Polyoxometalate-like structure of new potassium tri­phenyl­sil­oxides: [K₆(OSiPh₃)₆(C₃H₇OH)(H₂O)]·2C₆H₅CH₃ and [K₆(OSiPh₃)₆(H₂O)₂]

The synthesis and structural characterization of two new potassium tri­phenyl­sil­oxides, namely, aqua(­propan-2-o­l)hexa­kis­(tri­phenyl­silanolato)hexa­po­tas­sium toluene disolvate, [K₆(C₁₈H₁₅OSi)₆(C₃H₈O)(H₂O)]·2C₇H₈, and di­aqua­hexa­kis­(tri­phenyl­silanolato)hexa­potassium, [K₆(C₁₈H₁₅OSi)₆(H₂O)₂], are reported. Both com­pounds crystallize in the triclinic space group P. The structure in each case resembles an alkali metal polyoxometalate-like structure, in which electrostatic inter­actions are observed in the metal–oxygen core. Furthermore, both com­pounds also resemble a reverse micelles-like architecture, in which the hydro­philic core is enclosed in a hydro­phobic shell. The cores of the com­plexes are flanked by hydro­phobic aromatic rings derived from Ph₃SiO⁻ anions, where intra­molecular π-inter­actions between the aromatic rings and potassium cations stabilize the cores of the crystals. Moreover, in both structures, the presence of hydrogen bonds is observed; until now, no crystal structures have been described containing K atoms and tri­phenyl­sil­oxide mol­ecules in which the presence of hydrogen bonds was confirmed. Thus, these coordination entities could be considered as attractive reagents for further synthetic protocols towards heterometallic com­plexes.

Computing details

For both structures, data collection: CrysAlis PRO (Rigaku OD, 2020); cell refinement: CrysAlis PRO (Rigaku OD, 2020); data reduction: CrysAlis PRO (Rigaku OD, 2020); program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL2018 (Sheldrick, 2015).

(µ₆-Aqua)(µ₃-propan-2-ol)pentakis(µ₃-triphenylsilanolato)(µ₂-triphenylsilanolato)hexapotassium toluene disolvate (u777a)

Crystal data

[K6(C18H15OSi)6(C3H8O)(H2O)]·2C7H8	Z = 2
Mr = 2149.31	F(000) = 2256
Triclinic, P1	Dx = 1.266 Mg m^−3
a = 13.081 (2) Å	Cu Kα radiation, λ = 1.54184 Å
b = 14.960 (3) Å	Cell parameters from 43113 reflections
c = 31.017 (4) Å	θ = 2.8–60°
α = 82.52 (2)°	µ = 3.12 mm^−1
β = 87.24 (2)°	T = 100 K
γ = 69.51 (2)°	Needle, colorless
V = 5637.4 (18) Å^3	0.31 × 0.07 × 0.06 mm

Data collection

XtaLAB Synergy R, DW system, HyPix-Arc 150 diffractometer	20072 independent reflections
Radiation source: Rotating-anode X-ray tube, Rigaku (Cu) X-ray Source	15683 reflections with I > 2σ(I)
Mirror monochromator	Rint = 0.091
Detector resolution: 10.0000 pixels mm^-1	θmax = 67.0°, θmin = 2.9°
Absorption correction: analytical [CrysAlis PRO (Rigaku OD, 2020), based on expressions derived by Clark & Reid (1995)]	h = −15→15
Tmin = 0.569, Tmax = 0.869	k = −17→17
97762 measured reflections	l = −37→37

Refinement

Refinement on F^2	16 restraints
Least-squares matrix: full	Hydrogen site location: mixed
R[F^2 > 2σ(F^2)] = 0.077	H-atom parameters constrained
wR(F^2) = 0.221	w = 1/[σ^2(Fo^2) + (0.1182P)^2 + 6.1369P], where P = (Fo^2 + 2Fc^2)/3
S = 1.10	(Δ/σ)max = 0.001
20072 reflections	Δρmax = 0.96 e Å^−3
1250 parameters	Δρmin = −0.58 e Å^−3

Special details

Geometry. All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes.

Refinement. Diffraction data for 1 and 2 were collected at 100 K on an XCALIBUR PX monocrystalline diffractometer with a large CCD camera using Cu Kα radiation (λ = 1.54184 Å). The CrysAlisPro software from Oxford Diffraction was used to determine cell parameters, data reduction, and absorption correction. The structures were solved by direct methods (SHELXS97) and refined using the least-squares technique (SHELXL2013).

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Ų)

