W5xiv | 1.65 (11) |
O2—O13 | 2.7 (3) | O19—Al4xiii | 2.11 (10) |
O2—O8xiii | 2.84 (19) | O19—In4xiii | 2.11 (10) |
O2—O18xiv | 2.87 (19) | O19—O9xiv | 2.48 (15) |
O2—O3 | 2.88 (19) | O19—O17 | 2.7 (2) |
O2—O22xiii | 3.0 (3) | O19—O24xiv | 2.92 (17) |
O3—Al2xii | 1.81 (11) | O19—O23xiv | 2.9 (2) |
O3—In2xii | 1.81 (11) | O19—O21xiii | 3.00 (18) |
O3—W2xii | 1.89 (10) | O19—O15xxvi | 3.0 (2) |
O3—O4xv | 2.61 (13) | O19—O12xxvii | 3.20 (16) |
O3—O23xii | 2.68 (16) | O20—Al1xix | 1.72 (14) |
O3—O10xvi | 2.74 (19) | O20—In1xix | 1.72 (14) |
O3—O5xii | 2.87 (17) | O20—W1 | 1.99 (11) |
O3—O2 | 2.88 (19) | O20—O6xi | 2.36 (13) |
O3—O4 | 2.96 (16) | O20—O7iii | 2.47 (15) |
O3—O13 | 2.97 (14) | O20—O16xix | 2.5 (3) |
O4—W2xii | 1.78 (10) | O20—O7i | 2.58 (13) |
O4—Al2vii | 2.19 (9) | O20—O24xix | 2.87 (18) |
O4—In2vii | 2.19 (9) | O20—O12i | 3.07 (14) |
O4—O2 | 2.5 (2) | O21—W4 | 1.83 (11) |
O4—O3xvii | 2.61 (13) | O21—In4 | 2.33 (12) |
O4—O23vii | 2.84 (15) | O21—Al4 | 2.33 (12) |
O4—O13 | 2.86 (15) | O21—O18ii | 2.63 (19) |
O4—O1 | 2.86 (15) | O21—O15vi | 2.89 (16) |
O4—O3 | 2.96 (16) | O21—O14vi | 2.97 (13) |
O4—O10xi | 3.02 (19) | O21—O19ix | 3.00 (18) |
O5—W3xii | 1.76 (11) | O21—O16ii | 3.0 (2) |
O5—Al2 | 2.05 (12) | O21—O6ii | 3.2 (2) |
O5—In2 | 2.05 (12) | O22—W6 | 1.63 (11) |
O5—O1vii | 2.55 (16) | O22—Al3 | 2.12 (12) |
O5—O23 | 2.7 (2) | O22—In3 | 2.12 (12) |
O5—O15xii | 2.71 (17) | O22—O10iii | 2.45 (19) |
O5—O8xii | 2.86 (19) | O22—O11 | 2.60 (17) |
O5—O3i | 2.87 (17) | O22—O11iv | 2.78 (16) |
O5—O10viii | 3.11 (16) | O22—O18ii | 2.8 (2) |
O6—Al1xiv | 1.65 (17) | O22—O17ii | 2.82 (17) |
O6—In1xiv | 1.65 (17) | O22—O2ix | 3.0 (3) |
O6—W3xii | 2.01 (14) | O22—O1v | 3.16 (14) |
O6—O20xi | 2.36 (13) | O23—Al2 | 1.72 (19) |
O6—O24xiv | 2.6 (2) | O23—In2 | 1.72 (19) |
O6—O7xii | 2.68 (14) | O23—W5 | 1.93 (19) |
O6—O15xii | 2.9 (2) | O23—O1vii | 2.5 (3) |
O6—O13 | 3.0 (2) | O23—O3i | 2.68 (16) |
O6—O21xiv | 3.2 (2) | O23—O5 | 2.7 (2) |
O6—O8xii | 3.2 (2) | O23—O4vii | 2.84 (15) |
O7—W1xii | 1.57 (9) | O23—O19ii | 2.9 (2) |
O7—In1xviii | 2.28 (11) | O23—O17ii | 3.0 (3) |
O7—Al1xviii | 2.28 (11) | O23—O24 | 3.2 (2) |
O7—O12 | 2.29 (19) | O24—W5 | 1.87 (13) |
O7—O20xix | 2.47 (15) | O24—In1 | 1.95 (12) |
O7—O20xii | 2.58 (13) | O24—Al1 | 1.95 (12) |
O7—O6i | 2.68 (14) | O24—O6ii | 2.6 (2) |
O7—O9 | 2.88 (16) | O24—O20iii | 2.87 (18) |
O7—O16xviii | 3.1 (2) | O24—O16 | 2.91 (17) |
O8—W3 | 1.71 (16) | O24—O19ii | 2.92 (17) |
O8—Al3 | 2.03 (15) | O24—O17ii | 2.95 (17) |
O8—In3 | 2.03 (15) | O24—O13ii | 3.00 (17) |
O8—O15 | 2.5 (2) | O24—O23 | 3.2 (2) |
O12i—W1—O7i | 84 (6) | O5xx—O10—O3xxi | 58 (4) |
O20—W1—O12i | 106 (6) | O5xx—O10—O1xi | 52 (4) |
O20—W1—O7i | 92 (5) | O5xx—O10—O22xix | 127 (5) |
O9i—W1—O20 | 129 (5) | O5xx—O10—Al2xx | 41 (3) |
O9i—W1—O12i | 124 (4) | O5xx—O10—In2xx | 41 (3) |
O9i—W1—O7i | 104 (6) | O5xx—O10—W6xix | 89 (4) |
O2i—W2—O13i | 111 (7) | In3—O11—Al3 | 0.000 |
O4i—W2—O2i | 94 (7) | W6iv—O11—In3 | 164 (11) |
O4i—W2—O13i | 117 (6) | W6iv—O11—Al3 | 164 (11) |
O3i—W2—O4i | 108 (4) | O2ix—O11—W6iv | 110 (7) |
O3i—W2—O2i | 107 (7) | O2ix—O11—In3 | 54 (6) |
O3i—W2—O13i | 117 (5) | O2ix—O11—Al3 | 54 (6) |
O8—W3—O15 | 95 (7) | O22—O11—O2ix | 70 (7) |
O5i—W3—O8 | 111 (6) | O22—O11—W6iv | 126 (6) |
O5i—W3—O15 | 105 (8) | O22—O11—In3 | 54 (4) |
O6i—W3—O5i | 121 (6) | O22—O11—Al3 | 54 (4) |
O6i—W3—O8 | 117 (6) | O22iv—O11—O22 | 92 (5) |
O6i—W3—O15 | 103 (6) | O22iv—O11—O2ix | 104 (6) |
O21—W4—O16ii | 116 (6) | O22iv—O11—W6iv | 34 (3) |
O14iii—W4—O21 | 127 (4) | O22iv—O11—In3 | 143 (7) |
O14iii—W4—O16ii | 87 (6) | O22iv—O11—Al3 | 143 (7) |
O18ii—W4—O14iii | 124 (6) | O8—O11—O22iv | 157 (7) |
O18ii—W4—O21 | 89 (6) | O8—O11—O22 | 100 (6) |
O18ii—W4—O16ii | 117 (7) | O8—O11—O2ix | 64 (6) |
O17ii—W5—O19ii | 105 (7) | O8—O11—W6iv | 129 (7) |
O24—W5—O17ii | 109 (7) | O8—O11—In3 | 46 (5) |
O24—W5—O19ii | 112 (5) | O8—O11—Al3 | 46 (5) |
O23—W5—O24 | 114 (6) | O17ii—O11—O8 | 64 (5) |
O23—W5—O17ii | 107 (7) | O17ii—O11—O22iv | 139 (7) |
O23—W5—O19ii | 110 (8) | O17ii—O11—O22 | 63 (4) |
O10iii—W6—O22 | 91 (6) | O17ii—O11—O2ix | 97 (7) |
O11iv—W6—O10iii | 116 (7) | O17ii—O11—W6iv | 153 (10) |
O11iv—W6—O22 | 106 (5) | O17ii—O11—In3 | 43 (5) |
O1v—W6—O11iv | 122 (5) | O17ii—O11—Al3 | 43 (5) |
O1v—W6—O10iii | 101 (4) | O10xxiii—O11—O17ii | 172 (7) |
O1v—W6—O22 | 116 (6) | O10xxiii—O11—O8 | 108 (6) |
O20iii—In1—O6ii | 89 (7) | O10xxiii—O11—O22iv | 49 (4) |
O24—In1—O20iii | 103 (6) | O10xxiii—O11—O22 | 122 (5) |
O24—In1—O6ii | 92 (6) | O10xxiii—O11—O2ix | 79 (6) |
O16—In1—O24 | 92 (6) | O10xxiii—O11—W6iv | 32 (4) |
O16—In1—O20iii | 83 (7) | O10xxiii—O11—In3 | 133 (9) |
O16—In1—O6ii | 171 (7) | O10xxiii—O11—Al3 | 133 (9) |
O13ii—In1—O16 | 85 (5) | Al4xix—O12—W1xii | 126 (4) |
O13ii—In1—O24 | 92 (5) | In4xix—O12—Al4xix | 0.000 |
O13ii—In1—O20iii | 161 (4) | In4xix—O12—W1xii | 126 (4) |
O13ii—In1—O6ii | 102 (5) | O7—O12—In4xix | 168 (5) |
O7vi—In1—O13ii | 91 (4) | O7—O12—Al4xix | 168 (5) |
O7vi—In1—O16 | 91 (5) | O7—O12—W1xii | 43 (4) |
O7vi—In1—O24 | 176 (6) | O20xii—O12—O7 | 55 (4) |
O7vi—In1—O20iii | 75 (5) | O20xii—O12—In4xix | 113 (4) |
O7vi—In1—O6ii | 84 (6) | O20xii—O12—Al4xix | 113 (4) |
O23—In2—O1vii | 98 (7) | O20xii—O12—W1xii | 39 (4) |
O3i—In2—O23 | 98 (7) | O14iii—O12—O20xii | 152 (6) |
O3i—In2—O1vii | 163 (6) | O14iii—O12—O7 | 148 (5) |
O5—In2—O3i | 96 (5) | O14iii—O12—In4xix | 44 (3) |
O5—In2—O23 | 90 (7) | O14iii—O12—Al4xix | 44 (3) |
O5—In2—O1vii | 87 (6) | O14iii—O12—W1xii | 162 (6) |
O4vii—In2—O5 | 176 (6) | O19xxiv—O12—O14iii | 85 (5) |
O4vii—In2—O3i | 81 (4) | O19xxiv—O12—O20xii | 73 (4) |
O4vii—In2—O23 | 92 (6) | O19xxiv—O12—O7 | 127 (5) |
O4vii—In2—O1vii | 96 (5) | O19xxiv—O12—In4xix | 41 (3) |
O10viii—In2—O4vii | 85 (4) | O19xxiv—O12—Al4xix | 41 (3) |
O10viii—In2—O5 | 92 (6) | O19xxiv—O12—W1xii | 90 (4) |
O10viii—In2—O3i | 84 (5) | In1xiv—O13—W2xii | 139 (6) |
O10viii—In2—O23 | 176 (6) | Al1xiv—O13—In1xiv | 0.000 |
O10viii—In2—O1vii | 79 (5) | Al1xiv—O13—W2xii | 139 (6) |
O18ii—In3—O11 | 173 (5) | O2—O13—Al1xiv | 122 (6) |
O17ii—In3—O18ii | 85 (8) | O2—O13—In1xiv | 122 (6) |
O17ii—In3—O11 | 98 (8) | O2—O13—W2xii | 36 (4) |
O8—In3—O17ii | 97 (5) | O4—O13—O2 | 54 (5) |
O8—In3—O18ii | 92 (6) | O4—O13—Al1xiv | 108 (5) |
O8—In3—O11 | 94 (6) | O4—O13—In1xiv | 108 (5) |
O2ix—In3—O8 | 87 (6) | O4—O13—W2xii | 34 (3) |
O2ix—In3—O17ii | 176 (5) | O16xiv—O13—O4 | 108 (5) |
O2ix—In3—O18ii | 95 (9) | O16xiv—O13—O2 | 84 (6) |
O2ix—In3—O11 | 83 (8) | O16xiv—O13—Al1xiv | 45 (5) |
O22—In3—O2ix | 89 (6) | O16xiv—O13—In1xiv | 45 (5) |
O22—In3—O8 | 175 (4) | O16xiv—O13—W2xii | 117 (7) |
O22—In3—O17ii | 88 (5) | O3—O13—O16xiv | 144 (7) |
O22—In3—O18ii | 91 (6) | O3—O13—O4 | 61 (4) |
O22—In3—O11 | 83 (5) | O3—O13—O2 | 61 (5) |
O19ix—In4—O9ii | 79 (5) | O3—O13—Al1xiv | 166 (4) |
O14vi—In4—O19ix | 165 (7) | O3—O13—In1xiv | 166 (4) |
O14vi—In4—O9ii | 109 (4) | O3—O13—W2xii | 35 (3) |
O12iii—In4—O14vi | 91 (4) | O24xiv—O13—O3 | 129 (4) |
O12iii—In4—O19ix | 96 (5) | O24xiv—O13—O16xiv | 59 (4) |
O12iii—In4—O9ii | 113 (6) | O24xiv—O13—O4 | 68 (4) |
O15vi—In4—O12iii | 170 (5) | O24xiv—O13—O2 | 94 (6) |
O15vi—In4—O14vi | 83 (4) | O24xiv—O13—Al1xiv | 40 (3) |
O15vi—In4—O19ix | 87 (5) | O24xiv—O13—In1xiv | 40 (3) |
O15vi—In4—O9ii | 77 (5) | O24xiv—O13—W2xii | 99 (5) |
O21—In4—O15vi | 78 (5) | O6—O13—O24xiv | 51 (5) |
O21—In4—O12iii | 93 (5) | O6—O13—O3 | 138 (4) |
O21—In4—O14vi | 82 (4) | O6—O13—O16xiv | 77 (5) |
O21—In4—O19ix | 85 (5) | O6—O13—O4 | 104 (5) |
O21—In4—O9ii | 151 (4) | O6—O13—O2 | 145 (6) |
O20iii—Al1—O6ii | 89 (7) | O6—O13—Al1xiv | 32 (3) |
O24—Al1—O20iii | 103 (6) | O6—O13—In1xiv | 32 (3) |
O24—Al1—O6ii | 92 (6) | O6—O13—W2xii | 136 (5) |
O16—Al1—O24 | 92 (6) | In4xviii—O14—W4xix | 128 (8) |
O16—Al1—O20iii | 83 (7) | Al4xviii—O14—In4xviii | 0.000 |
O16—Al1—O6ii | 171 (7) | Al4xviii—O14—W4xix | 128 (8) |
O13ii—Al1—O16 | 85 (5) | O16xi—O14—Al4xviii | 172 (6) |
O13ii—Al1—O24 | 92 (5) | O16xi—O14—In4xviii | 172 (6) |
O13ii—Al1—O20iii | 161 (4) | O16xi—O14—W4xix | 45 (5) |
O13ii—Al1—O6ii | 102 (5) | O15—O14—O16xi | 127 (7) |
O7vi—Al1—O13ii | 91 (4) | O15—O14—Al4xviii | 49 (3) |
O7vi—Al1—O16 | 91 (5) | O15—O14—In4xviii | 49 (3) |
O7vi—Al1—O24 | 176 (6) | O15—O14—W4xix | 123 (5) |
O7vi—Al1—O20iii | 75 (5) | O21xviii—O14—O15 | 59 (3) |
O7vi—Al1—O6ii | 84 (6) | O21xviii—O14—O16xi | 136 (8) |
O23—Al2—O1vii | 98 (7) | O21xviii—O14—Al4xviii | 51 (3) |
O3i—Al2—O23 | 98 (7) | O21xviii—O14—In4xviii | 51 (3) |
O3i—Al2—O1vii | 163 (6) | O21xviii—O14—W4xix | 178 (7) |
O5—Al2—O3i | 96 (5) | O12xix—O14—O21xviii | 65 (4) |
O5—Al2—O23 | 90 (7) | O12xix—O14—O15 | 94 (4) |
O5—Al2—O1vii | 87 (6) | O12xix—O14—O16xi | 139 (7) |
O4vii—Al2—O5 | 176 (6) | O12xix—O14—Al4xviii | 45 (3) |
O4vii—Al2—O3i | 81 (4) | O12xix—O14—In4xviii | 45 (3) |
O4vii—Al2—O23 | 92 (6) | O12xix—O14—W4xix | 113 (8) |
O4vii—Al2—O1vii | 96 (5) | In4xviii—O15—W3 | 147 (7) |
O10viii—Al2—O4vii | 85 (4) | Al4xviii—O15—In4xviii | 0.000 |
O10viii—Al2—O5 | 92 (6) | Al4xviii—O15—W3 | 147 (7) |
O10viii—Al2—O3i | 84 (5) | O8—O15—Al4xviii | 170 (7) |
O10viii—Al2—O23 | 176 (6) | O8—O15—In4xviii | 170 (7) |
O10viii—Al2—O1vii | 79 (5) | O8—O15—W3 | 43 (5) |
O18ii—Al3—O11 | 173 (5) | O9i—O15—O8 | 129 (7) |
O17ii—Al3—O18ii | 85 (8) | O9i—O15—Al4xviii | 43 (3) |
O17ii—Al3—O11 | 98 (8) | O9i—O15—In4xviii | 43 (3) |
O8—Al3—O17ii | 97 (5) | O9i—O15—W3 | 156 (5) |
O8—Al3—O18ii | 92 (6) | O5i—O15—O9i | 119 (6) |
O8—Al3—O11 | 94 (6) | O5i—O15—O8 | 66 (5) |
O2ix—Al3—O8 | 87 (6) | O5i—O15—Al4xviii | 121 (6) |
O2ix—Al3—O17ii | 176 (5) | O5i—O15—In4xviii | 121 (6) |
O2ix—Al3—O18ii | 95 (9) | O5i—O15—W3 | 39 (5) |
O2ix—Al3—O11 | 83 (8) | O6i—O15—O5i | 72 (6) |
O22—Al3—O2ix | 89 (6) | O6i—O15—O9i | 158 (6) |
O22—Al3—O8 | 175 (4) | O6i—O15—O8 | 72 (6) |
O22—Al3—O17ii | 88 (5) | O6i—O15—Al4xviii | 116 (5) |
O22—Al3—O18ii | 91 (6) | O6i—O15—In4xviii | 116 (5) |
O22—Al3—O11 | 83 (5) | O6i—O15—W3 | 43 (4) |
O19ix—Al4—O9ii | 79 (5) | O21xviii—O15—O6i | 66 (5) |
O14vi—Al4—O19ix | 165 (7) | O21xviii—O15—O5i | 90 (5) |
O14vi—Al4—O9ii | 109 (4) | O21xviii—O15—O9i | 94 (5) |
O12iii—Al4—O14vi | 91 (4) | O21xviii—O15—O8 | 137 (7) |
O12iii—Al4—O19ix | 96 (5) | O21xviii—O15—Al4xviii | 52 (3) |
O12iii—Al4—O9ii | 113 (6) | O21xviii—O15—In4xviii | 52 (3) |
O15vi—Al4—O12iii | 170 (5) | O21xviii—O15—W3 | 96 (6) |
O15vi—Al4—O14vi | 83 (4) | O14—O15—O21xviii | 61 (3) |
O15vi—Al4—O19ix | 87 (5) | O14—O15—O6i | 90 (5) |
O15vi—Al4—O9ii | 77 (5) | O14—O15—O5i | 151 (6) |
O21—Al4—O15vi | 78 (5) | O14—O15—O9i | 72 (5) |
O21—Al4—O12iii | 93 (5) | O14—O15—O8 | 130 (5) |
O21—Al4—O14vi | 82 (4) | O14—O15—Al4xviii | 47 (3) |
O21—Al4—O19ix | 85 (5) | O14—O15—In4xviii | 47 (3) |
O21—Al4—O9ii | 151 (4) | O14—O15—W3 | 132 (7) |
Al2vii—O1—In2vii | 0.000 | O19xxv—O15—O14 | 91 (5) |
W6x—O1—Al2vii | 170 (7) | O19xxv—O15—O21xviii | 61 (4) |
W6x—O1—In2vii | 170 (7) | O19xxv—O15—O6i | 118 (6) |
O10xi—O1—W6x | 128 (7) | O19xxv—O15—O5i | 79 (5) |
O10xi—O1—Al2vii | 61 (4) | O19xxv—O15—O9i | 52 (4) |
O10xi—O1—In2vii | 61 (4) | O19xxv—O15—O8 | 139 (5) |
O23vii—O1—O10xi | 103 (6) | O19xxv—O15—Al4xviii | 44 (3) |
O23vii—O1—W6x | 129 (5) | O19xxv—O15—In4xviii | 44 (3) |
O23vii—O1—Al2vii | 42 (5) | O19xxv—O15—W3 | 115 (5) |
O23vii—O1—In2vii | 42 (5) | In1—O16—W4xiv | 165 (9) |
O5vii—O1—O23vii | 64 (6) | Al1—O16—In1 | 0.000 |
O5vii—O1—O10xi | 76 (4) | Al1—O16—W4xiv | 165 (9) |
O5vii—O1—W6x | 122 (5) | O14xi—O16—Al1 | 147 (9) |
O5vii—O1—Al2vii | 53 (5) | O14xi—O16—In1 | 147 (9) |
O5vii—O1—In2vii | 53 (5) | O14xi—O16—W4xiv | 48 (5) |
O4—O1—O5vii | 103 (6) | O20iii—O16—O14xi | 120 (8) |
O4—O1—O23vii | 63 (5) | O20iii—O16—Al1 | 42 (5) |
O4—O1—O10xi | 68 (4) | O20iii—O16—In1 | 42 (5) |
O4—O1—W6x | 134 (4) | O20iii—O16—W4xiv | 143 (7) |
O4—O1—Al2vii | 49 (3) | O24—O16—O20iii | 63 (6) |
O4—O1—In2vii | 49 (3) | O24—O16—O14xi | 170 (8) |
O10viii—O1—O4 | 153 (6) | O24—O16—Al1 | 42 (4) |
O10viii—O1—O5vii | 96 (5) | O24—O16—In1 | 42 (4) |
O10viii—O1—O23vii | 143 (5) | O24—O16—W4xiv | 123 (8) |
O10viii—O1—O10xi | 100 (5) | O13ii—O16—O24 | 62 (4) |
O10viii—O1—W6x | 36 (3) | O13ii—O16—O20iii | 91 (6) |
O10viii—O1—Al2vii | 146 (4) | O13ii—O16—O14xi | 125 (6) |
O10viii—O1—In2vii | 146 (4) | O13ii—O16—Al1 | 49 (4) |
O22x—O1—O10viii | 47 (4) | O13ii—O16—In1 | 49 (4) |
O22x—O1—O4 | 143 (4) | O13ii—O16—W4xiv | 125 (9) |
O22x—O1—O5vii | 102 (4) | O21xiv—O16—O13ii | 135 (7) |
O22x—O1—O23vii | 105 (5) | O21xiv—O16—O24 | 98 (5) |
O22x—O1—O10xi | 147 (7) | O21xiv—O16—O20iii | 117 (6) |
O22x—O1—W6x | 27 (3) | O21xiv—O16—O14xi | 72 (5) |
O22x—O1—Al2vii | 143 (7) | O21xiv—O16—Al1 | 137 (6) |
O22x—O1—In2vii | 143 (7) | O21xiv—O16—In1 | 137 (6) |
In3xiii—O2—W2xii | 170 (10) | O21xiv—O16—W4xiv | 33 (3) |
Al3xiii—O2—In3xiii | 0.000 | O7vi—O16—O21xiv | 160 (6) |
Al3xiii—O2—W2xii | 170 (10) | O7vi—O16—O13ii | 64 (4) |
O4—O2—Al3xiii | 145 (9) | O7vi—O16—O24 | 89 (6) |
O4—O2—In3xiii | 145 (9) | O7vi—O16—O20iii | 51 (5) |
O4—O2—W2xii | 44 (5) | O7vi—O16—O14xi | 100 (6) |
O11xiii—O2—O4 | 128 (8) | O7vi—O16—Al1 | 47 (4) |
O11xiii—O2—Al3xiii | 43 (5) | O7vi—O16—In1 | 47 (4) |
O11xiii—O2—In3xiii | 43 (5) | O7vi—O16—W4xiv | 147 (6) |
O11xiii—O2—W2xii | 141 (10) | O18—O16—O7vi | 146 (6) |
O13—O2—O11xiii | 157 (8) | O18—O16—O21xiv | 50 (5) |
O13—O2—O4 | 66 (7) | O18—O16—O13ii | 93 (6) |
O13—O2—Al3xiii | 138 (8) | O18—O16—O24 | 103 (6) |
O13—O2—In3xiii | 138 (8) | O18—O16—O20iii | 162 (6) |
O13—O2—W2xii | 33 (5) | O18—O16—O14xi | 71 (7) |
O8xiii—O2—O13 | 103 (7) | O18—O16—Al1 | 135 (6) |
O8xiii—O2—O11xiii | 62 (6) | O18—O16—In1 | 135 (6) |
O8xiii—O2—O4 | 169 (11) | O18—O16—W4xiv | 33 (5) |
O8xiii—O2—Al3xiii | 46 (5) | Al3xiv—O17—W5xiv | 160 (7) |
O8xiii—O2—In3xiii | 46 (5) | In3xiv—O17—Al3xiv | 0.000 |
O8xiii—O2—W2xii | 125 (10) | In3xiv—O17—W5xiv | 160 (7) |
O18xiv—O2—O8xiii | 58 (5) | O18—O17—In3xiv | 45 (6) |
O18xiv—O2—O13 | 105 (8) | O18—O17—Al3xiv | 45 (6) |
O18xiv—O2—O11xiii | 82 (8) | O18—O17—W5xiv | 129 (7) |
O18xiv—O2—O4 | 126 (8) | O19—O17—O18 | 122 (7) |
O18xiv—O2—Al3xiii | 38 (5) | O19—O17—In3xiv | 161 (9) |
O18xiv—O2—In3xiii | 38 (5) | O19—O17—Al3xiv | 161 (9) |
O18xiv—O2—W2xii | 136 (12) | O19—O17—W5xiv | 36 (4) |
O3—O2—O18xiv | 161 (8) | O11xiv—O17—O19 | 150 (8) |
O3—O2—O8xiii | 108 (6) | O11xiv—O17—O18 | 84 (7) |
O3—O2—O13 | 64 (6) | O11xiv—O17—In3xiv | 39 (5) |
O3—O2—O11xiii | 103 (7) | O11xiv—O17—Al3xiv | 39 (5) |
O3—O2—O4 | 66 (5) | O11xiv—O17—W5xiv | 138 (10) |
O3—O2—Al3xiii | 141 (9) | O22xiv—O17—O11xiv | 55 (4) |
O3—O2—In3xiii | 141 (9) | O22xiv—O17—O19 | 146 (6) |
O3—O2—W2xii | 39 (4) | O22xiv—O17—O18 | 63 (6) |
O22xiii—O2—O3 | 140 (8) | O22xiv—O17—In3xiv | 49 (4) |
O22xiii—O2—O18xiv | 57 (5) | O22xiv—O17—Al3xiv | 49 (4) |
O22xiii—O2—O8xiii | 91 (7) | O22xiv—O17—W5xiv | 112 (6) |
O22xiii—O2—O13 | 146 (8) | O24xiv—O17—O22xiv | 85 (4) |
O22xiii—O2—O11xiii | 56 (6) | O24xiv—O17—O11xiv | 135 (5) |
O22xiii—O2—O4 | 99 (6) | O24xiv—O17—O19 | 62 (5) |
O22xiii—O2—Al3xiii | 46 (5) | O24xiv—O17—O18 | 95 (6) |
O22xiii—O2—In3xiii | 46 (5) | O24xiv—O17—In3xiv | 126 (7) |
O22xiii—O2—W2xii | 143 (8) | O24xiv—O17—Al3xiv | 126 (7) |
In2xii—O3—Al2xii | 0.000 | O24xiv—O17—W5xiv | 37 (4) |
W2xii—O3—In2xii | 140 (5) | O23xiv—O17—O24xiv | 65 (6) |
W2xii—O3—Al2xii | 140 (5) | O23xiv—O17—O22xiv | 100 (6) |
O4xv—O3—W2xii | 162 (5) | O23xiv—O17—O11xiv | 100 (7) |
O4xv—O3—In2xii | 56 (4) | O23xiv—O17—O19 | 62 (6) |
O4xv—O3—Al2xii | 56 (4) | O23xiv—O17—O18 | 156 (6) |
O23xii—O3—O4xv | 65 (4) | O23xiv—O17—In3xiv | 136 (7) |
O23xii—O3—W2xii | 131 (4) | O23xiv—O17—Al3xiv | 136 (7) |
O23xii—O3—In2xii | 40 (5) | O23xiv—O17—W5xiv | 39 (5) |
O23xii—O3—Al2xii | 40 (5) | O8xiv—O17—O23xiv | 142 (6) |
O10xvi—O3—O23xii | 95 (6) | O8xiv—O17—O24xiv | 152 (9) |
O10xvi—O3—O4xv | 69 (5) | O8xiv—O17—O22xiv | 91 (7) |
O10xvi—O3—W2xii | 112 (5) | O8xiv—O17—O11xiv | 58 (5) |
O10xvi—O3—In2xii | 55 (4) | O8xiv—O17—O19 | 121 (5) |
O10xvi—O3—Al2xii | 55 (4) | O8xiv—O17—O18 | 59 (7) |
O5xii—O3—O10xvi | 67 (5) | O8xiv—O17—In3xiv | 43 (4) |
O5xii—O3—O23xii | 58 (5) | O8xiv—O17—Al3xiv | 43 (4) |
O5xii—O3—O4xv | 101 (5) | O8xiv—O17—W5xiv | 157 (6) |
O5xii—O3—W2xii | 95 (4) | In3xiv—O18—Al3xiv | 0.000 |
O5xii—O3—In2xii | 45 (3) | W4xiv—O18—In3xiv | 146 (10) |
O5xii—O3—Al2xii | 45 (3) | W4xiv—O18—Al3xiv | 146 (10) |
O2—O3—O5xii | 71 (5) | O17—O18—W4xiv | 147 (7) |
O2—O3—O10xvi | 81 (6) | O17—O18—In3xiv | 50 (6) |
O2—O3—O23xii | 125 (5) | O17—O18—Al3xiv | 50 (6) |
O2—O3—O4xv | 149 (7) | O21xiv—O18—O17 | 130 (8) |
O2—O3—W2xii | 34 (5) | O21xiv—O18—W4xiv | 44 (4) |
O2—O3—In2xii | 111 (6) | O21xiv—O18—In3xiv | 166 (8) |
O2—O3—Al2xii | 111 (6) | O21xiv—O18—Al3xiv | 166 (8) |
O4—O3—O2 | 51 (4) | O8xiv—O18—O21xiv | 146 (8) |
O4—O3—O5xii | 122 (5) | O8xiv—O18—O17 | 69 (6) |
O4—O3—O10xvi | 101 (5) | O8xiv—O18—W4xiv | 103 (7) |
O4—O3—O23xii | 163 (6) | O8xiv—O18—In3xiv | 48 (5) |
O4—O3—O4xv | 127 (3) | O8xiv—O18—Al3xiv | 48 (5) |
O4—O3—W2xii | 35 (2) | O22xiv—O18—O8xiv | 97 (6) |
O4—O3—In2xii | 154 (7) | O22xiv—O18—O21xiv | 117 (6) |
O4—O3—Al2xii | 154 (7) | O22xiv—O18—O17 | 64 (6) |
O13—O3—O4 | 58 (3) | O22xiv—O18—W4xiv | 149 (9) |
O13—O3—O2 | 55 (6) | O22xiv—O18—In3xiv | 49 (4) |
O13—O3—O5xii | 91 (4) | O22xiv—O18—Al3xiv | 49 (4) |
O13—O3—O10xvi | 135 (5) | O2ii—O18—O22xiv | 63 (6) |
O13—O3—O23xii | 106 (5) | O2ii—O18—O8xiv | 61 (5) |
O13—O3—O4xv | 156 (6) | O2ii—O18—O21xiv | 128 (9) |
O13—O3—W2xii | 28 (3) | O2ii—O18—O17 | 97 (8) |
O13—O3—In2xii | 132 (3) | O2ii—O18—W4xiv | 107 (9) |
O13—O3—Al2xii | 132 (3) | O2ii—O18—In3xiv | 47 (6) |
Al2vii—O4—W2xii | 136 (7) | O2ii—O18—Al3xiv | 47 (6) |
In2vii—O4—Al2vii | 0.000 | O16—O18—O2ii | 77 (7) |
In2vii—O4—W2xii | 136 (7) | O16—O18—O22xiv | 126 (7) |
O2—O4—In2vii | 157 (8) | O16—O18—O8xiv | 93 (7) |
O2—O4—Al2vii | 157 (8) | O16—O18—O21xiv | 63 (6) |
O2—O4—W2xii | 41 (5) | O16—O18—O17 | 161 (7) |
