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Crystal data for Mg3V10O28.28H2O were determined from oscillation, Weissenberg and precession photographs using Cu Kα radiation (λ = 1.54178 Å). The substance is triclinic, space group P{\bar 1}, Z = 2, and lattice constants a = 10.53 (5), b = 10.73 (6), c = 21.28 (9) Å, α = 90.2(1), β = 97.5(2) and γ = 104.1(3)°, V = 2310 (25) Å3 and the measured and calculated densities are 2.17(10) and 2.20 Mg m−3, respectively. The crystals were also characterized by TG/DTA measurements and vibrational spectroscopy.

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