	x	y	z	Uiso*/Ueq	Occ. (<1)
O1W	0.4928 (2)	0.6821 (2)	0.21617 (9)	0.0389 (6)
H1W	0.4368	0.7278	0.2068	0.058*
H2W	0.5139	0.6410	0.1986	0.058*
K1	0.45134 (7)	0.74130 (6)	0.11190 (3)	0.0350 (2)
K2	0.53723 (7)	0.88948 (7)	0.18830 (3)	0.0404 (2)
K3	0.72316 (8)	0.57815 (7)	0.17891 (3)	0.0426 (2)
K4	0.35004 (7)	0.81118 (7)	0.27618 (3)	0.0392 (2)
K5	0.52696 (8)	0.51277 (7)	0.27820 (3)	0.0408 (2)
K6	0.63599 (7)	0.69406 (7)	0.28138 (3)	0.0404 (2)
O1	0.6448 (2)	0.77325 (19)	0.12726 (9)	0.0341 (6)
Si1	0.70036 (8)	0.77269 (7)	0.08033 (3)	0.0289 (2)
C1A	0.5950 (3)	0.7954 (3)	0.03661 (12)	0.0303 (8)
C2A	0.5106 (3)	0.8836 (3)	0.03054 (14)	0.0394 (9)
H2A	0.5119	0.9333	0.0465	0.047*
C3A	0.4249 (4)	0.9022 (3)	0.00239 (16)	0.0455 (11)
H3A	0.3683	0.9632	−0.0004	0.055*
C4A	0.4219 (4)	0.8313 (4)	−0.02185 (16)	0.0484 (11)
H4A	0.3633	0.8433	−0.0413	0.058*
C5A	0.5049 (4)	0.7435 (3)	−0.01725 (15)	0.0425 (10)
H5A	0.5042	0.6948	−0.0339	0.051*
C6A	0.5904 (3)	0.7254 (3)	0.01180 (13)	0.0343 (8)
H6A	0.6466	0.6641	0.0147	0.041*
C1B	0.7649 (3)	0.8686 (3)	0.06927 (13)	0.0339 (8)
C2B	0.7621 (3)	0.9281 (3)	0.10037 (14)	0.0394 (9)
H2B	0.7218	0.9236	0.1264	0.047*
C3B	0.8160 (4)	0.9943 (3)	0.09491 (16)	0.0458 (10)
H3B	0.8125	1.0342	0.1168	0.055*
C4B	0.8746 (4)	1.0010 (3)	0.05733 (16)	0.0448 (10)
H4B	0.9143	1.0439	0.0537	0.054*
C5B	0.8758 (3)	0.9460 (3)	0.02515 (15)	0.0420 (10)
H5B	0.9136	0.9531	−0.0013	0.050*
C6B	0.8220 (3)	0.8798 (3)	0.03098 (14)	0.0372 (9)
H6B	0.8242	0.8416	0.0085	0.045*
C1C	0.8076 (3)	0.6525 (3)	0.07321 (12)	0.0306 (8)
C2C	0.9148 (3)	0.6414 (3)	0.06115 (17)	0.0483 (11)
H2C	0.9366	0.6961	0.0567	0.058*
C3C	0.9903 (4)	0.5516 (4)	0.0555 (2)	0.0667 (17)
H3C	1.0627	0.5460	0.0468	0.080*
C4C	0.9616 (4)	0.4705 (3)	0.06239 (19)	0.0577 (13)
H4C	1.0133	0.4096	0.0577	0.069*
C5C	0.8575 (4)	0.4784 (3)	0.07604 (14)	0.0402 (9)
H5C	0.8378	0.4227	0.0823	0.048*
C6C	0.7815 (3)	0.5687 (3)	0.08060 (12)	0.0331 (8)
H6C	0.7092	0.5737	0.0891	0.040*
O2	0.3591 (2)	0.8530 (2)	0.18254 (10)	0.0391 (6)
Si2	0.24249 (8)	0.91681 (8)	0.16263 (4)	0.0331 (2)
C1D	0.2011 (3)	0.8484 (3)	0.12363 (14)	0.0339 (8)
C2D	0.1946 (4)	0.7579 (3)	0.13785 (15)	0.0426 (10)
H2D	0.2050	0.7342	0.1678	0.051*
C3D	0.1736 (4)	0.7015 (3)	0.10965 (18)	0.0535 (12)
H3D	0.1699	0.6402	0.1204	0.064*
C4D	0.1581 (4)	0.7348 (3)	0.06603 (17)	0.0486 (11)
H4D	0.1421	0.6972	0.0467	0.058*
C5D	0.1658 (4)	0.8222 (4)	0.05080 (17)	0.0527 (12)
H5D	0.1567	0.8446	0.0206	0.063*
C6D	0.1867 (4)	0.8783 (3)	0.07906 (16)	0.0452 (10)
H6D	0.1914	0.9389	0.0678	0.054*
C1E	0.2425 (3)	1.0317 (3)	0.12975 (13)	0.0351 (9)
C2E	0.3303 (4)	1.0350 (3)	0.10350 (14)	0.0418 (10)
H2E	0.3944	0.9795	0.1045	0.050*
C3E	0.3276 (4)	1.1160 (3)	0.07605 (16)	0.0490 (11)
H3E	0.3892	1.1152	0.0583	0.059*
C4E	0.2376 (4)	1.1972 (3)	0.07411 (15)	0.0492 (11)
H4E	0.2346	1.2526	0.0546	0.059*
C5E	0.1511 (5)	1.1973 (4)	0.10101 (19)	0.0636 (15)
H5E	0.0887	1.2542	0.1007	0.076*
C6E	0.1531 (4)	1.1158 (3)	0.12872 (17)	0.0534 (12)
H6E	0.0924	1.1178	0.1471	0.064*
C1F	0.1319 (3)	0.9532 (3)	0.20435 (14)	0.0385 (9)
C2F	0.1464 (4)	0.9987 (3)	0.23949 (15)	0.0460 (10)
H2F	0.2142	1.0070	0.2426	0.055*
C3F	0.0646 (5)	1.0314 (4)	0.26946 (17)	0.0623 (15)
H3F	0.0764	1.0616	0.2929	0.075*
C4F	−0.0345 (5)	1.0200 (4)	0.2652 (2)	0.0701 (17)
H4F	−0.0906	1.0416	0.2860	0.084*
C5F	−0.0528 (4)	0.9771 (4)	0.2308 (2)	0.0674 (16)
H5F	−0.1215	0.9702	0.2277	0.081*
C6F	0.0301 (4)	0.9445 (4)	0.20098 (17)	0.0513 (12)
H6F	0.0170	0.9151	0.1774	0.062*
O3	0.7246 (2)	0.5091 (2)	0.26060 (9)	0.0402 (7)
Si3	0.83535 (9)	0.43955 (8)	0.28285 (4)	0.0393 (3)
C1G	0.9508 (3)	0.3970 (3)	0.24288 (14)	0.0396 (9)
C2G	1.0162 (4)	0.3008 (3)	0.24209 (17)	0.0500 (11)
H2G	1.0008	0.2528	0.2617	0.060*
C3G	1.1030 (4)	0.2736 (4)	0.21344 (19)	0.0598 (14)
H3G	1.1455	0.2075	0.2134	0.072*
C4G	1.1286 (4)	0.3420 (4)	0.18477 (19)	0.0619 (14)
H4G	1.1896	0.3231	0.1658	0.074*
C5G	1.0650 (4)	0.4373 (4)	0.18397 (18)	0.0588 (13)
H5G	1.0803	0.4847	0.1639	0.071*
C6G	0.9779 (4)	0.4637 (4)	0.21292 (16)	0.0482 (11)
H6G	0.9351	0.5298	0.2123	0.058*
C1H	0.8226 (4)	0.3285 (4)	0.31497 (17)	0.0538 (12)
C2H	0.7576 (5)	0.2809 (4)	0.30088 (19)	0.0637 (15)
H2H	0.7165	0.3066	0.2749	0.076*
C3H	0.7520 (6)	0.1957 (4)	0.3245 (3)	0.083 (2)
H3H	0.7064	0.1651	0.3148	0.099*
C4H	0.8116 (7)	0.1574 (5)	0.3612 (3)	0.110 (3)
H4H	0.8102	0.0986	0.3765	0.132*
C5H	0.8741 (7)	0.2035 (7)	0.3762 (3)	0.136 (4)
H5H	0.9140	0.1772	0.4025	0.163*
C6H	0.8798 (5)	0.2881 (6)	0.3536 (3)	0.102 (3)
H6H	0.9235	0.3190	0.3647	0.123*
C1I	0.8900 (4)	0.5012 (4)	0.32098 (15)	0.0513 (12)
C2I	0.9975 (4)	0.4987 (4)	0.32028 (19)	0.0617 (14)
H2I	1.0477	0.4608	0.3009	0.074*
C3I	1.0341 (6)	0.5489 (6)	0.3466 (2)	0.084 (2)
H3I	1.1082	0.5451	0.3454	0.101*
C4I	0.9621 (7)	0.6046 (6)	0.3746 (2)	0.098 (2)
H4I	0.9859	0.6413	0.3919	0.118*
C5I	0.8560 (7)	0.6074 (6)	0.3777 (2)	0.093 (2)
H5I	0.8074	0.6443	0.3977	0.112*
C6I	0.8195 (5)	0.5562 (4)	0.35134 (17)	0.0669 (15)
H6I	0.7460	0.5583	0.3538	0.080*
O4	0.5078 (2)	0.8783 (2)	0.27478 (9)	0.0416 (7)
Si4	0.49729 (9)	0.97845 (8)	0.28979 (4)	0.0367 (3)
C1J	0.5209 (4)	1.0600 (3)	0.24118 (14)	0.0411 (10)
C2J	0.4392 (5)	1.1044 (3)	0.20938 (16)	0.0531 (12)
H2J	0.3677	1.1032	0.2152	0.064*
C3J	0.4602 (6)	1.1495 (4)	0.17021 (17)	0.0632 (15)
H3J	0.4038	1.1785	0.1493	0.076*
C4J	0.5628 (6)	1.1525 (4)	0.16142 (19)	0.0701 (18)
H4J	0.5776	1.1828	0.1342	0.084*
C5J	0.6436 (5)	1.1124 (4)	0.1914 (2)	0.0652 (16)
H5J	0.7141	1.1158	0.1853	0.078*
C6J	0.6231 (4)	1.0663 (3)	0.23113 (17)	0.0513 (12)
H6J	0.6802	1.0385	0.2518	0.062*
C1K	0.3624 (4)	1.0450 (4)	0.31442 (15)	0.0449 (10)
C2K	0.3175 (4)	0.9961 (4)	0.34664 (16)	0.0552 (12)
H2K	0.3509	0.9285	0.3533	0.066*
C3K	0.2238 (5)	1.0450 (5)	0.36941 (19)	0.0725 (17)
H3K	0.1942	1.0099	0.3911	0.087*
C4K	0.1736 (5)	1.1438 (5)	0.3608 (2)	0.0766 (19)
H4K	0.1110	1.1768	0.3767	0.092*
C5K	0.2158 (5)	1.1924 (5)	0.3290 (2)	0.0699 (16)
H5K	0.1816	1.2600	0.3224	0.084*
C6K	0.3084 (4)	1.1443 (4)	0.30611 (18)	0.0554 (12)
H6K	0.3360	1.1801	0.2840	0.067*
C1L	0.5996 (4)	0.9643 (3)	0.33352 (15)	0.0454 (10)
C2L	0.5798 (5)	1.0260 (5)	0.36498 (19)	0.0718 (18)
H2L	0.5143	1.0804	0.3637	0.086*
C3L	0.6533 (7)	1.0104 (8)	0.3984 (2)	0.109 (3)
H3L	0.6359	1.0525	0.4202	0.131*
C4L	0.7498 (7)	0.9357 (8)	0.4004 (3)	0.107 (3)
H4L	0.8016	0.9277	0.4223	0.128*
C5L	0.7708 (6)	0.8735 (5)	0.3709 (3)	0.106 (3)
H5L	0.8366	0.8195	0.3727	0.127*
C6L	0.6966 (5)	0.8872 (4)	0.3375 (3)	0.0778 (19)
H6L	0.7134	0.8422	0.3170	0.093*
O5	0.5387 (2)	0.57040 (19)	0.15287 (9)	0.0352 (6)
Si5	0.51974 (9)	0.47271 (7)	0.14886 (3)	0.0314 (2)
C1M	0.6514 (3)	0.3727 (3)	0.13857 (14)	0.0353 (9)
C2M	0.6683 (3)	0.3295 (3)	0.10056 (15)	0.0388 (9)
H2M	0.6112	0.3500	0.0798	0.047*
C3M	0.7649 (4)	0.2577 (3)	0.09173 (16)	0.0449 (11)
H3M	0.7737	0.2301	0.0653	0.054*
C4M	0.8482 (4)	0.2268 (3)	0.12178 (18)	0.0499 (12)
H4M	0.9145	0.1772	0.1161	0.060*
C5M	0.8359 (4)	0.2675 (3)	0.15991 (18)	0.0519 (12)
H5M	0.8934	0.2459	0.1805	0.062*
C6M	0.7392 (4)	0.3400 (3)	0.16804 (15)	0.0435 (10)
H6M	0.7318	0.3685	0.1942	0.052*
C1N	0.4277 (3)	0.4839 (3)	0.10239 (13)	0.0346 (9)
C2N	0.3498 (3)	0.4381 (3)	0.10514 (15)	0.0402 (9)
H2N	0.3429	0.4002	0.1314	0.048*
C3N	0.2832 (4)	0.4469 (3)	0.07054 (17)	0.0487 (12)
H3N	0.2302	0.4164	0.0736	0.058*
C4N	0.2927 (4)	0.4995 (4)	0.03163 (16)	0.0515 (12)
H4N	0.2471	0.5047	0.0078	0.062*
C5N	0.3699 (4)	0.5451 (4)	0.02766 (15)	0.0488 (12)
H5N	0.3770	0.5819	0.0011	0.059*
C6N	0.4356 (3)	0.5365 (3)	0.06232 (13)	0.0401 (9)
H6N	0.4882	0.5674	0.0590	0.048*
C1O	0.4513 (3)	0.4353 (3)	0.19970 (13)	0.0381 (9)
C2O	0.3530 (4)	0.4984 (3)	0.21237 (14)	0.0425 (10)
H1O	0.3209	0.5577	0.1946	0.051*
C3O	0.2987 (4)	0.4790 (4)	0.24998 (16)	0.0535 (12)
H3O	0.2299	0.5234	0.2572	0.064*
C4O	0.3462 (5)	0.3936 (4)	0.27689 (16)	0.0567 (13)
H4O	0.3111	0.3800	0.3032	0.068*
C5O	0.4447 (5)	0.3287 (4)	0.26527 (15)	0.0514 (12)
H5O	0.4772	0.2703	0.2836	0.062*
C6O	0.4969 (4)	0.3481 (3)	0.22702 (14)	0.0437 (10)
H6O	0.5640	0.3022	0.2192	0.052*
O6	0.4741 (2)	0.6538 (2)	0.32452 (9)	0.0400 (7)
Si6	0.42260 (9)	0.63680 (9)	0.37061 (4)	0.0378 (3)
C1P	0.4232 (4)	0.5093 (3)	0.38294 (13)	0.0449 (10)
C2P	0.3300 (4)	0.4853 (4)	0.39166 (15)	0.0524 (12)
H2P	0.2614	0.5354	0.3933	0.063*
C3P	0.3341 (6)	0.3906 (5)	0.39800 (17)	0.0681 (16)
H3P	0.2688	0.3768	0.4035	0.082*
C4P	0.4322 (7)	0.3167 (5)	0.39630 (18)	0.0751 (19)
H4P	0.4349	0.2519	0.4006	0.090*
C5P	0.5266 (6)	0.3373 (4)	0.38836 (19)	0.0778 (19)
H5P	0.5947	0.2865	0.3871	0.093*
C6P	0.5225 (5)	0.4333 (4)	0.38206 (17)	0.0590 (13)
H6P	0.5883	0.4467	0.3771	0.071*
C1Q	0.4959 (4)	0.6602 (4)	0.41614 (14)	0.0450 (10)
C2Q	0.5474 (4)	0.7284 (4)	0.40888 (16)	0.0515 (12)
H2Q	0.5456	0.7621	0.3806	0.062*
C3Q	0.6012 (5)	0.7479 (5)	0.44204 (18)	0.0710 (17)
H3Q	0.6377	0.7930	0.4360	0.085*
C4Q	0.6019 (6)	0.7023 (6)	0.4833 (2)	0.089 (2)
H4Q	0.6372	0.7169	0.5061	0.106*
C5Q	0.5506 (7)	0.6344 (6)	0.49169 (19)	0.092 (2)
H5Q	0.5517	0.6017	0.5202	0.111*
C6Q	0.4979 (5)	0.6148 (5)	0.45838 (16)	0.0654 (15)
H6Q	0.4622	0.5691	0.4645	0.079*
C1R	0.2754 (4)	0.7207 (3)	0.37220 (15)	0.0453 (10)
C2R	0.2020 (4)	0.7242 (4)	0.34071 (17)	0.0538 (12)
H2R	0.2246	0.6803	0.3197	0.065*
C3R	0.0943 (5)	0.7914 (5)	0.3391 (2)	0.0717 (16)
H3R	0.0456	0.7926	0.3171	0.086*
C4R	0.0610 (5)	0.8539 (5)	0.3689 (3)	0.083 (2)
H4R	−0.0112	0.8993	0.3678	0.100*
C5R	0.1314 (5)	0.8523 (5)	0.4009 (3)	0.087 (2)
H5R	0.1075	0.8962	0.4219	0.105*
C6R	0.2365 (4)	0.7869 (4)	0.4024 (2)	0.0666 (15)
H6R	0.2841	0.7867	0.4246	0.080*
C1S	0.3057 (7)	1.0325 (6)	0.4751 (3)	0.062 (3)*	0.5
C2S	0.1999 (7)	1.0502 (6)	0.4908 (4)	0.090 (5)*	0.5
H2S	0.1489	1.1140	0.4883	0.108*	0.5
C3S	0.1688 (7)	0.9745 (8)	0.5102 (4)	0.104 (5)*	0.5
H3S	0.0965	0.9865	0.5209	0.125*	0.5
C4S	0.2434 (10)	0.8811 (7)	0.5138 (4)	0.098 (10)*	0.5
H4S	0.2221	0.8293	0.5271	0.118*	0.5
C5S	0.3492 (9)	0.8634 (5)	0.4982 (4)	0.106 (5)*	0.5
H5S	0.4002	0.7996	0.5007	0.127*	0.5
C6S	0.3803 (6)	0.9392 (6)	0.4788 (3)	0.076 (3)*	0.5
H6S	0.4526	0.9271	0.4681	0.092*	0.5
C7S	0.3454 (11)	1.1104 (11)	0.4548 (4)	0.076 (4)*	0.5
H7SA	0.3632	1.1025	0.4242	0.115*	0.5
H7SB	0.4109	1.1069	0.4701	0.115*	0.5
H7SC	0.2884	1.1731	0.4569	0.115*	0.5
C1X	0.2949 (8)	1.0073 (9)	0.4778 (4)	0.104 (6)*	0.5
C2X	0.1903 (10)	1.0744 (7)	0.4800 (4)	0.105 (6)*	0.5
H2X	0.1767	1.1401	0.4696	0.126*	0.5
C3X	0.1055 (7)	1.0454 (8)	0.4976 (4)	0.090 (4)*	0.5
H3X	0.0340	1.0912	0.4991	0.108*	0.5
C4X	0.1254 (9)	0.9493 (8)	0.5129 (4)	0.109 (5)*	0.5
H4X	0.0675	0.9294	0.5249	0.131*	0.5
C5X	0.2300 (11)	0.8822 (7)	0.5106 (5)	0.130 (14)*	0.5
H5X	0.2436	0.8165	0.5211	0.156*	0.5
C6X	0.3148 (8)	0.9112 (8)	0.4931 (4)	0.095 (4)*	0.5
H6X	0.3863	0.8654	0.4915	0.114*	0.5
C7X	0.3879 (17)	1.0422 (17)	0.4589 (7)	0.130 (7)*	0.5
H7XA	0.4300	1.0490	0.4828	0.195*	0.5
H7XB	0.3568	1.1044	0.4411	0.195*	0.5
H7XC	0.4360	0.9952	0.4409	0.195*	0.5
C1T	0.1240 (6)	0.6299 (7)	0.5276 (3)	0.073 (3)*	0.5
C2T	0.0357 (8)	0.6157 (7)	0.5503 (2)	0.083 (4)*	0.5
H2T	0.0455	0.5822	0.5788	0.099*	0.5
C3T	−0.0670 (6)	0.6505 (7)	0.5312 (3)	0.104 (5)*	0.5
H3T	−0.1274	0.6407	0.5467	0.125*	0.5
C4T	−0.0814 (6)	0.6995 (7)	0.4894 (3)	0.070 (3)*	0.5
H4T	−0.1516	0.7233	0.4764	0.084*	0.5
C5T	0.0070 (7)	0.7137 (7)	0.4667 (2)	0.084 (4)*	0.5
H5T	−0.0029	0.7472	0.4382	0.100*	0.5
C6T	0.1097 (6)	0.6790 (7)	0.4858 (3)	0.088 (4)*	0.5
H6T	0.1700	0.6887	0.4702	0.106*	0.5
C7T	0.2353 (16)	0.5905 (15)	0.5468 (7)	0.121 (6)*	0.5
H7T1	0.2331	0.6124	0.5754	0.182*	0.5
H7T2	0.2854	0.6130	0.5277	0.182*	0.5
H7T3	0.2607	0.5201	0.5501	0.182*	0.5
C1Y	0.108 (2)	0.633 (4)	0.5063 (15)	0.40 (4)*	0.5
C2Y	0.087 (2)	0.560 (3)	0.5335 (12)	0.33 (3)*	0.5
H2Y	0.1431	0.5136	0.5511	0.395*	0.5
C3Y	−0.017 (3)	0.5539 (18)	0.5347 (9)	0.35 (3)*	0.5
H3Y	−0.0318	0.5040	0.5533	0.414*	0.5
C4Y	−0.0996 (17)	0.6212 (18)	0.5089 (8)	0.145 (8)*	0.5
H4Y	−0.1706	0.6173	0.5098	0.174*	0.5
C5Y	−0.078 (3)	0.6942 (19)	0.4818 (10)	0.39 (4)*	0.5
H5Y	−0.1344	0.7402	0.4641	0.467*	0.5
C6Y	0.026 (4)	0.700 (3)	0.4805 (14)	0.47 (5)*	0.5
H6Y	0.0405	0.7498	0.4620	0.566*	0.5
C7Y	0.226 (2)	0.617 (2)	0.5134 (10)	0.185 (11)*	0.5
H7Y1	0.2334	0.6404	0.5409	0.277*	0.5
H7Y2	0.2520	0.6533	0.4894	0.277*	0.5
H7Y3	0.2689	0.5488	0.5147	0.277*	0.5
O1U	0.7502 (3)	0.7424 (2)	0.20138 (10)	0.0485 (8)
H1U	0.7272	0.7584	0.1757	0.073*
C1U	0.8417 (4)	0.7727 (4)	0.20348 (17)	0.0540 (12)
H1UC	0.8157	0.8444	0.1975	0.065*
C2U	0.9283 (4)	0.7327 (4)	0.17137 (19)	0.0602 (13)
H2UA	0.9868	0.7588	0.1731	0.090*
H2UB	0.8972	0.7503	0.1420	0.090*
H2UC	0.9579	0.6625	0.1778	0.090*
C3U	0.8854 (7)	0.7437 (6)	0.2494 (2)	0.091 (2)
H3UA	0.8997	0.6749	0.2576	0.137*
H3UB	0.8314	0.7806	0.2694	0.137*
H3UC	0.9533	0.7570	0.2510	0.137*

Atomic displacement parameters (Ų)