O3xvii—O4—O2 | 135 (8) | O16—O18—W4xiv | 30 (4) |
O3xvii—O4—In2vii | 43 (3) | O16—O18—In3xiv | 121 (8) |
O3xvii—O4—Al2vii | 43 (3) | O16—O18—Al3xiv | 121 (8) |
O3xvii—O4—W2xii | 172 (7) | Al4xiii—O19—W5xiv | 170 (10) |
O23vii—O4—O3xvii | 59 (4) | In4xiii—O19—Al4xiii | 0.000 |
O23vii—O4—O2 | 120 (8) | In4xiii—O19—W5xiv | 170 (10) |
O23vii—O4—In2vii | 37 (4) | O9xiv—O19—In4xiii | 44 (3) |
O23vii—O4—Al2vii | 37 (4) | O9xiv—O19—Al4xiii | 44 (3) |
O23vii—O4—W2xii | 116 (6) | O9xiv—O19—W5xiv | 146 (8) |
O13—O4—O23vii | 135 (6) | O17—O19—O9xiv | 109 (6) |
O13—O4—O3xvii | 158 (7) | O17—O19—In4xiii | 151 (8) |
O13—O4—O2 | 59 (6) | O17—O19—Al4xiii | 151 (8) |
O13—O4—In2vii | 133 (7) | O17—O19—W5xiv | 39 (4) |
O13—O4—Al2vii | 133 (7) | O24xiv—O19—O17 | 63 (4) |
O13—O4—W2xii | 30 (3) | O24xiv—O19—O9xiv | 159 (9) |
O1—O4—O13 | 98 (5) | O24xiv—O19—In4xiii | 136 (6) |
O1—O4—O23vii | 53 (5) | O24xiv—O19—Al4xiii | 136 (6) |
O1—O4—O3xvii | 77 (4) | O24xiv—O19—W5xiv | 37 (4) |
O1—O4—O2 | 143 (6) | O23xiv—O19—O24xiv | 66 (5) |
O1—O4—In2vii | 35 (3) | O23xiv—O19—O17 | 63 (6) |
O1—O4—Al2vii | 35 (3) | O23xiv—O19—O9xiv | 131 (7) |
O1—O4—W2xii | 104 (6) | O23xiv—O19—In4xiii | 139 (9) |
O3—O4—O1 | 80 (4) | O23xiv—O19—Al4xiii | 139 (9) |
O3—O4—O13 | 61 (4) | O23xiv—O19—W5xiv | 38 (5) |
O3—O4—O23vii | 78 (4) | O21xiii—O19—O23xiv | 100 (7) |
O3—O4—O3xvii | 137 (4) | O21xiii—O19—O24xiv | 99 (5) |
O3—O4—O2 | 63 (5) | O21xiii—O19—O17 | 158 (7) |
O3—O4—In2vii | 104 (4) | O21xiii—O19—O9xiv | 92 (4) |
O3—O4—Al2vii | 104 (4) | O21xiii—O19—In4xiii | 51 (4) |
O3—O4—W2xii | 38 (3) | O21xiii—O19—Al4xiii | 51 (4) |
O10xi—O4—O3 | 127 (5) | O21xiii—O19—W5xiv | 119 (8) |
O10xi—O4—O1 | 51 (3) | O15xxvi—O19—O21xiii | 58 (4) |
O10xi—O4—O13 | 103 (6) | O15xxvi—O19—O23xiv | 94 (7) |
O10xi—O4—O23vii | 86 (5) | O15xxvi—O19—O24xiv | 147 (8) |
O10xi—O4—O3xvii | 58 (4) | O15xxvi—O19—O17 | 132 (6) |
O10xi—O4—O2 | 155 (7) | O15xxvi—O19—O9xiv | 53 (4) |
O10xi—O4—In2vii | 48 (3) | O15xxvi—O19—In4xiii | 48 (4) |
O10xi—O4—Al2vii | 48 (3) | O15xxvi—O19—Al4xiii | 48 (4) |
O10xi—O4—W2xii | 129 (7) | O15xxvi—O19—W5xiv | 132 (9) |
Al2—O5—W3xii | 177 (11) | O12xxvii—O19—O15xxvi | 90 (4) |
In2—O5—Al2 | 0.000 | O12xxvii—O19—O21xiii | 64 (4) |
In2—O5—W3xii | 177 (11) | O12xxvii—O19—O23xiv | 156 (6) |
O1vii—O5—In2 | 40 (3) | O12xxvii—O19—O24xiv | 99 (5) |
O1vii—O5—Al2 | 40 (3) | O12xxvii—O19—O17 | 128 (8) |
O1vii—O5—W3xii | 143 (10) | O12xxvii—O19—O9xiv | 69 (4) |
O23—O5—O1vii | 58 (6) | O12xxvii—O19—In4xiii | 43 (3) |
O23—O5—In2 | 40 (4) | O12xxvii—O19—Al4xiii | 43 (3) |
O23—O5—Al2 | 40 (4) | O12xxvii—O19—W5xiv | 134 (8) |
O23—O5—W3xii | 141 (10) | In1xix—O20—Al1xix | 0.000 |
O15xii—O5—O23 | 107 (8) | W1—O20—In1xix | 158 (10) |
O15xii—O5—O1vii | 151 (7) | W1—O20—Al1xix | 158 (10) |
O15xii—O5—In2 | 143 (10) | O6xi—O20—W1 | 151 (9) |
O15xii—O5—Al2 | 143 (10) | O6xi—O20—In1xix | 44 (5) |
O15xii—O5—W3xii | 36 (4) | O6xi—O20—Al1xix | 44 (5) |
O8xii—O5—O15xii | 53 (4) | O7iii—O20—O6xi | 67 (4) |
O8xii—O5—O23 | 150 (10) | O7iii—O20—W1 | 130 (5) |
O8xii—O5—O1vii | 150 (9) | O7iii—O20—In1xix | 63 (4) |
O8xii—O5—In2 | 143 (7) | O7iii—O20—Al1xix | 63 (4) |
O8xii—O5—Al2 | 143 (7) | O16xix—O20—O7iii | 77 (6) |
O8xii—O5—W3xii | 34 (4) | O16xix—O20—O6xi | 99 (7) |
O3i—O5—O8xii | 108 (6) | O16xix—O20—W1 | 107 (6) |
O3i—O5—O15xii | 117 (8) | O16xix—O20—In1xix | 55 (6) |
O3i—O5—O23 | 58 (5) | O16xix—O20—Al1xix | 55 (6) |
O3i—O5—O1vii | 78 (4) | O7i—O20—O16xix | 96 (6) |
O3i—O5—In2 | 39 (3) | O7i—O20—O7iii | 93 (4) |
O3i—O5—Al2 | 39 (3) | O7i—O20—O6xi | 152 (8) |
O3i—O5—W3xii | 138 (8) | O7i—O20—W1 | 37 (3) |
O10viii—O5—O3i | 54 (4) | O7i—O20—In1xix | 144 (7) |
O10viii—O5—O8xii | 106 (6) | O7i—O20—Al1xix | 144 (7) |
O10viii—O5—O15xii | 157 (6) | O24xix—O20—O7i | 150 (7) |
O10viii—O5—O23 | 86 (5) | O24xix—O20—O16xix | 65 (6) |
O10viii—O5—O1vii | 52 (4) | O24xix—O20—O7iii | 104 (6) |
O10viii—O5—In2 | 46 (4) | O24xix—O20—O6xi | 58 (5) |
O10viii—O5—Al2 | 46 (4) | O24xix—O20—W1 | 123 (6) |
O10viii—O5—W3xii | 133 (9) | O24xix—O20—In1xix | 41 (4) |
In1xiv—O6—Al1xiv | 0.000 | O24xix—O20—Al1xix | 41 (4) |
W3xii—O6—In1xiv | 148 (9) | O12i—O20—O24xix | 103 (6) |
W3xii—O6—Al1xiv | 148 (9) | O12i—O20—O7i | 47 (4) |
O20xi—O6—W3xii | 148 (9) | O12i—O20—O16xix | 72 (5) |
O20xi—O6—In1xiv | 47 (5) | O12i—O20—O7iii | 124 (5) |
O20xi—O6—Al1xiv | 47 (5) | O12i—O20—O6xi | 161 (8) |
O24xiv—O6—O20xi | 71 (6) | O12i—O20—W1 | 36 (4) |
O24xiv—O6—W3xii | 141 (6) | O12i—O20—In1xix | 124 (9) |
O24xiv—O6—In1xiv | 49 (5) | O12i—O20—Al1xix | 124 (9) |
O24xiv—O6—Al1xiv | 49 (5) | In4—O21—W4 | 122 (6) |
O7xii—O6—O24xiv | 107 (7) | Al4—O21—In4 | 0.000 |
O7xii—O6—O20xi | 58 (4) | Al4—O21—W4 | 122 (6) |
O7xii—O6—W3xii | 103 (5) | O18ii—O21—Al4 | 159 (6) |
O7xii—O6—In1xiv | 58 (5) | O18ii—O21—In4 | 159 (6) |
O7xii—O6—Al1xiv | 58 (5) | O18ii—O21—W4 | 47 (5) |
O15xii—O6—O7xii | 91 (6) | O15vi—O21—O18ii | 135 (6) |
O15xii—O6—O24xiv | 161 (6) | O15vi—O21—Al4 | 49 (4) |
O15xii—O6—O20xi | 116 (8) | O15vi—O21—In4 | 49 (4) |
O15xii—O6—W3xii | 34 (4) | O15vi—O21—W4 | 166 (5) |
O15xii—O6—In1xiv | 149 (6) | O14vi—O21—O15vi | 60 (3) |
O15xii—O6—Al1xiv | 149 (6) | O14vi—O21—O18ii | 153 (5) |
O13—O6—O15xii | 131 (5) | O14vi—O21—Al4 | 47 (3) |
O13—O6—O7xii | 68 (5) | O14vi—O21—In4 | 47 (3) |
O13—O6—O24xiv | 64 (6) | O14vi—O21—W4 | 125 (4) |
O13—O6—O20xi | 91 (7) | O19ix—O21—O14vi | 91 (5) |
O13—O6—W3xii | 105 (5) | O19ix—O21—O15vi | 61 (4) |
O13—O6—In1xiv | 46 (5) | O19ix—O21—O18ii | 116 (5) |
O13—O6—Al1xiv | 46 (5) | O19ix—O21—Al4 | 45 (3) |
O21xiv—O6—O13 | 172 (6) | O19ix—O21—In4 | 45 (3) |
O21xiv—O6—O15xii | 57 (5) | O19ix—O21—W4 | 105 (5) |
O21xiv—O6—O7xii | 115 (6) | O16ii—O21—O19ix | 73 (5) |
O21xiv—O6—O24xiv | 108 (6) | O16ii—O21—O14vi | 121 (6) |
O21xiv—O6—O20xi | 84 (6) | O16ii—O21—O15vi | 135 (6) |
O21xiv—O6—W3xii | 82 (6) | O16ii—O21—O18ii | 67 (6) |
O21xiv—O6—In1xiv | 128 (6) | O16ii—O21—Al4 | 96 (5) |
O21xiv—O6—Al1xiv | 128 (6) | O16ii—O21—In4 | 96 (5) |
O8xii—O6—O21xiv | 105 (6) | O16ii—O21—W4 | 32 (4) |
O8xii—O6—O13 | 83 (5) | O6ii—O21—O16ii | 155 (5) |
O8xii—O6—O15xii | 48 (5) | O6ii—O21—O19ix | 111 (5) |
O8xii—O6—O7xii | 78 (4) | O6ii—O21—O14vi | 84 (4) |
O8xii—O6—O24xiv | 141 (7) | O6ii—O21—O15vi | 57 (4) |
O8xii—O6—O20xi | 134 (5) | O6ii—O21—O18ii | 90 (6) |
O8xii—O6—W3xii | 29 (3) | O6ii—O21—Al4 | 104 (5) |
O8xii—O6—In1xiv | 120 (7) | O6ii—O21—In4 | 104 (5) |
O8xii—O6—Al1xiv | 120 (7) | O6ii—O21—W4 | 134 (6) |
In1xviii—O7—W1xii | 155 (10) | Al3—O22—W6 | 166 (8) |
Al1xviii—O7—In1xviii | 0.000 | In3—O22—Al3 | 0.000 |
Al1xviii—O7—W1xii | 155 (10) | In3—O22—W6 | 166 (8) |
O12—O7—Al1xviii | 151 (6) | O10iii—O22—In3 | 144 (7) |
O12—O7—In1xviii | 151 (6) | O10iii—O22—Al3 | 144 (7) |
O12—O7—W1xii | 53 (5) | O10iii—O22—W6 | 48 (5) |
O20xix—O7—O12 | 134 (8) | O11—O22—O10iii | 129 (9) |
O20xix—O7—Al1xviii | 42 (4) | O11—O22—In3 | 43 (4) |
O20xix—O7—In1xviii | 42 (4) | O11—O22—Al3 | 43 (4) |
O20xix—O7—W1xii | 137 (5) | O11—O22—W6 | 127 (7) |
O20xii—O7—O20xix | 87 (4) | O11iv—O22—O11 | 88 (5) |
O20xii—O7—O12 | 78 (5) | O11iv—O22—O10iii | 72 (5) |
O20xii—O7—Al1xviii | 124 (5) | O11iv—O22—In3 | 129 (6) |
O20xii—O7—In1xviii | 124 (5) | O11iv—O22—Al3 | 129 (6) |
O20xii—O7—W1xii | 51 (3) | O11iv—O22—W6 | 39 (3) |
O6i—O7—O20xii | 137 (6) | O18ii—O22—O11iv | 160 (8) |
O6i—O7—O20xix | 54 (4) | O18ii—O22—O11 | 83 (5) |
O6i—O7—O12 | 113 (7) | O18ii—O22—O10iii | 127 (5) |
O6i—O7—Al1xviii | 38 (4) | O18ii—O22—In3 | 40 (4) |
O6i—O7—In1xviii | 38 (4) | O18ii—O22—Al3 | 40 (4) |
O6i—O7—W1xii | 166 (8) | O18ii—O22—W6 | 147 (9) |
O9—O7—O6i | 137 (6) | O17ii—O22—O18ii | 53 (6) |
O9—O7—O20xii | 84 (4) | O17ii—O22—O11iv | 136 (8) |
O9—O7—O20xix | 138 (7) | O17ii—O22—O11 | 62 (4) |
O9—O7—O12 | 83 (5) | O17ii—O22—O10iii | 100 (7) |
O9—O7—Al1xviii | 116 (6) | O17ii—O22—In3 | 44 (4) |
O9—O7—In1xviii | 116 (6) | O17ii—O22—Al3 | 44 (4) |
O9—O7—W1xii | 44 (4) | O17ii—O22—W6 | 147 (10) |
O16xviii—O7—O9 | 88 (6) | O2ix—O22—O17ii | 89 (6) |
O16xviii—O7—O6i | 79 (5) | O2ix—O22—O18ii | 60 (5) |
O16xviii—O7—O20xii | 92 (5) | O2ix—O22—O11iv | 100 (5) |
O16xviii—O7—O20xix | 52 (6) | O2ix—O22—O11 | 55 (6) |
O16xviii—O7—O12 | 167 (5) | O2ix—O22—O10iii | 171 (6) |
O16xviii—O7—Al1xviii | 42 (3) | O2ix—O22—In3 | 45 (4) |
O16xviii—O7—In1xviii | 42 (3) | O2ix—O22—Al3 | 45 (4) |
O16xviii—O7—W1xii | 114 (7) | O2ix—O22—W6 | 123 (7) |
Al3—O8—W3 | 139 (6) | O1v—O22—O2ix | 109 (6) |
In3—O8—Al3 | 0.000 | O1v—O22—O17ii | 146 (5) |
In3—O8—W3 | 139 (6) | O1v—O22—O18ii | 111 (7) |
O15—O8—In3 | 152 (8) | O1v—O22—O11iv | 70 (4) |
O15—O8—Al3 | 152 (8) | O1v—O22—O11 | 151 (5) |
O15—O8—W3 | 42 (5) | O1v—O22—O10iii | 63 (5) |
O18ii—O8—O15 | 128 (9) | O1v—O22—In3 | 145 (8) |
O18ii—O8—In3 | 41 (5) | O1v—O22—Al3 | 145 (8) |
O18ii—O8—Al3 | 41 (5) | O1v—O22—W6 | 36 (4) |
O18ii—O8—W3 | 164 (9) | In2—O23—Al2 | 0.000 |
O11—O8—O18ii | 80 (6) | W5—O23—In2 | 156 (8) |
O11—O8—O15 | 136 (6) | W5—O23—Al2 | 156 (8) |
O11—O8—In3 | 40 (3) | O1vii—O23—W5 | 153 (7) |
O11—O8—Al3 | 40 (3) | O1vii—O23—In2 | 40 (5) |
O11—O8—W3 | 102 (6) | O1vii—O23—Al2 | 40 (5) |
O2ix—O8—O11 | 55 (6) | O3i—O23—O1vii | 82 (6) |
O2ix—O8—O18ii | 62 (5) | O3i—O23—W5 | 119 (8) |
O2ix—O8—O15 | 105 (7) | O3i—O23—In2 | 42 (4) |
O2ix—O8—In3 | 48 (5) | O3i—O23—Al2 | 42 (4) |
O2ix—O8—Al3 | 48 (5) | O5—O23—O3i | 65 (5) |
O2ix—O8—W3 | 106 (6) | O5—O23—O1vii | 58 (6) |
O5i—O8—O2ix | 72 (5) | O5—O23—W5 | 112 (6) |
O5i—O8—O11 | 76 (5) | O5—O23—In2 | 50 (6) |
O5i—O8—O18ii | 133 (6) | O5—O23—Al2 | 50 (6) |
O5i—O8—O15 | 60 (5) | O4vii—O23—O5 | 100 (7) |
O5i—O8—In3 | 107 (5) | O4vii—O23—O3i | 56 (4) |
O5i—O8—Al3 | 107 (5) | O4vii—O23—O1vii | 64 (5) |
O5i—O8—W3 | 35 (3) | O4vii—O23—W5 | 141 (9) |
O17ii—O8—O5i | 133 (7) | O4vii—O23—In2 | 50 (4) |
O17ii—O8—O2ix | 88 (7) | O4vii—O23—Al2 | 50 (4) |
O17ii—O8—O11 | 58 (5) | O19ii—O23—O4vii | 159 (8) |
O17ii—O8—O18ii | 52 (6) | O19ii—O23—O5 | 81 (5) |
O17ii—O8—O15 | 165 (5) | O19ii—O23—O3i | 107 (5) |
O17ii—O8—In3 | 40 (4) | O19ii—O23—O1vii | 130 (7) |
O17ii—O8—Al3 | 40 (4) | O19ii—O23—W5 | 32 (4) |
O17ii—O8—W3 | 142 (9) | O19ii—O23—In2 | 127 (7) |
O6i—O8—O17ii | 116 (7) | O19ii—O23—Al2 | 127 (7) |
O6i—O8—O5i | 65 (5) | O17ii—O23—O19ii | 55 (5) |
O6i—O8—O2ix | 136 (6) | O17ii—O23—O4vii | 109 (7) |
O6i—O8—O11 | 106 (6) | O17ii—O23—O5 | 121 (6) |
O6i—O8—O18ii | 161 (6) | O17ii—O23—O3i | 91 (6) |
O6i—O8—O15 | 60 (6) | O17ii—O23—O1vii | 172 (6) |
O6i—O8—In3 | 142 (8) | O17ii—O23—W5 | 35 (4) |
O6i—O8—Al3 | 142 (8) | O17ii—O23—In2 | 133 (7) |
O6i—O8—W3 | 34 (4) | O17ii—O23—Al2 | 133 (7) |
Al4xiv—O9—In4xiv | 0.000 | O24—O23—O17ii | 57 (5) |
W1xii—O9—Al4xiv | 141 (5) | O24—O23—O19ii | 57 (4) |
W1xii—O9—In4xiv | 141 (5) | O24—O23—O4vii | 130 (6) |
O19ii—O9—W1xii | 127 (6) | O24—O23—O5 | 129 (5) |
O19ii—O9—Al4xiv | 57 (4) | O24—O23—O3i | 148 (9) |
O19ii—O9—In4xiv | 57 (4) | O24—O23—O1vii | 130 (6) |
O15xii—O9—O19ii | 74 (6) | O24—O23—W5 | 32 (3) |
O15xii—O9—W1xii | 154 (5) | O24—O23—In2 | 170 (9) |
O15xii—O9—Al4xiv | 60 (4) | O24—O23—Al2 | 170 (9) |
O15xii—O9—In4xiv | 60 (4) | In1—O24—W5 | 140 (5) |
O7—O9—O15xii | 130 (5) | Al1—O24—In1 | 0.000 |
O7—O9—O19ii | 118 (5) | Al1—O24—W5 | 140 (5) |
O7—O9—W1xii | 32 (3) | O6ii—O24—Al1 | 39 (4) |
O7—O9—Al4xiv | 168 (6) | O6ii—O24—In1 | 39 (4) |
O7—O9—In4xiv | 168 (6) | O6ii—O24—W5 | 142 (9) |
In2xx—O10—W6xix | 130 (4) | O20iii—O24—O6ii | 51 (4) |
Al2xx—O10—In2xx | 0.000 | O20iii—O24—Al1 | 36 (3) |
Al2xx—O10—W6xix | 130 (4) | O20iii—O24—In1 | 36 (3) |
O22xix—O10—Al2xx | 164 (6) | O20iii—O24—W5 | 108 (5) |
O22xix—O10—In2xx | 164 (6) | O16—O24—O20iii | 52 (5) |
O22xix—O10—W6xix | 42 (4) | O16—O24—O6ii | 85 (6) |
O1xi—O10—O22xix | 149 (8) | O16—O24—Al1 | 46 (4) |
O1xi—O10—Al2xx | 40 (4) | O16—O24—In1 | 46 (4) |
O1xi—O10—In2xx | 40 (4) | O16—O24—W5 | 106 (5) |
O1xi—O10—W6xix | 114 (5) | O19ii—O24—O16 | 77 (4) |
O3xxi—O10—O1xi | 80 (5) | O19ii—O24—O20iii | 80 (5) |
O3xxi—O10—O22xix | 127 (6) | O19ii—O24—O6ii | 127 (7) |
O3xxi—O10—Al2xx | 41 (3) | O19ii—O24—Al1 | 109 (4) |
O3xxi—O10—In2xx | 41 (3) | O19ii—O24—In1 | 109 (4) |
O3xxi—O10—W6xix | 126 (5) | O19ii—O24—W5 | 32 (3) |
O1xx—O10—O3xxi | 145 (4) | O17ii—O24—O19ii | 55 (4) |
O1xx—O10—O1xi | 80 (5) | O17ii—O24—O16 | 129 (5) |
O1xx—O10—O22xix | 70 (5) | O17ii—O24—O20iii | 101 (6) |
O1xx—O10—Al2xx | 114 (4) | O17ii—O24—O6ii | 111 (8) |
O1xx—O10—In2xx | 114 (4) | O17ii—O24—Al1 | 135 (8) |
O1xx—O10—W6xix | 43 (3) | O17ii—O24—In1 | 135 (8) |
O4xi—O10—O1xx | 134 (5) | O17ii—O24—W5 | 35 (5) |
O4xi—O10—O3xxi | 54 (4) | O13ii—O24—O17ii | 171 (6) |
O4xi—O10—O1xi | 61 (4) | O13ii—O24—O19ii | 133 (5) |
O4xi—O10—O22xix | 143 (5) | O13ii—O24—O16 | 59 (4) |
O4xi—O10—Al2xx | 46 (3) | O13ii—O24—O20iii | 83 (4) |
O4xi—O10—In2xx | 46 (3) | O13ii—O24—O6ii | 65 (5) |
O4xi—O10—W6xix | 176 (3) | O13ii—O24—Al1 | 48 (4) |
O11xxii—O10—O4xi | 147 (6) | O13ii—O24—In1 | 48 (4) |
O11xxii—O10—O1xx | 68 (4) | O13ii—O24—W5 | 151 (9) |
O11xxii—O10—O3xxi | 94 (5) | O23—O24—O13ii | 124 (7) |
O11xxii—O10—O1xi | 113 (4) | O23—O24—O17ii | 58 (6) |
O11xxii—O10—O22xix | 59 (4) | O23—O24—O19ii | 57 (5) |
O11xxii—O10—Al2xx | 107 (4) | O23—O24—O16 | 110 (7) |
O11xxii—O10—In2xx | 107 (4) | O23—O24—O20iii | 137 (5) |
O11xxii—O10—W6xix | 32 (4) | O23—O24—O6ii | 165 (7) |
O5xx—O10—O11xxii | 68 (4) | O23—O24—Al1 | 156 (7) |
O5xx—O10—O4xi | 87 (5) | O23—O24—In1 | 156 (7) |
O5xx—O10—O1xx | 87 (5) | O23—O24—W5 | 33 (4) |
Symmetry codes: (i) x−1/2, −y+1/2, z; (ii) x−1/2, −y+3/2, z; (iii) −x+1/2, y+1/2, −z+1; (iv) −x, −y+1, −z; (v) −x+1/2, y+1/2, −z; (vi) x, y+1, z; (vii) −x+1, −y+1, −z; (viii) x, y, z−1; (ix) x−1, y, z; (x) −x+1/2, y−1/2, −z; (xi) −x+1, −y+1, −z+1; (xii) x+1/2, −y+1/2, z; (xiii) x+1, y, z; (xiv) x+1/2, −y+3/2, z; (xv) −x+3/2, y−1/2, −z; (xvi) x+1/2, −y+1/2, z−1; (xvii) −x+3/2, y+1/2, −z; (xviii) x, y−1, z; (xix) −x+1/2, y−1/2, −z+1; (xx) x, y, z+1; (xxi) x−1/2, −y+1/2, z+1; (xxii) x+1/2, −y+1/2, z+1; (xxiii) x−1/2, −y+1/2, z−1; (xxiv) −x+3/2, y−1/2, −z+1; (xxv) x−1, y−1, z; (xxvi) x+1, y+1, z; (xxvii) −x+3/2, y+1/2, −z+1. |
(DD8T910_AlInW3O12_warmup-00000.xye_1) top
(AlInW3O12_ortho_1) top
Crystal data top
Mr = 885.31 | V = 1134.65 (6) Å3 |
Orthorhombic, Pbcn | Z = 4 |
a = 12.9767 (4) Å | Dx = 5.183 (1) Mg m−3 |
b = 9.2983 (3) Å | T = 500 K |
c = 9.4035 (3) Å |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
x | y | z | Biso*/Beq | Occ. (<1) | |
Al1 | 0.3787 (2) | 0.2485 (5) | 0.4696 (3) | 1.99 (4) | 0.5 |
In1 | 0.3787 (2) | 0.2485 (5) | 0.4696 (3) | 1.99 (4) | 0.5 |
W1 | 0 | 0.47162 (18) | 0.25 | 1.99 (4) | |
W2 | 0.35636 (11) | 0.39364 (16) | 0.11711 (14) | 1.99 (4) | |
O1 | 0.1451 (12) | 0.0815 (17) | 0.0886 (14) | 1.99 (4) | |
O2 | 0.0664 (9) | 0.3513 (17) | 0.1108 (17) | 1.99 (4) | |
O3 | 0.2788 (12) | 0.3110 (15) | −0.0090 (13) | 1.99 (4) | |
O4 | 0.4030 (9) | 0.0706 (14) | 0.3431 (14) | 1.99 (4) | |
O5 | 0.4736 (12) | 0.3147 (15) | 0.0691 (13) | 1.99 (4) | |
O6 | 0.3328 (10) | 0.3680 (15) | 0.2981 (16) | 1.99 (4) |
Geometric parameters (Å, º) top
Al1—In1 | 0.00000 | O2—O2v | 3.13 (3) |
Al1—O2i | 1.770 (16) | O3—W2 | 1.735 (13) |
Al1—O1i | 1.962 (15) | O3—In1vii | 2.126 (15) |
Al1—O5ii | 2.046 (15) | O3—Al1vii | 2.126 (15) |
Al1—O6 | 2.047 (15) | O3—O5 | 2.63 (2) |
Al1—O4 | 2.061 (13) | O3—O1iv | 2.85 (2) |
Al1—O3i | 2.126 (15) | O3—O6vii | 2.86 (2) |
In1—Al1 | 0.00000 | O3—O1 | 2.90 (2) |
In1—O2i | 1.770 (16) | O3—O4vii | 2.951 (19) |
In1—O1i | 1.962 (15) | O3—O2 | 3.000 (19) |
In1—O5ii | 2.046 (15) | O3—O6 | 3.018 (19) |
In1—O6 | 2.047 (15) | O4—W1vi | 1.788 (13) |
In1—O4 | 2.061 (13) | O4—In1 | 2.061 (13) |
In1—O3i | 2.126 (15) | O4—Al1 | 2.061 (13) |
W1—O4iii | 1.788 (13) | O4—O2i | 2.65 (2) |
W1—O4iv | 1.788 (13) | O4—O5ii | 2.898 (19) |
W1—O2v | 1.926 (15) | O4—O6 | 2.941 (19) |
W1—O2 | 1.926 (15) | O4—O3i | 2.951 (19) |
W2—O3 | 1.735 (13) | O4—O2ix | 2.974 (19) |
W2—O6 | 1.745 (15) | O4—O2vi | 3.02 (2) |
W2—O5 | 1.749 (15) | O4—O4ii | 3.07 (2) |
W2—O1iv | 1.767 (16) | O5—W2 | 1.749 (15) |
O1—W2vi | 1.767 (16) | O5—Al1ii | 2.046 (15) |
O1—In1vii | 1.962 (15) | O5—In1ii | 2.046 (15) |
O1—Al1vii | 1.962 (15) | O5—O2x | 2.59 (2) |
O1—O2 | 2.72 (2) | O5—O3 | 2.63 (2) |
O1—O6vii | 2.79 (2) | O5—O1x | 2.84 (2) |
O1—O6vi | 2.81 (2) | O5—O6ii | 2.85 (2) |
O1—O5viii | 2.84 (2) | O5—O6 | 2.87 (2) |
O1—O3vi | 2.85 (2) | O5—O4ii | 2.898 (19) |
O1—O3 | 2.90 (2) | O5—O1iv | 2.93 (2) |
O1—O5vi | 2.93 (2) | O6—W2 | 1.745 (15) |
O2—Al1vii | 1.770 (16) | O6—Al1 | 2.047 (15) |
O2—In1vii | 1.770 (16) | O6—In1 | 2.047 (15) |
O2—W1 | 1.926 (15) | O6—O1i | 2.79 (2) |
O2—O5viii | 2.59 (2) | O6—O1iv | 2.81 (2) |
O2—O4vii | 2.65 (2) | O6—O5ii | 2.85 (2) |
O2—O1 | 2.72 (2) | O6—O3i | 2.86 (2) |
O2—O4iii | 2.974 (19) | O6—O5 | 2.87 (2) |
O2—O3 | 3.000 (19) | O6—O4 | 2.941 (19) |
O2—O4iv | 3.02 (2) | O6—O3 | 3.018 (19) |
O1i—Al1—O2i | 93.3 (7) | O4vii—O3—O5 | 153.4 (7) |
O5ii—Al1—O1i | 90.4 (6) | O4vii—O3—Al1vii | 44.3 (4) |
O5ii—Al1—O2i | 85.1 (6) | O4vii—O3—In1vii | 44.3 (4) |
O6—Al1—O5ii | 88.2 (5) | O4vii—O3—W2 | 128.4 (7) |
O6—Al1—O1i | 88.1 (6) | O2—O3—O4vii | 52.9 (5) |
O6—Al1—O2i | 173.1 (6) | O2—O3—O1 | 54.8 (5) |
O4—Al1—O6 | 91.5 (6) | O2—O3—O6vii | 81.1 (6) |
O4—Al1—O5ii | 89.7 (5) | O2—O3—O1iv | 95.0 (6) |
O4—Al1—O1i | 179.5 (6) | O2—O3—O5 | 140.9 (6) |
O4—Al1—O2i | 87.2 (6) | O2—O3—Al1vii | 35.5 (4) |
O3i—Al1—O4 | 89.6 (5) | O2—O3—In1vii | 35.5 (4) |
O3i—Al1—O6 | 86.4 (5) | O2—O3—W2 | 102.8 (6) |
O3i—Al1—O5ii | 174.5 (5) | O6—O3—O2 | 80.4 (5) |
O3i—Al1—O1i | 90.3 (6) | O6—O3—O4vii | 124.9 (6) |
O3i—Al1—O2i | 100.3 (6) | O6—O3—O1 | 88.0 (5) |
O1i—In1—O2i | 93.3 (7) | O6—O3—O6vii | 145.9 (6) |
O5ii—In1—O1i | 90.4 (6) | O6—O3—O1iv | 57.1 (5) |
O5ii—In1—O2i | 85.1 (6) | O6—O3—O5 | 60.5 (5) |
O6—In1—O5ii | 88.2 (5) | O6—O3—Al1vii | 111.1 (6) |
O6—In1—O1i | 88.1 (6) | O6—O3—In1vii | 111.1 (6) |
O6—In1—O2i | 173.1 (6) | O6—O3—W2 | 30.0 (4) |
O4—In1—O6 | 91.5 (6) | In1—O4—W1vi | 143.4 (7) |