	U^11	U^22	U^33	U^12	U^13	U^23
O1W	0.0447 (16)	0.0372 (15)	0.0314 (14)	−0.0087 (13)	−0.0032 (12)	−0.0065 (12)
K1	0.0311 (4)	0.0327 (4)	0.0410 (5)	−0.0107 (3)	0.0008 (3)	−0.0045 (3)
K2	0.0375 (5)	0.0471 (5)	0.0421 (5)	−0.0181 (4)	0.0026 (4)	−0.0162 (4)
K3	0.0442 (5)	0.0515 (6)	0.0379 (5)	−0.0234 (4)	−0.0035 (4)	−0.0054 (4)
K4	0.0367 (5)	0.0409 (5)	0.0395 (5)	−0.0136 (4)	−0.0023 (4)	−0.0023 (4)
K5	0.0451 (5)	0.0421 (5)	0.0407 (5)	−0.0200 (4)	−0.0005 (4)	−0.0105 (4)
K6	0.0379 (5)	0.0399 (5)	0.0445 (5)	−0.0139 (4)	−0.0026 (4)	−0.0071 (4)
O1	0.0351 (14)	0.0365 (15)	0.0345 (14)	−0.0161 (12)	0.0067 (11)	−0.0100 (11)
Si1	0.0281 (5)	0.0270 (5)	0.0325 (5)	−0.0101 (4)	−0.0002 (4)	−0.0060 (4)
C1A	0.0259 (18)	0.030 (2)	0.035 (2)	−0.0095 (15)	0.0016 (15)	−0.0025 (15)
C2A	0.035 (2)	0.036 (2)	0.045 (2)	−0.0086 (18)	−0.0004 (18)	−0.0056 (18)
C3A	0.035 (2)	0.038 (2)	0.057 (3)	−0.0072 (19)	−0.007 (2)	0.004 (2)
C4A	0.036 (2)	0.057 (3)	0.055 (3)	−0.022 (2)	−0.015 (2)	0.005 (2)
C5A	0.040 (2)	0.046 (3)	0.047 (2)	−0.021 (2)	−0.0116 (19)	−0.004 (2)
C6A	0.032 (2)	0.032 (2)	0.040 (2)	−0.0136 (17)	−0.0040 (16)	−0.0013 (16)
C1B	0.0293 (19)	0.030 (2)	0.042 (2)	−0.0097 (16)	−0.0052 (16)	−0.0028 (16)
C2B	0.042 (2)	0.036 (2)	0.044 (2)	−0.0177 (19)	0.0034 (18)	−0.0097 (18)
C3B	0.048 (3)	0.038 (2)	0.058 (3)	−0.021 (2)	0.001 (2)	−0.011 (2)
C4B	0.038 (2)	0.035 (2)	0.065 (3)	−0.0168 (19)	−0.004 (2)	−0.004 (2)
C5B	0.034 (2)	0.040 (2)	0.048 (3)	−0.0115 (18)	0.0006 (18)	0.0045 (19)
C6B	0.035 (2)	0.035 (2)	0.040 (2)	−0.0118 (17)	−0.0010 (17)	−0.0031 (17)
C1C	0.0291 (19)	0.034 (2)	0.0295 (19)	−0.0119 (16)	−0.0031 (15)	−0.0044 (15)
C2C	0.033 (2)	0.032 (2)	0.075 (3)	−0.0082 (18)	0.004 (2)	−0.001 (2)
C3C	0.035 (3)	0.039 (3)	0.111 (5)	−0.001 (2)	0.018 (3)	0.005 (3)
C4C	0.042 (3)	0.032 (2)	0.085 (4)	0.002 (2)	0.007 (2)	−0.002 (2)
C5C	0.044 (2)	0.028 (2)	0.045 (2)	−0.0094 (18)	−0.0044 (19)	0.0008 (17)
C6C	0.034 (2)	0.033 (2)	0.032 (2)	−0.0112 (17)	−0.0012 (16)	−0.0050 (16)
O2	0.0312 (14)	0.0375 (16)	0.0476 (17)	−0.0094 (12)	−0.0067 (12)	−0.0067 (13)
Si2	0.0287 (5)	0.0311 (5)	0.0394 (6)	−0.0093 (4)	−0.0011 (4)	−0.0065 (4)
C1D	0.0237 (18)	0.029 (2)	0.046 (2)	−0.0036 (15)	−0.0016 (16)	−0.0082 (17)
C2D	0.042 (2)	0.038 (2)	0.050 (3)	−0.0163 (19)	−0.0008 (19)	−0.0078 (19)
C3D	0.054 (3)	0.037 (2)	0.076 (4)	−0.022 (2)	0.007 (3)	−0.017 (2)
C4D	0.036 (2)	0.046 (3)	0.069 (3)	−0.013 (2)	−0.006 (2)	−0.023 (2)
C5D	0.054 (3)	0.048 (3)	0.057 (3)	−0.015 (2)	−0.010 (2)	−0.013 (2)
C6D	0.047 (3)	0.037 (2)	0.054 (3)	−0.015 (2)	−0.010 (2)	−0.011 (2)
C1E	0.036 (2)	0.034 (2)	0.037 (2)	−0.0125 (17)	0.0002 (16)	−0.0095 (17)
C2E	0.042 (2)	0.041 (2)	0.042 (2)	−0.0136 (19)	0.0017 (19)	−0.0058 (19)
C3E	0.056 (3)	0.051 (3)	0.045 (3)	−0.026 (2)	0.005 (2)	−0.005 (2)
C4E	0.076 (3)	0.038 (2)	0.041 (2)	−0.029 (2)	0.006 (2)	−0.0066 (19)
C5E	0.063 (3)	0.033 (3)	0.075 (4)	0.003 (2)	0.015 (3)	0.006 (2)
C6E	0.048 (3)	0.038 (3)	0.061 (3)	−0.002 (2)	0.005 (2)	0.005 (2)
C1F	0.040 (2)	0.028 (2)	0.044 (2)	−0.0094 (17)	−0.0022 (18)	−0.0014 (17)
C2F	0.057 (3)	0.039 (2)	0.041 (2)	−0.016 (2)	−0.002 (2)	−0.0049 (19)
C3F	0.088 (4)	0.043 (3)	0.046 (3)	−0.008 (3)	0.005 (3)	−0.011 (2)
C4F	0.076 (4)	0.053 (3)	0.070 (4)	−0.009 (3)	0.028 (3)	−0.014 (3)
C5F	0.048 (3)	0.065 (4)	0.090 (4)	−0.020 (3)	0.026 (3)	−0.020 (3)
C6F	0.042 (3)	0.052 (3)	0.061 (3)	−0.014 (2)	0.005 (2)	−0.017 (2)
O3	0.0350 (15)	0.0410 (16)	0.0406 (16)	−0.0086 (13)	−0.0047 (12)	−0.0021 (13)
Si3	0.0356 (6)	0.0385 (6)	0.0402 (6)	−0.0091 (5)	−0.0036 (5)	−0.0010 (5)
C1G	0.034 (2)	0.042 (2)	0.043 (2)	−0.0124 (18)	−0.0087 (18)	−0.0043 (18)
C2G	0.043 (3)	0.046 (3)	0.058 (3)	−0.012 (2)	0.002 (2)	−0.001 (2)
C3G	0.054 (3)	0.044 (3)	0.070 (3)	−0.002 (2)	0.009 (3)	−0.011 (2)
C4G	0.054 (3)	0.059 (3)	0.070 (4)	−0.016 (3)	0.019 (3)	−0.012 (3)
C5G	0.058 (3)	0.059 (3)	0.061 (3)	−0.026 (3)	0.009 (2)	−0.002 (2)
C6G	0.040 (2)	0.048 (3)	0.056 (3)	−0.013 (2)	0.001 (2)	−0.005 (2)
C1H	0.042 (3)	0.048 (3)	0.059 (3)	−0.006 (2)	0.007 (2)	0.009 (2)
C2H	0.085 (4)	0.038 (3)	0.066 (3)	−0.020 (3)	0.025 (3)	−0.011 (2)
C3H	0.097 (5)	0.039 (3)	0.105 (5)	−0.021 (3)	0.054 (4)	−0.017 (3)
C4H	0.079 (5)	0.063 (4)	0.146 (8)	0.003 (4)	0.054 (5)	0.044 (5)
C5H	0.070 (5)	0.142 (8)	0.156 (9)	−0.029 (5)	−0.014 (5)	0.107 (7)
C6H	0.063 (4)	0.116 (6)	0.106 (6)	−0.030 (4)	−0.019 (4)	0.069 (5)
C1I	0.049 (3)	0.057 (3)	0.039 (2)	−0.008 (2)	−0.012 (2)	−0.001 (2)
C2I	0.054 (3)	0.067 (3)	0.062 (3)	−0.019 (3)	−0.018 (2)	0.000 (3)
C3I	0.075 (4)	0.107 (5)	0.076 (4)	−0.033 (4)	−0.027 (3)	−0.021 (4)
C4I	0.097 (6)	0.130 (7)	0.079 (5)	−0.040 (5)	−0.032 (4)	−0.037 (5)
C5I	0.097 (5)	0.109 (6)	0.064 (4)	−0.013 (4)	−0.020 (4)	−0.037 (4)
C6I	0.067 (4)	0.079 (4)	0.044 (3)	−0.011 (3)	−0.012 (2)	−0.009 (3)
O4	0.0499 (17)	0.0391 (16)	0.0421 (16)	−0.0210 (14)	0.0041 (13)	−0.0130 (13)
Si4	0.0376 (6)	0.0385 (6)	0.0396 (6)	−0.0173 (5)	0.0015 (5)	−0.0133 (5)
C1J	0.052 (3)	0.036 (2)	0.046 (2)	−0.025 (2)	0.005 (2)	−0.0181 (19)
C2J	0.072 (3)	0.042 (3)	0.052 (3)	−0.026 (2)	−0.002 (2)	−0.013 (2)
C3J	0.105 (5)	0.046 (3)	0.046 (3)	−0.035 (3)	−0.001 (3)	−0.011 (2)
C4J	0.126 (6)	0.052 (3)	0.048 (3)	−0.049 (4)	0.022 (3)	−0.016 (2)
C5J	0.089 (4)	0.057 (3)	0.067 (4)	−0.046 (3)	0.033 (3)	−0.025 (3)
C6J	0.059 (3)	0.048 (3)	0.055 (3)	−0.024 (2)	0.011 (2)	−0.019 (2)
C1K	0.038 (2)	0.060 (3)	0.045 (2)	−0.023 (2)	−0.0001 (19)	−0.018 (2)
C2K	0.061 (3)	0.067 (3)	0.046 (3)	−0.028 (3)	0.001 (2)	−0.022 (2)
C3K	0.066 (4)	0.106 (5)	0.059 (3)	−0.043 (4)	0.022 (3)	−0.031 (3)
C4K	0.042 (3)	0.103 (5)	0.082 (4)	−0.014 (3)	0.011 (3)	−0.038 (4)
C5K	0.056 (3)	0.073 (4)	0.068 (4)	0.001 (3)	0.002 (3)	−0.026 (3)
C6K	0.053 (3)	0.051 (3)	0.059 (3)	−0.010 (2)	−0.002 (2)	−0.013 (2)
C1L	0.046 (3)	0.052 (3)	0.044 (2)	−0.024 (2)	0.001 (2)	−0.006 (2)
C2L	0.055 (3)	0.115 (5)	0.059 (3)	−0.036 (3)	0.002 (3)	−0.042 (3)
C3L	0.097 (6)	0.226 (10)	0.051 (4)	−0.102 (7)	0.003 (4)	−0.050 (5)
C4L	0.102 (6)	0.174 (9)	0.080 (5)	−0.109 (7)	−0.045 (4)	0.050 (5)
C5L	0.084 (5)	0.073 (5)	0.168 (8)	−0.043 (4)	−0.081 (5)	0.031 (5)
C6L	0.058 (3)	0.053 (3)	0.126 (6)	−0.017 (3)	−0.027 (3)	−0.022 (3)
O5	0.0389 (15)	0.0310 (14)	0.0391 (15)	−0.0142 (12)	−0.0018 (12)	−0.0096 (11)
Si5	0.0331 (5)	0.0308 (5)	0.0334 (5)	−0.0138 (4)	−0.0018 (4)	−0.0066 (4)
C1M	0.040 (2)	0.029 (2)	0.043 (2)	−0.0182 (17)	−0.0010 (17)	−0.0063 (16)
C2M	0.034 (2)	0.037 (2)	0.049 (2)	−0.0152 (18)	−0.0002 (18)	−0.0123 (19)
C3M	0.040 (2)	0.038 (2)	0.063 (3)	−0.0170 (19)	0.004 (2)	−0.020 (2)
C4M	0.037 (2)	0.029 (2)	0.081 (4)	−0.0067 (18)	−0.002 (2)	−0.011 (2)
C5M	0.042 (3)	0.043 (3)	0.069 (3)	−0.015 (2)	−0.014 (2)	0.003 (2)
C6M	0.044 (2)	0.039 (2)	0.050 (3)	−0.017 (2)	−0.009 (2)	−0.0039 (19)
C1N	0.031 (2)	0.034 (2)	0.037 (2)	−0.0074 (16)	0.0000 (16)	−0.0093 (17)
C2N	0.040 (2)	0.039 (2)	0.046 (2)	−0.0169 (19)	0.0006 (18)	−0.0115 (19)
C3N	0.037 (2)	0.050 (3)	0.065 (3)	−0.013 (2)	−0.011 (2)	−0.025 (2)
C4N	0.038 (2)	0.058 (3)	0.050 (3)	0.002 (2)	−0.012 (2)	−0.026 (2)
C5N	0.045 (3)	0.053 (3)	0.034 (2)	0.002 (2)	0.0002 (19)	−0.009 (2)
C6N	0.036 (2)	0.049 (3)	0.033 (2)	−0.0095 (19)	0.0012 (17)	−0.0100 (18)
C1O	0.042 (2)	0.041 (2)	0.036 (2)	−0.0207 (19)	−0.0028 (17)	−0.0068 (18)
C2O	0.040 (2)	0.051 (3)	0.039 (2)	−0.018 (2)	−0.0010 (18)	−0.0082 (19)
C3O	0.053 (3)	0.065 (3)	0.048 (3)	−0.026 (3)	0.008 (2)	−0.014 (2)
C4O	0.073 (4)	0.069 (3)	0.042 (3)	−0.041 (3)	0.009 (2)	−0.013 (2)
C5O	0.079 (4)	0.047 (3)	0.036 (2)	−0.033 (3)	−0.001 (2)	−0.003 (2)
C6O	0.059 (3)	0.041 (2)	0.039 (2)	−0.026 (2)	0.000 (2)	−0.0084 (19)
O6	0.0436 (16)	0.0420 (16)	0.0339 (15)	−0.0147 (13)	−0.0009 (12)	−0.0026 (12)
Si6	0.0376 (6)	0.0464 (7)	0.0306 (6)	−0.0167 (5)	−0.0005 (4)	−0.0029 (5)
C1P	0.059 (3)	0.051 (3)	0.026 (2)	−0.023 (2)	−0.0032 (19)	0.0002 (18)
C2P	0.064 (3)	0.063 (3)	0.039 (2)	−0.036 (3)	−0.010 (2)	0.007 (2)
C3P	0.106 (5)	0.072 (4)	0.044 (3)	−0.054 (4)	−0.011 (3)	0.003 (3)
C4P	0.133 (6)	0.061 (4)	0.042 (3)	−0.048 (4)	0.013 (3)	−0.009 (3)
C5P	0.108 (5)	0.052 (3)	0.057 (3)	−0.012 (3)	0.026 (3)	−0.003 (3)
C6P	0.066 (3)	0.052 (3)	0.049 (3)	−0.012 (3)	0.013 (2)	0.003 (2)
C1Q	0.045 (2)	0.059 (3)	0.032 (2)	−0.021 (2)	−0.0029 (18)	−0.0020 (19)
C2Q	0.058 (3)	0.064 (3)	0.041 (2)	−0.031 (3)	−0.001 (2)	−0.002 (2)
C3Q	0.086 (4)	0.100 (5)	0.053 (3)	−0.063 (4)	−0.004 (3)	−0.009 (3)
C4Q	0.125 (6)	0.124 (6)	0.050 (3)	−0.084 (5)	−0.023 (4)	−0.002 (3)
C5Q	0.138 (6)	0.126 (6)	0.039 (3)	−0.085 (5)	−0.034 (3)	0.019 (3)
C6Q	0.093 (4)	0.090 (4)	0.032 (2)	−0.057 (4)	−0.010 (2)	0.004 (2)
C1R	0.041 (2)	0.053 (3)	0.049 (3)	−0.024 (2)	0.0011 (19)	−0.008 (2)
C2R	0.045 (3)	0.063 (3)	0.056 (3)	−0.024 (2)	−0.004 (2)	−0.001 (2)
C3R	0.051 (3)	0.072 (4)	0.093 (5)	−0.027 (3)	−0.011 (3)	0.004 (3)
C4R	0.048 (3)	0.076 (4)	0.125 (6)	−0.017 (3)	0.008 (4)	−0.022 (4)
C5R	0.052 (3)	0.091 (5)	0.121 (6)	−0.017 (3)	0.012 (4)	−0.048 (4)
C6R	0.047 (3)	0.078 (4)	0.078 (4)	−0.020 (3)	0.006 (3)	−0.028 (3)
O1U	0.0490 (18)	0.0536 (19)	0.0459 (18)	−0.0203 (15)	−0.0003 (14)	−0.0096 (14)
C1U	0.055 (3)	0.063 (3)	0.056 (3)	−0.036 (3)	−0.004 (2)	−0.005 (2)
C2U	0.049 (3)	0.059 (3)	0.073 (4)	−0.023 (3)	−0.005 (3)	0.000 (3)
C3U	0.127 (6)	0.118 (6)	0.059 (4)	−0.083 (5)	−0.020 (4)	0.004 (4)

Geometric parameters (Å, º)

O1W—K6	2.886 (3)	C6I—H6I	0.9500
O1W—K5	2.888 (3)	O4—Si4	1.585 (3)
O1W—K4	2.959 (3)	Si4—C1K	1.878 (5)
O1W—K3	3.112 (3)	Si4—C1L	1.891 (5)
O1W—K1	3.260 (3)	Si4—C1J	1.897 (5)
O1W—K2	3.351 (3)	C1J—C6J	1.390 (6)
O1W—H1W	0.8400	C1J—C2J	1.411 (7)
O1W—H2W	0.8400	C2J—C3J	1.375 (7)
K1—O5	2.590 (3)	C2J—H2J	0.9500
K1—O1	2.807 (3)	C3J—C4J	1.372 (9)
K1—O2	2.887 (3)	C3J—H3J	0.9500
K1—C1D	3.127 (4)	C4J—C5J	1.360 (9)
K1—C1A	3.129 (4)	C4J—H4J	0.9500
K1—C2A	3.327 (4)	C5J—C6J	1.393 (7)
K1—C2D	3.346 (4)	C5J—H5J	0.9500
K1—C6D	3.471 (5)	C6J—H6J	0.9500
K1—C6A	3.514 (4)	C1K—C2K	1.390 (7)
K1—Si1	3.5262 (14)	C1K—C6K	1.399 (7)
K1—Si2	3.5318 (16)	C2K—C3K	1.399 (7)
K1—H1W	2.9267	C2K—H2K	0.9500
K1—H2W	2.9065	C3K—C4K	1.387 (10)
K2—O2	2.591 (3)	C3K—H3K	0.9500
K2—O4	2.683 (3)	C4K—C5K	1.359 (9)
K2—O1	2.734 (3)	C4K—H4K	0.9500
K2—O1U	2.890 (3)	C5K—C6K	1.389 (7)
K2—C1J	3.149 (4)	C5K—H5K	0.9500
K2—C2J	3.161 (5)	C6K—H6K	0.9500
K2—Si4	3.5213 (15)	C1L—C6L	1.381 (7)
K2—K6	3.7506 (17)	C1L—C2L	1.384 (7)
K2—Si2	3.8436 (15)	C2L—C3L	1.390 (9)
K2—K4	3.9156 (15)	C2L—H2L	0.9500
K2—H1U	2.6210	C3L—C4L	1.360 (13)
K3—O3	2.607 (3)	C3L—H3L	0.9500
K3—O5	2.626 (3)	C4L—C5L	1.340 (13)
K3—O1U	2.780 (3)	C4L—H4L	0.9500
K3—O1	2.997 (3)	C5L—C6L	1.399 (9)
K3—C6C	3.117 (4)	C5L—H5L	0.9500
K3—C6G	3.321 (5)	C6L—H6L	0.9500
K3—Si3	3.6648 (17)	O5—Si5	1.587 (3)
K3—Si5	3.7414 (15)	Si5—C1N	1.876 (4)
K3—K6	3.7562 (15)	Si5—C1M	1.890 (4)
K3—Si1	3.8822 (17)	Si5—C1O	1.894 (4)
K3—H2W	2.6330	C1M—C2M	1.389 (6)
K3—H1U	2.7039	C1M—C6M	1.409 (6)
K4—O4	2.588 (3)	C2M—C3M	1.385 (6)
K4—O6	2.658 (3)	C2M—H2M	0.9500
K4—O2	2.896 (3)	C3M—C4M	1.379 (7)
K4—C2R	3.188 (5)	C3M—H3M	0.9500
K4—C2F	3.239 (5)	C4M—C5M	1.377 (7)
K4—C1R	3.354 (5)	C4M—H4M	0.9500
K4—K6	3.5332 (15)	C5M—C6M	1.387 (7)
K4—Si6	3.5819 (17)	C5M—H5M	0.9500
K4—Si4	3.7252 (16)	C6M—H6M	0.9500
K4—Si2	3.7885 (16)	C1N—C6N	1.402 (6)
K4—H1W	2.6352	C1N—C2N	1.408 (6)
K5—O6	2.582 (3)	C2N—C3N	1.379 (6)
K5—O3	2.600 (3)	C2N—H2N	0.9500
K5—C1O	3.166 (4)	C3N—C4N	1.378 (7)
K5—C2O	3.210 (4)	C3N—H3N	0.9500
K5—C6O	3.240 (4)	C4N—C5N	1.395 (7)
K5—C6P	3.291 (5)	C4N—H4N	0.9500
K5—C5O	3.361 (5)	C5N—C6N	1.374 (6)
K5—C3O	3.371 (5)	C5N—H5N	0.9500
K5—C4O	3.427 (5)	C6N—H6N	0.9500
K5—C1P	3.461 (4)	C1O—C2O	1.377 (6)
K5—K6	3.4916 (14)	C1O—C6O	1.411 (6)
K5—H2W	2.8967	C2O—C3O	1.388 (6)
K6—O6	2.655 (3)	C2O—H1O	0.9500
K6—O4	2.665 (3)	C3O—C4O	1.389 (8)
K6—O3	2.750 (3)	C3O—H3O	0.9500
K6—O1U	2.974 (3)	C4O—C5O	1.379 (7)
K6—C6I	3.255 (6)	C4O—H4O	0.9500
K6—Si3	3.7835 (18)	C5O—C6O	1.388 (6)
O1—Si1	1.595 (3)	C5O—H5O	0.9500
Si1—C1C	1.886 (4)	C6O—H6O	0.9500
Si1—C1B	1.893 (4)	O6—Si6	1.579 (3)
Si1—C1A	1.893 (4)	Si6—C1Q	1.878 (5)
C1A—C2A	1.390 (5)	Si6—C1P	1.894 (5)
C1A—C6A	1.397 (6)	Si6—C1R	1.898 (5)
C2A—C3A	1.382 (6)	C1P—C2P	1.392 (7)
C2A—H2A	0.9500	C1P—C6P	1.396 (7)
C3A—C4A	1.390 (7)	C2P—C3P	1.387 (7)
C3A—H3A	0.9500	C2P—H2P	0.9500
C4A—C5A	1.376 (7)	C3P—C4P	1.373 (9)
C4A—H4A	0.9500	C3P—H3P	0.9500
C5A—C6A	1.399 (6)	C4P—C5P	1.377 (10)
C5A—H5A	0.9500	C4P—H4P	0.9500
C6A—H6A	0.9500	C5P—C6P	1.407 (8)
C1B—C2B	1.386 (6)	C5P—H5P	0.9500
C1B—C6B	1.395 (6)	C6P—H6P	0.9500
C2B—C3B	1.393 (6)	C1Q—C6Q	1.392 (7)
C2B—H2B	0.9500	C1Q—C2Q	1.398 (7)
C3B—C4B	1.376 (7)	C2Q—C3Q	1.390 (7)
C3B—H3B	0.9500	C2Q—H2Q	0.9500
C4B—C5B	1.370 (7)	C3Q—C4Q	1.367 (8)
C4B—H4B	0.9500	C3Q—H3Q	0.9500
C5B—C6B	1.393 (6)	C4Q—C5Q	1.394 (9)
C5B—H5B	0.9500	C4Q—H4Q	0.9500
C6B—H6B	0.9500	C5Q—C6Q	1.384 (8)
C1C—C2C	1.391 (6)	C5Q—H5Q	0.9500
C1C—C6C	1.400 (5)	C6Q—H6Q	0.9500
C2C—C3C	1.387 (6)	C1R—C2R	1.386 (7)
C2C—H2C	0.9500	C1R—C6R	1.399 (7)
C3C—C4C	1.379 (7)	C2R—C3R	1.414 (8)
C3C—H3C	0.9500	C2R—H2R	0.9500
C4C—C5C	1.375 (7)	C3R—C4R	1.349 (9)
C4C—H4C	0.9500	C3R—H3R	0.9500
C5C—C6C	1.388 (6)	C4R—C5R	1.378 (10)
C5C—H5C	0.9500	C4R—H4R	0.9500
C6C—H6C	0.9500	C5R—C6R	1.380 (8)
O2—Si2	1.593 (3)	C5R—H5R	0.9500
Si2—C1F	1.875 (4)	C6R—H6R	0.9500
Si2—C1E	1.881 (4)	C1S—C2S	1.3900
Si2—C1D	1.891 (4)	C1S—C6S	1.3900
C1D—C6D	1.397 (6)	C1S—C7S	1.492 (16)
C1D—C2D	1.399 (6)	C2S—C3S	1.3900
C2D—C3D	1.390 (6)	C2S—H2S	0.9500
C2D—H2D	0.9500	C3S—C4S	1.3900
C3D—C4D	1.378 (7)	C3S—H3S	0.9500
C3D—H3D	0.9500	C4S—C5S	1.3900
C4D—C5D	1.367 (7)	C4S—H4S	0.9500
C4D—H4D	0.9500	C5S—C6S	1.3900
C5D—C6D	1.387 (6)	C5S—H5S	0.9500
C5D—H5D	0.9500	C6S—H6S	0.9500
C6D—H6D	0.9500	C7S—H7SA	0.9800
C1E—C6E	1.384 (6)	C7S—H7SB	0.9800
C1E—C2E	1.386 (6)	C7S—H7SC	0.9800
C2E—C3E	1.379 (6)	C1X—C2X	1.3900
C2E—H2E	0.9500	C1X—C6X	1.3900
C3E—C4E	1.361 (7)	C1X—C7X	1.55 (2)
C3E—H3E	0.9500	C2X—C3X	1.3900
C4E—C5E	1.372 (7)	C2X—H2X	0.9500
C4E—H4E	0.9500	C3X—C4X	1.3900
C5E—C6E	1.391 (7)	C3X—H3X	0.9500
C5E—H5E	0.9500	C4X—C5X	1.3900
C6E—H6E	0.9500	C4X—H4X	0.9500
C1F—C6F	1.394 (6)	C5X—C6X	1.3900
C1F—C2F	1.411 (6)	C5X—H5X	0.9500
C2F—C3F	1.380 (7)	C6X—H6X	0.9500
C2F—H2F	0.9500	C7X—H7XA	0.9800
C3F—C4F	1.381 (9)	C7X—H7XB	0.9800
C3F—H3F	0.9500	C7X—H7XC	0.9800
C4F—C5F	1.384 (9)	C1T—C2T	1.3900
C4F—H4F	0.9500	C1T—C6T	1.3900
C5F—C6F	1.385 (7)	C1T—C7T	1.49 (2)
C5F—H5F	0.9500	C2T—C3T	1.3900
C6F—H6F	0.9500	C2T—H2T	0.9500
O3—Si3	1.585 (3)	C3T—C4T	1.3900
Si3—C1H	1.877 (5)	C3T—H3T	0.9500
Si3—C1G	1.891 (4)	C4T—C5T	1.3900
Si3—C1I	1.894 (5)	C4T—H4T	0.9500
C1G—C2G	1.395 (6)	C5T—C6T	1.3900
C1G—C6G	1.400 (6)	C5T—H5T	0.9500
C2G—C3G	1.385 (7)	C6T—H6T	0.9500
C2G—H2G	0.9500	C7T—H7T1	0.9800
C3G—C4G	1.387 (8)	C7T—H7T2	0.9800
C3G—H3G	0.9500	C7T—H7T3	0.9800
C4G—C5G	1.373 (8)	C1Y—C2Y	1.3900
C4G—H4G	0.9500	C1Y—C6Y	1.3900
C5G—C6G	1.393 (7)	C1Y—C7Y	1.50 (4)
C5G—H5G	0.9500	C2Y—C3Y	1.3900
C6G—H6G	0.9500	C2Y—H2Y	0.9500
C1H—C6H	1.394 (8)	C3Y—C4Y	1.3900
C1H—C2H	1.401 (8)	C3Y—H3Y	0.9500
C2H—C3H	1.410 (8)	C4Y—C5Y	1.3900
C2H—H2H	0.9500	C4Y—H4Y	0.9500
C3H—C4H	1.353 (12)	C5Y—C6Y	1.3900
C3H—H3H	0.9500	C5Y—H5Y	0.9500
C4H—C5H	1.369 (14)	C6Y—H6Y	0.9500
C4H—H4H	0.9500	C7Y—H7Y1	0.9800
C5H—C6H	1.390 (10)	C7Y—H7Y2	0.9800
C5H—H5H	0.9500	C7Y—H7Y3	0.9800
C6H—H6H	0.9500	O1U—C1U	1.427 (6)
C1I—C2I	1.393 (7)	O1U—H1U	0.8400
C1I—C6I	1.415 (7)	C1U—C2U	1.485 (7)
C2I—C3I	1.383 (8)	C1U—C3U	1.512 (8)
C2I—H2I	0.9500	C1U—H1UC	1.0000
C3I—C4I	1.377 (10)	C2U—H2UA	0.9800
C3I—H3I	0.9500	C2U—H2UB	0.9800
C4I—C5I	1.373 (11)	C2U—H2UC	0.9800
C4I—H4I	0.9500	C3U—H3UA	0.9800
C5I—C6I	1.392 (9)	C3U—H3UB	0.9800
C5I—H5I	0.9500	C3U—H3UC	0.9800
K6—O1W—K5	74.42 (7)	C3C—C2C—H2C	119.4
K6—O1W—K4	74.37 (7)	C1C—C2C—H2C	119.4
K5—O1W—K4	93.02 (8)	C4C—C3C—C2C	120.8 (5)
K6—O1W—K3	77.44 (7)	C4C—C3C—H3C	119.6
K5—O1W—K3	87.49 (8)	C2C—C3C—H3C	119.6
K4—O1W—K3	150.55 (11)	C5C—C4C—C3C	119.6 (4)
K6—O1W—K1	138.44 (10)	C5C—C4C—H4C	120.2
K5—O1W—K1	137.33 (10)	C3C—C4C—H4C	120.2
K4—O1W—K1	118.48 (9)	C4C—C5C—C6C	119.3 (4)
K3—O1W—K1	78.41 (7)	C4C—C5C—H5C	120.3
K6—O1W—K2	73.51 (7)	C6C—C5C—H5C	120.3
K5—O1W—K2	147.87 (10)	C5C—C6C—C1C	122.5 (4)
K4—O1W—K2	76.43 (7)	C5C—C6C—K3	108.3 (3)
K3—O1W—K2	87.61 (8)	C1C—C6C—K3	97.2 (2)
K1—O1W—K2	72.16 (6)	C5C—C6C—H6C	118.8
K6—O1W—H1W	124.0	C1C—C6C—H6C	118.8
K5—O1W—H1W	133.4	K3—C6C—H6C	62.8
K4—O1W—H1W	59.6	Si2—O2—K2	131.99 (16)
K3—O1W—H1W	135.4	Si2—O2—K1	100.02 (13)
K1—O1W—H1W	59.7	K2—O2—K1	90.41 (9)
K2—O1W—H1W	66.6	Si2—O2—K4	111.82 (14)
K6—O1W—H2W	121.8	K2—O2—K4	90.87 (9)
K5—O1W—H2W	82.3	K1—O2—K4	135.14 (11)
K4—O1W—H2W	160.5	O2—Si2—C1F	114.07 (18)
K3—O1W—H2W	48.6	O2—Si2—C1E	112.81 (17)
K1—O1W—H2W	58.2	C1F—Si2—C1E	105.91 (18)
K2—O1W—H2W	116.9	O2—Si2—C1D	109.36 (16)
H1W—O1W—H2W	110.8	C1F—Si2—C1D	108.62 (18)
O5—K1—O1	87.60 (9)	C1E—Si2—C1D	105.65 (18)