O4—In1—O5ii | 89.7 (5) | Al1—O4—W1vi | 143.4 (7) |
O4—In1—O1i | 179.5 (6) | O2i—O4—Al1 | 41.8 (4) |
O4—In1—O2i | 87.2 (6) | O2i—O4—In1 | 41.8 (4) |
O3i—In1—O4 | 89.6 (5) | O2i—O4—W1vi | 120.0 (6) |
O3i—In1—O6 | 86.4 (5) | O5ii—O4—O2i | 55.4 (5) |
O3i—In1—O5ii | 174.5 (5) | O5ii—O4—Al1 | 44.9 (4) |
O3i—In1—O1i | 90.3 (6) | O5ii—O4—In1 | 44.9 (4) |
O3i—In1—O2i | 100.3 (6) | O5ii—O4—W1vi | 98.9 (6) |
O4iv—W1—O4iii | 118.0 (8) | O6—O4—O5ii | 58.4 (5) |
O2v—W1—O4iv | 106.3 (6) | O6—O4—O2i | 85.7 (6) |
O2v—W1—O4iii | 108.5 (6) | O6—O4—Al1 | 44.1 (4) |
O2—W1—O2v | 108.9 (10) | O6—O4—In1 | 44.1 (4) |
O2—W1—O4iv | 108.5 (6) | O6—O4—W1vi | 129.1 (7) |
O2—W1—O4iii | 106.3 (6) | O3i—O4—O6 | 58.0 (5) |
O6—W2—O3 | 120.3 (6) | O3i—O4—O5ii | 90.9 (5) |
O5—W2—O6 | 110.3 (6) | O3i—O4—O2i | 64.5 (5) |
O5—W2—O3 | 98.2 (7) | O3i—O4—Al1 | 46.1 (4) |
O1iv—W2—O5 | 112.6 (7) | O3i—O4—In1 | 46.1 (4) |
O1iv—W2—O6 | 106.3 (6) | O3i—O4—W1vi | 170.1 (7) |
O1iv—W2—O3 | 109.1 (7) | O2ix—O4—O3i | 139.2 (6) |
In1vii—O1—W2vi | 151.8 (9) | O2ix—O4—O6 | 152.4 (6) |
Al1vii—O1—W2vi | 151.8 (9) | O2ix—O4—O5ii | 95.8 (5) |
O2—O1—Al1vii | 40.6 (5) | O2ix—O4—O2i | 86.7 (6) |
O2—O1—In1vii | 40.6 (5) | O2ix—O4—Al1 | 125.1 (6) |
O2—O1—W2vi | 153.8 (8) | O2ix—O4—In1 | 125.1 (6) |
O6vii—O1—O2 | 87.6 (6) | O2ix—O4—W1vi | 38.4 (4) |
O6vii—O1—Al1vii | 47.2 (4) | O2vi—O4—O2ix | 63.1 (6) |
O6vii—O1—In1vii | 47.2 (4) | O2vi—O4—O3i | 134.3 (6) |
O6vii—O1—W2vi | 108.5 (7) | O2vi—O4—O6 | 124.9 (6) |
O6vi—O1—O6vii | 142.7 (7) | O2vi—O4—O5ii | 131.6 (6) |
O6vi—O1—O2 | 129.5 (7) | O2vi—O4—O2i | 148.6 (6) |
O6vi—O1—Al1vii | 170.1 (8) | O2vi—O4—Al1 | 168.8 (7) |
O6vi—O1—In1vii | 170.1 (8) | O2vi—O4—In1 | 168.8 (7) |
O6vi—O1—W2vi | 36.6 (4) | O2vi—O4—W1vi | 37.3 (3) |
O5viii—O1—O6vi | 133.2 (7) | O4ii—O4—O2vi | 58.5 (4) |
O5viii—O1—O6vii | 60.8 (5) | O4ii—O4—O2ix | 59.9 (4) |
O5viii—O1—O2 | 55.4 (5) | O4ii—O4—O3i | 157.7 (4) |
O5viii—O1—Al1vii | 46.0 (4) | O4ii—O4—O6 | 99.9 (4) |
O5viii—O1—In1vii | 46.0 (4) | O4ii—O4—O5ii | 73.1 (4) |
O5viii—O1—W2vi | 114.0 (7) | O4ii—O4—O2i | 114.8 (7) |
O3vi—O1—O5viii | 113.7 (6) | O4ii—O4—Al1 | 117.1 (4) |
O3vi—O1—O6vi | 64.4 (5) | O4ii—O4—In1 | 117.1 (4) |
O3vi—O1—O6vii | 78.3 (5) | O4ii—O4—W1vi | 31.0 (4) |
O3vi—O1—O2 | 165.6 (7) | Al1ii—O5—W2 | 170.9 (7) |
O3vi—O1—Al1vii | 125.5 (6) | In1ii—O5—W2 | 170.9 (7) |
O3vi—O1—In1vii | 125.5 (6) | O2x—O5—In1ii | 43.0 (4) |
O3vi—O1—W2vi | 35.1 (4) | O2x—O5—Al1ii | 43.0 (4) |
O3—O1—O3vi | 109.9 (5) | O2x—O5—W2 | 145.5 (8) |
O3—O1—O5viii | 93.0 (6) | O3—O5—O2x | 104.9 (6) |
O3—O1—O6vi | 132.9 (7) | O3—O5—In1ii | 147.8 (7) |
O3—O1—O6vii | 60.3 (5) | O3—O5—Al1ii | 147.8 (7) |
O3—O1—O2 | 64.5 (5) | O3—O5—W2 | 40.7 (4) |
O3—O1—Al1vii | 47.2 (4) | O1x—O5—O3 | 127.6 (6) |
O3—O1—In1vii | 47.2 (4) | O1x—O5—O2x | 59.8 (5) |
O3—O1—W2vi | 141.5 (8) | O1x—O5—In1ii | 43.6 (4) |
O5vi—O1—O3 | 156.8 (6) | O1x—O5—Al1ii | 43.6 (4) |
O5vi—O1—O3vi | 54.2 (5) | O1x—O5—W2 | 132.3 (8) |
O5vi—O1—O5viii | 81.0 (6) | O6ii—O5—O1x | 58.6 (5) |
O5vi—O1—O6vi | 59.9 (5) | O6ii—O5—O3 | 166.2 (6) |
O5vi—O1—O6vii | 97.8 (6) | O6ii—O5—O2x | 88.9 (6) |
O5vi—O1—O2 | 126.1 (7) | O6ii—O5—In1ii | 45.9 (4) |
O5vi—O1—Al1vii | 124.4 (7) | O6ii—O5—Al1ii | 45.9 (4) |
O5vi—O1—In1vii | 124.4 (7) | O6ii—O5—W2 | 125.5 (7) |
O5vi—O1—W2vi | 33.5 (4) | O6—O5—O6ii | 101.7 (5) |
In1vii—O2—Al1vii | 0.000 | O6—O5—O1x | 146.3 (7) |
W1—O2—In1vii | 174.2 (9) | O6—O5—O3 | 66.4 (5) |
W1—O2—Al1vii | 174.2 (9) | O6—O5—O2x | 153.0 (7) |
O5viii—O2—W1 | 125.7 (6) | O6—O5—In1ii | 141.5 (7) |
O5viii—O2—In1vii | 52.0 (5) | O6—O5—Al1ii | 141.5 (7) |
O5viii—O2—Al1vii | 52.0 (5) | O6—O5—W2 | 34.8 (4) |
O4vii—O2—O5viii | 67.2 (5) | O4ii—O5—O6 | 105.9 (6) |
O4vii—O2—W1 | 123.6 (8) | O4ii—O5—O6ii | 61.6 (5) |
O4vii—O2—In1vii | 51.0 (5) | O4ii—O5—O1x | 89.0 (6) |
O4vii—O2—Al1vii | 51.0 (5) | O4ii—O5—O3 | 126.9 (7) |
O1—O2—O4vii | 97.1 (6) | O4ii—O5—O2x | 57.4 (5) |
O1—O2—O5viii | 64.8 (6) | O4ii—O5—In1ii | 45.3 (4) |
O1—O2—W1 | 139.2 (8) | O4ii—O5—Al1ii | 45.3 (4) |
O1—O2—In1vii | 46.1 (5) | O4ii—O5—W2 | 137.4 (7) |
O1—O2—Al1vii | 46.1 (5) | O1iv—O5—O4ii | 159.6 (6) |
O4iii—O2—O1 | 155.9 (7) | O1iv—O5—O6 | 58.1 (5) |
O4iii—O2—O4vii | 93.3 (6) | O1iv—O5—O6ii | 106.8 (6) |
O4iii—O2—O5viii | 99.9 (6) | O1iv—O5—O1x | 99.0 (6) |
O4iii—O2—W1 | 35.2 (4) | O1iv—O5—O3 | 61.5 (5) |
O4iii—O2—In1vii | 139.1 (8) | O1iv—O5—O2x | 142.4 (6) |
O4iii—O2—Al1vii | 139.1 (8) | O1iv—O5—In1ii | 139.4 (7) |
O3—O2—O4iii | 142.7 (7) | O1iv—O5—Al1ii | 139.4 (7) |
O3—O2—O1 | 60.7 (5) | O1iv—O5—W2 | 33.9 (4) |
O3—O2—O4vii | 62.6 (5) | Al1—O6—W2 | 142.4 (8) |
O3—O2—O5viii | 96.2 (6) | In1—O6—W2 | 142.4 (8) |
O3—O2—W1 | 137.6 (7) | O1i—O6—In1 | 44.7 (5) |
O3—O2—In1vii | 44.2 (4) | O1i—O6—Al1 | 44.7 (5) |
O3—O2—Al1vii | 44.2 (4) | O1i—O6—W2 | 156.2 (7) |
O4iv—O2—O3 | 103.6 (5) | O1iv—O6—O1i | 123.9 (6) |
O4iv—O2—O4iii | 61.6 (5) | O1iv—O6—In1 | 154.9 (7) |
O4iv—O2—O1 | 129.1 (6) | O1iv—O6—Al1 | 154.9 (7) |
O4iv—O2—O4vii | 118.9 (6) | O1iv—O6—W2 | 37.1 (4) |
O4iv—O2—O5viii | 159.8 (6) | O5ii—O6—O1iv | 109.9 (6) |
O4iv—O2—W1 | 34.2 (4) | O5ii—O6—O1i | 60.6 (5) |
O4iv—O2—In1vii | 147.7 (7) | O5ii—O6—In1 | 45.9 (4) |
O4iv—O2—Al1vii | 147.7 (7) | O5ii—O6—Al1 | 45.9 (4) |
O2v—O2—O4iv | 57.8 (4) | O5ii—O6—W2 | 107.3 (7) |
O2v—O2—O3 | 144.9 (8) | O3i—O6—O5ii | 93.8 (6) |
O2v—O2—O4iii | 59.1 (4) | O3i—O6—O1iv | 155.3 (7) |
O2v—O2—O1 | 105.7 (5) | O3i—O6—O1i | 61.8 (5) |
O2v—O2—O4vii | 151.1 (7) | O3i—O6—In1 | 48.0 (4) |
O2v—O2—O5viii | 106.9 (6) | O3i—O6—Al1 | 48.0 (4) |
O2v—O2—W1 | 35.5 (5) | O3i—O6—W2 | 142.0 (8) |
O2v—O2—In1vii | 148.0 (5) | O5—O6—O3i | 134.4 (6) |
O2v—O2—Al1vii | 148.0 (5) | O5—O6—O5ii | 74.8 (5) |
In1vii—O3—W2 | 137.6 (7) | O5—O6—O1iv | 62.0 (5) |
Al1vii—O3—W2 | 137.6 (7) | O5—O6—O1i | 134.4 (7) |
O5—O3—Al1vii | 162.3 (7) | O5—O6—In1 | 108.2 (6) |
O5—O3—In1vii | 162.3 (7) | O5—O6—Al1 | 108.2 (6) |
O5—O3—W2 | 41.1 (4) | O5—O6—W2 | 34.9 (4) |
O1iv—O3—O5 | 64.3 (5) | O4—O6—O5 | 75.4 (5) |
O1iv—O3—Al1vii | 126.4 (7) | O4—O6—O3i | 61.2 (5) |
O1iv—O3—In1vii | 126.4 (7) | O4—O6—O5ii | 60.0 (5) |
O1iv—O3—W2 | 35.8 (4) | O4—O6—O1iv | 137.2 (7) |
O6vii—O3—O1iv | 153.3 (7) | O4—O6—O1i | 89.2 (6) |
O6vii—O3—O5 | 132.2 (7) | O4—O6—In1 | 44.5 (4) |
O6vii—O3—Al1vii | 45.6 (4) | O4—O6—Al1 | 44.5 (4) |
O6vii—O3—In1vii | 45.6 (4) | O4—O6—W2 | 102.4 (6) |
O6vii—O3—W2 | 170.5 (7) | O3—O6—O4 | 92.6 (5) |
O1—O3—O6vii | 57.9 (5) | O3—O6—O5 | 53.1 (5) |
O1—O3—O1iv | 139.0 (7) | O3—O6—O3i | 112.8 (5) |
O1—O3—O5 | 119.7 (6) | O3—O6—O5ii | 126.5 (6) |
O1—O3—Al1vii | 42.6 (4) | O3—O6—O1iv | 58.5 (5) |
O1—O3—In1vii | 42.6 (4) | O3—O6—O1i | 172.4 (7) |
O1—O3—W2 | 117.2 (7) | O3—O6—In1 | 136.6 (7) |
O4vii—O3—O1 | 86.9 (6) | O3—O6—Al1 | 136.6 (7) |
O4vii—O3—O6vii | 60.8 (5) | O3—O6—W2 | 29.8 (4) |
O4vii—O3—O1iv | 95.7 (6) |
Symmetry codes: (i) −x+1/2, −y+1/2, z+1/2; (ii) −x+1, y, −z+1/2; (iii) x−1/2, y+1/2, −z+1/2; (iv) −x+1/2, y+1/2, z; (v) −x, y, −z+1/2; (vi) −x+1/2, y−1/2, z; (vii) −x+1/2, −y+1/2, z−1/2; (viii) x−1/2, −y+1/2, −z; (ix) x+1/2, y−1/2, −z+1/2; (x) x+1/2, −y+1/2, −z. |
(DD8T910_AlInW3O12_warmup-00284.xye_1) top
(Al0.84In1.16Mo3O12_mono_1) top
Crystal data top
Mr = 1260.4 (13) | β = 125.762 (5)° |
Monoclinic, P121/a1 | V = 2249.2 (2) Å3 |
a = 15.9606 (11) Å | Z = 4 |
b = 9.3804 (3) Å | Dx = 3.722 (4) Mg m−3 |
c = 18.5138 (7) Å | T = 298 K |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
x | y | z | Biso*/Beq | Occ. (<1) | |
Mo1 | −0.0007 (8) | 0.2397 (10) | 0.4897 (6) | 0.79 (4) | |
Mo2 | 0.3612 (7) | 0.1205 (11) | 0.1308 (6) | 0.79 (4) | |
Mo3 | 0.1447 (8) | 0.1149 (9) | 0.2568 (5) | 0.79 (4) | |
Mo4 | 0.1517 (8) | 0.6092 (10) | 0.3789 (7) | 0.79 (4) | |
Mo5 | 0.3557 (7) | 0.6358 (9) | 0.2171 (5) | 0.79 (4) | |
Mo6 | −0.0132 (6) | 0.7432 (10) | 0.0136 (5) | 0.79 (4) | |
In1 | 0.3852 (10) | 0.9639 (14) | 0.3218 (9) | 0.79 (4) | 0.549 (4) |
In2 | 0.3727 (8) | 0.4538 (12) | 0.0513 (7) | 0.79 (4) | 0.549 (4) |
In3 | 0.1236 (10) | 0.4841 (11) | 0.1896 (8) | 0.79 (4) | 0.549 (4) |
In4 | 0.1168 (9) | 0.9742 (15) | 0.4282 (8) | 0.79 (4) | 0.549 (4) |
Al1 | 0.3852 (10) | 0.9639 (14) | 0.3218 (9) | 0.79 (4) | 0.451 (4) |
Al2 | 0.3727 (8) | 0.4538 (12) | 0.0513 (7) | 0.79 (4) | 0.451 (4) |
Al3 | 0.1236 (10) | 0.4841 (11) | 0.1896 (8) | 0.79 (4) | 0.451 (4) |
Al4 | 0.1168 (9) | 0.9742 (15) | 0.4282 (8) | 0.79 (4) | 0.451 (4) |
O1 | 0.565 (4) | 0.358 (5) | −0.044 (3) | 0.79 (4) | |
O2 | 0.970 (6) | 0.421 (8) | 0.142 (5) | 0.79 (4) | |
O3 | 0.807 (3) | 0.217 (6) | 0.062 (3) | 0.79 (4) | |
O4 | 0.794 (4) | 0.544 (5) | 0.049 (3) | 0.79 (4) | |
O5 | 0.515 (3) | 0.435 (6) | 0.149 (3) | 0.79 (4) | |
O6 | 0.773 (4) | 0.517 (6) | 0.283 (3) | 0.79 (4) | |
O7 | 0.445 (4) | 0.125 (5) | 0.419 (3) | 0.79 (4) | |
O8 | 0.184 (4) | 0.302 (6) | 0.264 (3) | 0.79 (4) | |
O9 | 0.542 (4) | 0.378 (5) | 0.416 (3) | 0.79 (4) | |
O10 | 0.425 (4) | 0.342 (5) | 0.990 (4) | 0.79 (4) | |
O11 | 0.090 (4) | 0.303 (4) | 0.112 (3) | 0.79 (4) | |
O12 | 0.402 (4) | 0.360 (6) | 0.488 (4) | 0.79 (4) | |
O13 | 0.864 (4) | 0.383 (7) | 0.222 (3) | 0.79 (4) | |
O14 | 0.249 (4) | 0.054 (4) | 0.526 (4) | 0.79 (4) | |
O15 | 0.113 (4) | 0.120 (7) | 0.344 (3) | 0.79 (4) | |
O16 | 0.543 (5) | 0.961 (5) | 0.375 (4) | 0.79 (4) | |
O17 | 0.771 (5) | 0.997 (6) | 0.235 (3) | 0.79 (4) | |
O18 | 0.686 (3) | 0.900 (5) | 0.303 (3) | 0.79 (4) | |
O19 | 0.969 (4) | 0.911 (5) | 0.310 (3) | 0.79 (4) | |
O20 | 0.087 (4) | 0.384 (5) | 0.582 (3) | 0.79 (4) | |
O21 | 0.167 (4) | 0.804 (7) | 0.406 (4) | 0.79 (4) | |
O22 | 0.114 (3) | 0.628 (5) | 0.097 (3) | 0.79 (4) | |
O23 | 0.370 (4) | 0.545 (5) | 0.132 (3) | 0.79 (4) | |
O24 | 0.346 (4) | 0.859 (5) | 0.221 (3) | 0.79 (4) |
Geometric parameters (Å, º) top
Mo1—O7i | 1.66 (4) | O8—O17iv | 2.58 (10) |
Mo1—O12i | 1.80 (8) | O8—O18iv | 2.89 (8) |
Mo1—O20 | 1.98 (5) | O8—O15 | 2.90 (10) |
Mo1—O9i | 2.14 (6) | O8—O2x | 3.00 (8) |
Mo2—O13i | 1.66 (7) | O8—O5i | 3.17 (7) |
Mo2—O2i | 1.67 (10) | O9—In4xviii | 1.76 (5) |
Mo2—O3i | 1.85 (5) | O9—Al4xviii | 1.76 (5) |
Mo2—O4i | 1.98 (4) | O9—Mo1xiii | 2.14 (6) |
Mo2—O24ii | 3.05 (6) | O9—O15xiii | 2.20 (10) |
Mo3—O8 | 1.84 (6) | O9—O19iv | 2.55 (6) |
Mo3—O5i | 1.91 (4) | O9—O14xiii | 2.76 (7) |
Mo3—O15 | 1.96 (7) | O9—O7 | 2.84 (7) |
Mo3—O6i | 2.19 (6) | O9—O12xii | 2.85 (7) |
Mo3—O11 | 2.88 (5) | O10—Mo6xix | 1.71 (7) |
Mo4—O14iii | 1.62 (4) | O10—In2xx | 2.06 (8) |
Mo4—O18iv | 1.79 (7) | O10—Al2xx | 2.06 (8) |
Mo4—O16iv | 1.81 (8) | O10—O22xix | 2.41 (7) |
Mo4—O21 | 1.87 (6) | O10—O5xx | 2.57 (8) |
Mo5—O19iv | 1.67 (4) | O10—O11xxi | 2.63 (6) |
Mo5—O23 | 1.91 (7) | O10—O1xx | 2.64 (11) |
Mo5—O17iv | 1.99 (8) | O10—O3xxii | 2.93 (11) |
Mo5—O24 | 2.10 (5) | O10—O1xii | 2.96 (7) |
Mo5—O22 | 3.13 (3) | O11—Mo6vi | 1.94 (5) |
Mo6—O1v | 1.64 (7) | O11—Al3 | 2.08 (5) |
Mo6—O10iii | 1.71 (7) | O11—In3 | 2.08 (5) |
Mo6—O11vi | 1.94 (5) | O11—O8 | 2.28 (7) |
Mo6—O22 | 2.00 (4) | O11—O2x | 2.54 (12) |
In1—Al1 | 0.00000 | O11—O10xxiii | 2.63 (6) |
In1—O6iv | 1.50 (6) | O11—O5i | 2.80 (8) |
In1—O20iii | 1.73 (7) | O11—Mo3 | 2.88 (5) |
In1—O24 | 1.87 (6) | O11—O17iv | 3.06 (7) |
In1—O7vii | 2.11 (5) | O11—O1i | 3.07 (9) |
In1—O16 | 2.11 (7) | O11—O22 | 3.11 (6) |
In1—O13iv | 2.21 (7) | O12—Mo1xiii | 1.80 (8) |
In2—Al2 | 0.00000 | O12—Al4xix | 2.04 (8) |
In2—O23 | 1.75 (7) | O12—In4xix | 2.04 (8) |
In2—O5 | 1.91 (4) | O12—O21xix | 2.80 (12) |
In2—O3i | 1.98 (6) | O12—O7 | 2.83 (9) |
In2—O10viii | 2.06 (8) | O12—O9xii | 2.85 (7) |
In2—O1ix | 2.07 (6) | O12—O14iii | 2.90 (10) |
In2—O4ix | 2.17 (5) | O12—O19xxiv | 3.07 (8) |
In3—Al3 | 0.00000 | O13—Mo2xiii | 1.66 (7) |
In3—O17iv | 2.00 (7) | O13—Al1xviii | 2.21 (7) |
In3—O18iv | 2.04 (5) | O13—In1xviii | 2.21 (7) |
In3—O8 | 2.05 (6) | O13—O24xviii | 2.43 (8) |
In3—O11 | 2.08 (5) | O13—O6 | 2.63 (10) |
In3—O22 | 2.12 (5) | O13—O2 | 2.83 (13) |
In3—O2x | 2.15 (9) | O13—O16xviii | 2.98 (7) |
In4—Al4 | 0.00000 | O13—O3 | 2.98 (9) |
In4—O9iv | 1.76 (5) | O13—O7xiii | 3.09 (8) |
In4—O21 | 1.94 (7) | O13—O4 | 3.09 (8) |
In4—O14vii | 1.96 (5) | O14—Mo4xix | 1.62 (4) |
In4—O12iii | 2.04 (8) | O14—Al4ii | 1.96 (5) |
In4—O15vii | 2.04 (7) | O14—In4ii | 1.96 (5) |
In4—O19x | 2.16 (4) | O14—O21xix | 2.63 (7) |
Al1—In1 | 0.00000 | O14—O16xii | 2.70 (8) |
Al1—O6iv | 1.50 (6) | O14—O18xii | 2.73 (9) |
Al1—O20iii | 1.73 (7) | O14—O9i | 2.76 (7) |
Al1—O24 | 1.87 (6) | O14—O15 | 2.81 (7) |
Al1—O7vii | 2.11 (5) | O14—O12xix | 2.90 (10) |
Al1—O16 | 2.11 (7) | O14—O21ii | 2.96 (7) |
Al1—O13iv | 2.21 (7) | O15—Mo3 | 1.96 (7) |
Al2—In2 | 0.00000 | O15—Al4ii | 2.04 (7) |
Al2—O23 | 1.75 (7) | O15—In4ii | 2.04 (7) |
Al2—O5 | 1.91 (4) | O15—O9i | 2.20 (10) |
Al2—O3i | 1.98 (6) | O15—O19xxv | 2.79 (8) |
Al2—O10viii | 2.06 (8) | O15—O14 | 2.81 (7) |
Al2—O1ix | 2.07 (6) | O15—O8 | 2.90 (10) |
Al2—O4ix | 2.17 (5) | O15—O5i | 3.02 (7) |
Al3—In3 | 0.00000 | O15—O21ii | 3.11 (9) |
Al3—O17iv | 2.00 (7) | O16—Mo4xviii | 1.81 (8) |
Al3—O18iv | 2.04 (5) | O16—Al1 | 2.11 (7) |
Al3—O8 | 2.05 (6) | O16—In1 | 2.11 (7) |
Al3—O11 | 2.08 (5) | O16—O7vii | 2.65 (10) |
Al3—O22 | 2.12 (5) | O16—O14xii | 2.70 (8) |
Al3—O2x | 2.15 (9) | O16—O20iii | 2.72 (12) |
Al4—In4 | 0.00000 | O16—O24 | 2.91 (6) |
Al4—O9iv | 1.76 (5) | O16—O13iv | 2.98 (7) |
Al4—O21 | 1.94 (7) | O16—O21xviii | 3.02 (9) |
Al4—O14vii | 1.96 (5) | O17—Mo5xviii | 1.99 (8) |
Al4—O12iii | 2.04 (8) | O17—In3xviii | 2.00 (7) |
Al4—O15vii | 2.04 (7) | O17—Al3xviii | 2.00 (7) |
Al4—O19x | 2.16 (4) | O17—O18 | 2.51 (11) |
O1—Mo6xi | 1.64 (7) | O17—O8xviii | 2.58 (10) |
O1—Al2ix | 2.07 (6) | O17—O22xviii | 2.59 (6) |
O1—In2ix | 2.07 (6) | O17—O19 | 2.72 (8) |
O1—O5ix | 2.51 (7) | O17—O11xviii | 3.06 (7) |
O1—O23ix | 2.57 (11) | O17—O23xviii | 3.11 (12) |
O1—O10viii | 2.64 (11) | O18—Mo4xviii | 1.79 (7) |
O1—O10xii | 2.96 (7) | O18—Al3xviii | 2.04 (5) |
O1—O11xiii | 3.07 (9) | O18—In3xviii | 2.04 (5) |
O2—Mo2xiii | 1.67 (10) | O18—O17 | 2.51 (11) |
O2—Al3xiv | 2.15 (9) | O18—O14xii | 2.73 (9) |
O2—In3xiv | 2.15 (9) | O18—O21xviii | 2.84 (9) |
O2—O11xiv | 2.54 (12) | O18—O8xviii | 2.89 (8) |
O2—O4 | 2.56 (9) | O19—Mo5xviii | 1.67 (4) |
O2—O13 | 2.83 (13) | O19—In4xiv | 2.16 (4) |
O2—O3 | 2.85 (9) | O19—Al4xiv | 2.16 (4) |
O2—O8xiv | 3.00 (8) | O19—O9xviii | 2.55 (6) |
O3—Mo2xiii | 1.85 (5) | O19—O23xviii | 2.72 (7) |
O3—Al2xiii | 1.98 (6) | O19—O17 | 2.72 (8) |
O3—In2xiii | 1.98 (6) | O19—O21xiv | 2.75 (7) |
O3—O4xv | 2.35 (7) | O19—O15xxvi | 2.79 (8) |
O3—O23xiii | 2.68 (7) | O19—O24xviii | 3.04 (6) |
O3—O2 | 2.85 (9) | O19—O12xxvii | 3.07 (8) |
O3—O10xvi | 2.93 (11) | O20—In1xix | 1.73 (7) |
O3—O13 | 2.98 (9) | O20—Al1xix | 1.73 (7) |
O3—O5xiii | 3.05 (7) | O20—Mo1 | 1.98 (5) |
O3—O4 | 3.08 (7) | O20—O7iii | 2.31 (7) |
O4—Mo2xiii | 1.98 (4) | O20—O6xii | 2.36 (6) |
O4—In2ix | 2.17 (5) | O20—O7i | 2.50 (6) |
O4—Al2ix | 2.17 (5) | O20—O16xix | 2.72 (12) |
O4—O3xvii | 2.35 (7) | O20—O24xix | 3.16 (9) |
O4—O2 | 2.56 (9) | O21—Mo4 | 1.87 (6) |
O4—O24xviii | 2.92 (8) | O21—In4 | 1.94 (7) |
O4—O23ix | 2.92 (6) | O21—Al4 | 1.94 (7) |
O4—O3 | 3.08 (7) | O21—O14iii | 2.63 (7) |
O4—O13 | 3.09 (8) | O21—O19x | 2.75 (7) |
O5—Al2 | 1.91 (4) | O21—O12iii | 2.80 (12) |
O5—In2 | 1.91 (4) | O21—O18iv | 2.84 (9) |
O5—Mo3xiii | 1.91 (4) | O21—O14vii | 2.96 (7) |
O5—O23 | 2.38 (9) | O21—O16iv | 3.02 (9) |
O5—O1ix | 2.51 (7) | O21—O15vii | 3.11 (9) |
O5—O10viii | 2.57 (8) | O22—Mo6 | 2.00 (4) |
O5—O11xiii | 2.80 (8) | O22—In3 | 2.12 (5) |
O5—O15xiii | 3.02 (7) | O22—Al3 | 2.12 (5) |
O5—O3i | 3.05 (7) | O22—O10iii | 2.41 (7) |
O5—O8xiii | 3.17 (7) | O22—O17iv | 2.59 (6) |
O6—In1xviii | 1.50 (6) | O22—O11 | 3.11 (6) |
O6—Al1xviii | 1.50 (6) | O22—Mo5 | 3.13 (3) |
O6—Mo3xiii | 2.19 (6) | O23—Al2 | 1.75 (7) |
O6—O20xii | 2.36 (6) | O23—In2 | 1.75 (7) |
O6—O24xviii | 2.37 (10) | O23—Mo5 | 1.91 (7) |
O6—O13 | 2.63 (10) | O23—O5 | 2.38 (9) |
O6—O7xiii | 2.75 (6) | O23—O1ix | 2.57 (11) |
O7—Mo1xiii | 1.66 (4) | O23—O3i | 2.68 (7) |
O7—Al1ii | 2.11 (5) | O23—O19iv | 2.72 (7) |
O7—In1ii | 2.11 (5) | O23—O4ix | 2.92 (6) |
O7—O20xix | 2.31 (7) | O23—O17iv | 3.11 (12) |
O7—O20xiii | 2.50 (6) | O24—In1 | 1.87 (6) |
O7—O16ii | 2.65 (10) | O24—Al1 | 1.87 (6) |
O7—O6i | 2.75 (6) | O24—Mo5 | 2.10 (5) |
O7—O12 | 2.83 (9) | O24—O6iv | 2.37 (10) |
O7—O9 | 2.84 (7) | O24—O13iv | 2.43 (8) |
O7—O13i | 3.09 (8) | O24—O16 | 2.91 (6) |
O8—Mo3 | 1.84 (6) | O24—O4iv | 2.92 (8) |
O8—Al3 | 2.05 (6) | O24—O19iv | 3.04 (6) |
O8—In3 | 2.05 (6) | O24—Mo2vii | 3.05 (6) |
O8—O11 | 2.28 (7) | O24—O20iii | 3.16 (9) |
O12i—Mo1—O7i | 110 (3) | O8—O11—In3 | 56 (2) |
O20—Mo1—O12i | 122 (3) | O8—O11—Al3 | 56 (2) |
O20—Mo1—O7i | 86 (2) | O8—O11—Mo6vi | 167 (3) |
O9i—Mo1—O20 | 125 (3) | O2x—O11—O8 | 77 (3) |
O9i—Mo1—O12i | 108 (3) | O2x—O11—In3 | 54 (2) |
O9i—Mo1—O7i | 96 (3) | O2x—O11—Al3 | 54 (2) |
O2i—Mo2—O13i | 117 (3) | O2x—O11—Mo6vi | 109 (2) |
O3i—Mo2—O2i | 108 (3) | O10xxiii—O11—O2x | 85 (3) |
O3i—Mo2—O13i | 117 (3) | O10xxiii—O11—O8 | 132 (4) |
O4i—Mo2—O3i | 107 (2) | O10xxiii—O11—In3 | 138 (3) |
O4i—Mo2—O2i | 88 (3) | O10xxiii—O11—Al3 | 138 (3) |
O4i—Mo2—O13i | 116 (3) | O10xxiii—O11—Mo6vi | 41 (2) |
O24ii—Mo2—O4i | 67.0 (19) | O5i—O11—O10xxiii | 56.4 (19) |
O24ii—Mo2—O3i | 152 (2) | O5i—O11—O2x | 79 (3) |
O24ii—Mo2—O2i | 99 (3) | O5i—O11—O8 | 76 (2) |
O24ii—Mo2—O13i | 53 (2) | O5i—O11—In3 | 117 (3) |
O5i—Mo3—O8 | 115 (2) | O5i—O11—Al3 | 117 (3) |
O15—Mo3—O5i | 103 (3) | O5i—O11—Mo6vi | 93.4 (19) |
O15—Mo3—O8 | 99 (3) | Mo3—O11—O5i | 39.3 (11) |
O6i—Mo3—O15 | 119 (2) | Mo3—O11—O10xxiii | 95 (2) |
O6i—Mo3—O5i | 114 (2) | Mo3—O11—O2x | 86 (3) |
O6i—Mo3—O8 | 107 (2) | Mo3—O11—O8 | 39.7 (17) |
O11—Mo3—O6i | 107 (2) | Mo3—O11—In3 | 92 (2) |
O11—Mo3—O15 | 132 (2) | Mo3—O11—Al3 | 92 (2) |
O11—Mo3—O5i | 68 (2) | Mo3—O11—Mo6vi | 127.9 (19) |
O11—Mo3—O8 | 52.3 (19) | O17iv—O11—Mo3 | 92.6 (16) |
O18iv—Mo4—O14iii | 106 (3) | O17iv—O11—O5i | 131 (2) |
O16iv—Mo4—O18iv | 133 (2) | O17iv—O11—O10xxiii | 172 (3) |
O16iv—Mo4—O14iii | 104 (3) | O17iv—O11—O2x | 94 (3) |
O21—Mo4—O16iv | 110 (3) | O17iv—O11—O8 | 55 (2) |
O21—Mo4—O18iv | 102 (3) | O17iv—O11—In3 | 40.3 (17) |
O21—Mo4—O14iii | 97 (2) | O17iv—O11—Al3 | 40.3 (17) |
O23—Mo5—O19iv | 99 (3) | O17iv—O11—Mo6vi | 133 (3) |
O17iv—Mo5—O23 | 106 (3) | O1i—O11—O17iv | 123 (3) |
O17iv—Mo5—O19iv | 96 (2) | O1i—O11—Mo3 | 112.1 (17) |
O24—Mo5—O17iv | 123 (3) | O1i—O11—O5i | 90 (2) |
O24—Mo5—O23 | 121 (3) | O1i—O11—O10xxiii | 55 (2) |
O24—Mo5—O19iv | 106.5 (19) | O1i—O11—O2x | 136 (2) |
O22—Mo5—O24 | 87.8 (17) | O1i—O11—O8 | 142 (3) |
O22—Mo5—O17iv | 55.5 (17) | O1i—O11—In3 | 153 (3) |
O22—Mo5—O23 | 95.4 (18) | O1i—O11—Al3 | 153 (3) |
O22—Mo5—O19iv | 150 (2) | O1i—O11—Mo6vi | 28.3 (14) |
O10iii—Mo6—O1v | 104 (3) | O22—O11—O1i | 111 (2) |
O11vi—Mo6—O10iii | 92 (3) | O22—O11—O17iv | 49.5 (13) |
O11vi—Mo6—O1v | 118 (2) | O22—O11—Mo3 | 134.2 (19) |
O22—Mo6—O11vi | 117 (2) | O22—O11—O5i | 154 (3) |
O22—Mo6—O10iii | 80 (2) | O22—O11—O10xxiii | 122.9 (18) |
O22—Mo6—O1v | 125 (2) | O22—O11—O2x | 75 (2) |
O20iii—In1—O6iv | 94 (3) | O22—O11—O8 | 95 (2) |
O24—In1—O20iii | 123 (2) | O22—O11—In3 | 42.7 (13) |
O24—In1—O6iv | 89 (3) | O22—O11—Al3 | 42.7 (13) |
O7vii—In1—O24 | 162 (3) | O22—O11—Mo6vi | 98 (2) |
O7vii—In1—O20iii | 73 (2) | Al4xix—O12—Mo1xiii | 140 (3) |
O7vii—In1—O6iv | 98 (3) | In4xix—O12—Al4xix | 0.000 |
O16—In1—O7vii | 78 (2) | In4xix—O12—Mo1xiii | 140 (3) |
O16—In1—O24 | 94 (3) | O21xix—O12—In4xix | 44 (2) |
O16—In1—O20iii | 90 (3) | O21xix—O12—Al4xix | 44 (2) |
O16—In1—O6iv | 174 (3) | O21xix—O12—Mo1xiii | 126 (3) |
O13iv—In1—O16 | 87 (2) | O7—O12—O21xix | 118 (3) |
O13iv—In1—O7vii | 91 (2) | O7—O12—In4xix | 159 (3) |
O13iv—In1—O24 | 73 (2) | O7—O12—Al4xix | 159 (3) |
O13iv—In1—O20iii | 165 (2) | O7—O12—Mo1xiii | 33.5 (15) |
O13iv—In1—O6iv | 88 (3) | O9xii—O12—O7 | 152 (3) |
O5—In2—O23 | 81 (3) | O9xii—O12—O21xix | 81 (3) |
O3i—In2—O5 | 103 (2) | O9xii—O12—In4xix | 37.8 (17) |
O3i—In2—O23 | 92 (3) | O9xii—O12—Al4xix | 37.8 (17) |
O10viii—In2—O3i | 93 (2) | O9xii—O12—Mo1xiii | 119 (3) |
O10viii—In2—O5 | 81 (2) | O14iii—O12—O9xii | 57.4 (19) |
O10viii—In2—O23 | 161 (2) | O14iii—O12—O7 | 149 (2) |
O1ix—In2—O10viii | 92 (3) | O14iii—O12—O21xix | 62 (3) |
O1ix—In2—O3i | 175 (3) | O14iii—O12—In4xix | 42.3 (17) |
O1ix—In2—O5 | 78 (2) | O14iii—O12—Al4xix | 42.3 (17) |
O1ix—In2—O23 | 84 (3) | O14iii—O12—Mo1xiii | 171 (4) |
O4ix—In2—O1ix | 109.3 (19) | O19xxiv—O12—O14iii | 87 (3) |
O4ix—In2—O10viii | 103 (2) | O19xxiv—O12—O9xii | 50.8 (16) |
O4ix—In2—O3i | 68.8 (18) | O19xxiv—O12—O7 | 120 (2) |
O4ix—In2—O5 | 171 (3) | O19xxiv—O12—O21xix | 56 (2) |
O4ix—In2—O23 | 96 (2) | O19xxiv—O12—In4xix | 44.5 (16) |
O18iv—In3—O17iv | 77 (3) | O19xxiv—O12—Al4xix | 44.5 (16) |
O8—In3—O18iv | 90 (2) | O19xxiv—O12—Mo1xiii | 96 (2) |
O8—In3—O17iv | 79 (2) | Al1xviii—O13—Mo2xiii | 140 (4) |
O11—In3—O8 | 67 (2) | In1xviii—O13—Al1xviii | 0.000 |
O11—In3—O18iv | 157 (2) | In1xviii—O13—Mo2xiii | 140 (4) |
O11—In3—O17iv | 97 (3) | O24xviii—O13—In1xviii | 47 (2) |
O22—In3—O11 | 95 (2) | O24xviii—O13—Al1xviii | 47 (2) |
O22—In3—O8 | 149 (3) | O24xviii—O13—Mo2xiii | 95 (3) |
O22—In3—O18iv | 105 (2) | O6—O13—O24xviii | 56 (3) |
O22—In3—O17iv | 78 (2) | O6—O13—In1xviii | 34.7 (15) |
O2x—In3—O22 | 109 (2) | O6—O13—Al1xviii | 34.7 (15) |
O2x—In3—O11 | 74 (3) | O6—O13—Mo2xiii | 139 (3) |
O2x—In3—O8 | 91 (3) | O2—O13—O6 | 144 (3) |
O2x—In3—O18iv | 109 (3) | O2—O13—O24xviii | 89 (3) |
O2x—In3—O17iv | 169 (3) | O2—O13—In1xviii | 121 (3) |
O21—In4—O9iv | 163.7 (18) | O2—O13—Al1xviii | 121 (3) |
O14vii—In4—O21 | 99 (2) | O2—O13—Mo2xiii | 31.6 (19) |
O14vii—In4—O9iv | 96 (2) | O16xviii—O13—O2 | 84 (3) |
O12iii—In4—O14vii | 93 (2) | O16xviii—O13—O6 | 80 (2) |
O12iii—In4—O21 | 89 (3) | O16xviii—O13—O24xviii | 64.2 (18) |
O12iii—In4—O9iv | 97 (3) | O16xviii—O13—In1xviii | 45.0 (18) |
O15vii—In4—O12iii | 167 (3) | O16xviii—O13—Al1xviii | 45.0 (18) |
O15vii—In4—O14vii | 89 (2) | O16xviii—O13—Mo2xiii | 115 (3) |
O15vii—In4—O21 | 103 (3) | O3—O13—O16xviii | 140 (3) |
O15vii—In4—O9iv | 70 (3) | O3—O13—O2 | 59 (2) |
O19x—In4—O15vii | 83 (2) | O3—O13—O6 | 139 (2) |
O19x—In4—O12iii | 94 (2) | O3—O13—O24xviii | 123 (3) |
O19x—In4—O14vii | 172 (2) | O3—O13—In1xviii | 169 (3) |
O19x—In4—O21 | 84 (2) | O3—O13—Al1xviii | 169 (3) |
O19x—In4—O9iv | 80.3 (19) | O3—O13—Mo2xiii | 33.7 (18) |
O20iii—Al1—O6iv | 94 (3) | O7xiii—O13—O3 | 147 (3) |
O24—Al1—O20iii | 123 (2) | O7xiii—O13—O16xviii | 52 (2) |
O24—Al1—O6iv | 89 (3) | O7xiii—O13—O2 | 131 (2) |
O7vii—Al1—O24 | 162 (3) | O7xiii—O13—O6 | 56.8 (19) |
O7vii—Al1—O20iii | 73 (2) | O7xiii—O13—O24xviii | 90 (3) |
O7vii—Al1—O6iv | 98 (3) | O7xiii—O13—In1xviii | 43.0 (15) |
O16—Al1—O7vii | 78 (2) | O7xiii—O13—Al1xviii | 43.0 (15) |
O16—Al1—O24 | 94 (3) | O7xiii—O13—Mo2xiii | 161 (3) |
O16—Al1—O20iii | 90 (3) | O4—O13—O7xiii | 152 (3) |
O16—Al1—O6iv | 174 (3) | O4—O13—O3 | 60.9 (19) |
O13iv—Al1—O16 | 87 (2) | O4—O13—O16xviii | 108 (3) |
O13iv—Al1—O7vii | 91 (2) | O4—O13—O2 | 51 (2) |
O13iv—Al1—O24 | 73 (2) | O4—O13—O6 | 105 (2) |
O13iv—Al1—O20iii | 165 (2) | O4—O13—O24xviii | 62 (2) |
O13iv—Al1—O6iv | 88 (3) | O4—O13—In1xviii | 110 (3) |
O5—Al2—O23 | 81 (3) | O4—O13—Al1xviii | 110 (3) |
O3i—Al2—O5 | 103 (2) | O4—O13—Mo2xiii | 35.2 (17) |
O3i—Al2—O23 | 92 (3) | Al4ii—O14—Mo4xix | 166 (5) |
O10viii—Al2—O3i | 93 (2) | In4ii—O14—Al4ii | 0.000 |
O10viii—Al2—O5 | 81 (2) | In4ii—O14—Mo4xix | 166 (5) |
O10viii—Al2—O23 | 161 (2) | O21xix—O14—In4ii | 139 (2) |
O1ix—Al2—O10viii | 92 (3) | O21xix—O14—Al4ii | 139 (2) |
O1ix—Al2—O3i | 175 (3) | O21xix—O14—Mo4xix | 45.0 (15) |
O1ix—Al2—O5 | 78 (2) | O16xii—O14—O21xix | 69 (2) |
O1ix—Al2—O23 | 84 (3) | O16xii—O14—In4ii | 147 (3) |
O4ix—Al2—O1ix | 109.3 (19) | O16xii—O14—Al4ii | 147 (3) |
O4ix—Al2—O10viii | 103 (2) | O16xii—O14—Mo4xix | 41 (2) |
O4ix—Al2—O3i | 68.8 (18) | O18xii—O14—O16xii | 75 (2) |
O4ix—Al2—O5 | 171 (3) | O18xii—O14—O21xix | 64 (2) |
O4ix—Al2—O23 | 96 (2) | O18xii—O14—In4ii | 127 (4) |
O18iv—Al3—O17iv | 77 (3) | O18xii—O14—Al4ii | 127 (4) |
O8—Al3—O18iv | 90 (2) | O18xii—O14—Mo4xix | 39 (2) |
O8—Al3—O17iv | 79 (2) | O9i—O14—O18xii | 107 (3) |
O11—Al3—O8 | 67 (2) | O9i—O14—O16xii | 169 (3) |
O11—Al3—O18iv | 157 (2) | O9i—O14—O21xix | 102 (2) |
O11—Al3—O17iv | 97 (3) | O9i—O14—In4ii | 39.4 (14) |
O22—Al3—O11 | 95 (2) | O9i—O14—Al4ii | 39.4 (14) |
O22—Al3—O8 | 149 (3) | O9i—O14—Mo4xix | 136 (4) |
O22—Al3—O18iv | 105 (2) | O15—O14—O9i | 47 (2) |
O22—Al3—O17iv | 78 (2) | O15—O14—O18xii | 149 (3) |
O2x—Al3—O22 | 109 (2) | O15—O14—O16xii | 128 (4) |
O2x—Al3—O11 | 74 (3) | O15—O14—O21xix | 101 (2) |
O2x—Al3—O8 | 91 (3) | O15—O14—In4ii | 46.6 (18) |
O2x—Al3—O18iv | 109 (3) | O15—O14—Al4ii | 46.6 (18) |
O2x—Al3—O17iv | 169 (3) | O15—O14—Mo4xix | 144 (3) |
O21—Al4—O9iv | 163.7 (18) | O12xix—O14—O15 | 91 (2) |
O14vii—Al4—O21 | 99 (2) | O12xix—O14—O9i | 60.4 (19) |
O14vii—Al4—O9iv | 96 (2) | O12xix—O14—O18xii | 86 (3) |
O12iii—Al4—O14vii | 93 (2) | O12xix—O14—O16xii | 131 (2) |
O12iii—Al4—O21 | 89 (3) | O12xix—O14—O21xix | 140 (4) |
O12iii—Al4—O9iv | 97 (3) | O12xix—O14—In4ii | 44.6 (18) |
O15vii—Al4—O12iii | 167 (3) | O12xix—O14—Al4ii | 44.6 (18) |
O15vii—Al4—O14vii | 89 (2) | O12xix—O14—Mo4xix | 122 (4) |
O15vii—Al4—O21 | 103 (3) | O21ii—O14—O12xix | 57 (2) |
O15vii—Al4—O9iv | 70 (3) | O21ii—O14—O15 | 65 (2) |
O19x—Al4—O15vii | 83 (2) | O21ii—O14—O9i | 79.6 (18) |
O19x—Al4—O12iii | 94 (2) | O21ii—O14—O18xii | 134 (3) |
O19x—Al4—O14vii | 172 (2) | O21ii—O14—O16xii | 107 (3) |
O19x—Al4—O21 | 84 (2) | O21ii—O14—O21xix | 161 (3) |
O19x—Al4—O9iv | 80.3 (19) | O21ii—O14—In4ii | 40.3 (16) |
Al2ix—O1—Mo6xi | 160 (4) | O21ii—O14—Al4ii | 40.3 (16) |
In2ix—O1—Al2ix | 0.000 | O21ii—O14—Mo4xix | 142 (3) |
In2ix—O1—Mo6xi | 160 (4) | Al4ii—O15—Mo3 | 135 (3) |
O5ix—O1—In2ix | 48.1 (16) | In4ii—O15—Al4ii | 0.000 |
O5ix—O1—Al2ix | 48.1 (16) | In4ii—O15—Mo3 | 135 (3) |
O5ix—O1—Mo6xi | 130 (3) | O9i—O15—In4ii | 49 (2) |
O23ix—O1—O5ix | 56 (2) | O9i—O15—Al4ii | 49 (2) |
O23ix—O1—In2ix | 42.7 (18) | O9i—O15—Mo3 | 167 (3) |
O23ix—O1—Al2ix | 42.7 (18) | O19xxv—O15—O9i | 60 (2) |
O23ix—O1—Mo6xi | 157 (3) | O19xxv—O15—In4ii | 50.2 (17) |
O10viii—O1—O23ix | 152 (2) | O19xxv—O15—Al4ii | 50.2 (17) |
O10viii—O1—O5ix | 97 (3) | O19xxv—O15—Mo3 | 112 (3) |
O10viii—O1—In2ix | 125 (3) | O14—O15—O19xxv | 94 (2) |
O10viii—O1—Al2ix | 125 (3) | O14—O15—O9i | 66 (2) |
O10viii—O1—Mo6xi | 39 (2) | O14—O15—In4ii | 44.2 (15) |
O10xii—O1—O10viii | 82 (3) | O14—O15—Al4ii | 44.2 (15) |
O10xii—O1—O23ix | 85 (2) | O14—O15—Mo3 | 126 (3) |
O10xii—O1—O5ix | 55.3 (19) | O8—O15—O14 | 119 (2) |
O10xii—O1—In2ix | 44.0 (19) | O8—O15—O19xxv | 144 (2) |
O10xii—O1—Al2ix | 44.0 (19) | O8—O15—O9i | 143 (3) |
O10xii—O1—Mo6xi | 117 (4) | O8—O15—In4ii | 160 (3) |
O11xiii—O1—O10xii | 101 (3) | O8—O15—Al4ii | 160 (3) |
O11xiii—O1—O10viii | 54 (2) | O8—O15—Mo3 | 38.8 (18) |
O11xiii—O1—O23ix | 154 (3) | O5i—O15—O8 | 65 (2) |
O11xiii—O1—O5ix | 147 (4) | O5i—O15—O14 | 153 (3) |
O11xiii—O1—In2ix | 133 (2) | O5i—O15—O19xxv | 80 (2) |
O11xiii—O1—Al2ix | 133 (2) | O5i—O15—O9i | 129 (3) |
O11xiii—O1—Mo6xi | 34.1 (15) | O5i—O15—In4ii | 124 (3) |
Al3xiv—O2—Mo2xiii | 166 (5) | O5i—O15—Al4ii | 124 (3) |
In3xiv—O2—Al3xiv | 0.000 | O5i—O15—Mo3 | 38.2 (14) |
In3xiv—O2—Mo2xiii | 166 (5) | O21ii—O15—O5i | 97 (2) |
O11xiv—O2—In3xiv | 52 (2) | O21ii—O15—O8 | 130 (3) |
O11xiv—O2—Al3xiv | 52 (2) | O21ii—O15—O14 | 59.8 (17) |
O11xiv—O2—Mo2xiii | 137 (4) | O21ii—O15—O19xxv | 55.4 (18) |
O4—O2—O11xiv | 136 (4) | O21ii—O15—O9i | 85 (3) |
O4—O2—In3xiv | 134 (4) | O21ii—O15—In4ii | 37.5 (19) |
O4—O2—Al3xiv | 134 (4) | O21ii—O15—Al4ii | 37.5 (19) |
O4—O2—Mo2xiii | 51 (2) | O21ii—O15—Mo3 | 97 (3) |
O13—O2—O4 | 70 (3) | Al1—O16—Mo4xviii | 152 (3) |
O13—O2—O11xiv | 144 (3) | In1—O16—Al1 | 0.000 |
O13—O2—In3xiv | 135 (3) | In1—O16—Mo4xviii | 152 (3) |
O13—O2—Al3xiv | 135 (3) | O7vii—O16—In1 | 51 (2) |
O13—O2—Mo2xiii | 31 (2) | O7vii—O16—Al1 | 51 (2) |
O3—O2—O13 | 63 (3) | O7vii—O16—Mo4xviii | 157 (2) |
O3—O2—O4 | 69 (2) | O14xii—O16—O7vii | 122 (2) |
O3—O2—O11xiv | 99 (3) | O14xii—O16—In1 | 168 (4) |
O3—O2—In3xiv | 151 (4) | O14xii—O16—Al1 | 168 (4) |
O3—O2—Al3xiv | 151 (4) | O14xii—O16—Mo4xviii | 35.7 (18) |
O3—O2—Mo2xiii | 38 (2) | O20iii—O16—O14xii | 129 (3) |
O8xiv—O2—O3 | 116 (3) | O20iii—O16—O7vii | 51 (2) |
O8xiv—O2—O13 | 109 (3) | O20iii—O16—In1 | 39.5 (18) |
O8xiv—O2—O4 | 174 (3) | O20iii—O16—Al1 | 39.5 (18) |
O8xiv—O2—O11xiv | 48 (2) | O20iii—O16—Mo4xviii | 140 (3) |
O8xiv—O2—In3xiv | 42.9 (18) | O24—O16—O20iii | 68 (2) |
O8xiv—O2—Al3xiv | 42.9 (18) | O24—O16—O14xii | 148 (3) |
O8xiv—O2—Mo2xiii | 131 (4) | O24—O16—O7vii | 90 (3) |
Al2xiii—O3—Mo2xiii | 132 (2) | O24—O16—In1 | 39.9 (18) |
In2xiii—O3—Al2xiii | 0.000 | O24—O16—Al1 | 39.9 (18) |
In2xiii—O3—Mo2xiii | 132 (2) | O24—O16—Mo4xviii | 113 (3) |
O4xv—O3—In2xiii | 59 (2) | O13iv—O16—O24 | 48.8 (16) |
O4xv—O3—Al2xiii | 59 (2) | O13iv—O16—O20iii | 86 (3) |
O4xv—O3—Mo2xiii | 167 (3) | O13iv—O16—O14xii | 142 (3) |
O23xiii—O3—O4xv | 70 (2) | O13iv—O16—O7vii | 66 (2) |
O23xiii—O3—In2xiii | 41 (2) | O13iv—O16—In1 | 47.8 (18) |
O23xiii—O3—Al2xiii | 41 (2) | O13iv—O16—Al1 | 47.8 (18) |
O23xiii—O3—Mo2xiii | 122 (2) | O13iv—O16—Mo4xviii | 125 (4) |
O2—O3—O23xiii | 113 (2) | O21xviii—O16—O13iv | 138 (3) |
O2—O3—O4xv | 150 (4) | O21xviii—O16—O24 | 98 (2) |
O2—O3—In2xiii | 103 (3) | O21xviii—O16—O20iii | 105 (2) |
O2—O3—Al2xiii | 103 (3) | O21xviii—O16—O14xii | 54.5 (18) |
O2—O3—Mo2xiii | 34 (2) | O21xviii—O16—O7vii | 149 (3) |
O10xvi—O3—O2 | 74 (3) | O21xviii—O16—In1 | 125 (2) |
O10xvi—O3—O23xiii | 84 (3) | O21xviii—O16—Al1 | 125 (2) |
O10xvi—O3—O4xv | 77 (3) | O21xviii—O16—Mo4xviii | 35.8 (17) |
O10xvi—O3—In2xiii | 44.6 (17) | In3xviii—O17—Mo5xviii | 137 (3) |
O10xvi—O3—Al2xiii | 44.6 (17) | Al3xviii—O17—In3xviii | 0.000 |
O10xvi—O3—Mo2xiii | 108 (3) | Al3xviii—O17—Mo5xviii | 137 (3) |
O13—O3—O10xvi | 130 (2) | O18—O17—Al3xviii | 52 (2) |
O13—O3—O2 | 58 (3) | O18—O17—In3xviii | 52 (2) |
O13—O3—O23xiii | 101 (2) | O18—O17—Mo5xviii | 118 (3) |
O13—O3—O4xv | 152 (4) | O8xviii—O17—O18 | 69 (3) |
O13—O3—In2xiii | 130 (2) | O8xviii—O17—Al3xviii | 51 (2) |
O13—O3—Al2xiii | 130 (2) | O8xviii—O17—In3xviii | 51 (2) |
O13—O3—Mo2xiii | 29.8 (18) | O8xviii—O17—Mo5xviii | 171 (4) |
O5xiii—O3—O13 | 96.2 (17) | O22xviii—O17—O8xviii | 102 (3) |
O5xiii—O3—O10xvi | 50.8 (18) | O22xviii—O17—O18 | 80 (2) |
O5xiii—O3—O2 | 70 (2) | O22xviii—O17—Al3xviii | 53.2 (17) |
O5xiii—O3—O23xiii | 48 (2) | O22xviii—O17—In3xviii | 53.2 (17) |
O5xiii—O3—O4xv | 97 (3) | O22xviii—O17—Mo5xviii | 85 (2) |
O5xiii—O3—In2xiii | 37.5 (12) | O19—O17—O22xviii | 122 (3) |
O5xiii—O3—Al2xiii | 37.5 (12) | O19—O17—O8xviii | 136 (2) |
O5xiii—O3—Mo2xiii | 95.4 (17) | O19—O17—O18 | 116 (2) |
O4—O3—O5xiii | 121 (2) | O19—O17—Al3xviii | 167 (3) |
O4—O3—O13 | 61.3 (19) | O19—O17—In3xviii | 167 (3) |
O4—O3—O10xvi | 101 (2) | O19—O17—Mo5xviii | 37.7 (16) |
O4—O3—O2 | 50.9 (19) | O11xviii—O17—O19 | 151 (3) |
O4—O3—O23xiii | 160 (2) | O11xviii—O17—O22xviii | 66.2 (16) |
O4—O3—O4xv | 129.6 (19) | O11xviii—O17—O8xviii | 46.8 (19) |
O4—O3—In2xiii | 145 (3) | O11xviii—O17—O18 | 92 (3) |
O4—O3—Al2xiii | 145 (3) | O11xviii—O17—Al3xviii | 42.4 (16) |
O4—O3—Mo2xiii | 38.1 (14) | O11xviii—O17—In3xviii | 42.4 (16) |
In2ix—O4—Mo2xiii | 120 (3) | O11xviii—O17—Mo5xviii | 134 (3) |
Al2ix—O4—In2ix | 0.000 | O23xviii—O17—O11xviii | 103 (2) |
Al2ix—O4—Mo2xiii | 120 (3) | O23xviii—O17—O19 | 55 (2) |
O3xvii—O4—Al2ix | 51.7 (16) | O23xviii—O17—O22xviii | 84 (2) |
O3xvii—O4—In2ix | 51.7 (16) | O23xviii—O17—O8xviii | 138 (3) |
O3xvii—O4—Mo2xiii | 172 (3) | O23xviii—O17—O18 | 151 (3) |
O2—O4—O3xvii | 145 (4) | O23xviii—O17—Al3xviii | 131 (2) |
O2—O4—Al2ix | 153 (3) | O23xviii—O17—In3xviii | 131 (2) |
O2—O4—In2ix | 153 (3) | O23xviii—O17—Mo5xviii | 36.3 (17) |
O2—O4—Mo2xiii | 41 (2) | Al3xviii—O18—Mo4xviii | 130 (3) |
O24xviii—O4—O2 | 84 (3) | In3xviii—O18—Al3xviii | 0.000 |
O24xviii—O4—O3xvii | 110 (3) | In3xviii—O18—Mo4xviii | 130 (3) |
O24xviii—O4—Al2ix | 111 (3) | O17—O18—In3xviii | 50.9 (19) |
O24xviii—O4—In2ix | 111 (3) | O17—O18—Al3xviii | 50.9 (19) |
O24xviii—O4—Mo2xiii | 74.2 (18) | O17—O18—Mo4xviii | 157 (3) |
O23ix—O4—O24xviii | 147 (3) | O14xii—O18—O17 | 125 (2) |
O23ix—O4—O2 | 123 (3) | O14xii—O18—In3xviii | 137 (3) |
O23ix—O4—O3xvii | 60.1 (17) | O14xii—O18—Al3xviii | 137 (3) |
O23ix—O4—Al2ix | 36.6 (16) | O14xii—O18—Mo4xviii | 34.7 (17) |
O23ix—O4—In2ix | 36.6 (16) | O21xviii—O18—O14xii | 56 (2) |
O23ix—O4—Mo2xiii | 112 (2) | O21xviii—O18—O17 | 152 (3) |
O3—O4—O23ix | 77.1 (16) | O21xviii—O18—In3xviii | 151 (2) |
O3—O4—O24xviii | 105 (2) | O21xviii—O18—Al3xviii | 151 (2) |
O3—O4—O2 | 60 (2) | O21xviii—O18—Mo4xviii | 40.3 (19) |
O3—O4—O3xvii | 137 (2) | O8xviii—O18—O21xviii | 146 (3) |
O3—O4—Al2ix | 94.0 (18) | O8xviii—O18—O14xii | 94 (2) |
O3—O4—In2ix | 94.0 (18) | O8xviii—O18—O17 | 57 (2) |
O3—O4—Mo2xiii | 35.1 (12) | O8xviii—O18—In3xviii | 45.1 (15) |
O13—O4—O3 | 57.8 (18) | O8xviii—O18—Al3xviii | 45.1 (15) |
O13—O4—O23ix | 126 (2) | O8xviii—O18—Mo4xviii | 106 (3) |
O13—O4—O24xviii | 47.6 (17) | In4xiv—O19—Mo5xviii | 179 (4) |
O13—O4—O2 | 59 (3) | Al4xiv—O19—In4xiv | 0.000 |
O13—O4—O3xvii | 152 (4) | Al4xiv—O19—Mo5xviii | 179 (4) |
O13—O4—Al2ix | 114 (3) | O9xviii—O19—Al4xiv | 43.0 (13) |
O13—O4—In2ix | 114 (3) | O9xviii—O19—In4xiv | 43.0 (13) |
O13—O4—Mo2xiii | 28.7 (16) | O9xviii—O19—Mo5xviii | 137 (3) |
In2—O5—Al2 | 0.000 | O23xviii—O19—O9xviii | 120 (2) |
Mo3xiii—O5—In2 | 167 (4) | O23xviii—O19—Al4xiv | 135 (3) |
Mo3xiii—O5—Al2 | 167 (4) | O23xviii—O19—In4xiv | 135 (3) |
O23—O5—Mo3xiii | 129 (3) | O23xviii—O19—Mo5xviii | 44.0 (19) |
O23—O5—In2 | 46.6 (17) | O17—O19—O23xviii | 70 (2) |
O23—O5—Al2 | 46.6 (17) | O17—O19—O9xviii | 92 (2) |
O1ix—O5—O23 | 63 (3) | O17—O19—Al4xiv | 134 (3) |
O1ix—O5—Mo3xiii | 138 (3) | O17—O19—In4xiv | 134 (3) |
O1ix—O5—In2 | 53.8 (17) | O17—O19—Mo5xviii | 46.7 (18) |
O1ix—O5—Al2 | 53.8 (17) | O21xiv—O19—O17 | 171 (3) |
O10viii—O5—O1ix | 71 (2) | O21xiv—O19—O23xviii | 118 (3) |
O10viii—O5—O23 | 99 (2) | O21xiv—O19—O9xviii | 87 (2) |
O10viii—O5—Mo3xiii | 130 (3) | O21xiv—O19—Al4xiv | 44.4 (16) |
O10viii—O5—In2 | 52.2 (18) | O21xiv—O19—In4xiv | 44.4 (16) |
O10viii—O5—Al2 | 52.2 (18) | O21xiv—O19—Mo5xviii | 136 (3) |
O11xiii—O5—O10viii | 58.4 (18) | O15xxvi—O19—O21xiv | 68 (2) |
O11xiii—O5—O1ix | 121 (3) | O15xxvi—O19—O17 | 117 (2) |
O11xiii—O5—O23 | 147 (2) | O15xxvi—O19—O23xviii | 89 (2) |
O11xiii—O5—Mo3xiii | 72.6 (19) | O15xxvi—O19—O9xviii | 48 (2) |
O11xiii—O5—In2 | 106 (2) | O15xxvi—O19—Al4xiv | 46.6 (14) |
O11xiii—O5—Al2 | 106 (2) | O15xxvi—O19—In4xiv | 46.6 (14) |
O15xiii—O5—O11xiii | 99 (2) | O15xxvi—O19—Mo5xviii | 132 (3) |
O15xiii—O5—O10viii | 150 (3) | O24xviii—O19—O15xxvi | 153 (3) |
O15xiii—O5—O1ix | 137 (3) | O24xviii—O19—O21xiv | 100 (2) |
O15xiii—O5—O23 | 91 (3) | O24xviii—O19—O17 | 77.2 (19) |
O15xiii—O5—Mo3xiii | 39.3 (18) | O24xviii—O19—O23xviii | 74.6 (18) |
O15xiii—O5—In2 | 131 (3) | O24xviii—O19—O9xviii | 158 (4) |
O15xiii—O5—Al2 | 131 (3) | O24xviii—O19—Al4xiv | 139 (2) |
O3i—O5—O15xiii | 102 (3) | O24xviii—O19—In4xiv | 139 (2) |
O3i—O5—O11xiii | 89 (2) | O24xviii—O19—Mo5xviii | 41.6 (14) |
O3i—O5—O10viii | 62 (2) | O12xxvii—O19—O24xviii | 107 (2) |
O3i—O5—O1ix | 93 (2) | O12xxvii—O19—O15xxvi | 87.4 (18) |
O3i—O5—O23 | 57.7 (19) | O12xxvii—O19—O21xiv | 57 (2) |
O3i—O5—Mo3xiii | 128 (3) | O12xxvii—O19—O17 | 115 (3) |
O3i—O5—In2 | 39.1 (15) | O12xxvii—O19—O23xviii | 175 (3) |
O3i—O5—Al2 | 39.1 (15) | O12xxvii—O19—O9xviii | 60.2 (17) |
O8xiii—O5—O3i | 105 (2) | O12xxvii—O19—Al4xiv | 41.5 (16) |
O8xiii—O5—O15xiii | 55.9 (19) | O12xxvii—O19—In4xiv | 41.5 (16) |
O8xiii—O5—O11xiii | 44.4 (17) | O12xxvii—O19—Mo5xviii | 140 (3) |
O8xiii—O5—O10viii | 102 (2) | Al1xix—O20—In1xix | 0.000 |