O5—K1—O2	101.77 (9)	C1F—Si2—K1	151.90 (13)
O1—K1—O2	86.13 (8)	C1E—Si2—K1	102.17 (13)
O5—K1—C1D	118.32 (10)	C1D—Si2—K1	62.00 (11)
O1—K1—C1D	136.62 (9)	C1F—Si2—K4	68.91 (14)
O2—K1—C1D	56.35 (9)	C1E—Si2—K4	129.49 (13)
O5—K1—C1A	114.40 (10)	C1D—Si2—K4	123.97 (13)
O1—K1—C1A	57.46 (9)	K1—Si2—K4	93.76 (4)
O2—K1—C1A	125.28 (9)	C1F—Si2—K2	120.48 (14)
C1D—K1—C1A	125.10 (11)	C1E—Si2—K2	83.25 (13)
O5—K1—O1W	52.46 (8)	C1D—Si2—K2	125.51 (12)
O1—K1—O1W	75.13 (8)	K1—Si2—K2	63.56 (3)
O2—K1—O1W	50.69 (8)	K4—Si2—K2	61.73 (3)
C1D—K1—O1W	93.17 (10)	C6D—C1D—C2D	115.8 (4)
C1A—K1—O1W	132.10 (9)	C6D—C1D—Si2	123.6 (3)
O5—K1—C2A	139.02 (10)	C2D—C1D—Si2	120.3 (3)
O1—K1—C2A	68.14 (10)	C6D—C1D—K1	92.1 (3)
O2—K1—C2A	108.61 (10)	C2D—C1D—K1	86.5 (2)
C1D—K1—C2A	101.44 (11)	Si2—C1D—K1	85.73 (13)
C1A—K1—C2A	24.62 (10)	C3D—C2D—C1D	122.3 (5)
O1W—K1—C2A	139.30 (10)	C3D—C2D—K1	102.3 (3)
O5—K1—C2D	94.86 (10)	C1D—C2D—K1	68.9 (2)
O1—K1—C2D	151.45 (10)	C3D—C2D—H2D	118.8
O2—K1—C2D	65.50 (10)	C1D—C2D—H2D	118.8
C1D—K1—C2D	24.66 (10)	K1—C2D—H2D	98.8
C1A—K1—C2D	142.62 (11)	C4D—C3D—C2D	119.7 (4)
O1W—K1—C2D	83.88 (10)	C4D—C3D—H3D	120.1
C2A—K1—C2D	122.38 (11)	C2D—C3D—H3D	120.1
O5—K1—C6D	133.28 (11)	C5D—C4D—C3D	119.6 (4)
O1—K1—C6D	137.36 (10)	C5D—C4D—H4D	120.2
O2—K1—C6D	75.34 (9)	C3D—C4D—H4D	120.2
C1D—K1—C6D	23.72 (11)	C4D—C5D—C6D	120.5 (5)
C1A—K1—C6D	103.50 (11)	C4D—C5D—H5D	119.8
O1W—K1—C6D	116.84 (10)	C6D—C5D—H5D	119.8
C2A—K1—C6D	81.77 (11)	C5D—C6D—C1D	122.0 (4)
C2D—K1—C6D	40.62 (12)	C5D—C6D—K1	101.7 (3)
O5—K1—C6A	102.99 (9)	C1D—C6D—K1	64.2 (2)
O1—K1—C6A	74.97 (9)	C5D—C6D—H6D	119.0
O2—K1—C6A	147.97 (9)	C1D—C6D—H6D	119.0
C1D—K1—C6A	125.05 (11)	K1—C6D—H6D	103.9
C1A—K1—C6A	23.36 (9)	C6E—C1E—C2E	116.6 (4)
O1W—K1—C6A	141.73 (9)	C6E—C1E—Si2	121.9 (3)
C2A—K1—C6A	40.36 (10)	C2E—C1E—Si2	121.5 (3)
C2D—K1—C6A	131.44 (11)	C3E—C2E—C1E	122.2 (4)
C6D—K1—C6A	101.33 (11)	C3E—C2E—H2E	118.9
O5—K1—Si1	95.65 (7)	C1E—C2E—H2E	118.9
O1—K1—Si1	26.16 (6)	C4E—C3E—C2E	120.6 (4)
O2—K1—Si1	108.69 (6)	C4E—C3E—H3E	119.7
C1D—K1—Si1	144.24 (8)	C2E—C3E—H3E	119.7
C1A—K1—Si1	32.36 (7)	C3E—C4E—C5E	118.5 (4)
O1W—K1—Si1	99.75 (6)	C3E—C4E—H4E	120.8
C2A—K1—Si1	49.03 (8)	C5E—C4E—H4E	120.8
C2D—K1—Si1	168.90 (8)	C4E—C5E—C6E	121.2 (5)
C6D—K1—Si1	130.01 (9)	C4E—C5E—H5E	119.4
C6A—K1—Si1	48.88 (7)	C6E—C5E—H5E	119.4
O5—K1—Si2	119.55 (7)	C1E—C6E—C5E	120.8 (5)
O1—K1—Si2	105.50 (6)	C1E—C6E—H6E	119.6
O2—K1—Si2	26.36 (6)	C5E—C6E—H6E	119.6
C1D—K1—Si2	32.27 (8)	C6F—C1F—C2F	116.6 (4)
C1A—K1—Si2	122.36 (8)	C6F—C1F—Si2	123.1 (3)
O1W—K1—Si2	74.03 (6)	C2F—C1F—Si2	120.1 (3)
C2A—K1—Si2	99.10 (8)	C3F—C2F—C1F	121.8 (5)
C2D—K1—Si2	49.11 (8)	C3F—C2F—K4	114.6 (3)
C6D—K1—Si2	49.04 (8)	C1F—C2F—K4	91.7 (3)
C6A—K1—Si2	137.46 (7)	C3F—C2F—H2F	119.1
Si1—K1—Si2	121.60 (4)	C1F—C2F—H2F	119.1
O5—K1—H1W	64.5	K4—C2F—H2F	62.6
O1—K1—H1W	82.0	C2F—C3F—C4F	119.6 (5)
O2—K1—H1W	37.4	C2F—C3F—H3F	120.2
C1D—K1—H1W	79.7	C4F—C3F—H3F	120.2
C1A—K1—H1W	139.1	C3F—C4F—C5F	120.5 (5)
O1W—K1—H1W	14.3	C3F—C4F—H4F	119.8
C2A—K1—H1W	137.6	C5F—C4F—H4F	119.8
C2D—K1—H1W	73.6	C4F—C5F—C6F	119.3 (5)
C6D—K1—H1W	103.2	C4F—C5F—H5F	120.3
C6A—K1—H1W	154.4	C6F—C5F—H5F	120.3
Si1—K1—H1W	108.0	C5F—C6F—C1F	122.2 (5)
Si2—K1—H1W	59.8	C5F—C6F—H6F	118.9
O5—K1—H2W	38.3	C1F—C6F—H6F	118.9
O1—K1—H2W	76.8	Si3—O3—K5	128.63 (16)
O2—K1—H2W	64.6	Si3—O3—K3	119.95 (15)
C1D—K1—H2W	101.7	K5—O3—K3	105.76 (10)
C1A—K1—H2W	129.8	Si3—O3—K6	119.14 (15)
O1W—K1—H2W	14.2	K5—O3—K6	81.43 (8)
C2A—K1—H2W	144.8	K3—O3—K6	89.01 (9)
C2D—K1—H2W	87.6	O3—Si3—C1H	113.2 (2)
C6D—K1—H2W	125.2	O3—Si3—C1G	113.52 (18)
C6A—K1—H2W	132.4	C1H—Si3—C1G	106.4 (2)
Si1—K1—H2W	98.5	O3—Si3—C1I	112.06 (19)
Si2—K1—H2W	86.9	C1H—Si3—C1I	107.2 (2)
H1W—K1—H2W	27.4	C1G—Si3—C1I	103.7 (2)
O2—K2—O4	88.06 (10)	C1H—Si3—K3	133.75 (19)
O2—K2—O1	93.78 (9)	C1G—Si3—K3	76.06 (13)
O4—K2—O1	138.89 (9)	C1I—Si3—K3	117.14 (16)
O2—K2—O1U	123.65 (10)	C1H—Si3—K6	126.87 (15)
O4—K2—O1U	89.33 (10)	C1G—Si3—K6	125.67 (14)
O1—K2—O1U	55.98 (9)	C1I—Si3—K6	72.66 (15)
O2—K2—C1J	116.06 (11)	K3—Si3—K6	60.54 (3)
O4—K2—C1J	57.65 (11)	C1H—Si3—K5	82.18 (16)
O1—K2—C1J	148.28 (10)	C1G—Si3—K5	134.89 (13)
O1U—K2—C1J	109.31 (11)	C1I—Si3—K5	116.02 (16)
O2—K2—C2J	100.16 (12)	K3—Si3—K5	67.59 (4)
O4—K2—C2J	74.39 (11)	K6—Si3—K5	54.85 (3)
O1—K2—C2J	144.63 (12)	C2G—C1G—C6G	116.0 (4)
O1U—K2—C2J	132.84 (12)	C2G—C1G—Si3	123.8 (3)
C1J—K2—C2J	25.83 (13)	C6G—C1G—Si3	120.1 (3)
O2—K2—O1W	51.09 (8)	C3G—C2G—C1G	121.7 (5)
O4—K2—O1W	75.05 (8)	C3G—C2G—H2G	119.2
O1—K2—O1W	74.51 (8)	C1G—C2G—H2G	119.2
O1U—K2—O1W	73.99 (8)	C2G—C3G—C4G	120.6 (5)
C1J—K2—O1W	132.22 (10)	C2G—C3G—H3G	119.7
C2J—K2—O1W	138.26 (11)	C4G—C3G—H3G	119.7
O2—K2—Si4	100.48 (7)	C5G—C4G—C3G	119.5 (5)
O4—K2—Si4	25.27 (6)	C5G—C4G—H4G	120.2
O1—K2—Si4	156.30 (7)	C3G—C4G—H4G	120.2
O1U—K2—Si4	100.33 (7)	C4G—C5G—C6G	119.3 (5)
C1J—K2—Si4	32.43 (9)	C4G—C5G—H5G	120.4
C2J—K2—Si4	50.75 (10)	C6G—C5G—H5G	120.4
O1W—K2—Si4	99.96 (6)	C5G—C6G—C1G	122.9 (5)
O2—K2—K6	91.57 (7)	C5G—C6G—K3	121.9 (4)
O4—K2—K6	45.27 (7)	C1G—C6G—K3	94.2 (3)
O1—K2—K6	93.62 (7)	C5G—C6G—H6G	118.5
O1U—K2—K6	51.23 (7)	C1G—C6G—H6G	118.5
C1J—K2—K6	95.93 (9)	K3—C6G—H6G	51.0
C2J—K2—K6	118.09 (10)	C6H—C1H—C2H	116.7 (6)
O1W—K2—K6	47.54 (5)	C6H—C1H—Si3	121.4 (5)
Si4—K2—K6	67.36 (3)	C2H—C1H—Si3	121.9 (4)
O2—K2—Si2	17.94 (7)	C1H—C2H—C3H	121.2 (6)
O4—K2—Si2	94.85 (7)	C1H—C2H—H2H	119.4
O1—K2—Si2	99.32 (7)	C3H—C2H—H2H	119.4
O1U—K2—Si2	140.16 (7)	C4H—C3H—C2H	120.0 (8)
C1J—K2—Si2	106.24 (9)	C4H—C3H—H3H	120.0
C2J—K2—Si2	86.02 (11)	C2H—C3H—H3H	120.0
O1W—K2—Si2	68.98 (6)	C3H—C4H—C5H	120.1 (7)
Si4—K2—Si2	100.01 (4)	C3H—C4H—H4H	120.0
K6—K2—Si2	108.08 (4)	C5H—C4H—H4H	120.0
O2—K2—K1	47.86 (7)	C4H—C5H—C6H	120.8 (8)
O4—K2—K1	125.14 (7)	C4H—C5H—H5H	119.6
O1—K2—K1	46.13 (6)	C6H—C5H—H5H	119.6
O1U—K2—K1	91.48 (7)	C5H—C6H—C1H	121.2 (8)
C1J—K2—K1	159.22 (9)	C5H—C6H—H6H	119.4
C2J—K2—K1	134.18 (10)	C1H—C6H—H6H	119.4
O1W—K2—K1	52.84 (5)	C2I—C1I—C6I	116.3 (5)
Si4—K2—K1	146.03 (4)	C2I—C1I—Si3	123.6 (4)
K6—K2—K1	97.48 (3)	C6I—C1I—Si3	120.0 (4)
Si2—K2—K1	54.31 (3)	C3I—C2I—C1I	122.7 (6)
O2—K2—K4	47.70 (7)	C3I—C2I—H2I	118.6
O4—K2—K4	41.11 (6)	C1I—C2I—H2I	118.6
O1—K2—K4	121.39 (6)	C4I—C3I—C2I	119.3 (7)
O1U—K2—K4	104.96 (7)	C4I—C3I—H3I	120.4
C1J—K2—K4	88.42 (8)	C2I—C3I—H3I	120.4
C2J—K2—K4	91.30 (10)	C5I—C4I—C3I	120.5 (7)
O1W—K2—K4	47.28 (5)	C5I—C4I—H4I	119.7
Si4—K2—K4	59.84 (3)	C3I—C4I—H4I	119.7
K6—K2—K4	54.84 (3)	C4I—C5I—C6I	120.1 (7)
Si2—K2—K4	58.44 (3)	C4I—C5I—H5I	120.0
K1—K2—K4	86.41 (3)	C6I—C5I—H5I	120.0
O2—K2—H1U	120.3	C5I—C6I—C1I	121.0 (6)
O4—K2—H1U	105.7	C5I—C6I—K6	113.1 (4)
O1—K2—H1U	40.0	C1I—C6I—K6	96.5 (3)
O1U—K2—H1U	16.6	C5I—C6I—H6I	119.5
C1J—K2—H1U	120.3	C1I—C6I—H6I	119.5
C2J—K2—H1U	139.5	K6—C6I—H6I	59.1
O1W—K2—H1U	76.5	Si4—O4—K4	124.68 (16)
Si4—K2—H1U	116.4	Si4—O4—K6	142.33 (17)
K6—K2—H1U	65.2	K4—O4—K6	84.52 (9)
Si2—K2—H1U	133.3	Si4—O4—K2	108.43 (15)
K1—K2—H1U	79.9	K4—O4—K2	95.92 (10)
K4—K2—H1U	115.7	K6—O4—K2	89.06 (9)
O3—K3—O5	101.18 (9)	O4—Si4—C1K	115.49 (19)
O3—K3—O1U	90.92 (10)	O4—Si4—C1L	111.9 (2)
O5—K3—O1U	124.70 (10)	C1K—Si4—C1L	103.8 (2)
O3—K3—O1	136.33 (9)	O4—Si4—C1J	109.10 (17)
O5—K3—O1	83.07 (8)	C1K—Si4—C1J	107.4 (2)
O1U—K3—O1	54.29 (9)	C1L—Si4—C1J	108.9 (2)
O3—K3—O1W	73.13 (9)	C1K—Si4—K2	126.16 (14)
O5—K3—O1W	54.31 (8)	C1L—Si4—K2	129.85 (15)
O1U—K3—O1W	79.41 (9)	C1J—Si4—K2	62.93 (12)
O1—K3—O1W	74.90 (8)	C1K—Si4—K4	80.78 (14)