O8xiii—O5—O1ix | 155 (3) | Mo1—O20—Al1xix | 144 (5) |
O8xiii—O5—O23 | 141 (3) | Mo1—O20—In1xix | 144 (5) |
O8xiii—O5—Mo3xiii | 31.8 (13) | O7iii—O20—Mo1 | 128 (2) |
O8xiii—O5—In2 | 141 (3) | O7iii—O20—Al1xix | 61 (2) |
O8xiii—O5—Al2 | 141 (3) | O7iii—O20—In1xix | 61 (2) |
Al1xviii—O6—In1xviii | 0.000 | O6xii—O20—O7iii | 72 (2) |
Mo3xiii—O6—Al1xviii | 151 (3) | O6xii—O20—Mo1 | 159 (2) |
Mo3xiii—O6—In1xviii | 151 (3) | O6xii—O20—Al1xix | 39 (2) |
O20xii—O6—Mo3xiii | 130 (4) | O6xii—O20—In1xix | 39 (2) |
O20xii—O6—Al1xviii | 47 (2) | O7i—O20—O6xii | 157 (3) |
O20xii—O6—In1xviii | 47 (2) | O7i—O20—O7iii | 89 (2) |
O24xviii—O6—O20xii | 84 (3) | O7i—O20—Mo1 | 41.4 (15) |
O24xviii—O6—Mo3xiii | 146 (2) | O7i—O20—Al1xix | 140 (3) |
O24xviii—O6—Al1xviii | 52 (2) | O7i—O20—In1xix | 140 (3) |
O24xviii—O6—In1xviii | 52 (2) | O16xix—O20—O7i | 93 (3) |
O13—O6—O24xviii | 58 (3) | O16xix—O20—O6xii | 90 (3) |
O13—O6—O20xii | 103 (3) | O16xix—O20—O7iii | 63 (3) |
O13—O6—Mo3xiii | 109 (2) | O16xix—O20—Mo1 | 99 (3) |
O13—O6—Al1xviii | 57 (3) | O16xix—O20—Al1xix | 51 (2) |
O13—O6—In1xviii | 57 (3) | O16xix—O20—In1xix | 51 (2) |
O7xiii—O6—O13 | 70 (2) | O24xix—O20—O16xix | 59 (2) |
O7xiii—O6—O24xviii | 100 (3) | O24xix—O20—O7i | 148 (3) |
O7xiii—O6—O20xii | 53.1 (17) | O24xix—O20—O6xii | 48 (2) |
O7xiii—O6—Mo3xiii | 104 (2) | O24xix—O20—O7iii | 91 (3) |
O7xiii—O6—Al1xviii | 49.3 (19) | O24xix—O20—Mo1 | 123 (3) |
O7xiii—O6—In1xviii | 49.3 (19) | O24xix—O20—Al1xix | 30.0 (15) |
Al1ii—O7—Mo1xiii | 173 (3) | O24xix—O20—In1xix | 30.0 (15) |
In1ii—O7—Al1ii | 0.000 | In4—O21—Mo4 | 149 (4) |
In1ii—O7—Mo1xiii | 173 (3) | Al4—O21—In4 | 0.000 |
O20xix—O7—In1ii | 45.8 (19) | Al4—O21—Mo4 | 149 (4) |
O20xix—O7—Al1ii | 45.8 (19) | O14iii—O21—Al4 | 142 (4) |
O20xix—O7—Mo1xiii | 140 (3) | O14iii—O21—In4 | 142 (4) |
O20xiii—O7—O20xix | 91 (2) | O14iii—O21—Mo4 | 37.6 (14) |
O20xiii—O7—In1ii | 130 (2) | O19x—O21—O14iii | 135 (3) |
O20xiii—O7—Al1ii | 130 (2) | O19x—O21—Al4 | 51.2 (17) |
O20xiii—O7—Mo1xiii | 52.3 (15) | O19x—O21—In4 | 51.2 (17) |
O16ii—O7—O20xiii | 94 (2) | O19x—O21—Mo4 | 105 (2) |
O16ii—O7—O20xix | 66 (3) | O12iii—O21—O19x | 67 (2) |
O16ii—O7—In1ii | 51.0 (17) | O12iii—O21—O14iii | 97 (3) |
O16ii—O7—Al1ii | 51.0 (17) | O12iii—O21—Al4 | 47 (2) |
O16ii—O7—Mo1xiii | 124 (3) | O12iii—O21—In4 | 47 (2) |
O6i—O7—O16ii | 84 (2) | O12iii—O21—Mo4 | 109 (3) |
O6i—O7—O20xiii | 143 (3) | O18iv—O21—O12iii | 147 (3) |
O6i—O7—O20xix | 54.8 (17) | O18iv—O21—O19x | 110 (2) |
O6i—O7—In1ii | 32.6 (16) | O18iv—O21—O14iii | 60 (2) |
O6i—O7—Al1ii | 32.6 (16) | O18iv—O21—Al4 | 157 (3) |
O6i—O7—Mo1xiii | 151 (3) | O18iv—O21—In4 | 157 (3) |
O12—O7—O6i | 114 (3) | O18iv—O21—Mo4 | 38 (2) |
O12—O7—O16ii | 160 (3) | O14vii—O21—O18iv | 150 (3) |
O12—O7—O20xiii | 77 (2) | O14vii—O21—O12iii | 60 (2) |
O12—O7—O20xix | 131 (4) | O14vii—O21—O19x | 92 (2) |
O12—O7—In1ii | 147 (2) | O14vii—O21—O14iii | 118.0 (16) |
O12—O7—Al1ii | 147 (2) | O14vii—O21—Al4 | 40.8 (16) |
O12—O7—Mo1xiii | 36.9 (18) | O14vii—O21—In4 | 40.8 (16) |
O9—O7—O12 | 69 (2) | O14vii—O21—Mo4 | 155 (3) |
O9—O7—O6i | 130 (2) | O16iv—O21—O14vii | 138 (4) |
O9—O7—O16ii | 93 (3) | O16iv—O21—O18iv | 68 (2) |
O9—O7—O20xiii | 86.2 (19) | O16iv—O21—O12iii | 79 (3) |
O9—O7—O20xix | 159 (4) | O16iv—O21—O19x | 78 (2) |
O9—O7—In1ii | 124 (3) | O16iv—O21—O14iii | 57 (2) |
O9—O7—Al1ii | 124 (3) | O16iv—O21—Al4 | 114 (3) |
O9—O7—Mo1xiii | 48.5 (19) | O16iv—O21—In4 | 114 (3) |
O13i—O7—O9 | 82 (2) | O16iv—O21—Mo4 | 34 (2) |
O13i—O7—O12 | 121 (2) | O15vii—O21—O16iv | 135 (2) |
O13i—O7—O6i | 53 (2) | O15vii—O21—O14vii | 55.1 (16) |
O13i—O7—O16ii | 62 (2) | O15vii—O21—O18iv | 121 (3) |
O13i—O7—O20xiii | 152 (3) | O15vii—O21—O12iii | 87 (3) |
O13i—O7—O20xix | 91 (2) | O15vii—O21—O19x | 56.5 (19) |
O13i—O7—In1ii | 45.7 (16) | O15vii—O21—O14iii | 169 (3) |
O13i—O7—Al1ii | 45.7 (16) | O15vii—O21—Al4 | 39.8 (19) |
O13i—O7—Mo1xiii | 128 (3) | O15vii—O21—In4 | 39.8 (19) |
Al3—O8—Mo3 | 138 (2) | O15vii—O21—Mo4 | 150 (3) |
In3—O8—Al3 | 0.000 | In3—O22—Mo6 | 122 (3) |
In3—O8—Mo3 | 138 (2) | Al3—O22—In3 | 0.000 |
O11—O8—In3 | 57.2 (17) | Al3—O22—Mo6 | 122 (3) |
O11—O8—Al3 | 57.2 (17) | O10iii—O22—Al3 | 159 (3) |
O11—O8—Mo3 | 88 (2) | O10iii—O22—In3 | 159 (3) |
O17iv—O8—O11 | 78 (3) | O10iii—O22—Mo6 | 44.4 (17) |
O17iv—O8—In3 | 49.5 (19) | O17iv—O22—O10iii | 139 (2) |
O17iv—O8—Al3 | 49.5 (19) | O17iv—O22—Al3 | 49.1 (19) |
O17iv—O8—Mo3 | 152 (4) | O17iv—O22—In3 | 49.1 (19) |
O18iv—O8—O17iv | 54 (2) | O17iv—O22—Mo6 | 165 (3) |
O18iv—O8—O11 | 102 (2) | O11—O22—O17iv | 64.3 (17) |
O18iv—O8—In3 | 44.9 (16) | O11—O22—O10iii | 151 (2) |
O18iv—O8—Al3 | 44.9 (16) | O11—O22—Al3 | 41.8 (15) |
O18iv—O8—Mo3 | 154 (4) | O11—O22—In3 | 41.8 (15) |
O15—O8—O18iv | 113 (3) | O11—O22—Mo6 | 118.2 (18) |
O15—O8—O17iv | 164 (3) | Mo5—O22—O11 | 97.2 (14) |
O15—O8—O11 | 117 (3) | Mo5—O22—O17iv | 39.5 (17) |
O15—O8—In3 | 132 (3) | Mo5—O22—O10iii | 101 (2) |
O15—O8—Al3 | 132 (3) | Mo5—O22—Al3 | 88.0 (11) |
O15—O8—Mo3 | 42 (2) | Mo5—O22—In3 | 88.0 (11) |
O2x—O8—O15 | 89 (3) | Mo5—O22—Mo6 | 144 (2) |
O2x—O8—O18iv | 71 (2) | In2—O23—Al2 | 0.000 |
O2x—O8—O17iv | 95 (3) | Mo5—O23—In2 | 175 (4) |
O2x—O8—O11 | 56 (3) | Mo5—O23—Al2 | 175 (4) |
O2x—O8—In3 | 46 (2) | O5—O23—Mo5 | 131 (2) |
O2x—O8—Al3 | 46 (2) | O5—O23—In2 | 53 (2) |
O2x—O8—Mo3 | 96 (2) | O5—O23—Al2 | 53 (2) |
O5i—O8—O2x | 66.8 (18) | O1ix—O23—O5 | 61 (3) |
O5i—O8—O15 | 59.5 (18) | O1ix—O23—Mo5 | 131 (2) |
O5i—O8—O18iv | 137 (2) | O1ix—O23—In2 | 53 (2) |
O5i—O8—O17iv | 137 (3) | O1ix—O23—Al2 | 53 (2) |
O5i—O8—O11 | 59 (2) | O3i—O23—O1ix | 101 (3) |
O5i—O8—In3 | 104.6 (17) | O3i—O23—O5 | 74 (2) |
O5i—O8—Al3 | 104.6 (17) | O3i—O23—Mo5 | 128 (4) |
O5i—O8—Mo3 | 33.2 (11) | O3i—O23—In2 | 47.5 (19) |
Al4xviii—O9—In4xviii | 0.000 | O3i—O23—Al2 | 47.5 (19) |
Mo1xiii—O9—Al4xviii | 140 (3) | O19iv—O23—O3i | 121 (3) |
Mo1xiii—O9—In4xviii | 140 (3) | O19iv—O23—O1ix | 123 (3) |
O15xiii—O9—Mo1xiii | 149 (3) | O19iv—O23—O5 | 94 (2) |
O15xiii—O9—Al4xviii | 61 (3) | O19iv—O23—Mo5 | 37.4 (15) |
O15xiii—O9—In4xviii | 61 (3) | O19iv—O23—In2 | 145 (3) |
O19iv—O9—O15xiii | 72 (3) | O19iv—O23—Al2 | 145 (3) |
O19iv—O9—Mo1xiii | 136 (3) | O4ix—O23—O19iv | 158 (4) |
O19iv—O9—Al4xviii | 56.7 (17) | O4ix—O23—O3i | 49.5 (15) |
O19iv—O9—In4xviii | 56.7 (17) | O4ix—O23—O1ix | 78 (2) |
O14xiii—O9—O19iv | 101 (2) | O4ix—O23—O5 | 100 (3) |
O14xiii—O9—O15xiii | 68 (3) | O4ix—O23—Mo5 | 128 (3) |
O14xiii—O9—Mo1xiii | 110 (2) | O4ix—O23—In2 | 47.8 (17) |
O14xiii—O9—Al4xviii | 44.8 (15) | O4ix—O23—Al2 | 47.8 (17) |
O14xiii—O9—In4xviii | 44.8 (15) | O17iv—O23—O4ix | 103 (2) |
O7—O9—O14xiii | 127.6 (19) | O17iv—O23—O19iv | 55 (2) |
O7—O9—O19iv | 131 (2) | O17iv—O23—O3i | 90 (3) |
O7—O9—O15xiii | 120 (3) | O17iv—O23—O1ix | 166 (3) |
O7—O9—Mo1xiii | 35.4 (14) | O17iv—O23—O5 | 131 (2) |
O7—O9—Al4xviii | 172.3 (15) | O17iv—O23—Mo5 | 38.1 (18) |
O7—O9—In4xviii | 172.3 (15) | O17iv—O23—In2 | 137 (3) |
O12xii—O9—O7 | 133 (3) | O17iv—O23—Al2 | 137 (3) |
O12xii—O9—O14xiii | 62.2 (19) | Al1—O24—In1 | 0.000 |
O12xii—O9—O19iv | 69.1 (19) | Mo5—O24—Al1 | 125 (3) |
O12xii—O9—O15xiii | 106 (3) | Mo5—O24—In1 | 125 (3) |
O12xii—O9—Mo1xiii | 99 (3) | O6iv—O24—Mo5 | 125 (4) |
O12xii—O9—Al4xviii | 45 (2) | O6iv—O24—Al1 | 39.2 (18) |
O12xii—O9—In4xviii | 45 (2) | O6iv—O24—In1 | 39.2 (18) |
In2xx—O10—Mo6xix | 155 (3) | O13iv—O24—O6iv | 66 (3) |
Al2xx—O10—In2xx | 0.000 | O13iv—O24—Mo5 | 168 (4) |
Al2xx—O10—Mo6xix | 155 (3) | O13iv—O24—Al1 | 60 (2) |
O22xix—O10—Al2xx | 139 (3) | O13iv—O24—In1 | 60 (2) |
O22xix—O10—In2xx | 139 (3) | O16—O24—O13iv | 67.0 (17) |
O22xix—O10—Mo6xix | 55.1 (18) | O16—O24—O6iv | 85 (2) |
O5xx—O10—O22xix | 143 (3) | O16—O24—Mo5 | 107.4 (19) |
O5xx—O10—Al2xx | 47.2 (19) | O16—O24—Al1 | 46.3 (19) |
O5xx—O10—In2xx | 47.2 (19) | O16—O24—In1 | 46.3 (19) |
O5xx—O10—Mo6xix | 108 (2) | O4iv—O24—O16 | 115 (3) |
O11xxi—O10—O5xx | 65 (2) | O4iv—O24—O13iv | 70 (2) |
O11xxi—O10—O22xix | 83.5 (19) | O4iv—O24—O6iv | 118 (2) |
O11xxi—O10—Al2xx | 108 (3) | O4iv—O24—Mo5 | 105 (3) |
O11xxi—O10—In2xx | 108 (3) | O4iv—O24—Al1 | 130 (2) |
O11xxi—O10—Mo6xix | 47.6 (19) | O4iv—O24—In1 | 130 (2) |
O1xx—O10—O11xxi | 71 (2) | O19iv—O24—O4iv | 122 (3) |
O1xx—O10—O5xx | 106 (2) | O19iv—O24—O16 | 75.7 (15) |
O1xx—O10—O22xix | 80 (3) | O19iv—O24—O13iv | 142 (2) |
O1xx—O10—Al2xx | 141 (2) | O19iv—O24—O6iv | 119 (3) |
O1xx—O10—In2xx | 141 (2) | O19iv—O24—Mo5 | 31.9 (10) |
O1xx—O10—Mo6xix | 37 (2) | O19iv—O24—Al1 | 99 (2) |
O3xxii—O10—O1xx | 167 (2) | O19iv—O24—In1 | 99 (2) |
O3xxii—O10—O11xxi | 95 (3) | Mo2vii—O24—O19iv | 137 (3) |
O3xxii—O10—O5xx | 67 (3) | Mo2vii—O24—O4iv | 38.7 (12) |
O3xxii—O10—O22xix | 99 (2) | Mo2vii—O24—O16 | 83.4 (18) |
O3xxii—O10—Al2xx | 42.5 (19) | Mo2vii—O24—O13iv | 32.7 (18) |
O3xxii—O10—In2xx | 42.5 (19) | Mo2vii—O24—O6iv | 95 (2) |
O3xxii—O10—Mo6xix | 132 (3) | Mo2vii—O24—Mo5 | 139 (3) |
O1xii—O10—O3xxii | 87 (3) | Mo2vii—O24—Al1 | 92.1 (18) |
O1xii—O10—O1xx | 98 (3) | Mo2vii—O24—In1 | 92.1 (18) |
O1xii—O10—O11xxi | 111.8 (19) | O20iii—O24—Mo2vii | 119.3 (17) |
O1xii—O10—O5xx | 53.5 (18) | O20iii—O24—O19iv | 76.0 (18) |
O1xii—O10—O22xix | 163 (3) | O20iii—O24—O4iv | 158 (2) |
O1xii—O10—Al2xx | 44.4 (18) | O20iii—O24—O16 | 53 (2) |
O1xii—O10—In2xx | 44.4 (18) | O20iii—O24—O13iv | 88 (2) |
O1xii—O10—Mo6xix | 130 (3) | O20iii—O24—O6iv | 48.0 (18) |
Al3—O11—Mo6vi | 137 (2) | O20iii—O24—Mo5 | 97 (2) |
In3—O11—Al3 | 0.000 | O20iii—O24—Al1 | 27.5 (14) |
In3—O11—Mo6vi | 137 (2) | O20iii—O24—In1 | 27.5 (14) |
Symmetry codes: (i) x−1/2, −y+1/2, z; (ii) x, y−1, z; (iii) −x+1/2, y+1/2, −z+1; (iv) x−1/2, −y+3/2, z; (v) −x+1/2, y+1/2, −z; (vi) −x, −y+1, −z; (vii) x, y+1, z; (viii) x, y, z−1; (ix) −x+1, −y+1, −z; (x) x−1, y, z; (xi) −x+1/2, y−1/2, −z; (xii) −x+1, −y+1, −z+1; (xiii) x+1/2, −y+1/2, z; (xiv) x+1, y, z; (xv) −x+3/2, y−1/2, −z; (xvi) x+1/2, −y+1/2, z−1; (xvii) −x+3/2, y+1/2, −z; (xviii) x+1/2, −y+3/2, z; (xix) −x+1/2, y−1/2, −z+1; (xx) x, y, z+1; (xxi) x+1/2, −y+1/2, z+1; (xxii) x−1/2, −y+1/2, z+1; (xxiii) x−1/2, −y+1/2, z−1; (xxiv) −x+3/2, y−1/2, −z+1; (xxv) x−1, y−1, z; (xxvi) x+1, y+1, z; (xxvii) −x+3/2, y+1/2, −z+1. |
(Al1.36In0.64Mo3O12_mono_2) top
Crystal data top
Mr = 1143.4 (19) | β = 125.65 (3)° |
Monoclinic, P121/a1 | V = 2151.1 (11) Å3 |
a = 15.694 (6) Å | Z = 4 |
b = 9.2419 (7) Å | Dx = 3.531 (6) Mg m−3 |
c = 18.2507 (15) Å | T = 298 K |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
x | y | z | Biso*/Beq | Occ. (<1) | |
Mo1 | −0.0007 (8) | 0.2397 (10) | 0.4897 (6) | 0.79 (4) | |
Mo2 | 0.3612 (7) | 0.1205 (11) | 0.1308 (6) | 0.79 (4) | |
Mo3 | 0.1447 (8) | 0.1149 (9) | 0.2568 (5) | 0.79 (4) | |
Mo4 | 0.1517 (8) | 0.6092 (10) | 0.3789 (7) | 0.79 (4) | |
Mo5 | 0.3557 (7) | 0.6358 (9) | 0.2171 (5) | 0.79 (4) | |
Mo6 | −0.0132 (6) | 0.7432 (10) | 0.0136 (5) | 0.79 (4) | |
In1 | 0.3852 (10) | 0.9639 (14) | 0.3218 (9) | 0.79 (4) | 0.216 (5) |
In2 | 0.3727 (8) | 0.4538 (12) | 0.0513 (7) | 0.79 (4) | 0.216 (5) |
In3 | 0.1236 (10) | 0.4841 (11) | 0.1896 (8) | 0.79 (4) | 0.216 (5) |
In4 | 0.1168 (9) | 0.9742 (15) | 0.4282 (8) | 0.79 (4) | 0.216 (5) |
Al1 | 0.3852 (10) | 0.9639 (14) | 0.3218 (9) | 0.79 (4) | 0.784 (5) |
Al2 | 0.3727 (8) | 0.4538 (12) | 0.0513 (7) | 0.79 (4) | 0.784 (5) |
Al3 | 0.1236 (10) | 0.4841 (11) | 0.1896 (8) | 0.79 (4) | 0.784 (5) |
Al4 | 0.1168 (9) | 0.9742 (15) | 0.4282 (8) | 0.79 (4) | 0.784 (5) |
O1 | 0.565 (4) | 0.358 (5) | −0.044 (3) | 0.79 (4) | |
O2 | 0.970 (6) | 0.421 (8) | 0.142 (5) | 0.79 (4) | |
O3 | 0.807 (3) | 0.217 (6) | 0.062 (3) | 0.79 (4) | |
O4 | 0.794 (4) | 0.544 (5) | 0.049 (3) | 0.79 (4) | |
O5 | 0.515 (3) | 0.435 (6) | 0.149 (3) | 0.79 (4) | |
O6 | 0.773 (4) | 0.517 (6) | 0.283 (3) | 0.79 (4) | |
O7 | 0.445 (4) | 0.125 (5) | 0.419 (3) | 0.79 (4) | |
O8 | 0.184 (4) | 0.302 (6) | 0.264 (3) | 0.79 (4) | |
O9 | 0.542 (4) | 0.378 (5) | 0.416 (3) | 0.79 (4) | |
O10 | 0.425 (4) | 0.342 (5) | 0.990 (4) | 0.79 (4) | |
O11 | 0.090 (4) | 0.303 (4) | 0.112 (3) | 0.79 (4) | |
O12 | 0.402 (4) | 0.360 (6) | 0.488 (4) | 0.79 (4) | |
O13 | 0.864 (4) | 0.383 (7) | 0.222 (3) | 0.79 (4) | |
O14 | 0.249 (4) | 0.054 (4) | 0.526 (4) | 0.79 (4) | |
O15 | 0.113 (4) | 0.120 (7) | 0.344 (3) | 0.79 (4) | |
O16 | 0.543 (5) | 0.961 (5) | 0.375 (4) | 0.79 (4) | |
O17 | 0.771 (5) | 0.997 (6) | 0.235 (3) | 0.79 (4) | |
O18 | 0.686 (3) | 0.900 (5) | 0.303 (3) | 0.79 (4) | |
O19 | 0.969 (4) | 0.911 (5) | 0.310 (3) | 0.79 (4) | |
O20 | 0.087 (4) | 0.384 (5) | 0.582 (3) | 0.79 (4) | |
O21 | 0.167 (4) | 0.804 (7) | 0.406 (4) | 0.79 (4) | |
O22 | 0.114 (3) | 0.628 (5) | 0.097 (3) | 0.79 (4) | |
O23 | 0.370 (4) | 0.545 (5) | 0.132 (3) | 0.79 (4) | |
O24 | 0.346 (4) | 0.859 (5) | 0.221 (3) | 0.79 (4) |
Geometric parameters (Å, º) top
Mo1—O7i | 1.63 (4) | O8—O18iv | 2.84 (8) |
Mo1—O12i | 1.77 (8) | O8—O15 | 2.86 (10) |
Mo1—O20 | 1.95 (5) | O8—O2x | 2.96 (8) |
Mo1—O9i | 2.11 (6) | O8—O5i | 3.12 (7) |
Mo2—O13i | 1.63 (7) | O8—O6i | 3.19 (8) |
Mo2—O2i | 1.64 (10) | O9—Al4xviii | 1.74 (5) |
Mo2—O3i | 1.82 (5) | O9—In4xviii | 1.74 (5) |
Mo2—O4i | 1.96 (4) | O9—Mo1xiii | 2.11 (6) |
Mo2—O24ii | 3.01 (6) | O9—O15xiii | 2.17 (10) |
Mo3—O8 | 1.82 (6) | O9—O19iv | 2.51 (6) |
Mo3—O5i | 1.89 (4) | O9—O14xiii | 2.72 (7) |
Mo3—O15 | 1.93 (7) | O9—O7 | 2.80 (7) |
Mo3—O6i | 2.16 (6) | O9—O12xii | 2.81 (7) |
Mo3—O11 | 2.84 (5) | O9—O12 | 3.15 (11) |
Mo4—O14iii | 1.60 (4) | O10—Mo6xix | 1.68 (7) |
Mo4—O18iv | 1.76 (7) | O10—In2xx | 2.03 (7) |
Mo4—O16iv | 1.78 (8) | O10—Al2xx | 2.03 (7) |
Mo4—O21 | 1.85 (6) | O10—O22xix | 2.37 (7) |
Mo5—O19iv | 1.65 (4) | O10—O5xx | 2.54 (8) |
Mo5—O23 | 1.89 (7) | O10—O11xxi | 2.59 (6) |
Mo5—O17iv | 1.96 (7) | O10—O1xx | 2.60 (11) |
Mo5—O24 | 2.07 (5) | O10—O3xxii | 2.88 (10) |
Mo5—O22 | 3.08 (3) | O10—O1xii | 2.92 (7) |
Mo6—O1v | 1.61 (7) | O11—Mo6vi | 1.92 (5) |
Mo6—O10iii | 1.68 (7) | O11—Al3 | 2.05 (5) |
Mo6—O11vi | 1.92 (5) | O11—In3 | 2.05 (5) |
Mo6—O22 | 1.98 (4) | O11—O8 | 2.25 (7) |
In1—Al1 | 0.00000 | O11—O2x | 2.50 (12) |
In1—O6iv | 1.47 (6) | O11—O10xxiii | 2.59 (6) |
In1—O20iii | 1.71 (6) | O11—O5i | 2.76 (8) |
In1—O24 | 1.84 (6) | O11—Mo3 | 2.84 (5) |
In1—O16 | 2.07 (7) | O11—O17iv | 3.02 (6) |
In1—O7vii | 2.08 (5) | O11—O1i | 3.02 (9) |
In1—O13iv | 2.18 (7) | O11—O22 | 3.07 (6) |
In2—Al2 | 0.00000 | O12—Mo1xiii | 1.77 (8) |
In2—O23 | 1.72 (7) | O12—Al4xix | 2.01 (8) |
In2—O5 | 1.88 (4) | O12—In4xix | 2.01 (8) |
In2—O3i | 1.95 (6) | O12—O21xix | 2.76 (12) |
In2—O10viii | 2.03 (7) | O12—O7 | 2.78 (9) |
In2—O1ix | 2.04 (6) | O12—O9xii | 2.81 (7) |
In2—O4ix | 2.14 (5) | O12—O14iii | 2.86 (9) |
In3—Al3 | 0.00000 | O12—O19xxiv | 3.03 (8) |
In3—O17iv | 1.97 (7) | O12—O9 | 3.15 (11) |
In3—O18iv | 2.01 (5) | O13—Mo2xiii | 1.63 (7) |
In3—O8 | 2.02 (5) | O13—Al1xviii | 2.18 (7) |
In3—O11 | 2.05 (5) | O13—In1xviii | 2.18 (7) |
In3—O22 | 2.09 (5) | O13—O24xviii | 2.40 (8) |
In3—O2x | 2.12 (9) | O13—O6 | 2.59 (10) |
In4—Al4 | 0.00000 | O13—O2 | 2.79 (13) |
In4—O9iv | 1.74 (5) | O13—O16xviii | 2.93 (6) |
In4—O21 | 1.91 (7) | O13—O3 | 2.94 (8) |
In4—O14vii | 1.93 (5) | O13—O7xiii | 3.05 (8) |
In4—O12iii | 2.01 (8) | O13—O4 | 3.05 (8) |
In4—O15vii | 2.01 (7) | O14—Mo4xix | 1.60 (4) |
In4—O19x | 2.13 (4) | O14—Al4ii | 1.93 (5) |
Al1—In1 | 0.00000 | O14—In4ii | 1.93 (5) |
Al1—O6iv | 1.47 (6) | O14—O21xix | 2.59 (7) |
Al1—O20iii | 1.71 (6) | O14—O16xii | 2.65 (8) |
Al1—O24 | 1.84 (6) | O14—O18xii | 2.69 (9) |
Al1—O16 | 2.07 (7) | O14—O9i | 2.72 (7) |
Al1—O7vii | 2.08 (5) | O14—O15 | 2.77 (7) |
Al1—O13iv | 2.18 (7) | O14—O12xix | 2.86 (9) |
Al2—In2 | 0.00000 | O14—O21ii | 2.92 (7) |
Al2—O23 | 1.72 (7) | O15—Mo3 | 1.93 (7) |
Al2—O5 | 1.88 (4) | O15—Al4ii | 2.01 (7) |
Al2—O3i | 1.95 (6) | O15—In4ii | 2.01 (7) |
Al2—O10viii | 2.03 (7) | O15—O9i | 2.17 (10) |
Al2—O1ix | 2.04 (6) | O15—O19xxv | 2.75 (8) |
Al2—O4ix | 2.14 (5) | O15—O14 | 2.77 (7) |
Al3—In3 | 0.00000 | O15—O8 | 2.86 (10) |
Al3—O17iv | 1.97 (7) | O15—O5i | 2.98 (7) |
Al3—O18iv | 2.01 (5) | O15—O21ii | 3.06 (8) |
Al3—O8 | 2.02 (5) | O16—Mo4xviii | 1.78 (8) |
Al3—O11 | 2.05 (5) | O16—Al1 | 2.07 (7) |
Al3—O22 | 2.09 (5) | O16—In1 | 2.07 (7) |
Al3—O2x | 2.12 (9) | O16—O7vii | 2.61 (10) |
Al4—In4 | 0.00000 | O16—O14xii | 2.65 (8) |
Al4—O9iv | 1.74 (5) | O16—O20iii | 2.67 (12) |
Al4—O21 | 1.91 (7) | O16—O24 | 2.87 (6) |
Al4—O14vii | 1.93 (5) | O16—O13iv | 2.93 (6) |
Al4—O12iii | 2.01 (8) | O16—O21xviii | 2.97 (9) |
Al4—O15vii | 2.01 (7) | O17—Mo5xviii | 1.96 (7) |
Al4—O19x | 2.13 (4) | O17—In3xviii | 1.97 (7) |
O1—Mo6xi | 1.61 (7) | O17—Al3xviii | 1.97 (7) |
O1—In2ix | 2.04 (6) | O17—O18 | 2.47 (11) |
O1—Al2ix | 2.04 (6) | O17—O8xviii | 2.54 (9) |
O1—O5ix | 2.48 (7) | O17—O22xviii | 2.55 (6) |
O1—O23ix | 2.53 (11) | O17—O19 | 2.68 (8) |
O1—O10viii | 2.60 (11) | O17—O11xviii | 3.02 (6) |
O1—O10xii | 2.92 (7) | O17—O23xviii | 3.07 (12) |
O1—O11xiii | 3.02 (9) | O18—Mo4xviii | 1.76 (7) |
O1—O22xi | 3.19 (7) | O18—Al3xviii | 2.01 (5) |
O2—Mo2xiii | 1.64 (10) | O18—In3xviii | 2.01 (5) |
O2—Al3xiv | 2.12 (9) | O18—O17 | 2.47 (11) |
O2—In3xiv | 2.12 (9) | O18—O14xii | 2.69 (9) |
O2—O11xiv | 2.50 (12) | O18—O21xviii | 2.80 (9) |
O2—O4 | 2.52 (8) | O18—O8xviii | 2.84 (8) |
O2—O13 | 2.79 (13) | O19—Mo5xviii | 1.65 (4) |
O2—O3 | 2.81 (9) | O19—In4xiv | 2.13 (4) |
O2—O8xiv | 2.96 (8) | O19—Al4xiv | 2.13 (4) |
O3—Mo2xiii | 1.82 (5) | O19—O9xviii | 2.51 (6) |
O3—Al2xiii | 1.95 (6) | O19—O17 | 2.68 (8) |
O3—In2xiii | 1.95 (6) | O19—O23xviii | 2.69 (7) |
O3—O4xv | 2.32 (7) | O19—O21xiv | 2.71 (7) |
O3—O23xiii | 2.65 (7) | O19—O15xxvi | 2.75 (8) |
O3—O2 | 2.81 (9) | O19—O24xviii | 2.99 (6) |
O3—O10xvi | 2.88 (10) | O19—O12xxvii | 3.03 (8) |
O3—O13 | 2.94 (8) | O20—In1xix | 1.71 (6) |
O3—O5xiii | 3.01 (7) | O20—Al1xix | 1.71 (6) |
O3—O4 | 3.03 (7) | O20—Mo1 | 1.95 (5) |
O4—Mo2xiii | 1.96 (4) | O20—O7iii | 2.28 (7) |
O4—In2ix | 2.14 (5) | O20—O6xii | 2.33 (5) |
O4—Al2ix | 2.14 (5) | O20—O7i | 2.46 (6) |