O3—K3—C6C	155.41 (10)	C1L—Si4—K4	126.94 (15)
O5—K3—C6C	82.19 (10)	C1J—Si4—K4	120.14 (13)
O1U—K3—C6C	107.31 (10)	K2—Si4—K4	65.34 (3)
O1—K3—C6C	68.11 (9)	C6J—C1J—C2J	116.3 (5)
O1W—K3—C6C	125.51 (10)	C6J—C1J—Si4	122.3 (4)
O3—K3—C6G	69.79 (11)	C2J—C1J—Si4	120.5 (3)
O5—K3—C6G	148.97 (11)	C6J—C1J—K2	98.6 (3)
O1U—K3—C6G	85.83 (11)	C2J—C1J—K2	77.6 (2)
O1—K3—C6G	124.50 (10)	Si4—C1J—K2	84.63 (14)
O1W—K3—C6G	139.68 (10)	C3J—C2J—C1J	121.8 (5)
C6C—K3—C6G	94.66 (12)	C3J—C2J—K2	98.7 (3)
O3—K3—Si3	22.00 (6)	C1J—C2J—K2	76.6 (3)
O5—K3—Si3	117.72 (7)	C3J—C2J—H2J	119.1
O1U—K3—Si3	92.12 (8)	C1J—C2J—H2J	119.1
O1—K3—Si3	145.88 (6)	K2—C2J—H2J	94.7
O1W—K3—Si3	94.93 (6)	C4J—C3J—C2J	119.8 (6)
C6C—K3—Si3	137.16 (8)	C4J—C3J—H3J	120.1
C6G—K3—Si3	48.07 (9)	C2J—C3J—H3J	120.1
O3—K3—Si5	93.26 (7)	C5J—C4J—C3J	120.4 (5)
O5—K3—Si5	20.73 (6)	C5J—C4J—H4J	119.8
O1U—K3—Si5	144.79 (8)	C3J—C4J—H4J	119.8
O1—K3—Si5	101.88 (6)	C4J—C5J—C6J	120.0 (6)
O1W—K3—Si5	68.51 (6)	C4J—C5J—H5J	120.0
C6C—K3—Si5	81.40 (8)	C6J—C5J—H5J	120.0
C6G—K3—Si5	128.23 (9)	C1J—C6J—C5J	121.5 (5)
Si3—K3—Si5	104.39 (4)	C1J—C6J—H6J	119.2
O3—K3—K6	47.05 (7)	C5J—C6J—H6J	119.2
O5—K3—K6	101.65 (7)	C2K—C1K—C6K	116.3 (4)
O1U—K3—K6	51.53 (7)	C2K—C1K—Si4	119.1 (4)
O1—K3—K6	89.35 (6)	C6K—C1K—Si4	124.2 (4)
O1W—K3—K6	48.58 (6)	C1K—C2K—C3K	121.1 (6)
C6C—K3—K6	156.67 (8)	C1K—C2K—H2K	119.5
C6G—K3—K6	93.35 (9)	C3K—C2K—H2K	119.5
Si3—K3—K6	61.29 (3)	C4K—C3K—C2K	120.9 (6)
Si5—K3—K6	110.27 (4)	C4K—C3K—H3K	119.5
O3—K3—Si1	156.76 (7)	C2K—C3K—H3K	119.5
O5—K3—Si1	87.11 (7)	C5K—C4K—C3K	118.7 (5)
O1U—K3—Si1	66.85 (7)	C5K—C4K—H4K	120.7
O1—K3—Si1	22.43 (5)	C3K—C4K—H4K	120.7
O1W—K3—Si1	95.20 (6)	C4K—C5K—C6K	120.7 (6)
C6C—K3—Si1	46.63 (8)	C4K—C5K—H5K	119.7
C6G—K3—Si1	113.08 (9)	C6K—C5K—H5K	119.7
Si3—K3—Si1	154.43 (4)	C5K—C6K—C1K	122.3 (6)
Si5—K3—Si1	101.17 (4)	C5K—C6K—H6K	118.8
K6—K3—Si1	110.21 (3)	C1K—C6K—H6K	118.8
O3—K3—K1	124.21 (7)	C6L—C1L—C2L	115.8 (5)
O5—K3—K1	39.09 (6)	C6L—C1L—Si4	121.4 (4)
O1U—K3—K1	90.32 (8)	C2L—C1L—Si4	122.7 (4)
O1—K3—K1	44.12 (6)	C1L—C2L—C3L	121.6 (7)
O1W—K3—K1	52.42 (5)	C1L—C2L—H2L	119.2
C6C—K3—K1	73.24 (8)	C3L—C2L—H2L	119.2
C6G—K3—K1	165.61 (9)	C4L—C3L—C2L	120.9 (7)
Si3—K3—K1	146.12 (4)	C4L—C3L—H3L	119.5
Si5—K3—K1	58.86 (3)	C2L—C3L—H3L	119.5
K6—K3—K1	95.09 (3)	C5L—C4L—C3L	119.0 (6)
Si1—K3—K1	52.90 (3)	C5L—C4L—H4L	120.5
O3—K3—H2W	78.1	C3L—C4L—H4L	120.5
O5—K3—H2W	40.7	C4L—C5L—C6L	120.6 (7)
O1U—K3—H2W	92.1	C4L—C5L—H5L	119.7
O1—K3—H2W	77.9	C6L—C5L—H5L	119.7
O1W—K3—H2W	13.8	C1L—C6L—C5L	122.0 (7)
C6C—K3—H2W	116.4	C1L—C6L—H6L	119.0
C6G—K3—H2W	147.8	C5L—C6L—H6L	119.0
Si3—K3—H2W	100.1	Si5—O5—K1	131.25 (15)
Si5—K3—H2W	54.9	Si5—O5—K3	123.40 (15)
K6—K3—H2W	61.5	K1—O5—K3	101.18 (10)
Si1—K3—H2W	95.3	O5—Si5—C1N	112.35 (17)
K1—K3—H2W	46.1	O5—Si5—C1M	112.04 (16)
O3—K3—H1U	107.6	C1N—Si5—C1M	105.70 (18)
O5—K3—H1U	114.2	O5—Si5—C1O	110.40 (17)
O1U—K3—H1U	17.6	C1N—Si5—C1O	106.24 (18)
O1—K3—H1U	37.1	C1M—Si5—C1O	109.85 (19)
O1W—K3—H1U	79.7	C1N—Si5—K3	139.14 (14)
C6C—K3—H1U	92.7	C1M—Si5—K3	79.64 (12)
C6G—K3—H1U	96.7	C1O—Si5—K3	109.76 (13)
Si3—K3—H1U	109.6	C1N—Si5—K1	81.95 (13)
Si5—K3—H1U	134.9	C1M—Si5—K1	126.68 (13)
K6—K3—H1U	64.6	C1O—Si5—K1	118.43 (14)
Si1—K3—H1U	49.7	K3—Si5—K1	64.33 (3)
K1—K3—H1U	76.5	C2M—C1M—C6M	116.2 (4)
H2W—K3—H1U	90.2	C2M—C1M—Si5	121.5 (3)
O4—K4—O6	88.80 (10)	C6M—C1M—Si5	122.2 (3)
O4—K4—O2	83.71 (9)	C3M—C2M—C1M	122.7 (4)
O6—K4—O2	126.55 (9)	C3M—C2M—H2M	118.6
O4—K4—O1W	83.75 (9)	C1M—C2M—H2M	118.6
O6—K4—O1W	72.75 (8)	C4M—C3M—C2M	119.2 (4)
O2—K4—O1W	53.86 (8)	C4M—C3M—H3M	120.4
O4—K4—C2R	142.42 (12)	C2M—C3M—H3M	120.4
O6—K4—C2R	69.79 (11)	C5M—C4M—C3M	120.4 (4)
O2—K4—C2R	133.86 (11)	C5M—C4M—H4M	119.8
O1W—K4—C2R	116.47 (12)	C3M—C4M—H4M	119.8
O4—K4—C2F	102.49 (12)	C4M—C5M—C6M	119.7 (4)
O6—K4—C2F	162.93 (11)	C4M—C5M—H5M	120.2
O2—K4—C2F	68.15 (10)	C6M—C5M—H5M	120.2
O1W—K4—C2F	120.72 (10)	C5M—C6M—C1M	121.8 (4)
C2R—K4—C2F	93.79 (13)	C5M—C6M—H6M	119.1
O4—K4—C1R	118.40 (11)	C1M—C6M—H6M	119.1
O6—K4—C1R	55.20 (10)	C6N—C1N—C2N	116.3 (4)
O2—K4—C1R	157.51 (10)	C6N—C1N—Si5	121.2 (3)
O1W—K4—C1R	120.54 (10)	C2N—C1N—Si5	122.4 (3)
C2R—K4—C1R	24.30 (12)	C3N—C2N—C1N	121.5 (4)
C2F—K4—C1R	107.80 (12)	C3N—C2N—H2N	119.3
O4—K4—K6	48.66 (7)	C1N—C2N—H2N	119.3
O6—K4—K6	48.28 (7)	C4N—C3N—C2N	120.7 (4)
O2—K4—K6	91.24 (6)	C4N—C3N—H3N	119.6
O1W—K4—K6	51.86 (6)	C2N—C3N—H3N	119.6
C2R—K4—K6	118.05 (10)	C3N—C4N—C5N	119.2 (4)
C2F—K4—K6	147.62 (9)	C3N—C4N—H4N	120.4
C1R—K4—K6	100.47 (9)	C5N—C4N—H4N	120.4
O4—K4—Si6	100.27 (8)	C6N—C5N—C4N	119.8 (5)
O6—K4—Si6	23.96 (6)	C6N—C5N—H5N	120.1
O2—K4—Si6	148.22 (7)	C4N—C5N—H5N	120.1
O1W—K4—Si6	94.95 (6)	C5N—C6N—C1N	122.4 (4)
C2R—K4—Si6	49.63 (9)	C5N—C6N—H6N	118.8
C2F—K4—Si6	139.23 (9)	C1N—C6N—H6N	118.8
C1R—K4—Si6	31.54 (8)	C2O—C1O—C6O	117.1 (4)
K6—K4—Si6	69.62 (4)	C2O—C1O—Si5	118.6 (3)
O4—K4—Si4	20.47 (6)	C6O—C1O—Si5	124.2 (3)
O6—K4—Si4	100.28 (7)	C2O—C1O—K5	79.3 (2)
O2—K4—Si4	90.45 (6)	C6O—C1O—K5	80.2 (2)
O1W—K4—Si4	103.30 (7)	Si5—C1O—K5	107.22 (16)
C2R—K4—Si4	132.27 (10)	C1O—C2O—C3O	122.9 (5)
C2F—K4—Si4	87.21 (9)	C1O—C2O—K5	75.8 (2)
C1R—K4—Si4	111.72 (8)	C3O—C2O—K5	84.4 (3)
K6—K4—Si4	67.53 (3)	C1O—C2O—H1O	118.6
Si6—K4—Si4	104.27 (4)	C3O—C2O—H1O	118.6
O4—K4—Si2	97.81 (8)	K5—C2O—H1O	111.0
O6—K4—Si2	144.68 (7)	C2O—C3O—C4O	119.1 (5)
O2—K4—Si2	22.97 (6)	C2O—C3O—K5	71.4 (3)
O1W—K4—Si2	73.56 (6)	C4O—C3O—K5	80.5 (3)
C2R—K4—Si2	117.68 (10)	C2O—C3O—H3O	120.5
C2F—K4—Si2	47.16 (8)	C4O—C3O—H3O	120.5
C1R—K4—Si2	141.40 (8)	K5—C3O—H3O	118.6
K6—K4—Si2	114.15 (4)	C5O—C4O—C3O	119.7 (5)
Si6—K4—Si2	157.36 (4)	C5O—C4O—K5	75.6 (3)
Si4—K4—Si2	97.43 (4)	C3O—C4O—K5	76.0 (3)
O4—K4—K2	42.97 (7)	C5O—C4O—H4O	120.2
O6—K4—K2	107.88 (7)	C3O—C4O—H4O	120.2
O2—K4—K2	41.43 (6)	K5—C4O—H4O	119.3
O1W—K4—K2	56.29 (6)	C4O—C5O—C6O	120.6 (5)
C2R—K4—K2	172.46 (11)	C4O—C5O—K5	81.0 (3)
C2F—K4—K2	89.00 (9)	C6O—C5O—K5	73.0 (3)
C1R—K4—K2	158.75 (8)	C4O—C5O—H5O	119.7
K6—K4—K2	60.21 (3)	C6O—C5O—H5O	119.7
Si6—K4—K2	129.75 (4)	K5—C5O—H5O	117.0
Si4—K4—K2	54.82 (3)	C5O—C6O—C1O	120.7 (5)
Si2—K4—K2	59.83 (3)	C5O—C6O—K5	82.8 (3)
O4—K4—H1W	88.4	C1O—C6O—K5	74.4 (2)
O6—K4—H1W	88.0	C5O—C6O—H6O	119.7
O2—K4—H1W	39.1	C1O—C6O—H6O	119.7
O1W—K4—H1W	16.0	K5—C6O—H6O	113.5
C2R—K4—H1W	120.0	Si6—O6—K5	116.16 (15)
C2F—K4—H1W	104.8	Si6—O6—K6	146.05 (17)
C1R—K4—H1W	130.8	K5—O6—K6	83.62 (9)
K6—K4—H1W	65.6	Si6—O6—K4	112.91 (15)
Si6—K4—H1W	109.2	K5—O6—K4	108.10 (10)
Si4—K4—H1W	105.6	K6—O6—K4	83.37 (9)
Si2—K4—H1W	57.7	O6—Si6—C1Q	112.90 (18)
K2—K4—H1W	52.4	O6—Si6—C1P	111.49 (18)
O6—K5—O3	96.22 (10)	C1Q—Si6—C1P	107.6 (2)
O6—K5—O1W	75.05 (9)	O6—Si6—C1R	109.93 (19)
O3—K5—O1W	77.20 (9)	C1Q—Si6—C1R	107.1 (2)
O6—K5—C1O	143.65 (11)	C1P—Si6—C1R	107.6 (2)
O3—K5—C1O	106.78 (11)	C1Q—Si6—K5	130.46 (15)
O1W—K5—C1O	82.93 (10)	C1P—Si6—K5	71.18 (13)
O6—K5—C2O	119.93 (11)	C1R—Si6—K5	120.70 (15)
O3—K5—C2O	127.46 (10)	C1Q—Si6—K4	118.67 (16)
O1W—K5—C2O	77.21 (11)	C1P—Si6—K4	132.99 (14)
C1O—K5—C2O	24.94 (11)	C1R—Si6—K4	67.59 (15)
O6—K5—C6O	158.27 (11)	K5—Si6—K4	72.75 (3)
O3—K5—C6O	105.42 (11)	C2P—C1P—C6P	117.0 (5)
O1W—K5—C6O	107.47 (10)	C2P—C1P—Si6	124.2 (4)
C1O—K5—C6O	25.41 (11)	C6P—C1P—Si6	118.7 (4)
C2O—K5—C6O	43.27 (12)	C2P—C1P—K5	119.7 (3)
O6—K5—C6P	69.63 (12)	C6P—C1P—K5	71.3 (3)
O3—K5—C6P	106.67 (13)	Si6—C1P—K5	77.63 (14)
O1W—K5—C6P	144.67 (11)	C3P—C2P—C1P	122.0 (6)
C1O—K5—C6P	126.72 (14)	C3P—C2P—H2P	119.0
C2O—K5—C6P	120.50 (14)	C1P—C2P—H2P	119.0