O4—O3xvii | 2.32 (7) | O20—O16xix | 2.67 (12) |
O4—O2 | 2.52 (8) | O20—O24xix | 3.12 (9) |
O4—O24xviii | 2.88 (8) | O21—Mo4 | 1.85 (6) |
O4—O23ix | 2.88 (6) | O21—In4 | 1.91 (7) |
O4—O3 | 3.03 (7) | O21—Al4 | 1.91 (7) |
O4—O13 | 3.05 (8) | O21—O14iii | 2.59 (7) |
O5—Al2 | 1.88 (4) | O21—O19x | 2.71 (7) |
O5—In2 | 1.88 (4) | O21—O12iii | 2.76 (12) |
O5—Mo3xiii | 1.89 (4) | O21—O18iv | 2.80 (9) |
O5—O23 | 2.34 (9) | O21—O14vii | 2.92 (7) |
O5—O1ix | 2.48 (7) | O21—O16iv | 2.97 (9) |
O5—O10viii | 2.54 (8) | O21—O15vii | 3.06 (8) |
O5—O11xiii | 2.76 (8) | O22—Mo6 | 1.98 (4) |
O5—O15xiii | 2.98 (7) | O22—In3 | 2.09 (5) |
O5—O3i | 3.01 (7) | O22—Al3 | 2.09 (5) |
O5—O8xiii | 3.12 (7) | O22—O10iii | 2.37 (7) |
O6—Al1xviii | 1.47 (6) | O22—O17iv | 2.55 (6) |
O6—In1xviii | 1.47 (6) | O22—O11 | 3.07 (6) |
O6—Mo3xiii | 2.16 (6) | O22—Mo5 | 3.08 (3) |
O6—O20xii | 2.33 (5) | O22—O1v | 3.19 (7) |
O6—O24xviii | 2.33 (10) | O23—Al2 | 1.72 (7) |
O6—O13 | 2.59 (10) | O23—In2 | 1.72 (7) |
O6—O7xiii | 2.71 (6) | O23—Mo5 | 1.89 (7) |
O6—O8xiii | 3.19 (8) | O23—O5 | 2.34 (9) |
O7—Mo1xiii | 1.63 (4) | O23—O1ix | 2.53 (11) |
O7—Al1ii | 2.08 (5) | O23—O3i | 2.65 (7) |
O7—In1ii | 2.08 (5) | O23—O19iv | 2.69 (7) |
O7—O20xix | 2.28 (7) | O23—O4ix | 2.88 (6) |
O7—O20xiii | 2.46 (6) | O23—O17iv | 3.07 (12) |
O7—O16ii | 2.61 (10) | O24—In1 | 1.84 (6) |
O7—O6i | 2.71 (6) | O24—Al1 | 1.84 (6) |
O7—O12 | 2.78 (9) | O24—Mo5 | 2.07 (5) |
O7—O9 | 2.80 (7) | O24—O6iv | 2.33 (10) |
O7—O13i | 3.05 (8) | O24—O13iv | 2.40 (8) |
O8—Mo3 | 1.82 (6) | O24—O16 | 2.87 (6) |
O8—In3 | 2.02 (5) | O24—O4iv | 2.88 (8) |
O8—Al3 | 2.02 (5) | O24—O19iv | 2.99 (6) |
O8—O11 | 2.25 (7) | O24—Mo2vii | 3.01 (6) |
O8—O17iv | 2.54 (9) | O24—O20iii | 3.12 (9) |
O12i—Mo1—O7i | 110 (3) | O1xii—O10—O5xx | 53.5 (18) |
O20—Mo1—O12i | 122 (3) | O1xii—O10—O22xix | 163 (3) |
O20—Mo1—O7i | 86 (2) | O1xii—O10—Al2xx | 44.3 (18) |
O9i—Mo1—O20 | 125 (3) | O1xii—O10—In2xx | 44.3 (18) |
O9i—Mo1—O12i | 108 (3) | O1xii—O10—Mo6xix | 130 (3) |
O9i—Mo1—O7i | 96 (3) | Al3—O11—Mo6vi | 137 (2) |
O2i—Mo2—O13i | 117 (3) | In3—O11—Al3 | 0.000 |
O3i—Mo2—O2i | 108 (3) | In3—O11—Mo6vi | 137 (2) |
O3i—Mo2—O13i | 117 (3) | O8—O11—In3 | 56 (2) |
O4i—Mo2—O3i | 107 (2) | O8—O11—Al3 | 56 (2) |
O4i—Mo2—O2i | 88 (3) | O8—O11—Mo6vi | 167 (3) |
O4i—Mo2—O13i | 116 (3) | O2x—O11—O8 | 77 (3) |
O24ii—Mo2—O4i | 67.1 (19) | O2x—O11—In3 | 54 (2) |
O24ii—Mo2—O3i | 153 (2) | O2x—O11—Al3 | 54 (2) |
O24ii—Mo2—O2i | 98 (3) | O2x—O11—Mo6vi | 109 (2) |
O24ii—Mo2—O13i | 53 (2) | O10xxiii—O11—O2x | 85 (3) |
O5i—Mo3—O8 | 115 (2) | O10xxiii—O11—O8 | 132 (4) |
O15—Mo3—O5i | 103 (3) | O10xxiii—O11—In3 | 138 (3) |
O15—Mo3—O8 | 99 (3) | O10xxiii—O11—Al3 | 138 (3) |
O6i—Mo3—O15 | 119 (2) | O10xxiii—O11—Mo6vi | 40 (2) |
O6i—Mo3—O5i | 114 (2) | O5i—O11—O10xxiii | 56.5 (19) |
O6i—Mo3—O8 | 107 (2) | O5i—O11—O2x | 79 (3) |
O11—Mo3—O6i | 107 (2) | O5i—O11—O8 | 76 (2) |
O11—Mo3—O15 | 132 (2) | O5i—O11—In3 | 117 (3) |
O11—Mo3—O5i | 68 (2) | O5i—O11—Al3 | 117 (3) |
O11—Mo3—O8 | 52.4 (19) | O5i—O11—Mo6vi | 93.4 (19) |
O18iv—Mo4—O14iii | 107 (3) | Mo3—O11—O5i | 39.3 (11) |
O16iv—Mo4—O18iv | 133 (2) | Mo3—O11—O10xxiii | 96 (2) |
O16iv—Mo4—O14iii | 104 (3) | Mo3—O11—O2x | 86 (3) |
O21—Mo4—O16iv | 110 (3) | Mo3—O11—O8 | 39.7 (17) |
O21—Mo4—O18iv | 102 (3) | Mo3—O11—In3 | 92 (2) |
O21—Mo4—O14iii | 97 (2) | Mo3—O11—Al3 | 92 (2) |
O23—Mo5—O19iv | 99 (3) | Mo3—O11—Mo6vi | 128.0 (19) |
O17iv—Mo5—O23 | 106 (3) | O17iv—O11—Mo3 | 92.4 (16) |
O17iv—Mo5—O19iv | 95 (2) | O17iv—O11—O5i | 131 (2) |
O24—Mo5—O17iv | 123 (3) | O17iv—O11—O10xxiii | 172 (3) |
O24—Mo5—O23 | 121 (3) | O17iv—O11—O2x | 94 (3) |
O24—Mo5—O19iv | 106.5 (19) | O17iv—O11—O8 | 55 (2) |
O22—Mo5—O24 | 87.8 (17) | O17iv—O11—In3 | 40.2 (17) |
O22—Mo5—O17iv | 55.6 (17) | O17iv—O11—Al3 | 40.2 (17) |
O22—Mo5—O23 | 95.2 (18) | O17iv—O11—Mo6vi | 133 (3) |
O22—Mo5—O19iv | 150 (2) | O1i—O11—O17iv | 123 (3) |
O10iii—Mo6—O1v | 104 (3) | O1i—O11—Mo3 | 112.1 (17) |
O11vi—Mo6—O10iii | 92 (3) | O1i—O11—O5i | 90 (2) |
O11vi—Mo6—O1v | 118 (2) | O1i—O11—O10xxiii | 54 (2) |
O22—Mo6—O11vi | 117 (2) | O1i—O11—O2x | 136 (2) |
O22—Mo6—O10iii | 81 (2) | O1i—O11—O8 | 142 (3) |
O22—Mo6—O1v | 125 (2) | O1i—O11—In3 | 153 (3) |
O20iii—In1—O6iv | 94 (3) | O1i—O11—Al3 | 153 (3) |
O24—In1—O20iii | 123 (2) | O1i—O11—Mo6vi | 28.2 (14) |
O24—In1—O6iv | 89 (3) | O22—O11—O1i | 111 (2) |
O16—In1—O24 | 94 (3) | O22—O11—O17iv | 49.5 (13) |
O16—In1—O20iii | 90 (3) | O22—O11—Mo3 | 134.2 (19) |
O16—In1—O6iv | 174 (3) | O22—O11—O5i | 154 (3) |
O7vii—In1—O16 | 78 (2) | O22—O11—O10xxiii | 122.9 (18) |
O7vii—In1—O24 | 163 (3) | O22—O11—O2x | 75 (2) |
O7vii—In1—O20iii | 73 (2) | O22—O11—O8 | 95 (2) |
O7vii—In1—O6iv | 98 (3) | O22—O11—In3 | 42.7 (13) |
O13iv—In1—O7vii | 91 (2) | O22—O11—Al3 | 42.7 (13) |
O13iv—In1—O16 | 87 (2) | O22—O11—Mo6vi | 98 (2) |
O13iv—In1—O24 | 73 (2) | Al4xix—O12—Mo1xiii | 140 (3) |
O13iv—In1—O20iii | 165 (2) | In4xix—O12—Al4xix | 0.000 |
O13iv—In1—O6iv | 88 (3) | In4xix—O12—Mo1xiii | 140 (3) |
O5—In2—O23 | 81 (3) | O21xix—O12—In4xix | 44 (2) |
O3i—In2—O5 | 103 (2) | O21xix—O12—Al4xix | 44 (2) |
O3i—In2—O23 | 92 (3) | O21xix—O12—Mo1xiii | 126 (3) |
O10viii—In2—O3i | 93 (2) | O7—O12—O21xix | 118 (3) |
O10viii—In2—O5 | 81 (2) | O7—O12—In4xix | 159 (3) |
O10viii—In2—O23 | 161 (2) | O7—O12—Al4xix | 159 (3) |
O1ix—In2—O10viii | 92 (3) | O7—O12—Mo1xiii | 33.5 (15) |
O1ix—In2—O3i | 175 (3) | O9xii—O12—O7 | 152 (3) |
O1ix—In2—O5 | 78 (2) | O9xii—O12—O21xix | 81 (3) |
O1ix—In2—O23 | 84 (3) | O9xii—O12—In4xix | 37.8 (17) |
O4ix—In2—O1ix | 109.2 (19) | O9xii—O12—Al4xix | 37.8 (17) |
O4ix—In2—O10viii | 103 (2) | O9xii—O12—Mo1xiii | 119 (3) |
O4ix—In2—O3i | 68.9 (18) | O14iii—O12—O9xii | 57.4 (19) |
O4ix—In2—O5 | 171 (3) | O14iii—O12—O7 | 149 (2) |
O4ix—In2—O23 | 96 (2) | O14iii—O12—O21xix | 63 (3) |
O18iv—In3—O17iv | 77 (3) | O14iii—O12—In4xix | 42.4 (17) |
O8—In3—O18iv | 90 (2) | O14iii—O12—Al4xix | 42.4 (17) |
O8—In3—O17iv | 79 (2) | O14iii—O12—Mo1xiii | 171 (4) |
O11—In3—O8 | 67 (2) | O19xxiv—O12—O14iii | 87 (3) |
O11—In3—O18iv | 157 (2) | O19xxiv—O12—O9xii | 50.7 (16) |
O11—In3—O17iv | 97 (3) | O19xxiv—O12—O7 | 120 (2) |
O22—In3—O11 | 95 (2) | O19xxiv—O12—O21xix | 56 (2) |
O22—In3—O8 | 149 (3) | O19xxiv—O12—In4xix | 44.4 (16) |
O22—In3—O18iv | 105 (2) | O19xxiv—O12—Al4xix | 44.4 (16) |
O22—In3—O17iv | 78 (2) | O19xxiv—O12—Mo1xiii | 96 (2) |
O2x—In3—O22 | 109 (2) | O9—O12—O19xxiv | 111 (2) |
O2x—In3—O11 | 74 (3) | O9—O12—O14iii | 132 (3) |
O2x—In3—O8 | 91 (3) | O9—O12—O9xii | 100 (2) |
O2x—In3—O18iv | 109 (3) | O9—O12—O7 | 56 (2) |
O2x—In3—O17iv | 169 (3) | O9—O12—O21xix | 163 (2) |
O21—In4—O9iv | 163.7 (18) | O9—O12—In4xix | 137 (3) |
O14vii—In4—O21 | 99 (2) | O9—O12—Al4xix | 137 (3) |
O14vii—In4—O9iv | 96 (2) | O9—O12—Mo1xiii | 39 (2) |
O12iii—In4—O14vii | 93 (2) | Al1xviii—O13—Mo2xiii | 140 (4) |
O12iii—In4—O21 | 89 (3) | In1xviii—O13—Al1xviii | 0.000 |
O12iii—In4—O9iv | 97 (3) | In1xviii—O13—Mo2xiii | 140 (4) |
O15vii—In4—O12iii | 167 (3) | O24xviii—O13—In1xviii | 47 (2) |
O15vii—In4—O14vii | 89 (2) | O24xviii—O13—Al1xviii | 47 (2) |
O15vii—In4—O21 | 103 (3) | O24xviii—O13—Mo2xiii | 95 (3) |
O15vii—In4—O9iv | 70 (3) | O6—O13—O24xviii | 56 (3) |
O19x—In4—O15vii | 83 (2) | O6—O13—In1xviii | 34.7 (15) |
O19x—In4—O12iii | 94 (2) | O6—O13—Al1xviii | 34.7 (15) |
O19x—In4—O14vii | 172 (2) | O6—O13—Mo2xiii | 139 (3) |
O19x—In4—O21 | 84 (2) | O2—O13—O6 | 144 (3) |
O19x—In4—O9iv | 80.4 (19) | O2—O13—O24xviii | 89 (3) |
O20iii—Al1—O6iv | 94 (3) | O2—O13—In1xviii | 121 (3) |
O24—Al1—O20iii | 123 (2) | O2—O13—Al1xviii | 121 (3) |
O24—Al1—O6iv | 89 (3) | O2—O13—Mo2xiii | 31.6 (19) |
O16—Al1—O24 | 94 (3) | O16xviii—O13—O2 | 85 (3) |
O16—Al1—O20iii | 90 (3) | O16xviii—O13—O6 | 80 (2) |
O16—Al1—O6iv | 174 (3) | O16xviii—O13—O24xviii | 64.2 (18) |
O7vii—Al1—O16 | 78 (2) | O16xviii—O13—In1xviii | 44.9 (18) |
O7vii—Al1—O24 | 163 (3) | O16xviii—O13—Al1xviii | 44.9 (18) |
O7vii—Al1—O20iii | 73 (2) | O16xviii—O13—Mo2xiii | 115 (3) |
O7vii—Al1—O6iv | 98 (3) | O3—O13—O16xviii | 140 (3) |
O13iv—Al1—O7vii | 91 (2) | O3—O13—O2 | 59 (2) |
O13iv—Al1—O16 | 87 (2) | O3—O13—O6 | 139 (2) |
O13iv—Al1—O24 | 73 (2) | O3—O13—O24xviii | 123 (3) |
O13iv—Al1—O20iii | 165 (2) | O3—O13—In1xviii | 169 (3) |
O13iv—Al1—O6iv | 88 (3) | O3—O13—Al1xviii | 169 (3) |
O5—Al2—O23 | 81 (3) | O3—O13—Mo2xiii | 33.7 (18) |
O3i—Al2—O5 | 103 (2) | O7xiii—O13—O3 | 147 (3) |
O3i—Al2—O23 | 92 (3) | O7xiii—O13—O16xviii | 52 (2) |
O10viii—Al2—O3i | 93 (2) | O7xiii—O13—O2 | 131 (2) |
O10viii—Al2—O5 | 81 (2) | O7xiii—O13—O6 | 56.8 (19) |
O10viii—Al2—O23 | 161 (2) | O7xiii—O13—O24xviii | 90 (3) |
O1ix—Al2—O10viii | 92 (3) | O7xiii—O13—In1xviii | 43.0 (15) |
O1ix—Al2—O3i | 175 (3) | O7xiii—O13—Al1xviii | 43.0 (15) |
O1ix—Al2—O5 | 78 (2) | O7xiii—O13—Mo2xiii | 161 (3) |
O1ix—Al2—O23 | 84 (3) | O4—O13—O7xiii | 152 (3) |
O4ix—Al2—O1ix | 109.2 (19) | O4—O13—O3 | 60.8 (18) |
O4ix—Al2—O10viii | 103 (2) | O4—O13—O16xviii | 108 (3) |
O4ix—Al2—O3i | 68.9 (18) | O4—O13—O2 | 51 (2) |
O4ix—Al2—O5 | 171 (3) | O4—O13—O6 | 105 (2) |
O4ix—Al2—O23 | 96 (2) | O4—O13—O24xviii | 63 (2) |
O18iv—Al3—O17iv | 77 (3) | O4—O13—In1xviii | 110 (3) |
O8—Al3—O18iv | 90 (2) | O4—O13—Al1xviii | 110 (3) |
O8—Al3—O17iv | 79 (2) | O4—O13—Mo2xiii | 35.1 (17) |
O11—Al3—O8 | 67 (2) | Al4ii—O14—Mo4xix | 166 (5) |
O11—Al3—O18iv | 157 (2) | In4ii—O14—Al4ii | 0.000 |
O11—Al3—O17iv | 97 (3) | In4ii—O14—Mo4xix | 166 (5) |
O22—Al3—O11 | 95 (2) | O21xix—O14—In4ii | 139 (2) |
O22—Al3—O8 | 149 (3) | O21xix—O14—Al4ii | 139 (2) |
O22—Al3—O18iv | 105 (2) | O21xix—O14—Mo4xix | 45.0 (15) |
O22—Al3—O17iv | 78 (2) | O16xii—O14—O21xix | 69 (2) |
O2x—Al3—O22 | 109 (2) | O16xii—O14—In4ii | 147 (3) |
O2x—Al3—O11 | 74 (3) | O16xii—O14—Al4ii | 147 (3) |
O2x—Al3—O8 | 91 (3) | O16xii—O14—Mo4xix | 41 (2) |
O2x—Al3—O18iv | 109 (3) | O18xii—O14—O16xii | 75 (2) |
O2x—Al3—O17iv | 169 (3) | O18xii—O14—O21xix | 64 (2) |
O21—Al4—O9iv | 163.7 (18) | O18xii—O14—In4ii | 128 (4) |
O14vii—Al4—O21 | 99 (2) | O18xii—O14—Al4ii | 128 (4) |
O14vii—Al4—O9iv | 96 (2) | O18xii—O14—Mo4xix | 39 (2) |
O12iii—Al4—O14vii | 93 (2) | O9i—O14—O18xii | 107 (3) |
O12iii—Al4—O21 | 89 (3) | O9i—O14—O16xii | 169 (3) |
O12iii—Al4—O9iv | 97 (3) | O9i—O14—O21xix | 102 (2) |
O15vii—Al4—O12iii | 167 (3) | O9i—O14—In4ii | 39.4 (14) |
O15vii—Al4—O14vii | 89 (2) | O9i—O14—Al4ii | 39.4 (14) |
O15vii—Al4—O21 | 103 (3) | O9i—O14—Mo4xix | 136 (4) |
O15vii—Al4—O9iv | 70 (3) | O15—O14—O9i | 46 (2) |
O19x—Al4—O15vii | 83 (2) | O15—O14—O18xii | 149 (3) |
O19x—Al4—O12iii | 94 (2) | O15—O14—O16xii | 128 (4) |
O19x—Al4—O14vii | 172 (2) | O15—O14—O21xix | 101 (2) |
O19x—Al4—O21 | 84 (2) | O15—O14—In4ii | 46.5 (18) |
O19x—Al4—O9iv | 80.4 (19) | O15—O14—Al4ii | 46.5 (18) |
In2ix—O1—Mo6xi | 160 (4) | O15—O14—Mo4xix | 144 (3) |
Al2ix—O1—In2ix | 0.000 | O12xix—O14—O15 | 90 (2) |
Al2ix—O1—Mo6xi | 160 (4) | O12xix—O14—O9i | 60.5 (19) |
O5ix—O1—Al2ix | 48.1 (16) | O12xix—O14—O18xii | 87 (3) |
O5ix—O1—In2ix | 48.1 (16) | O12xix—O14—O16xii | 131 (2) |
O5ix—O1—Mo6xi | 130 (3) | O12xix—O14—O21xix | 140 (4) |
O23ix—O1—O5ix | 56 (2) | O12xix—O14—In4ii | 44.7 (18) |
O23ix—O1—Al2ix | 42.7 (18) | O12xix—O14—Al4ii | 44.7 (18) |
O23ix—O1—In2ix | 42.7 (18) | O12xix—O14—Mo4xix | 122 (4) |
O23ix—O1—Mo6xi | 157 (3) | O21ii—O14—O12xix | 57 (2) |
O10viii—O1—O23ix | 152 (2) | O21ii—O14—O15 | 65 (2) |
O10viii—O1—O5ix | 97 (3) | O21ii—O14—O9i | 79.5 (18) |
O10viii—O1—Al2ix | 125 (3) | O21ii—O14—O18xii | 135 (3) |
O10viii—O1—In2ix | 125 (3) | O21ii—O14—O16xii | 107 (3) |
O10viii—O1—Mo6xi | 39 (2) | O21ii—O14—O21xix | 161 (3) |
O10xii—O1—O10viii | 82 (3) | O21ii—O14—In4ii | 40.3 (15) |
O10xii—O1—O23ix | 85 (2) | O21ii—O14—Al4ii | 40.3 (15) |
O10xii—O1—O5ix | 55.4 (19) | O21ii—O14—Mo4xix | 143 (3) |
O10xii—O1—Al2ix | 43.9 (19) | Al4ii—O15—Mo3 | 135 (3) |
O10xii—O1—In2ix | 43.9 (19) | In4ii—O15—Al4ii | 0.000 |
O10xii—O1—Mo6xi | 117 (4) | In4ii—O15—Mo3 | 135 (3) |
O11xiii—O1—O10xii | 101 (3) | O9i—O15—In4ii | 49 (2) |
O11xiii—O1—O10viii | 54 (2) | O9i—O15—Al4ii | 49 (2) |
O11xiii—O1—O23ix | 154 (3) | O9i—O15—Mo3 | 167 (3) |
O11xiii—O1—O5ix | 147 (4) | O19xxv—O15—O9i | 60 (2) |
O11xiii—O1—Al2ix | 133 (2) | O19xxv—O15—In4ii | 50.3 (17) |
O11xiii—O1—In2ix | 133 (2) | O19xxv—O15—Al4ii | 50.3 (17) |
O11xiii—O1—Mo6xi | 34.2 (15) | O19xxv—O15—Mo3 | 112 (3) |
O22xi—O1—O11xiii | 64.4 (17) | O14—O15—O19xxv | 94 (2) |
O22xi—O1—O10xii | 127 (3) | O14—O15—O9i | 66 (2) |
O22xi—O1—O10viii | 47.1 (17) | O14—O15—In4ii | 44.1 (15) |
O22xi—O1—O23ix | 131 (2) | O14—O15—Al4ii | 44.1 (15) |
O22xi—O1—O5ix | 109 (2) | O14—O15—Mo3 | 127 (3) |
O22xi—O1—Al2ix | 157 (2) | O8—O15—O14 | 119 (2) |
O22xi—O1—In2ix | 157 (2) | O8—O15—O19xxv | 144 (2) |
O22xi—O1—Mo6xi | 30.4 (13) | O8—O15—O9i | 143 (3) |
Al3xiv—O2—Mo2xiii | 166 (5) | O8—O15—In4ii | 160 (3) |
In3xiv—O2—Al3xiv | 0.000 | O8—O15—Al4ii | 160 (3) |
In3xiv—O2—Mo2xiii | 166 (5) | O8—O15—Mo3 | 38.9 (18) |
O11xiv—O2—In3xiv | 52 (3) | O5i—O15—O8 | 65 (2) |
O11xiv—O2—Al3xiv | 52 (3) | O5i—O15—O14 | 153 (3) |
O11xiv—O2—Mo2xiii | 137 (4) | O5i—O15—O19xxv | 80 (2) |
O4—O2—O11xiv | 136 (4) | O5i—O15—O9i | 129 (3) |
O4—O2—In3xiv | 134 (4) | O5i—O15—In4ii | 124 (3) |
O4—O2—Al3xiv | 134 (4) | O5i—O15—Al4ii | 124 (3) |
O4—O2—Mo2xiii | 51 (2) | O5i—O15—Mo3 | 38.1 (14) |
O13—O2—O4 | 70 (3) | O21ii—O15—O5i | 97 (2) |
O13—O2—O11xiv | 144 (3) | O21ii—O15—O8 | 130 (3) |
O13—O2—In3xiv | 135 (3) | O21ii—O15—O14 | 59.8 (17) |
O13—O2—Al3xiv | 135 (3) | O21ii—O15—O19xxv | 55.4 (18) |
O13—O2—Mo2xiii | 31 (2) | O21ii—O15—O9i | 85 (3) |
O3—O2—O13 | 63 (3) | O21ii—O15—In4ii | 37.5 (19) |
O3—O2—O4 | 69 (2) | O21ii—O15—Al4ii | 37.5 (19) |
O3—O2—O11xiv | 99 (3) | O21ii—O15—Mo3 | 98 (3) |
O3—O2—In3xiv | 151 (4) | Al1—O16—Mo4xviii | 152 (3) |
O3—O2—Al3xiv | 151 (4) | In1—O16—Al1 | 0.000 |
O3—O2—Mo2xiii | 38 (2) | In1—O16—Mo4xviii | 152 (3) |
O8xiv—O2—O3 | 116 (3) | O7vii—O16—In1 | 51 (2) |
O8xiv—O2—O13 | 109 (3) | O7vii—O16—Al1 | 51 (2) |
O8xiv—O2—O4 | 174 (3) | O7vii—O16—Mo4xviii | 157 (2) |
O8xiv—O2—O11xiv | 48 (2) | O14xii—O16—O7vii | 122 (2) |
O8xiv—O2—In3xiv | 43.0 (18) | O14xii—O16—In1 | 168 (4) |
O8xiv—O2—Al3xiv | 43.0 (18) | O14xii—O16—Al1 | 168 (4) |
O8xiv—O2—Mo2xiii | 131 (4) | O14xii—O16—Mo4xviii | 35.8 (18) |
Al2xiii—O3—Mo2xiii | 132 (2) | O20iii—O16—O14xii | 129 (3) |
In2xiii—O3—Al2xiii | 0.000 | O20iii—O16—O7vii | 51 (2) |
In2xiii—O3—Mo2xiii | 132 (2) | O20iii—O16—In1 | 39.6 (18) |
O4xv—O3—In2xiii | 59 (2) | O20iii—O16—Al1 | 39.6 (18) |
O4xv—O3—Al2xiii | 59 (2) | O20iii—O16—Mo4xviii | 140 (3) |
O4xv—O3—Mo2xiii | 167 (3) | O24—O16—O20iii | 68 (2) |
O23xiii—O3—O4xv | 71 (2) | O24—O16—O14xii | 148 (3) |
O23xiii—O3—In2xiii | 41 (2) | O24—O16—O7vii | 90 (3) |
O23xiii—O3—Al2xiii | 41 (2) | O24—O16—In1 | 39.9 (18) |
O23xiii—O3—Mo2xiii | 122 (2) | O24—O16—Al1 | 39.9 (18) |
O2—O3—O23xiii | 113 (2) | O24—O16—Mo4xviii | 112 (3) |
O2—O3—O4xv | 150 (4) | O13iv—O16—O24 | 48.8 (16) |
O2—O3—In2xiii | 103 (3) | O13iv—O16—O20iii | 87 (3) |
O2—O3—Al2xiii | 103 (3) | O13iv—O16—O14xii | 142 (3) |
O2—O3—Mo2xiii | 34 (2) | O13iv—O16—O7vii | 66 (2) |
O10xvi—O3—O2 | 75 (3) | O13iv—O16—In1 | 47.8 (18) |
O10xvi—O3—O23xiii | 84 (3) | O13iv—O16—Al1 | 47.8 (18) |
O10xvi—O3—O4xv | 77 (3) | O13iv—O16—Mo4xviii | 125 (4) |
O10xvi—O3—In2xiii | 44.6 (17) | O21xviii—O16—O13iv | 138 (3) |
O10xvi—O3—Al2xiii | 44.6 (17) | O21xviii—O16—O24 | 98 (2) |
O10xvi—O3—Mo2xiii | 108 (3) | O21xviii—O16—O20iii | 105 (2) |
O13—O3—O10xvi | 130 (2) | O21xviii—O16—O14xii | 54.5 (18) |
O13—O3—O2 | 58 (3) | O21xviii—O16—O7vii | 149 (3) |
O13—O3—O23xiii | 101 (2) | O21xviii—O16—In1 | 125 (2) |
O13—O3—O4xv | 152 (4) | O21xviii—O16—Al1 | 125 (2) |
O13—O3—In2xiii | 130 (2) | O21xviii—O16—Mo4xviii | 35.8 (17) |
O13—O3—Al2xiii | 130 (2) | In3xviii—O17—Mo5xviii | 137 (3) |
O13—O3—Mo2xiii | 29.7 (18) | Al3xviii—O17—In3xviii | 0.000 |
O5xiii—O3—O13 | 96.0 (17) | Al3xviii—O17—Mo5xviii | 137 (3) |
O5xiii—O3—O10xvi | 51.0 (18) | O18—O17—Al3xviii | 52 (2) |
O5xiii—O3—O2 | 70 (2) | O18—O17—In3xviii | 52 (2) |
O5xiii—O3—O23xiii | 48 (2) | O18—O17—Mo5xviii | 118 (3) |
O5xiii—O3—O4xv | 97 (3) | O8xviii—O17—O18 | 69 (3) |
O5xiii—O3—In2xiii | 37.6 (12) | O8xviii—O17—Al3xviii | 51 (2) |
O5xiii—O3—Al2xiii | 37.6 (12) | O8xviii—O17—In3xviii | 51 (2) |
O5xiii—O3—Mo2xiii | 95.3 (17) | O8xviii—O17—Mo5xviii | 171 (4) |
O4—O3—O5xiii | 121 (2) | O22xviii—O17—O8xviii | 102 (3) |
O4—O3—O13 | 61.4 (19) | O22xviii—O17—O18 | 81 (2) |
O4—O3—O10xvi | 101 (2) | O22xviii—O17—Al3xviii | 53.2 (17) |
O4—O3—O2 | 50.9 (19) | O22xviii—O17—In3xviii | 53.2 (17) |
O4—O3—O23xiii | 160 (2) | O22xviii—O17—Mo5xviii | 85 (2) |
O4—O3—O4xv | 129.5 (19) | O19—O17—O22xviii | 122 (3) |
O4—O3—In2xiii | 145 (3) | O19—O17—O8xviii | 135 (2) |
O4—O3—Al2xiii | 145 (3) | O19—O17—O18 | 116 (2) |
O4—O3—Mo2xiii | 38.1 (14) | O19—O17—Al3xviii | 167 (3) |
In2ix—O4—Mo2xiii | 120 (3) | O19—O17—In3xviii | 167 (3) |
Al2ix—O4—In2ix | 0.000 | O19—O17—Mo5xviii | 37.8 (16) |
Al2ix—O4—Mo2xiii | 120 (3) | O11xviii—O17—O19 | 151 (3) |
O3xvii—O4—Al2ix | 51.6 (16) | O11xviii—O17—O22xviii | 66.2 (16) |
O3xvii—O4—In2ix | 51.6 (16) | O11xviii—O17—O8xviii | 46.9 (19) |
O3xvii—O4—Mo2xiii | 172 (3) | O11xviii—O17—O18 | 92 (3) |
O2—O4—O3xvii | 145 (4) | O11xviii—O17—Al3xviii | 42.4 (16) |
O2—O4—Al2ix | 153 (3) | O11xviii—O17—In3xviii | 42.4 (16) |
O2—O4—In2ix | 153 (3) | O11xviii—O17—Mo5xviii | 134 (3) |
O2—O4—Mo2xiii | 41 (2) | O23xviii—O17—O11xviii | 103 (2) |
O24xviii—O4—O2 | 84 (3) | O23xviii—O17—O19 | 55 (2) |
O24xviii—O4—O3xvii | 111 (3) | O23xviii—O17—O22xviii | 83 (2) |
O24xviii—O4—Al2ix | 111 (3) | O23xviii—O17—O8xviii | 138 (3) |
O24xviii—O4—In2ix | 111 (3) | O23xviii—O17—O18 | 151 (3) |
O24xviii—O4—Mo2xiii | 74.1 (18) | O23xviii—O17—Al3xviii | 130 (2) |
O23ix—O4—O24xviii | 147 (3) | O23xviii—O17—In3xviii | 130 (2) |
O23ix—O4—O2 | 123 (3) | O23xviii—O17—Mo5xviii | 36.3 (17) |
O23ix—O4—O3xvii | 60.0 (17) | Al3xviii—O18—Mo4xviii | 130 (3) |
O23ix—O4—Al2ix | 36.5 (16) | In3xviii—O18—Al3xviii | 0.000 |
O23ix—O4—In2ix | 36.5 (16) | In3xviii—O18—Mo4xviii | 130 (3) |
O23ix—O4—Mo2xiii | 112 (2) | O17—O18—In3xviii | 50.8 (19) |
O3—O4—O23ix | 77.2 (16) | O17—O18—Al3xviii | 50.8 (19) |
O3—O4—O24xviii | 105 (2) | O17—O18—Mo4xviii | 157 (3) |
O3—O4—O2 | 60 (2) | O14xii—O18—O17 | 125 (2) |
O3—O4—O3xvii | 137 (2) | O14xii—O18—In3xviii | 137 (3) |
O3—O4—Al2ix | 94.0 (18) | O14xii—O18—Al3xviii | 137 (3) |
O3—O4—In2ix | 94.0 (18) | O14xii—O18—Mo4xviii | 34.6 (17) |
O3—O4—Mo2xiii | 35.2 (12) | O21xviii—O18—O14xii | 56 (2) |
O13—O4—O3 | 57.8 (18) | O21xviii—O18—O17 | 152 (3) |
O13—O4—O23ix | 126 (2) | O21xviii—O18—In3xviii | 151 (2) |
O13—O4—O24xviii | 47.5 (17) | O21xviii—O18—Al3xviii | 151 (2) |
O13—O4—O2 | 59 (3) | O21xviii—O18—Mo4xviii | 40.3 (19) |
O13—O4—O3xvii | 152 (4) | O8xviii—O18—O21xviii | 146 (3) |
O13—O4—Al2ix | 115 (3) | O8xviii—O18—O14xii | 94 (2) |
O13—O4—In2ix | 115 (3) | O8xviii—O18—O17 | 57 (2) |
O13—O4—Mo2xiii | 28.7 (16) | O8xviii—O18—In3xviii | 45.2 (15) |
In2—O5—Al2 | 0.000 | O8xviii—O18—Al3xviii | 45.2 (15) |
Mo3xiii—O5—In2 | 167 (4) | O8xviii—O18—Mo4xviii | 106 (3) |
Mo3xiii—O5—Al2 | 167 (4) | In4xiv—O19—Mo5xviii | 179 (4) |
O23—O5—Mo3xiii | 129 (3) | Al4xiv—O19—In4xiv | 0.000 |
O23—O5—In2 | 46.7 (17) | Al4xiv—O19—Mo5xviii | 179 (4) |
O23—O5—Al2 | 46.7 (17) | O9xviii—O19—Al4xiv | 43.0 (13) |
O1ix—O5—O23 | 63 (3) | O9xviii—O19—In4xiv | 43.0 (13) |
O1ix—O5—Mo3xiii | 138 (3) | O9xviii—O19—Mo5xviii | 137 (3) |
O1ix—O5—In2 | 53.7 (17) | O17—O19—O9xviii | 92 (2) |
O1ix—O5—Al2 | 53.7 (17) | O17—O19—Al4xiv | 134 (3) |
O10viii—O5—O1ix | 71 (2) | O17—O19—In4xiv | 134 (3) |
O10viii—O5—O23 | 99 (2) | O17—O19—Mo5xviii | 46.8 (18) |
O10viii—O5—Mo3xiii | 131 (3) | O23xviii—O19—O17 | 70 (2) |
O10viii—O5—In2 | 52.0 (18) | O23xviii—O19—O9xviii | 120 (2) |
O10viii—O5—Al2 | 52.0 (18) | O23xviii—O19—Al4xiv | 135 (3) |
O11xiii—O5—O10viii | 58.4 (18) | O23xviii—O19—In4xiv | 135 (3) |
O11xiii—O5—O1ix | 121 (3) | O23xviii—O19—Mo5xviii | 43.9 (19) |
O11xiii—O5—O23 | 147 (2) | O21xiv—O19—O23xviii | 118 (3) |
O11xiii—O5—Mo3xiii | 72.7 (19) | O21xiv—O19—O17 | 171 (3) |
O11xiii—O5—In2 | 106 (2) | O21xiv—O19—O9xviii | 87 (2) |
O11xiii—O5—Al2 | 106 (2) | O21xiv—O19—Al4xiv | 44.4 (16) |
O15xiii—O5—O11xiii | 99 (2) | O21xiv—O19—In4xiv | 44.4 (16) |
O15xiii—O5—O10viii | 150 (3) | O21xiv—O19—Mo5xviii | 136 (3) |
O15xiii—O5—O1ix | 137 (3) | O15xxvi—O19—O21xiv | 68 (2) |
O15xiii—O5—O23 | 91 (3) | O15xxvi—O19—O23xviii | 90 (2) |
O15xiii—O5—Mo3xiii | 39.2 (18) | O15xxvi—O19—O17 | 117 (2) |
O15xiii—O5—In2 | 131 (3) | O15xxvi—O19—O9xviii | 48 (2) |
O15xiii—O5—Al2 | 131 (3) | O15xxvi—O19—Al4xiv | 46.6 (14) |
O3i—O5—O15xiii | 102 (3) | O15xxvi—O19—In4xiv | 46.6 (14) |
O3i—O5—O11xiii | 89 (2) | O15xxvi—O19—Mo5xviii | 132 (3) |
O3i—O5—O10viii | 62 (2) | O24xviii—O19—O15xxvi | 153 (3) |
O3i—O5—O1ix | 93 (2) | O24xviii—O19—O21xiv | 100 (2) |
O3i—O5—O23 | 57.7 (19) | O24xviii—O19—O23xviii | 74.5 (18) |
O3i—O5—Mo3xiii | 128 (3) | O24xviii—O19—O17 | 77.2 (19) |
O3i—O5—In2 | 39.1 (15) | O24xviii—O19—O9xviii | 158 (4) |
O3i—O5—Al2 | 39.1 (15) | O24xviii—O19—Al4xiv | 139 (2) |
O8xiii—O5—O3i | 105 (2) | O24xviii—O19—In4xiv | 139 (2) |
O8xiii—O5—O15xiii | 55.8 (19) | O24xviii—O19—Mo5xviii | 41.6 (14) |
O8xiii—O5—O11xiii | 44.5 (17) | O12xxvii—O19—O24xviii | 107 (2) |
O8xiii—O5—O10viii | 102 (2) | O12xxvii—O19—O15xxvi | 87.3 (18) |
O8xiii—O5—O1ix | 155 (3) | O12xxvii—O19—O21xiv | 57 (2) |
O8xiii—O5—O23 | 141 (3) | O12xxvii—O19—O23xviii | 175 (3) |
O8xiii—O5—Mo3xiii | 31.8 (13) | O12xxvii—O19—O17 | 115 (3) |
O8xiii—O5—In2 | 141 (3) | O12xxvii—O19—O9xviii | 60.1 (17) |
O8xiii—O5—Al2 | 141 (3) | O12xxvii—O19—Al4xiv | 41.4 (16) |
In1xviii—O6—Al1xviii | 0.000 | O12xxvii—O19—In4xiv | 41.4 (16) |
Mo3xiii—O6—In1xviii | 151 (3) | O12xxvii—O19—Mo5xviii | 140 (3) |
Mo3xiii—O6—Al1xviii | 151 (3) | Al1xix—O20—In1xix | 0.000 |
O20xii—O6—Mo3xiii | 130 (4) | Mo1—O20—Al1xix | 144 (5) |
O20xii—O6—In1xviii | 47 (2) | Mo1—O20—In1xix | 144 (5) |
O20xii—O6—Al1xviii | 47 (2) | O7iii—O20—Mo1 | 128 (2) |
O24xviii—O6—O20xii | 84 (3) | O7iii—O20—Al1xix | 61 (2) |
O24xviii—O6—Mo3xiii | 146 (2) | O7iii—O20—In1xix | 61 (2) |
O24xviii—O6—In1xviii | 52 (2) | O6xii—O20—O7iii | 72 (2) |
O24xviii—O6—Al1xviii | 52 (2) | O6xii—O20—Mo1 | 159 (2) |
O13—O6—O24xviii | 58 (3) | O6xii—O20—Al1xix | 39 (2) |
O13—O6—O20xii | 103 (3) | O6xii—O20—In1xix | 39 (2) |
O13—O6—Mo3xiii | 108 (2) | O7i—O20—O6xii | 157 (3) |
O13—O6—In1xviii | 57 (3) | O7i—O20—O7iii | 89 (2) |
O13—O6—Al1xviii | 57 (3) | O7i—O20—Mo1 | 41.4 (15) |
O7xiii—O6—O13 | 70 (2) | O7i—O20—Al1xix | 140 (3) |
O7xiii—O6—O24xviii | 100 (3) | O7i—O20—In1xix | 140 (3) |
O7xiii—O6—O20xii | 53.1 (17) | O16xix—O20—O7i | 93 (3) |
O7xiii—O6—Mo3xiii | 103 (2) | O16xix—O20—O6xii | 90 (3) |
O7xiii—O6—In1xviii | 49.3 (19) | O16xix—O20—O7iii | 63 (3) |
O7xiii—O6—Al1xviii | 49.3 (19) | O16xix—O20—Mo1 | 99 (3) |
O8xiii—O6—O7xiii | 78.0 (18) | O16xix—O20—Al1xix | 51 (2) |
O8xiii—O6—O13 | 80 (2) | O16xix—O20—In1xix | 51 (2) |
O8xiii—O6—O24xviii | 135 (3) | O24xix—O20—O16xix | 59 (2) |
O8xiii—O6—O20xii | 124 (2) | O24xix—O20—O7i | 148 (3) |
O8xiii—O6—Mo3xiii | 33.0 (13) | O24xix—O20—O6xii | 48 (2) |
O8xiii—O6—In1xviii | 119 (3) | O24xix—O20—O7iii | 91 (3) |
O8xiii—O6—Al1xviii | 119 (3) | O24xix—O20—Mo1 | 123 (3) |
Al1ii—O7—Mo1xiii | 173 (3) | O24xix—O20—Al1xix | 29.9 (15) |
In1ii—O7—Al1ii | 0.000 | O24xix—O20—In1xix | 29.9 (15) |
In1ii—O7—Mo1xiii | 173 (3) | In4—O21—Mo4 | 149 (4) |
O20xix—O7—In1ii | 45.9 (19) | Al4—O21—In4 | 0.000 |
O20xix—O7—Al1ii | 45.9 (19) | Al4—O21—Mo4 | 149 (4) |
O20xix—O7—Mo1xiii | 140 (3) | O14iii—O21—Al4 | 142 (4) |
O20xiii—O7—O20xix | 91 (2) | O14iii—O21—In4 | 142 (4) |
O20xiii—O7—In1ii | 130 (2) | O14iii—O21—Mo4 | 37.6 (14) |
O20xiii—O7—Al1ii | 130 (2) | O19x—O21—O14iii | 135 (3) |
O20xiii—O7—Mo1xiii | 52.2 (15) | O19x—O21—Al4 | 51.3 (17) |
O16ii—O7—O20xiii | 94 (2) | O19x—O21—In4 | 51.3 (17) |
O16ii—O7—O20xix | 66 (3) | O19x—O21—Mo4 | 105 (2) |
O16ii—O7—In1ii | 51.0 (17) | O12iii—O21—O19x | 67 (2) |
O16ii—O7—Al1ii | 51.0 (17) | O12iii—O21—O14iii | 97 (3) |
O16ii—O7—Mo1xiii | 124 (3) | O12iii—O21—Al4 | 47 (2) |
O6i—O7—O16ii | 83 (2) | O12iii—O21—In4 | 47 (2) |
O6i—O7—O20xiii | 143 (3) | O12iii—O21—Mo4 | 109 (3) |
O6i—O7—O20xix | 54.8 (17) | O18iv—O21—O12iii | 147 (3) |
O6i—O7—In1ii | 32.6 (16) | O18iv—O21—O19x | 110 (2) |
O6i—O7—Al1ii | 32.6 (16) | O18iv—O21—O14iii | 60 (2) |
O6i—O7—Mo1xiii | 151 (3) | O18iv—O21—Al4 | 157 (3) |
O12—O7—O6i | 115 (3) | O18iv—O21—In4 | 157 (3) |
O12—O7—O16ii | 160 (3) | O18iv—O21—Mo4 | 38 (2) |
O12—O7—O20xiii | 77 (2) | O14vii—O21—O18iv | 150 (3) |
O12—O7—O20xix | 131 (4) | O14vii—O21—O12iii | 60 (2) |
O12—O7—In1ii | 147 (2) | O14vii—O21—O19x | 92 (2) |
O12—O7—Al1ii | 147 (2) | O14vii—O21—O14iii | 118.0 (16) |
O12—O7—Mo1xiii | 36.9 (18) | O14vii—O21—Al4 | 40.8 (16) |
O9—O7—O12 | 69 (2) | O14vii—O21—In4 | 40.8 (16) |
O9—O7—O6i | 130 (2) | O14vii—O21—Mo4 | 155 (3) |
O9—O7—O16ii | 93 (3) | O16iv—O21—O14vii | 138 (4) |
O9—O7—O20xiii | 86.2 (19) | O16iv—O21—O18iv | 68 (2) |
O9—O7—O20xix | 159 (4) | O16iv—O21—O12iii | 79 (3) |
O9—O7—In1ii | 124 (3) | O16iv—O21—O19x | 78 (2) |
O9—O7—Al1ii | 124 (3) | O16iv—O21—O14iii | 57 (2) |
O9—O7—Mo1xiii | 48.5 (19) | O16iv—O21—Al4 | 114 (3) |
O13i—O7—O9 | 82 (2) | O16iv—O21—In4 | 114 (3) |
O13i—O7—O12 | 121 (2) | O16iv—O21—Mo4 | 34 (2) |
O13i—O7—O6i | 53 (2) | O15vii—O21—O16iv | 135 (2) |
O13i—O7—O16ii | 62 (2) | O15vii—O21—O14vii | 55.1 (16) |
O13i—O7—O20xiii | 152 (3) | O15vii—O21—O18iv | 121 (3) |
O13i—O7—O20xix | 91 (2) | O15vii—O21—O12iii | 87 (3) |
O13i—O7—In1ii | 45.6 (16) | O15vii—O21—O19x | 56.4 (19) |
O13i—O7—Al1ii | 45.6 (16) | O15vii—O21—O14iii | 169 (3) |
O13i—O7—Mo1xiii | 128 (3) | O15vii—O21—Al4 | 39.8 (19) |
In3—O8—Mo3 | 138 (2) | O15vii—O21—In4 | 39.8 (19) |
Al3—O8—In3 | 0.000 | O15vii—O21—Mo4 | 150 (3) |
Al3—O8—Mo3 | 138 (2) | In3—O22—Mo6 | 122 (3) |
O11—O8—Al3 | 57.2 (17) | Al3—O22—In3 | 0.000 |
O11—O8—In3 | 57.2 (17) | Al3—O22—Mo6 | 122 (3) |
O11—O8—Mo3 | 88 (2) | O10iii—O22—Al3 | 159 (3) |
O17iv—O8—O11 | 78 (3) | O10iii—O22—In3 | 159 (3) |
O17iv—O8—Al3 | 49.5 (19) | O10iii—O22—Mo6 | 44.3 (17) |
O17iv—O8—In3 | 49.5 (19) | O17iv—O22—O10iii | 140 (2) |
O17iv—O8—Mo3 | 152 (4) | O17iv—O22—Al3 | 48.9 (19) |
O18iv—O8—O17iv | 54 (2) | O17iv—O22—In3 | 48.9 (19) |
O18iv—O8—O11 | 102 (2) | O17iv—O22—Mo6 | 165 (3) |
O18iv—O8—Al3 | 45.0 (16) | O11—O22—O17iv | 64.3 (17) |
O18iv—O8—In3 | 45.0 (16) | O11—O22—O10iii | 151 (2) |
O18iv—O8—Mo3 | 154 (4) | O11—O22—Al3 | 41.9 (15) |
O15—O8—O18iv | 113 (3) | O11—O22—In3 | 41.9 (15) |
O15—O8—O17iv | 164 (3) | O11—O22—Mo6 | 118.2 (18) |
O15—O8—O11 | 117 (3) | Mo5—O22—O11 | 97.2 (14) |
O15—O8—Al3 | 132 (3) | Mo5—O22—O17iv | 39.4 (17) |
O15—O8—In3 | 132 (3) | Mo5—O22—O10iii | 101 (2) |
O15—O8—Mo3 | 42 (2) | Mo5—O22—Al3 | 87.9 (11) |
O2x—O8—O15 | 90 (3) | Mo5—O22—In3 | 87.9 (11) |
O2x—O8—O18iv | 71 (2) | Mo5—O22—Mo6 | 144 (2) |
O2x—O8—O17iv | 95 (3) | O1v—O22—Mo5 | 134.6 (17) |
O2x—O8—O11 | 55 (3) | O1v—O22—O11 | 123 (2) |
O2x—O8—Al3 | 46 (2) | O1v—O22—O17iv | 141 (3) |
O2x—O8—In3 | 46 (2) | O1v—O22—O10iii | 53 (2) |
O2x—O8—Mo3 | 96 (2) | O1v—O22—Al3 | 108 (2) |
O5i—O8—O2x | 66.8 (18) | O1v—O22—In3 | 108 (2) |
O5i—O8—O15 | 59.6 (18) | O1v—O22—Mo6 | 24.4 (13) |
O5i—O8—O18iv | 137 (2) | In2—O23—Al2 | 0.000 |
O5i—O8—O17iv | 136 (3) | Mo5—O23—In2 | 175 (4) |
O5i—O8—O11 | 59 (2) | Mo5—O23—Al2 | 175 (4) |
O5i—O8—Al3 | 104.6 (17) | O5—O23—Mo5 | 131 (2) |
O5i—O8—In3 | 104.6 (17) | O5—O23—In2 | 53 (2) |
O5i—O8—Mo3 | 33.2 (11) | O5—O23—Al2 | 53 (2) |
O6i—O8—O5i | 64.8 (16) | O1ix—O23—O5 | 61 (3) |
O6i—O8—O2x | 131 (2) | O1ix—O23—Mo5 | 131 (2) |
O6i—O8—O15 | 71 (2) | O1ix—O23—In2 | 53 (2) |
O6i—O8—O18iv | 157.9 (17) | O1ix—O23—Al2 | 53 (2) |
O6i—O8—O17iv | 116 (3) | O3i—O23—O1ix | 101 (3) |
O6i—O8—O11 | 94 (2) | O3i—O23—O5 | 74 (2) |
O6i—O8—Al3 | 148 (3) | O3i—O23—Mo5 | 128 (4) |
O6i—O8—In3 | 148 (3) | O3i—O23—In2 | 47.4 (19) |
O6i—O8—Mo3 | 40.3 (16) | O3i—O23—Al2 | 47.4 (19) |
In4xviii—O9—Al4xviii | 0.000 | O19iv—O23—O3i | 121 (3) |
Mo1xiii—O9—In4xviii | 140 (3) | O19iv—O23—O1ix | 123 (3) |
Mo1xiii—O9—Al4xviii | 140 (3) | O19iv—O23—O5 | 94 (2) |
O15xiii—O9—Mo1xiii | 149 (3) | O19iv—O23—Mo5 | 37.3 (15) |
O15xiii—O9—In4xviii | 61 (3) | O19iv—O23—In2 | 145 (3) |
O15xiii—O9—Al4xviii | 61 (3) | O19iv—O23—Al2 | 145 (3) |
O19iv—O9—O15xiii | 72 (3) | O4ix—O23—O19iv | 158 (4) |
O19iv—O9—Mo1xiii | 136 (3) | O4ix—O23—O3i | 49.4 (15) |
O19iv—O9—In4xviii | 56.7 (17) | O4ix—O23—O1ix | 78 (2) |
O19iv—O9—Al4xviii | 56.7 (17) | O4ix—O23—O5 | 100 (3) |
O14xiii—O9—O19iv | 101 (2) | O4ix—O23—Mo5 | 128 (3) |
O14xiii—O9—O15xiii | 68 (3) | O4ix—O23—In2 | 47.7 (17) |
O14xiii—O9—Mo1xiii | 110 (2) | O4ix—O23—Al2 | 47.7 (17) |
O14xiii—O9—In4xviii | 44.9 (15) | O17iv—O23—O4ix | 104 (2) |
O14xiii—O9—Al4xviii | 44.9 (15) | O17iv—O23—O19iv | 55 (2) |
O7—O9—O14xiii | 127.5 (19) | O17iv—O23—O3i | 90 (3) |
O7—O9—O19iv | 131 (2) | O17iv—O23—O1ix | 166 (3) |
O7—O9—O15xiii | 120 (3) | O17iv—O23—O5 | 131 (3) |
O7—O9—Mo1xiii | 35.4 (14) | O17iv—O23—Mo5 | 38.1 (18) |
O7—O9—In4xviii | 172.2 (15) | O17iv—O23—In2 | 137 (3) |
O7—O9—Al4xviii | 172.2 (15) | O17iv—O23—Al2 | 137 (3) |
O12xii—O9—O7 | 133 (3) | Al1—O24—In1 | 0.000 |
O12xii—O9—O14xiii | 62.1 (19) | Mo5—O24—Al1 | 125 (3) |
O12xii—O9—O19iv | 69.2 (19) | Mo5—O24—In1 | 125 (3) |
O12xii—O9—O15xiii | 106 (3) | O6iv—O24—Mo5 | 125 (4) |
O12xii—O9—Mo1xiii | 99 (3) | O6iv—O24—Al1 | 39.2 (18) |
O12xii—O9—In4xviii | 45 (2) | O6iv—O24—In1 | 39.2 (18) |
O12xii—O9—Al4xviii | 45 (2) | O13iv—O24—O6iv | 66 (3) |
O12—O9—O12xii | 80 (2) | O13iv—O24—Mo5 | 168 (4) |
O12—O9—O7 | 55 (2) | O13iv—O24—Al1 | 60 (2) |
O12—O9—O14xiii | 122 (2) | O13iv—O24—In1 | 60 (2) |
O12—O9—O19iv | 105 (3) | O16—O24—O13iv | 67.1 (17) |
O12—O9—O15xiii | 170 (2) | O16—O24—O6iv | 85 (2) |
O12—O9—Mo1xiii | 32.3 (14) | O16—O24—Mo5 | 107.4 (19) |
O12—O9—In4xviii | 125 (3) | O16—O24—Al1 | 46.1 (19) |
O12—O9—Al4xviii | 125 (3) | O16—O24—In1 | 46.1 (19) |
In2xx—O10—Mo6xix | 155 (3) | O4iv—O24—O16 | 115 (3) |
Al2xx—O10—In2xx | 0.000 | O4iv—O24—O13iv | 70 (2) |
Al2xx—O10—Mo6xix | 155 (3) | O4iv—O24—O6iv | 118 (2) |
O22xix—O10—Al2xx | 140 (3) | O4iv—O24—Mo5 | 105 (3) |
O22xix—O10—In2xx | 140 (3) | O4iv—O24—Al1 | 130 (2) |
O22xix—O10—Mo6xix | 55.1 (18) | O4iv—O24—In1 | 130 (2) |
O5xx—O10—O22xix | 143 (3) | O19iv—O24—O4iv | 122 (3) |
O5xx—O10—Al2xx | 47.1 (19) | O19iv—O24—O16 | 75.7 (15) |
O5xx—O10—In2xx | 47.1 (19) | O19iv—O24—O13iv | 142 (2) |
O5xx—O10—Mo6xix | 108 (2) | O19iv—O24—O6iv | 119 (3) |
O11xxi—O10—O5xx | 65 (2) | O19iv—O24—Mo5 | 31.9 (10) |
O11xxi—O10—O22xix | 83.6 (19) | O19iv—O24—Al1 | 99 (2) |
O11xxi—O10—Al2xx | 108 (3) | O19iv—O24—In1 | 99 (2) |
O11xxi—O10—In2xx | 108 (3) | Mo2vii—O24—O19iv | 137 (3) |
O11xxi—O10—Mo6xix | 47.7 (19) | Mo2vii—O24—O4iv | 38.8 (12) |
O1xx—O10—O11xxi | 71 (2) | Mo2vii—O24—O16 | 83.6 (18) |
O1xx—O10—O5xx | 106 (2) | Mo2vii—O24—O13iv | 32.7 (18) |
O1xx—O10—O22xix | 80 (3) | Mo2vii—O24—O6iv | 95 (2) |
O1xx—O10—Al2xx | 141 (2) | Mo2vii—O24—Mo5 | 139 (3) |
O1xx—O10—In2xx | 141 (2) | Mo2vii—O24—Al1 | 92.2 (18) |
O1xx—O10—Mo6xix | 37 (2) | Mo2vii—O24—In1 | 92.2 (18) |
O3xxii—O10—O1xx | 167 (2) | O20iii—O24—Mo2vii | 119.3 (17) |
O3xxii—O10—O11xxi | 95 (3) | O20iii—O24—O19iv | 75.9 (18) |
O3xxii—O10—O5xx | 67 (3) | O20iii—O24—O4iv | 158 (2) |
O3xxii—O10—O22xix | 99 (2) | O20iii—O24—O16 | 53 (2) |
O3xxii—O10—Al2xx | 42.5 (19) | O20iii—O24—O13iv | 88 (2) |
O3xxii—O10—In2xx | 42.5 (19) | O20iii—O24—O6iv | 48.0 (18) |
O3xxii—O10—Mo6xix | 132 (3) | O20iii—O24—Mo5 | 97 (2) |
O1xii—O10—O3xxii | 87 (3) | O20iii—O24—Al1 | 27.5 (14) |
O1xii—O10—O1xx | 98 (3) | O20iii—O24—In1 | 27.5 (14) |
O1xii—O10—O11xxi | 111.7 (19) |
Symmetry codes: (i) x−1/2, −y+1/2, z; (ii) x, y−1, z; (iii) −x+1/2, y+1/2, −z+1; (iv) x−1/2, −y+3/2, z; (v) −x+1/2, y+1/2, −z; (vi) −x, −y+1, −z; (vii) x, y+1, z; (viii) x, y, z−1; (ix) −x+1, −y+1, −z; (x) x−1, y, z; (xi) −x+1/2, y−1/2, −z; (xii) −x+1, −y+1, −z+1; (xiii) x+1/2, −y+1/2, z; (xiv) x+1, y, z; (xv) −x+3/2, y−1/2, −z; (xvi) x+1/2, −y+1/2, z−1; (xvii) −x+3/2, y+1/2, −z; (xviii) x+1/2, −y+3/2, z; (xix) −x+1/2, y−1/2, −z+1; (xx) x, y, z+1; (xxi) x+1/2, −y+1/2, z+1; (xxii) x−1/2, −y+1/2, z+1; (xxiii) x−1/2, −y+1/2, z−1; (xxiv) −x+3/2, y−1/2, −z+1; (xxv) x−1, y−1, z; (xxvi) x+1, y+1, z; (xxvii) −x+3/2, y+1/2, −z+1. |
(LL154H600_725_3h_warmup-00000.xye_2) top
(Al0.84In1.16Mo3O12_ortho_1) top
Crystal data top
Mr = 636.0 (4) | V = 1142.20 (10) Å3 |
Orthorhombic, Pbcn | Z = 4 |
a = 12.9993 (6) Å | Dx = 3.698 (2) Mg m−3 |
b = 9.3221 (5) Å | T = 723 K |
c = 9.4256 (5) Å |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
x | y | z | Biso*/Beq | Occ. (<1) | |
Al1 | 0.38039 (15) | 0.2459 (4) | 0.46884 (19) | 1.60 (3) | 0.418 (2) |
In1 | 0.38039 (15) | 0.2459 (4) | 0.46884 (19) | 1.60 (3) | 0.582 (2) |
Mo1 | 0 | 0.4678 (3) | 0.25 | 1.60 (3) | |
Mo2 | 0.35626 (15) | 0.3983 (3) | 0.11691 (18) | 1.60 (3) | |
O1 | 0.1515 (10) | 0.1071 (12) | 0.0821 (10) | 1.60 (3) | |
O2 | 0.0640 (5) | 0.3688 (13) | 0.1363 (11) | 1.60 (3) | |
O3 | 0.2828 (8) | 0.3006 (12) | 0.0055 (10) | 1.60 (3) | |
O4 | 0.4071 (6) | 0.0832 (11) | 0.3404 (11) | 1.60 (3) | |
O5 | 0.4710 (8) | 0.3069 (10) | 0.0692 (10) | 1.60 (3) | |
O6 | 0.3271 (9) | 0.3386 (10) | 0.2962 (12) | 1.60 (3) |
Geometric parameters (Å, º) top
Al1—In1 | 0.00000 | O2—O3 | 3.164 (13) |
Al1—O1i | 1.786 (11) | O3—Mo2 | 1.687 (10) |
Al1—O6 | 1.969 (11) | O3—In1vi | 2.192 (11) |
Al1—O4 | 1.971 (11) | O3—Al1vi | 2.192 (11) |
Al1—O2i | 2.039 (11) | O3—O5 | 2.519 (15) |
Al1—O5ii | 2.046 (11) | O3—O1 | 2.586 (16) |
Al1—O3i | 2.192 (11) | O3—O6vi | 2.760 (15) |
In1—Al1 | 0.00000 | O3—O6 | 2.822 (15) |
In1—O1i | 1.786 (11) | O3—O1v | 3.068 (15) |
In1—O6 | 1.969 (11) | O3—O4vi | 3.112 (13) |
In1—O4 | 1.971 (11) | O3—O2 | 3.164 (13) |
In1—O2i | 2.039 (11) | O4—Mo1vii | 1.829 (10) |
In1—O5ii | 2.046 (11) | O4—In1 | 1.971 (11) |
In1—O3i | 2.192 (11) | O4—Al1 | 1.971 (11) |
Mo1—O2iii | 1.641 (10) | O4—O6 | 2.632 (14) |
Mo1—O2 | 1.641 (10) | O4—O5ii | 2.755 (14) |
Mo1—O4iv | 1.829 (10) | O4—O2vii | 2.800 (15) |
Mo1—O4v | 1.829 (10) | O4—O2i | 2.849 (15) |
Mo2—O3 | 1.687 (10) | O4—O2ix | 2.864 (13) |
Mo2—O5 | 1.775 (11) | O4—O4ii | 2.957 (17) |
Mo2—O6 | 1.819 (11) | O4—O3i | 3.112 (13) |
Mo2—O1v | 1.976 (11) | O5—Mo2 | 1.775 (11) |
O1—In1vi | 1.786 (11) | O5—Al1ii | 2.046 (11) |
O1—Al1vi | 1.786 (11) | O5—In1ii | 2.046 (11) |
O1—Mo2vii | 1.976 (11) | O5—O3 | 2.519 (15) |
O1—O3 | 2.586 (16) | O5—O4ii | 2.755 (14) |
O1—O2 | 2.740 (16) | O5—O2x | 2.810 (15) |
O1—O6vi | 2.756 (15) | O5—O6 | 2.857 (15) |
O1—O5viii | 2.860 (16) | O5—O1x | 2.860 (16) |
O1—O3vii | 3.068 (15) | O5—O6ii | 2.931 (15) |
O2—Mo1 | 1.641 (10) | O6—Mo2 | 1.819 (11) |
O2—In1vi | 2.039 (11) | O6—In1 | 1.969 (11) |
O2—Al1vi | 2.039 (11) | O6—Al1 | 1.969 (11) |
O2—O2iii | 2.714 (19) | O6—O4 | 2.632 (14) |
O2—O1 | 2.740 (16) | O6—O1i | 2.756 (15) |
O2—O4v | 2.800 (15) | O6—O3i | 2.760 (15) |
O2—O5viii | 2.810 (15) | O6—O3 | 2.822 (15) |
O2—O4vi | 2.849 (15) | O6—O5 | 2.857 (15) |
O2—O4iv | 2.864 (13) | O6—O5ii | 2.931 (15) |
O6—Al1—O1i | 94.3 (5) | O1v—O3—O5 | 69.6 (4) |
O4—Al1—O6 | 83.8 (4) | O1v—O3—Al1vi | 119.4 (5) |
O4—Al1—O1i | 176.7 (5) | O1v—O3—In1vi | 119.4 (5) |
O2i—Al1—O4 | 90.5 (4) | O1v—O3—Mo2 | 36.2 (3) |
O2i—Al1—O6 | 174.2 (5) | O4vi—O3—O1v | 90.8 (4) |
O2i—Al1—O1i | 91.3 (5) | O4vi—O3—O6 | 127.1 (5) |
O5ii—Al1—O2i | 86.9 (3) | O4vi—O3—O6vi | 52.8 (3) |
O5ii—Al1—O4 | 86.6 (4) | O4vi—O3—O1 | 81.9 (4) |
O5ii—Al1—O6 | 93.8 (4) | O4vi—O3—O5 | 151.7 (5) |
O5ii—Al1—O1i | 96.3 (5) | O4vi—O3—Al1vi | 39.0 (3) |
O3i—Al1—O5ii | 175.1 (4) | O4vi—O3—In1vi | 39.0 (3) |
O3i—Al1—O2i | 96.7 (4) | O4vi—O3—Mo2 | 124.9 (6) |