C6O—K5—C6P	105.19 (13)	C4P—C3P—C2P	120.3 (6)
O6—K5—C5O	138.05 (11)	C4P—C3P—H3P	119.8
O3—K5—C5O	122.59 (12)	C2P—C3P—H3P	119.8
O1W—K5—C5O	125.08 (11)	C3P—C4P—C5P	119.6 (6)
C1O—K5—C5O	43.64 (11)	C3P—C4P—H4P	120.2
C2O—K5—C5O	49.35 (12)	C5P—C4P—H4P	120.2
C6O—K5—C5O	24.19 (11)	C4P—C5P—C6P	120.2 (6)
C6P—K5—C5O	83.31 (13)	C4P—C5P—H5P	119.9
O6—K5—C3O	109.15 (11)	C6P—C5P—H5P	119.9
O3—K5—C3O	150.20 (11)	C1P—C6P—C5P	120.9 (6)
O1W—K5—C3O	94.10 (11)	C1P—C6P—K5	85.0 (3)
C1O—K5—C3O	43.47 (11)	C5P—C6P—K5	111.7 (4)
C2O—K5—C3O	24.19 (11)	C1P—C6P—H6P	119.5
C6O—K5—C3O	49.56 (13)	C5P—C6P—H6P	119.5
C6P—K5—C3O	96.89 (14)	K5—C6P—H6P	73.3
C5O—K5—C3O	41.65 (13)	C6Q—C1Q—C2Q	117.0 (4)
O6—K5—C4O	116.92 (11)	C6Q—C1Q—Si6	122.7 (4)
O3—K5—C4O	145.89 (12)	C2Q—C1Q—Si6	120.2 (3)
O1W—K5—C4O	117.33 (12)	C3Q—C2Q—C1Q	121.5 (5)
C1O—K5—C4O	50.28 (11)	C3Q—C2Q—H2Q	119.2
C2O—K5—C4O	42.13 (12)	C1Q—C2Q—H2Q	119.2
C6O—K5—C4O	42.16 (12)	C4Q—C3Q—C2Q	120.2 (5)
C6P—K5—C4O	79.60 (14)	C4Q—C3Q—H3Q	119.9
C5O—K5—C4O	23.42 (13)	C2Q—C3Q—H3Q	119.9
C3O—K5—C4O	23.57 (13)	C3Q—C4Q—C5Q	119.7 (5)
O6—K5—C1P	54.52 (10)	C3Q—C4Q—H4Q	120.2
O3—K5—C1P	122.84 (11)	C5Q—C4Q—H4Q	120.2
O1W—K5—C1P	125.69 (10)	C6Q—C5Q—C4Q	119.7 (5)
C1O—K5—C1P	125.78 (11)	C6Q—C5Q—H5Q	120.2
C2O—K5—C1P	109.40 (11)	C4Q—C5Q—H5Q	120.2
C6O—K5—C1P	112.58 (11)	C5Q—C6Q—C1Q	121.8 (5)
C6P—K5—C1P	23.70 (12)	C5Q—C6Q—H6Q	119.1
C5O—K5—C1P	88.40 (11)	C1Q—C6Q—H6Q	119.1
C3O—K5—C1P	85.51 (12)	C2R—C1R—C6R	116.1 (5)
C4O—K5—C1P	75.65 (12)	C2R—C1R—Si6	120.6 (4)
O6—K5—K6	49.08 (7)	C6R—C1R—Si6	123.1 (4)
O3—K5—K6	51.15 (7)	C2R—C1R—K4	71.1 (3)
O1W—K5—K6	52.76 (6)	C6R—C1R—K4	114.6 (4)
C1O—K5—K6	131.76 (8)	Si6—C1R—K4	80.87 (15)
C2O—K5—K6	129.81 (9)	C1R—C2R—C3R	121.7 (5)
C6O—K5—K6	149.07 (9)	C1R—C2R—K4	84.6 (3)
C6P—K5—K6	101.51 (11)	C3R—C2R—K4	108.3 (4)
C5O—K5—K6	172.86 (9)	C1R—C2R—H2R	119.1
C3O—K5—K6	141.37 (10)	C3R—C2R—H2R	119.1
C4O—K5—K6	162.23 (10)	K4—C2R—H2R	76.9
C1P—K5—K6	98.13 (8)	C4R—C3R—C2R	119.7 (6)
O6—K5—H2W	91.7	C4R—C3R—H3R	120.2
O3—K5—H2W	73.6	C2R—C3R—H3R	120.2
O1W—K5—H2W	16.7	C3R—C4R—C5R	120.3 (6)
C1O—K5—H2W	69.1	C3R—C4R—H4R	119.8
C2O—K5—H2W	68.9	C5R—C4R—H4R	119.8
C6O—K5—H2W	92.4	C4R—C5R—C6R	119.9 (6)
C6P—K5—H2W	161.3	C4R—C5R—H5R	120.1
C5O—K5—H2W	112.7	C6R—C5R—H5R	120.1
C3O—K5—H2W	89.8	C5R—C6R—C1R	122.2 (6)
C4O—K5—H2W	111.0	C5R—C6R—H6R	118.9
C1P—K5—H2W	141.4	C1R—C6R—H6R	118.9
K6—K5—H2W	63.6	C2S—C1S—C6S	120.0
O6—K6—O4	87.27 (9)	C2S—C1S—C7S	122.9 (8)
O6—K6—O3	91.07 (9)	C6S—C1S—C7S	117.1 (8)
O4—K6—O3	158.39 (9)	C1S—C2S—C3S	120.0
O6—K6—O1W	74.02 (9)	C1S—C2S—H2S	120.0
O4—K6—O1W	83.88 (9)	C3S—C2S—H2S	120.0
O3—K6—O1W	74.98 (9)	C4S—C3S—C2S	120.0
O6—K6—O1U	154.09 (10)	C4S—C3S—H3S	120.0
O4—K6—O1U	87.91 (9)	C2S—C3S—H3S	120.0
O3—K6—O1U	84.21 (9)	C5S—C4S—C3S	120.0
O1W—K6—O1U	80.15 (9)	C5S—C4S—H4S	120.0
O6—K6—C6I	93.38 (14)	C3S—C4S—H4S	120.0
O4—K6—C6I	133.70 (13)	C4S—C5S—C6S	120.0
O3—K6—C6I	67.90 (12)	C4S—C5S—H5S	120.0
O1W—K6—C6I	140.54 (13)	C6S—C5S—H5S	120.0
O1U—K6—C6I	108.19 (13)	C5S—C6S—C1S	120.0
O6—K6—K5	47.30 (7)	C5S—C6S—H6S	120.0
O4—K6—K5	120.97 (7)	C1S—C6S—H6S	120.0
O3—K6—K5	47.42 (6)	C1S—C7S—H7SA	109.5
O1W—K6—K5	52.82 (6)	C1S—C7S—H7SB	109.5
O1U—K6—K5	116.28 (7)	H7SA—C7S—H7SB	109.5
C6I—K6—K5	90.97 (12)	C1S—C7S—H7SC	109.5
O6—K6—K4	48.36 (7)	H7SA—C7S—H7SC	109.5
O4—K6—K4	46.82 (7)	H7SB—C7S—H7SC	109.5
O3—K6—K4	119.13 (7)	C2X—C1X—C6X	120.0
O1W—K6—K4	53.77 (6)	C2X—C1X—C7X	118.8 (12)
O1U—K6—K4	112.95 (7)	C6X—C1X—C7X	121.2 (12)
C6I—K6—K4	138.70 (12)	C3X—C2X—C1X	120.0
K5—K6—K4	74.30 (3)	C3X—C2X—H2X	120.0
O6—K6—K2	112.66 (7)	C1X—C2X—H2X	120.0
O4—K6—K2	45.67 (7)	C2X—C3X—C4X	120.0
O3—K6—K2	116.58 (7)	C2X—C3X—H3X	120.0
O1W—K6—K2	58.94 (6)	C4X—C3X—H3X	120.0
O1U—K6—K2	49.25 (7)	C5X—C4X—C3X	120.0
C6I—K6—K2	152.96 (13)	C5X—C4X—H4X	120.0
K5—K6—K2	111.73 (4)	C3X—C4X—H4X	120.0
K4—K6—K2	64.96 (3)	C6X—C5X—C4X	120.0
O6—K6—K3	115.12 (7)	C6X—C5X—H5X	120.0
O4—K6—K3	118.47 (7)	C4X—C5X—H5X	120.0
O3—K6—K3	43.94 (6)	C5X—C6X—C1X	120.0
O1W—K6—K3	53.98 (6)	C5X—C6X—H6X	120.0
O1U—K6—K3	47.04 (6)	C1X—C6X—H6X	120.0
C6I—K6—K3	103.00 (10)	C1X—C7X—H7XA	109.5
K5—K6—K3	69.79 (3)	C1X—C7X—H7XB	109.5
K4—K6—K3	107.30 (4)	H7XA—C7X—H7XB	109.5
K2—K6—K3	73.23 (3)	C1X—C7X—H7XC	109.5
O6—K6—Si3	98.00 (7)	H7XA—C7X—H7XC	109.5
O4—K6—Si3	174.60 (7)	H7XB—C7X—H7XC	109.5
O3—K6—Si3	21.46 (6)	C2T—C1T—C6T	120.0
O1W—K6—Si3	96.41 (7)	C2T—C1T—C7T	120.8 (10)
O1U—K6—Si3	86.83 (7)	C6T—C1T—C7T	119.2 (10)
C6I—K6—Si3	47.51 (10)	C3T—C2T—C1T	120.0
K5—K6—Si3	62.77 (3)	C3T—C2T—H2T	120.0
K4—K6—Si3	137.06 (4)	C1T—C2T—H2T	120.0
K2—K6—Si3	130.19 (4)	C2T—C3T—C4T	120.0
K3—K6—Si3	58.16 (3)	C2T—C3T—H3T	120.0
Si1—O1—K2	143.67 (15)	C4T—C3T—H3T	120.0
Si1—O1—K1	102.96 (13)	C5T—C4T—C3T	120.0
K2—O1—K1	89.27 (8)	C5T—C4T—H4T	120.0
Si1—O1—K3	111.76 (13)	C3T—C4T—H4T	120.0
K2—O1—K3	102.65 (9)	C4T—C5T—C6T	120.0
K1—O1—K3	87.86 (8)	C4T—C5T—H5T	120.0
O1—Si1—C1C	112.06 (16)	C6T—C5T—H5T	120.0
O1—Si1—C1B	111.80 (16)	C5T—C6T—C1T	120.0
C1C—Si1—C1B	108.60 (17)	C5T—C6T—H6T	120.0
O1—Si1—C1A	110.26 (16)	C1T—C6T—H6T	120.0
C1C—Si1—C1A	105.92 (17)	C1T—C7T—H7T1	109.5
C1B—Si1—C1A	107.94 (17)	C1T—C7T—H7T2	109.5
C1C—Si1—K1	109.67 (12)	H7T1—C7T—H7T2	109.5
C1B—Si1—K1	141.71 (13)	C1T—C7T—H7T3	109.5
C1A—Si1—K1	62.19 (11)	H7T1—C7T—H7T3	109.5
C1C—Si1—K3	66.42 (12)	H7T2—C7T—H7T3	109.5
C1B—Si1—K3	131.44 (13)	C2Y—C1Y—C6Y	120.0
C1A—Si1—K3	120.04 (12)	C2Y—C1Y—C7Y	106 (4)
K1—Si1—K3	65.69 (3)	C6Y—C1Y—C7Y	134 (4)
C2A—C1A—C6A	116.2 (4)	C3Y—C2Y—C1Y	120.0
C2A—C1A—Si1	119.6 (3)	C3Y—C2Y—H2Y	120.0
C6A—C1A—Si1	123.9 (3)	C1Y—C2Y—H2Y	120.0
C2A—C1A—K1	85.7 (2)	C4Y—C3Y—C2Y	120.0
C6A—C1A—K1	94.0 (2)	C4Y—C3Y—H3Y	120.0
Si1—C1A—K1	85.45 (13)	C2Y—C3Y—H3Y	120.0
C3A—C2A—C1A	122.9 (4)	C3Y—C4Y—C5Y	120.0
C3A—C2A—K1	101.8 (3)	C3Y—C4Y—H4Y	120.0
C1A—C2A—K1	69.7 (2)	C5Y—C4Y—H4Y	120.0
C3A—C2A—H2A	118.5	C6Y—C5Y—C4Y	120.0
C1A—C2A—H2A	118.5	C6Y—C5Y—H5Y	120.0
K1—C2A—H2A	98.6	C4Y—C5Y—H5Y	120.0
C2A—C3A—C4A	119.8 (4)	C5Y—C6Y—C1Y	120.0
C2A—C3A—H3A	120.1	C5Y—C6Y—H6Y	120.0
C4A—C3A—H3A	120.1	C1Y—C6Y—H6Y	120.0
C5A—C4A—C3A	119.0 (4)	C1Y—C7Y—H7Y1	109.5
C5A—C4A—H4A	120.5	C1Y—C7Y—H7Y2	109.5
C3A—C4A—H4A	120.5	H7Y1—C7Y—H7Y2	109.5
C4A—C5A—C6A	120.5 (4)	C1Y—C7Y—H7Y3	109.5
C4A—C5A—H5A	119.7	H7Y1—C7Y—H7Y3	109.5
C6A—C5A—H5A	119.7	H7Y2—C7Y—H7Y3	109.5
C1A—C6A—C5A	121.5 (4)	C1U—O1U—K3	134.3 (3)
C1A—C6A—K1	62.6 (2)	C1U—O1U—K2	117.8 (3)
C5A—C6A—K1	101.4 (3)	K3—O1U—K2	104.29 (11)
C1A—C6A—H6A	119.2	C1U—O1U—K6	121.5 (3)
C5A—C6A—H6A	119.2	K3—O1U—K6	81.43 (9)
K1—C6A—H6A	105.5	K2—O1U—K6	79.52 (8)
C2B—C1B—C6B	116.9 (4)	C1U—O1U—H1U	106.6
C2B—C1B—Si1	120.7 (3)	K3—O1U—H1U	76.1
C6B—C1B—Si1	122.3 (3)	K2—O1U—H1U	63.2
C1B—C2B—C3B	122.5 (4)	K6—O1U—H1U	129.1
C1B—C2B—H2B	118.8	O1U—C1U—C2U	113.1 (4)
C3B—C2B—H2B	118.8	O1U—C1U—C3U	107.6 (4)
C4B—C3B—C2B	119.0 (4)	C2U—C1U—C3U	111.1 (5)
C4B—C3B—H3B	120.5	O1U—C1U—H1UC	108.3
C2B—C3B—H3B	120.5	C2U—C1U—H1UC	108.3
C5B—C4B—C3B	120.1 (4)	C3U—C1U—H1UC	108.3
C5B—C4B—H4B	119.9	C1U—C2U—H2UA	109.5
C3B—C4B—H4B	119.9	C1U—C2U—H2UB	109.5
C4B—C5B—C6B	120.4 (4)	H2UA—C2U—H2UB	109.5
C4B—C5B—H5B	119.8	C1U—C2U—H2UC	109.5
C6B—C5B—H5B	119.8	H2UA—C2U—H2UC	109.5
C5B—C6B—C1B	121.1 (4)	H2UB—C2U—H2UC	109.5
C5B—C6B—H6B	119.5	C1U—C3U—H3UA	109.5
C1B—C6B—H6B	119.5	C1U—C3U—H3UB	109.5
C2C—C1C—C6C	116.6 (4)	H3UA—C3U—H3UB	109.5
C2C—C1C—Si1	123.2 (3)	C1U—C3U—H3UC	109.5
C6C—C1C—Si1	120.1 (3)	H3UA—C3U—H3UC	109.5
C3C—C2C—C1C	121.1 (4)	H3UB—C3U—H3UC	109.5
K2—O1—Si1—C1C	155.1 (2)	O4—Si4—C1J—C6J	−93.3 (4)