O3i—Al1—O4 | 96.6 (4) | O2—O3—O4vi | 54.0 (3) |
O3i—Al1—O6 | 82.9 (4) | O2—O3—O1v | 88.4 (4) |
O3i—Al1—O1i | 80.4 (5) | O2—O3—O6 | 77.3 (4) |
O6—In1—O1i | 94.3 (5) | O2—O3—O6vi | 84.7 (4) |
O4—In1—O6 | 83.8 (4) | O2—O3—O1 | 55.8 (4) |
O4—In1—O1i | 176.7 (5) | O2—O3—O5 | 140.8 (5) |
O2i—In1—O4 | 90.5 (4) | O2—O3—Al1vi | 39.8 (3) |
O2i—In1—O6 | 174.2 (5) | O2—O3—In1vi | 39.8 (3) |
O2i—In1—O1i | 91.3 (5) | O2—O3—Mo2 | 99.1 (5) |
O5ii—In1—O2i | 86.9 (3) | In1—O4—Mo1vii | 148.8 (5) |
O5ii—In1—O4 | 86.6 (4) | Al1—O4—In1 | 0.000 |
O5ii—In1—O6 | 93.8 (4) | Al1—O4—Mo1vii | 148.8 (5) |
O5ii—In1—O1i | 96.3 (5) | O6—O4—Al1 | 48.1 (3) |
O3i—In1—O5ii | 175.1 (4) | O6—O4—In1 | 48.1 (3) |
O3i—In1—O2i | 96.7 (4) | O6—O4—Mo1vii | 136.0 (5) |
O3i—In1—O4 | 96.6 (4) | O5ii—O4—O6 | 65.9 (4) |
O3i—In1—O6 | 82.9 (4) | O5ii—O4—Al1 | 47.8 (3) |
O3i—In1—O1i | 80.4 (5) | O5ii—O4—In1 | 47.8 (3) |
O2—Mo1—O2iii | 111.6 (8) | O5ii—O4—Mo1vii | 102.1 (4) |
O4iv—Mo1—O2 | 111.2 (5) | O2vii—O4—O5ii | 132.5 (4) |
O4iv—Mo1—O2iii | 107.5 (4) | O2vii—O4—O6 | 126.2 (5) |
O4v—Mo1—O4iv | 107.9 (6) | O2vii—O4—Al1 | 174.2 (6) |
O4v—Mo1—O2 | 107.5 (4) | O2vii—O4—In1 | 174.2 (6) |
O4v—Mo1—O2iii | 111.2 (5) | O2vii—O4—Mo1vii | 34.0 (2) |
O5—Mo2—O3 | 93.4 (5) | O2i—O4—O2vii | 140.1 (4) |
O6—Mo2—O5 | 105.3 (5) | O2i—O4—O5ii | 60.2 (3) |
O6—Mo2—O3 | 107.1 (5) | O2i—O4—O6 | 93.7 (5) |
O1v—Mo2—O6 | 116.4 (4) | O2i—O4—Al1 | 45.7 (3) |
O1v—Mo2—O5 | 118.2 (5) | O2i—O4—In1 | 45.7 (3) |
O1v—Mo2—O3 | 113.6 (5) | O2i—O4—Mo1vii | 117.5 (4) |
Al1vi—O1—In1vi | 0.000 | O2ix—O4—O2i | 86.6 (4) |
Mo2vii—O1—Al1vi | 147.5 (7) | O2ix—O4—O2vii | 57.2 (4) |
Mo2vii—O1—In1vi | 147.5 (7) | O2ix—O4—O5ii | 95.4 (4) |
O3—O1—Mo2vii | 140.1 (6) | O2ix—O4—O6 | 157.7 (5) |
O3—O1—Al1vi | 56.7 (4) | O2ix—O4—Al1 | 128.0 (5) |
O3—O1—In1vi | 56.7 (4) | O2ix—O4—In1 | 128.0 (5) |
O2—O1—O3 | 72.8 (4) | O2ix—O4—Mo1vii | 32.3 (3) |
O2—O1—Mo2vii | 145.6 (6) | O4ii—O4—O2ix | 57.5 (3) |
O2—O1—Al1vi | 48.1 (4) | O4ii—O4—O2i | 117.1 (5) |
O2—O1—In1vi | 48.1 (4) | O4ii—O4—O2vii | 59.6 (3) |
O6vi—O1—O2 | 93.5 (4) | O4ii—O4—O5ii | 73.0 (3) |
O6vi—O1—O3 | 62.1 (4) | O4ii—O4—O6 | 103.4 (4) |
O6vi—O1—Mo2vii | 110.4 (5) | O4ii—O4—Al1 | 119.8 (3) |
O6vi—O1—Al1vi | 45.4 (3) | O4ii—O4—In1 | 119.8 (3) |
O6vi—O1—In1vi | 45.4 (3) | O4ii—O4—Mo1vii | 36.0 (3) |
O5viii—O1—O6vi | 62.9 (4) | O3i—O4—O4ii | 159.4 (3) |
O5viii—O1—O2 | 60.2 (4) | O3i—O4—O2ix | 140.3 (5) |
O5viii—O1—O3 | 101.9 (5) | O3i—O4—O2i | 63.9 (3) |
O5viii—O1—Mo2vii | 108.5 (5) | O3i—O4—O2vii | 134.3 (4) |
O5viii—O1—Al1vi | 45.3 (3) | O3i—O4—O5ii | 92.2 (4) |
O5viii—O1—In1vi | 45.3 (3) | O3i—O4—O6 | 56.7 (4) |
O3vii—O1—O5viii | 111.9 (4) | O3i—O4—Al1 | 44.4 (3) |
O3vii—O1—O6vi | 85.0 (4) | O3i—O4—In1 | 44.4 (3) |
O3vii—O1—O2 | 171.4 (6) | O3i—O4—Mo1vii | 164.1 (5) |
O3vii—O1—O3 | 113.6 (4) | Al1ii—O5—Mo2 | 166.2 (6) |
O3vii—O1—Mo2vii | 30.3 (3) | In1ii—O5—Al1ii | 0.000 |
O3vii—O1—Al1vi | 129.7 (5) | In1ii—O5—Mo2 | 166.2 (6) |
O3vii—O1—In1vi | 129.7 (5) | O3—O5—In1ii | 150.3 (5) |
In1vi—O2—Mo1 | 168.7 (6) | O3—O5—Al1ii | 150.3 (5) |
Al1vi—O2—In1vi | 0.000 | O3—O5—Mo2 | 41.9 (3) |
Al1vi—O2—Mo1 | 168.7 (6) | O4ii—O5—O3 | 127.9 (5) |
O2iii—O2—Al1vi | 146.0 (3) | O4ii—O5—In1ii | 45.6 (3) |
O2iii—O2—In1vi | 146.0 (3) | O4ii—O5—Al1ii | 45.6 (3) |
O2iii—O2—Mo1 | 34.2 (4) | O4ii—O5—Mo2 | 140.2 (5) |
O1—O2—O2iii | 113.7 (3) | O2x—O5—O4ii | 61.6 (4) |
O1—O2—Al1vi | 40.7 (3) | O2x—O5—O3 | 103.9 (4) |
O1—O2—In1vi | 40.7 (3) | O2x—O5—In1ii | 46.4 (3) |
O1—O2—Mo1 | 146.4 (6) | O2x—O5—Al1ii | 46.4 (3) |
O4v—O2—O1 | 135.1 (4) | O2x—O5—Mo2 | 144.7 (5) |
O4v—O2—O2iii | 62.6 (4) | O6—O5—O2x | 149.1 (5) |
O4v—O2—Al1vi | 149.2 (4) | O6—O5—O4ii | 102.9 (4) |
O4v—O2—In1vi | 149.2 (4) | O6—O5—O3 | 62.9 (4) |
O4v—O2—Mo1 | 38.5 (3) | O6—O5—In1ii | 141.1 (5) |
O5viii—O2—O4v | 161.4 (4) | O6—O5—Al1ii | 141.1 (5) |
O5viii—O2—O1 | 62.0 (4) | O6—O5—Mo2 | 37.9 (3) |
O5viii—O2—O2iii | 106.3 (4) | O1x—O5—O6 | 151.8 (5) |
O5viii—O2—Al1vi | 46.6 (3) | O1x—O5—O2x | 57.8 (3) |
O5viii—O2—In1vi | 46.6 (3) | O1x—O5—O4ii | 83.9 (4) |
O5viii—O2—Mo1 | 124.1 (4) | O1x—O5—O3 | 133.2 (5) |
O4vi—O2—O5viii | 58.3 (3) | O1x—O5—In1ii | 38.4 (3) |
O4vi—O2—O4v | 122.9 (4) | O1x—O5—Al1ii | 38.4 (3) |
O4vi—O2—O1 | 84.4 (4) | O1x—O5—Mo2 | 132.9 (5) |
O4vi—O2—O2iii | 148.7 (5) | O6ii—O5—O1x | 56.8 (4) |
O4vi—O2—Al1vi | 43.8 (3) | O6ii—O5—O6 | 104.6 (4) |
O4vi—O2—In1vi | 43.8 (3) | O6ii—O5—O2x | 88.4 (4) |
O4vi—O2—Mo1 | 128.2 (6) | O6ii—O5—O4ii | 55.0 (3) |
O4iv—O2—O4vi | 93.4 (4) | O6ii—O5—O3 | 167.2 (5) |
O4iv—O2—O5viii | 98.8 (4) | O6ii—O5—In1ii | 42.1 (3) |
O4iv—O2—O4v | 62.9 (4) | O6ii—O5—Al1ii | 42.1 (3) |
O4iv—O2—O1 | 158.6 (5) | O6ii—O5—Mo2 | 126.5 (5) |
O4iv—O2—O2iii | 60.2 (3) | In1—O6—Mo2 | 146.0 (7) |
O4iv—O2—Al1vi | 132.7 (5) | Al1—O6—In1 | 0.000 |
O4iv—O2—In1vi | 132.7 (5) | Al1—O6—Mo2 | 146.0 (7) |
O4iv—O2—Mo1 | 36.5 (3) | O4—O6—Al1 | 48.1 (3) |
O3—O2—O4iv | 144.1 (5) | O4—O6—In1 | 48.1 (3) |
O3—O2—O4vi | 62.1 (3) | O4—O6—Mo2 | 110.0 (5) |
O3—O2—O5viii | 90.1 (4) | O1i—O6—O4 | 88.3 (5) |
O3—O2—O4v | 106.9 (4) | O1i—O6—Al1 | 40.2 (3) |
O3—O2—O1 | 51.3 (4) | O1i—O6—In1 | 40.2 (3) |
O3—O2—O2iii | 149.2 (5) | O1i—O6—Mo2 | 146.2 (5) |
O3—O2—Al1vi | 43.5 (2) | O3i—O6—O1i | 55.9 (4) |
O3—O2—In1vi | 43.5 (2) | O3i—O6—O4 | 70.5 (4) |
O3—O2—Mo1 | 145.4 (5) | O3i—O6—Al1 | 52.0 (3) |
In1vi—O3—Mo2 | 138.9 (6) | O3i—O6—In1 | 52.0 (3) |
Al1vi—O3—In1vi | 0.000 | O3i—O6—Mo2 | 156.4 (6) |
Al1vi—O3—Mo2 | 138.9 (6) | O3—O6—O3i | 122.0 (4) |
O5—O3—Al1vi | 169.0 (6) | O3—O6—O1i | 173.2 (5) |
O5—O3—In1vi | 169.0 (6) | O3—O6—O4 | 96.9 (4) |
O5—O3—Mo2 | 44.7 (3) | O3—O6—Al1 | 145.0 (5) |
O1—O3—O5 | 126.2 (5) | O3—O6—In1 | 145.0 (5) |
O1—O3—Al1vi | 42.9 (3) | O3—O6—Mo2 | 34.8 (3) |
O1—O3—In1vi | 42.9 (3) | O5—O6—O3 | 52.7 (4) |
O1—O3—Mo2 | 125.2 (6) | O5—O6—O3i | 145.6 (5) |
O6vi—O3—O1 | 62.0 (4) | O5—O6—O1i | 133.2 (5) |
O6vi—O3—O5 | 133.1 (5) | O5—O6—O4 | 76.5 (4) |
O6vi—O3—Al1vi | 45.1 (3) | O5—O6—Al1 | 110.1 (5) |
O6vi—O3—In1vi | 45.1 (3) | O5—O6—In1 | 110.1 (5) |
O6vi—O3—Mo2 | 172.8 (5) | O5—O6—Mo2 | 36.8 (3) |
O6—O3—O6vi | 149.2 (5) | O5ii—O6—O5 | 74.2 (4) |
O6—O3—O1 | 87.2 (4) | O5ii—O6—O3 | 126.2 (5) |
O6—O3—O5 | 64.4 (4) | O5ii—O6—O3i | 96.1 (4) |
O6—O3—Al1vi | 112.1 (4) | O5ii—O6—O1i | 60.3 (4) |
O6—O3—In1vi | 112.1 (4) | O5ii—O6—O4 | 59.1 (3) |
O6—O3—Mo2 | 38.0 (3) | O5ii—O6—Al1 | 44.1 (3) |
O1v—O3—O6 | 66.3 (3) | O5ii—O6—In1 | 44.1 (3) |
O1v—O3—O6vi | 138.6 (5) | O5ii—O6—Mo2 | 104.2 (5) |
O1v—O3—O1 | 140.2 (5) |
Symmetry codes: (i) −x+1/2, −y+1/2, z+1/2; (ii) −x+1, y, −z+1/2; (iii) −x, y, −z+1/2; (iv) x−1/2, y+1/2, −z+1/2; (v) −x+1/2, y+1/2, z; (vi) −x+1/2, −y+1/2, z−1/2; (vii) −x+1/2, y−1/2, z; (viii) x−1/2, −y+1/2, −z; (ix) x+1/2, y−1/2, −z+1/2; (x) x+1/2, −y+1/2, −z. |
(Al1.36In0.64Mo3O12_ortho_2) top
Crystal data top
Mr = 575.9 (8) | V = 1089.2 (2) Å3 |
Orthorhombic, Pbcn | Z = 4 |
a = 12.8047 (12) Å | Dx = 3.512 (5) Mg m−3 |
b = 9.1777 (11) Å | T = 723 K |
c = 9.2688 (10) Å |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
x | y | z | Biso*/Beq | Occ. (<1) | |
Al1 | 0.38039 (15) | 0.2459 (4) | 0.46884 (19) | 1.60 (3) | 0.760 (5) |
In1 | 0.38039 (15) | 0.2459 (4) | 0.46884 (19) | 1.60 (3) | 0.240 (5) |
Mo1 | 0 | 0.4678 (3) | 0.25 | 1.60 (3) | |
Mo2 | 0.35626 (15) | 0.3983 (3) | 0.11691 (18) | 1.60 (3) | |
O1 | 0.1515 (10) | 0.1071 (12) | 0.0821 (10) | 1.60 (3) | |
O2 | 0.0640 (5) | 0.3688 (13) | 0.1363 (11) | 1.60 (3) | |
O3 | 0.2828 (8) | 0.3006 (12) | 0.0055 (10) | 1.60 (3) | |
O4 | 0.4071 (6) | 0.0832 (11) | 0.3404 (11) | 1.60 (3) | |
O5 | 0.4710 (8) | 0.3069 (10) | 0.0692 (10) | 1.60 (3) | |
O6 | 0.3271 (9) | 0.3386 (10) | 0.2962 (12) | 1.60 (3) |
Geometric parameters (Å, º) top
Al1—In1 | 0.00000 | O2—O3 | 3.116 (13) |
Al1—O1i | 1.757 (11) | O3—Mo2 | 1.660 (10) |
Al1—O6 | 1.937 (11) | O3—In1vi | 2.159 (10) |
Al1—O4 | 1.940 (10) | O3—Al1vi | 2.159 (10) |
Al1—O2i | 2.006 (11) | O3—O5 | 2.482 (15) |
Al1—O5ii | 2.015 (11) | O3—O1 | 2.546 (15) |
Al1—O3i | 2.159 (10) | O3—O6vi | 2.716 (15) |
In1—Al1 | 0.00000 | O3—O6 | 2.775 (15) |
In1—O1i | 1.757 (11) | O3—O1v | 3.021 (15) |
In1—O6 | 1.937 (11) | O3—O4vi | 3.064 (13) |
In1—O4 | 1.940 (10) | O3—O2 | 3.116 (13) |
In1—O2i | 2.006 (11) | O4—Mo1vii | 1.800 (10) |
In1—O5ii | 2.015 (11) | O4—In1 | 1.940 (10) |
In1—O3i | 2.159 (10) | O4—Al1 | 1.940 (10) |
Mo1—O2 | 1.615 (10) | O4—O6 | 2.591 (14) |
Mo1—O2iii | 1.615 (10) | O4—O5ii | 2.713 (14) |
Mo1—O4iv | 1.800 (10) | O4—O2vii | 2.755 (15) |
Mo1—O4v | 1.800 (10) | O4—O2i | 2.802 (14) |
Mo2—O3 | 1.660 (10) | O4—O2ix | 2.821 (13) |
Mo2—O5 | 1.748 (11) | O4—O4ii | 2.912 (17) |
Mo2—O6 | 1.789 (11) | O4—O3i | 3.064 (13) |
Mo2—O1v | 1.945 (11) | O5—Mo2 | 1.748 (11) |
O1—Al1vi | 1.757 (11) | O5—Al1ii | 2.015 (11) |
O1—In1vi | 1.757 (11) | O5—In1ii | 2.015 (11) |
O1—Mo2vii | 1.945 (11) | O5—O3 | 2.482 (15) |
O1—O3 | 2.546 (15) | O5—O4ii | 2.713 (14) |
O1—O2 | 2.697 (16) | O5—O2x | 2.765 (14) |
O1—O6vi | 2.711 (14) | O5—O6 | 2.812 (15) |
O1—O5viii | 2.816 (16) | O5—O1x | 2.816 (16) |
O1—O3vii | 3.021 (15) | O5—O6ii | 2.887 (15) |
O1—O5vii | 3.172 (15) | O5—O1v | 3.172 (15) |
O1—O6vii | 3.175 (14) | O6—Mo2 | 1.789 (11) |
O2—Mo1 | 1.615 (10) | O6—In1 | 1.937 (11) |
O2—In1vi | 2.006 (11) | O6—Al1 | 1.937 (11) |
O2—Al1vi | 2.006 (11) | O6—O4 | 2.591 (14) |
O2—O2iii | 2.670 (18) | O6—O1i | 2.711 (14) |
O2—O1 | 2.697 (16) | O6—O3i | 2.716 (15) |
O2—O4v | 2.755 (15) | O6—O3 | 2.775 (15) |
O2—O5viii | 2.765 (14) | O6—O5 | 2.812 (15) |
O2—O4vi | 2.802 (14) | O6—O5ii | 2.887 (15) |
O2—O4iv | 2.821 (13) | O6—O1v | 3.175 (14) |
O6—Al1—O1i | 94.3 (5) | O1v—O3—O5 | 69.6 (4) |
O4—Al1—O6 | 83.9 (4) | O1v—O3—Al1vi | 119.4 (5) |
O4—Al1—O1i | 176.7 (5) | O1v—O3—In1vi | 119.4 (5) |
O2i—Al1—O4 | 90.5 (4) | O1v—O3—Mo2 | 36.2 (3) |
O2i—Al1—O6 | 174.2 (5) | O4vi—O3—O1v | 90.8 (4) |
O2i—Al1—O1i | 91.3 (5) | O4vi—O3—O6 | 127.1 (5) |
O5ii—Al1—O2i | 86.9 (3) | O4vi—O3—O6vi | 52.9 (3) |
O5ii—Al1—O4 | 86.6 (4) | O4vi—O3—O1 | 81.8 (4) |
O5ii—Al1—O6 | 93.8 (4) | O4vi—O3—O5 | 151.8 (5) |
O5ii—Al1—O1i | 96.3 (5) | O4vi—O3—Al1vi | 39.0 (3) |
O3i—Al1—O5ii | 175.1 (4) | O4vi—O3—In1vi | 39.0 (3) |
O3i—Al1—O2i | 96.8 (4) | O4vi—O3—Mo2 | 124.9 (6) |
O3i—Al1—O4 | 96.6 (4) | O2—O3—O4vi | 53.9 (3) |
O3i—Al1—O6 | 82.9 (4) | O2—O3—O1v | 88.4 (4) |
O3i—Al1—O1i | 80.4 (5) | O2—O3—O6 | 77.4 (4) |
O6—In1—O1i | 94.3 (5) | O2—O3—O6vi | 84.7 (4) |
O4—In1—O6 | 83.9 (4) | O2—O3—O1 | 55.8 (4) |
O4—In1—O1i | 176.7 (5) | O2—O3—O5 | 140.9 (5) |
O2i—In1—O4 | 90.5 (4) | O2—O3—Al1vi | 39.7 (3) |
O2i—In1—O6 | 174.2 (5) | O2—O3—In1vi | 39.7 (3) |
O2i—In1—O1i | 91.3 (5) | O2—O3—Mo2 | 99.2 (5) |
O5ii—In1—O2i | 86.9 (3) | In1—O4—Mo1vii | 148.8 (5) |
O5ii—In1—O4 | 86.6 (4) | Al1—O4—In1 | 0.000 |
O5ii—In1—O6 | 93.8 (4) | Al1—O4—Mo1vii | 148.8 (5) |
O5ii—In1—O1i | 96.3 (5) | O6—O4—Al1 | 48.0 (3) |
O3i—In1—O5ii | 175.1 (4) | O6—O4—In1 | 48.0 (3) |
O3i—In1—O2i | 96.8 (4) | O6—O4—Mo1vii | 136.0 (5) |
O3i—In1—O4 | 96.6 (4) | O5ii—O4—O6 | 65.9 (4) |
O3i—In1—O6 | 82.9 (4) | O5ii—O4—Al1 | 47.9 (3) |
O3i—In1—O1i | 80.4 (5) | O5ii—O4—In1 | 47.9 (3) |
O2iii—Mo1—O2 | 111.5 (8) | O5ii—O4—Mo1vii | 102.0 (4) |
O4iv—Mo1—O2iii | 107.4 (4) | O2vii—O4—O5ii | 132.5 (4) |
O4iv—Mo1—O2 | 111.2 (5) | O2vii—O4—O6 | 126.2 (5) |
O4v—Mo1—O4iv | 107.9 (6) | O2vii—O4—Al1 | 174.2 (6) |
O4v—Mo1—O2iii | 111.2 (5) | O2vii—O4—In1 | 174.2 (6) |
O4v—Mo1—O2 | 107.4 (4) | O2vii—O4—Mo1vii | 34.0 (2) |
O5—Mo2—O3 | 93.4 (5) | O2i—O4—O2vii | 140.1 (4) |
O6—Mo2—O5 | 105.3 (5) | O2i—O4—O5ii | 60.2 (3) |
O6—Mo2—O3 | 107.1 (5) | O2i—O4—O6 | 93.7 (5) |
O1v—Mo2—O6 | 116.4 (4) | O2i—O4—Al1 | 45.7 (3) |
O1v—Mo2—O5 | 118.2 (5) | O2i—O4—In1 | 45.7 (3) |
O1v—Mo2—O3 | 113.6 (5) | O2i—O4—Mo1vii | 117.4 (4) |
In1vi—O1—Al1vi | 0.000 | O2ix—O4—O2i | 86.6 (4) |
Mo2vii—O1—In1vi | 147.5 (7) | O2ix—O4—O2vii | 57.2 (4) |
Mo2vii—O1—Al1vi | 147.5 (7) | O2ix—O4—O5ii | 95.4 (4) |
O3—O1—Mo2vii | 140.1 (6) | O2ix—O4—O6 | 157.7 (5) |
O3—O1—In1vi | 56.7 (4) | O2ix—O4—Al1 | 128.0 (5) |
O3—O1—Al1vi | 56.7 (4) | O2ix—O4—In1 | 128.0 (5) |
O2—O1—O3 | 72.8 (4) | O2ix—O4—Mo1vii | 32.2 (3) |
O2—O1—Mo2vii | 145.6 (6) | O4ii—O4—O2ix | 57.4 (3) |
O2—O1—In1vi | 48.0 (4) | O4ii—O4—O2i | 117.1 (5) |
O2—O1—Al1vi | 48.0 (4) | O4ii—O4—O2vii | 59.6 (3) |
O6vi—O1—O2 | 93.5 (4) | O4ii—O4—O5ii | 73.0 (3) |
O6vi—O1—O3 | 62.1 (4) | O4ii—O4—O6 | 103.4 (4) |
O6vi—O1—Mo2vii | 110.4 (5) | O4ii—O4—Al1 | 119.8 (3) |
O6vi—O1—In1vi | 45.4 (3) | O4ii—O4—In1 | 119.8 (3) |
O6vi—O1—Al1vi | 45.4 (3) | O4ii—O4—Mo1vii | 36.0 (3) |
O5viii—O1—O6vi | 62.9 (4) | O3i—O4—O4ii | 159.4 (3) |
O5viii—O1—O2 | 60.2 (4) | O3i—O4—O2ix | 140.3 (5) |
O5viii—O1—O3 | 102.0 (5) | O3i—O4—O2i | 64.0 (3) |
O5viii—O1—Mo2vii | 108.5 (5) | O3i—O4—O2vii | 134.3 (4) |
O5viii—O1—In1vi | 45.3 (3) | O3i—O4—O5ii | 92.2 (4) |
O5viii—O1—Al1vi | 45.3 (3) | O3i—O4—O6 | 56.7 (4) |
O3vii—O1—O5viii | 111.9 (4) | O3i—O4—Al1 | 44.4 (3) |
O3vii—O1—O6vi | 85.0 (4) | O3i—O4—In1 | 44.4 (3) |
O3vii—O1—O2 | 171.4 (6) | O3i—O4—Mo1vii | 164.1 (5) |
O3vii—O1—O3 | 113.6 (4) | Al1ii—O5—Mo2 | 166.2 (6) |
O3vii—O1—Mo2vii | 30.2 (3) | In1ii—O5—Al1ii | 0.000 |
O3vii—O1—In1vi | 129.7 (5) | In1ii—O5—Mo2 | 166.2 (6) |
O3vii—O1—Al1vi | 129.7 (5) | O3—O5—In1ii | 150.4 (5) |
O5vii—O1—O3vii | 47.2 (3) | O3—O5—Al1ii | 150.4 (5) |
O5vii—O1—O5viii | 79.6 (4) | O3—O5—Mo2 | 41.9 (3) |
O5vii—O1—O6vi | 100.0 (4) | O4ii—O5—O3 | 127.9 (5) |
O5vii—O1—O2 | 125.1 (5) | O4ii—O5—In1ii | 45.5 (3) |
O5vii—O1—O3 | 157.2 (5) | O4ii—O5—Al1ii | 45.5 (3) |
O5vii—O1—Mo2vii | 29.0 (3) | O4ii—O5—Mo2 | 140.2 (5) |
O5vii—O1—In1vi | 122.0 (5) | O2x—O5—O4ii | 61.5 (4) |
O5vii—O1—Al1vi | 122.0 (5) | O2x—O5—O3 | 103.9 (4) |
O6vii—O1—O5vii | 52.6 (3) | O2x—O5—In1ii | 46.4 (3) |
O6vii—O1—O3vii | 53.1 (3) | O2x—O5—Al1ii | 46.4 (3) |
O6vii—O1—O5viii | 126.8 (5) | O2x—O5—Mo2 | 144.7 (5) |
O6vii—O1—O6vi | 138.1 (4) | O6—O5—O2x | 149.1 (5) |
O6vii—O1—O2 | 127.6 (5) | O6—O5—O4ii | 103.0 (4) |
O6vii—O1—O3 | 131.2 (5) | O6—O5—O3 | 62.9 (4) |
O6vii—O1—Mo2vii | 30.3 (2) | O6—O5—In1ii | 141.1 (5) |
O6vii—O1—In1vi | 171.5 (7) | O6—O5—Al1ii | 141.1 (5) |
O6vii—O1—Al1vi | 171.5 (7) | O6—O5—Mo2 | 37.9 (3) |
In1vi—O2—Mo1 | 168.6 (6) | O1x—O5—O6 | 151.8 (5) |
Al1vi—O2—In1vi | 0.000 | O1x—O5—O2x | 57.8 (3) |
Al1vi—O2—Mo1 | 168.6 (6) | O1x—O5—O4ii | 83.9 (4) |
O2iii—O2—Al1vi | 146.0 (3) | O1x—O5—O3 | 133.3 (5) |
O2iii—O2—In1vi | 146.0 (3) | O1x—O5—In1ii | 38.3 (3) |
O2iii—O2—Mo1 | 34.2 (4) | O1x—O5—Al1ii | 38.3 (3) |
O1—O2—O2iii | 113.7 (3) | O1x—O5—Mo2 | 132.9 (5) |
O1—O2—Al1vi | 40.6 (3) | O6ii—O5—O1x | 56.7 (4) |
O1—O2—In1vi | 40.6 (3) | O6ii—O5—O6 | 104.7 (4) |
O1—O2—Mo1 | 146.4 (6) | O6ii—O5—O2x | 88.3 (4) |
O4v—O2—O1 | 135.1 (4) | O6ii—O5—O4ii | 55.0 (3) |
O4v—O2—O2iii | 62.6 (4) | O6ii—O5—O3 | 167.2 (5) |
O4v—O2—Al1vi | 149.1 (4) | O6ii—O5—In1ii | 42.0 (3) |
O4v—O2—In1vi | 149.1 (4) | O6ii—O5—Al1ii | 42.0 (3) |
O4v—O2—Mo1 | 38.6 (3) | O6ii—O5—Mo2 | 126.5 (5) |
O5viii—O2—O4v | 161.4 (4) | O1v—O5—O6ii | 109.8 (4) |
O5viii—O2—O1 | 62.1 (4) | O1v—O5—O1x | 100.4 (4) |
O5viii—O2—O2iii | 106.2 (4) | O1v—O5—O6 | 63.8 (3) |
O5viii—O2—Al1vi | 46.7 (3) | O1v—O5—O2x | 138.2 (4) |
O5viii—O2—In1vi | 46.7 (3) | O1v—O5—O4ii | 158.5 (4) |
O5viii—O2—Mo1 | 124.0 (4) | O1v—O5—O3 | 63.2 (4) |
O4vi—O2—O5viii | 58.3 (3) | O1v—O5—In1ii | 135.6 (5) |
O4vi—O2—O4v | 122.8 (4) | O1v—O5—Al1ii | 135.6 (5) |
O4vi—O2—O1 | 84.4 (4) | O1v—O5—Mo2 | 32.7 (3) |
O4vi—O2—O2iii | 148.7 (5) | In1—O6—Mo2 | 145.9 (7) |
O4vi—O2—Al1vi | 43.8 (3) | Al1—O6—In1 | 0.000 |
O4vi—O2—In1vi | 43.8 (3) | Al1—O6—Mo2 | 145.9 (7) |
O4vi—O2—Mo1 | 128.1 (6) | O4—O6—Al1 | 48.1 (3) |
O4iv—O2—O4vi | 93.4 (4) | O4—O6—In1 | 48.1 (3) |
O4iv—O2—O5viii | 98.8 (4) | O4—O6—Mo2 | 110.0 (5) |
O4iv—O2—O4v | 62.9 (4) | O1i—O6—O4 | 88.4 (5) |
O4iv—O2—O1 | 158.6 (5) | O1i—O6—Al1 | 40.3 (3) |
O4iv—O2—O2iii | 60.2 (3) | O1i—O6—In1 | 40.3 (3) |
O4iv—O2—Al1vi | 132.7 (5) | O1i—O6—Mo2 | 146.2 (5) |
O4iv—O2—In1vi | 132.7 (5) | O3i—O6—O1i | 56.0 (4) |
O4iv—O2—Mo1 | 36.5 (3) | O3i—O6—O4 | 70.5 (4) |
O3—O2—O4iv | 144.1 (5) | O3i—O6—Al1 | 52.1 (3) |
O3—O2—O4vi | 62.1 (3) | O3i—O6—In1 | 52.1 (3) |
O3—O2—O5viii | 90.1 (4) | O3i—O6—Mo2 | 156.3 (6) |
O3—O2—O4v | 106.8 (4) | O3—O6—O3i | 121.9 (4) |
O3—O2—O1 | 51.3 (4) | O3—O6—O1i | 173.2 (5) |
O3—O2—O2iii | 149.2 (5) | O3—O6—O4 | 96.9 (4) |
O3—O2—Al1vi | 43.5 (2) | O3—O6—Al1 | 145.0 (5) |
O3—O2—In1vi | 43.5 (2) | O3—O6—In1 | 145.0 (5) |
O3—O2—Mo1 | 145.4 (5) | O3—O6—Mo2 | 34.9 (3) |
In1vi—O3—Mo2 | 138.9 (6) | O5—O6—O3 | 52.7 (4) |
Al1vi—O3—In1vi | 0.000 | O5—O6—O3i | 145.6 (5) |
Al1vi—O3—Mo2 | 138.9 (6) | O5—O6—O1i | 133.2 (5) |
O5—O3—Al1vi | 169.0 (6) | O5—O6—O4 | 76.5 (4) |
O5—O3—In1vi | 169.0 (6) | O5—O6—Al1 | 110.0 (5) |
O5—O3—Mo2 | 44.7 (3) | O5—O6—In1 | 110.0 (5) |
O1—O3—O5 | 126.2 (5) | O5—O6—Mo2 | 36.9 (3) |
O1—O3—Al1vi | 42.9 (3) | O5ii—O6—O5 | 74.1 (4) |
O1—O3—In1vi | 42.9 (3) | O5ii—O6—O3 | 126.2 (5) |
O1—O3—Mo2 | 125.3 (6) | O5ii—O6—O3i | 96.2 (4) |
O6vi—O3—O1 | 61.9 (4) | O5ii—O6—O1i | 60.3 (4) |
O6vi—O3—O5 | 133.1 (5) | O5ii—O6—O4 | 59.1 (3) |
O6vi—O3—Al1vi | 45.0 (3) | O5ii—O6—Al1 | 44.2 (3) |
O6vi—O3—In1vi | 45.0 (3) | O5ii—O6—In1 | 44.2 (3) |
O6vi—O3—Mo2 | 172.8 (5) | O5ii—O6—Mo2 | 104.2 (5) |
O6—O3—O6vi | 149.2 (5) | O1v—O6—O5ii | 105.7 (4) |
O6—O3—O1 | 87.3 (4) | O1v—O6—O5 | 63.6 (4) |
O6—O3—O5 | 64.4 (4) | O1v—O6—O3 | 60.6 (4) |
O6—O3—Al1vi | 112.1 (4) | O1v—O6—O3i | 148.9 (5) |
O6—O3—In1vi | 112.1 (4) | O1v—O6—O1i | 117.4 (3) |
O6—O3—Mo2 | 38.0 (3) | O1v—O6—O4 | 140.1 (5) |
O1v—O3—O6 | 66.3 (3) | O1v—O6—Al1 | 145.8 (5) |
O1v—O3—O6vi | 138.6 (5) | O1v—O6—In1 | 145.8 (5) |
O1v—O3—O1 | 140.2 (5) | O1v—O6—Mo2 | 33.3 (3) |
Symmetry codes: (i) −x+1/2, −y+1/2, z+1/2; (ii) −x+1, y, −z+1/2; (iii) −x, y, −z+1/2; (iv) x−1/2, y+1/2, −z+1/2; (v) −x+1/2, y+1/2, z; (vi) −x+1/2, −y+1/2, z−1/2; (vii) −x+1/2, y−1/2, z; (viii) x−1/2, −y+1/2, −z; (ix) x+1/2, y−1/2, −z+1/2; (x) x+1/2, −y+1/2, −z. |
(LL154H600_725_3h_warmup-00299.xye_2) top