K1—O1—Si1—C1C	−97.96 (16)	C1K—Si4—C1J—C6J	140.9 (4)
K3—O1—Si1—C1C	−5.06 (19)	C1L—Si4—C1J—C6J	29.1 (4)
K2—O1—Si1—C1B	32.9 (3)	K2—Si4—C1J—C6J	−96.8 (4)
K1—O1—Si1—C1B	139.84 (14)	K4—Si4—C1J—C6J	−129.8 (3)
K3—O1—Si1—C1B	−127.25 (15)	O4—Si4—C1J—C2J	75.7 (4)
K2—O1—Si1—C1A	−87.2 (3)	C1K—Si4—C1J—C2J	−50.2 (4)
K1—O1—Si1—C1A	19.76 (17)	C1L—Si4—C1J—C2J	−162.0 (3)
K3—O1—Si1—C1A	112.67 (16)	K2—Si4—C1J—C2J	72.1 (3)
K2—O1—Si1—K1	−106.9 (3)	K4—Si4—C1J—C2J	39.1 (4)
K3—O1—Si1—K1	92.91 (13)	O4—Si4—C1J—K2	3.53 (18)
K2—O1—Si1—K3	160.2 (3)	C1K—Si4—C1J—K2	−122.31 (15)
K1—O1—Si1—K3	−92.91 (13)	C1L—Si4—C1J—K2	125.86 (17)
O1—Si1—C1A—C2A	65.2 (3)	K4—Si4—C1J—K2	−33.03 (15)
C1C—Si1—C1A—C2A	−173.4 (3)	C6J—C1J—C2J—C3J	1.5 (6)
C1B—Si1—C1A—C2A	−57.2 (4)	Si4—C1J—C2J—C3J	−168.1 (4)
K1—Si1—C1A—C2A	82.4 (3)	K2—C1J—C2J—C3J	−92.1 (4)
K3—Si1—C1A—C2A	115.0 (3)	C6J—C1J—C2J—K2	93.5 (4)
O1—Si1—C1A—C6A	−109.0 (3)	Si4—C1J—C2J—K2	−76.0 (3)
C1C—Si1—C1A—C6A	12.4 (4)	C1J—C2J—C3J—C4J	−0.4 (7)
C1B—Si1—C1A—C6A	128.6 (3)	K2—C2J—C3J—C4J	−80.1 (5)
K1—Si1—C1A—C6A	−91.8 (3)	C2J—C3J—C4J—C5J	−0.9 (8)
K3—Si1—C1A—C6A	−59.2 (4)	C3J—C4J—C5J—C6J	1.2 (8)
O1—Si1—C1A—K1	−17.25 (15)	C2J—C1J—C6J—C5J	−1.2 (6)
C1C—Si1—C1A—K1	104.20 (14)	Si4—C1J—C6J—C5J	168.2 (4)
C1B—Si1—C1A—K1	−139.63 (14)	K2—C1J—C6J—C5J	79.1 (5)
K3—Si1—C1A—K1	32.59 (12)	C4J—C5J—C6J—C1J	−0.1 (7)
C6A—C1A—C2A—C3A	1.2 (6)	O4—Si4—C1K—C2K	48.4 (4)
Si1—C1A—C2A—C3A	−173.4 (3)	C1L—Si4—C1K—C2K	−74.4 (4)
K1—C1A—C2A—C3A	−91.1 (4)	C1J—Si4—C1K—C2K	170.4 (3)
C6A—C1A—C2A—K1	92.3 (3)	K2—Si4—C1K—C2K	101.6 (4)
Si1—C1A—C2A—K1	−82.3 (2)	K4—Si4—C1K—C2K	51.6 (3)
C1A—C2A—C3A—C4A	−1.0 (7)	O4—Si4—C1K—C6K	−139.1 (4)
K1—C2A—C3A—C4A	−74.3 (4)	C1L—Si4—C1K—C6K	98.1 (4)
C2A—C3A—C4A—C5A	0.0 (7)	C1J—Si4—C1K—C6K	−17.1 (5)
C3A—C4A—C5A—C6A	0.8 (7)	K2—Si4—C1K—C6K	−85.9 (4)
C2A—C1A—C6A—C5A	−0.4 (6)	K4—Si4—C1K—C6K	−136.0 (4)
Si1—C1A—C6A—C5A	174.0 (3)	C6K—C1K—C2K—C3K	−0.5 (7)
K1—C1A—C6A—C5A	86.8 (4)	Si4—C1K—C2K—C3K	172.6 (4)
C2A—C1A—C6A—K1	−87.2 (3)	C1K—C2K—C3K—C4K	−0.6 (8)
Si1—C1A—C6A—K1	87.2 (3)	C2K—C3K—C4K—C5K	1.4 (9)
C4A—C5A—C6A—C1A	−0.6 (7)	C3K—C4K—C5K—C6K	−1.0 (9)
C4A—C5A—C6A—K1	64.1 (4)	C4K—C5K—C6K—C1K	−0.1 (9)
O1—Si1—C1B—C2B	1.0 (4)	C2K—C1K—C6K—C5K	0.9 (7)
C1C—Si1—C1B—C2B	−123.2 (3)	Si4—C1K—C6K—C5K	−171.8 (4)
C1A—Si1—C1B—C2B	122.4 (3)	O4—Si4—C1L—C6L	25.5 (5)
K1—Si1—C1B—C2B	54.8 (4)	C1K—Si4—C1L—C6L	150.7 (5)
K3—Si1—C1B—C2B	−48.6 (4)	C1J—Si4—C1L—C6L	−95.1 (5)
O1—Si1—C1B—C6B	177.6 (3)	K2—Si4—C1L—C6L	−25.1 (5)
C1C—Si1—C1B—C6B	53.4 (4)	K4—Si4—C1L—C6L	61.9 (5)
C1A—Si1—C1B—C6B	−61.0 (4)	O4—Si4—C1L—C2L	−150.2 (4)
K1—Si1—C1B—C6B	−128.6 (3)	C1K—Si4—C1L—C2L	−25.0 (5)
K3—Si1—C1B—C6B	128.0 (3)	C1J—Si4—C1L—C2L	89.2 (5)
C6B—C1B—C2B—C3B	−2.1 (6)	K2—Si4—C1L—C2L	159.2 (4)
Si1—C1B—C2B—C3B	174.7 (3)	K4—Si4—C1L—C2L	−113.8 (4)
C1B—C2B—C3B—C4B	−0.1 (7)	C6L—C1L—C2L—C3L	−0.2 (9)
C2B—C3B—C4B—C5B	2.6 (7)	Si4—C1L—C2L—C3L	175.7 (5)
C3B—C4B—C5B—C6B	−2.9 (7)	C1L—C2L—C3L—C4L	2.7 (11)
C4B—C5B—C6B—C1B	0.7 (6)	C2L—C3L—C4L—C5L	−3.8 (12)
C2B—C1B—C6B—C5B	1.7 (6)	C3L—C4L—C5L—C6L	2.6 (12)
Si1—C1B—C6B—C5B	−175.0 (3)	C2L—C1L—C6L—C5L	−1.0 (9)
O1—Si1—C1C—C2C	−124.8 (4)	Si4—C1L—C6L—C5L	−177.0 (5)
C1B—Si1—C1C—C2C	−0.8 (4)	C4L—C5L—C6L—C1L	−0.1 (12)
C1A—Si1—C1C—C2C	114.9 (4)	K1—O5—Si5—C1N	6.7 (3)
K1—Si1—C1C—C2C	−179.5 (3)	K3—O5—Si5—C1N	−145.79 (17)
K3—Si1—C1C—C2C	−128.8 (4)	K1—O5—Si5—C1M	125.6 (2)
O1—Si1—C1C—C6C	54.4 (3)	K3—O5—Si5—C1M	−27.0 (2)
C1B—Si1—C1C—C6C	178.4 (3)	K1—O5—Si5—C1O	−111.7 (2)
C1A—Si1—C1C—C6C	−65.9 (3)	K3—O5—Si5—C1O	95.8 (2)
K1—Si1—C1C—C6C	−0.3 (3)	K1—O5—Si5—K3	152.5 (3)
K3—Si1—C1C—C6C	50.5 (3)	K3—O5—Si5—K1	−152.5 (3)
C6C—C1C—C2C—C3C	2.0 (7)	O5—Si5—C1M—C2M	−117.1 (3)
Si1—C1C—C2C—C3C	−178.7 (4)	C1N—Si5—C1M—C2M	5.5 (4)
C1C—C2C—C3C—C4C	−1.1 (9)	C1O—Si5—C1M—C2M	119.8 (3)
C2C—C3C—C4C—C5C	−1.6 (9)	K3—Si5—C1M—C2M	−132.8 (3)
C3C—C4C—C5C—C6C	3.1 (8)	K1—Si5—C1M—C2M	−86.1 (3)
C4C—C5C—C6C—C1C	−2.2 (7)	O5—Si5—C1M—C6M	60.6 (4)
C4C—C5C—C6C—K3	−113.7 (4)	C1N—Si5—C1M—C6M	−176.7 (3)
C2C—C1C—C6C—C5C	−0.4 (6)	C1O—Si5—C1M—C6M	−62.5 (4)
Si1—C1C—C6C—C5C	−179.7 (3)	K3—Si5—C1M—C6M	44.9 (3)
C2C—C1C—C6C—K3	116.7 (4)	K1—Si5—C1M—C6M	91.6 (4)
Si1—C1C—C6C—K3	−62.5 (3)	C6M—C1M—C2M—C3M	0.6 (6)
K2—O2—Si2—C1F	−109.7 (2)	Si5—C1M—C2M—C3M	178.4 (3)
K1—O2—Si2—C1F	150.57 (15)	C1M—C2M—C3M—C4M	0.4 (7)
K4—O2—Si2—C1F	2.8 (2)	C2M—C3M—C4M—C5M	−0.6 (7)
K2—O2—Si2—C1E	11.2 (3)	C3M—C4M—C5M—C6M	−0.1 (7)
K1—O2—Si2—C1E	−88.52 (16)	C4M—C5M—C6M—C1M	1.1 (7)
K4—O2—Si2—C1E	123.69 (16)	C2M—C1M—C6M—C5M	−1.3 (6)
K2—O2—Si2—C1D	128.5 (2)	Si5—C1M—C6M—C5M	−179.1 (4)
K1—O2—Si2—C1D	28.73 (18)	O5—Si5—C1N—C6N	40.2 (4)
K4—O2—Si2—C1D	−119.06 (17)	C1M—Si5—C1N—C6N	−82.3 (3)
K2—O2—Si2—K1	99.7 (2)	C1O—Si5—C1N—C6N	161.0 (3)
K4—O2—Si2—K1	−147.79 (17)	K3—Si5—C1N—C6N	10.0 (4)
K2—O2—Si2—K4	−112.5 (2)	K1—Si5—C1N—C6N	43.7 (3)
K1—O2—Si2—K4	147.79 (17)	O5—Si5—C1N—C2N	−141.8 (3)
K1—O2—Si2—K2	−99.7 (2)	C1M—Si5—C1N—C2N	95.7 (3)
K4—O2—Si2—K2	112.5 (2)	C1O—Si5—C1N—C2N	−21.0 (4)
O2—Si2—C1D—C6D	−115.7 (4)	K3—Si5—C1N—C2N	−172.0 (2)
C1F—Si2—C1D—C6D	119.3 (4)	K1—Si5—C1N—C2N	−138.3 (3)
C1E—Si2—C1D—C6D	6.0 (4)	C6N—C1N—C2N—C3N	−1.6 (6)
K1—Si2—C1D—C6D	−89.7 (3)	Si5—C1N—C2N—C3N	−179.7 (3)
K4—Si2—C1D—C6D	−164.1 (3)	C1N—C2N—C3N—C4N	1.4 (7)
K2—Si2—C1D—C6D	−86.9 (4)	C2N—C3N—C4N—C5N	−0.7 (7)
O2—Si2—C1D—C2D	57.4 (4)	C3N—C4N—C5N—C6N	0.4 (6)
C1F—Si2—C1D—C2D	−67.7 (4)	C4N—C5N—C6N—C1N	−0.6 (6)
C1E—Si2—C1D—C2D	179.1 (3)	C2N—C1N—C6N—C5N	1.3 (6)
K1—Si2—C1D—C2D	83.4 (3)	Si5—C1N—C6N—C5N	179.4 (3)
K4—Si2—C1D—C2D	9.0 (4)	O5—Si5—C1O—C2O	56.8 (4)
K2—Si2—C1D—C2D	86.2 (3)	C1N—Si5—C1O—C2O	−65.3 (4)
O2—Si2—C1D—K1	−26.00 (17)	C1M—Si5—C1O—C2O	−179.2 (3)
C1F—Si2—C1D—K1	−151.06 (15)	K3—Si5—C1O—C2O	95.0 (3)
C1E—Si2—C1D—K1	95.68 (15)	K1—Si5—C1O—C2O	24.3 (4)
K4—Si2—C1D—K1	−74.42 (13)	O5—Si5—C1O—C6O	−120.0 (4)
K2—Si2—C1D—K1	2.82 (16)	C1N—Si5—C1O—C6O	118.0 (4)
C6D—C1D—C2D—C3D	−0.9 (6)	C1M—Si5—C1O—C6O	4.1 (4)
Si2—C1D—C2D—C3D	−174.5 (4)	K3—Si5—C1O—C6O	−81.7 (4)
K1—C1D—C2D—C3D	−91.5 (4)	K1—Si5—C1O—C6O	−152.5 (3)
C6D—C1D—C2D—K1	90.6 (3)	O5—Si5—C1O—K5	−30.2 (2)
Si2—C1D—C2D—K1	−83.0 (2)	C1N—Si5—C1O—K5	−152.28 (16)
C1D—C2D—C3D—C4D	−0.2 (7)	C1M—Si5—C1O—K5	93.84 (19)
K1—C2D—C3D—C4D	−72.8 (5)	K3—Si5—C1O—K5	8.05 (18)
C2D—C3D—C4D—C5D	1.4 (7)	K1—Si5—C1O—K5	−62.75 (17)
C3D—C4D—C5D—C6D	−1.4 (7)	C6O—C1O—C2O—C3O	−0.5 (6)
C4D—C5D—C6D—C1D	0.3 (7)	Si5—C1O—C2O—C3O	−177.5 (4)
C4D—C5D—C6D—K1	67.0 (5)	K5—C1O—C2O—C3O	−73.6 (4)
C2D—C1D—C6D—C5D	0.8 (6)	C6O—C1O—C2O—K5	73.1 (3)
Si2—C1D—C6D—C5D	174.2 (4)	Si5—C1O—C2O—K5	−103.9 (3)
K1—C1D—C6D—C5D	87.9 (4)	C1O—C2O—C3O—C4O	1.9 (7)
C2D—C1D—C6D—K1	−87.1 (3)	K5—C2O—C3O—C4O	−67.2 (4)
Si2—C1D—C6D—K1	86.3 (3)	C1O—C2O—C3O—K5	69.1 (4)
O2—Si2—C1E—C6E	−145.6 (4)	C2O—C3O—C4O—C5O	−1.7 (7)
C1F—Si2—C1E—C6E	−20.1 (4)	K5—C3O—C4O—C5O	−64.1 (4)
C1D—Si2—C1E—C6E	95.0 (4)	C2O—C3O—C4O—K5	62.4 (4)
K1—Si2—C1E—C6E	159.0 (4)	C3O—C4O—C5O—C6O	0.2 (7)
K4—Si2—C1E—C6E	−95.6 (4)	K5—C4O—C5O—C6O	−64.0 (4)
K2—Si2—C1E—C6E	−139.9 (4)	C3O—C4O—C5O—K5	64.3 (5)
O2—Si2—C1E—C2E	37.9 (4)	C4O—C5O—C6O—C1O	1.2 (7)
C1F—Si2—C1E—C2E	163.3 (4)	K5—C5O—C6O—C1O	−67.0 (4)
C1D—Si2—C1E—C2E	−81.5 (4)	C4O—C5O—C6O—K5	68.2 (4)
K1—Si2—C1E—C2E	−17.5 (4)	C2O—C1O—C6O—C5O	−1.1 (6)
K4—Si2—C1E—C2E	87.8 (4)	Si5—C1O—C6O—C5O	175.7 (3)
K2—Si2—C1E—C2E	43.5 (3)	K5—C1O—C6O—C5O	71.5 (4)
C6E—C1E—C2E—C3E	−3.0 (7)	C2O—C1O—C6O—K5	−72.6 (3)
Si2—C1E—C2E—C3E	173.7 (4)	Si5—C1O—C6O—K5	104.3 (3)
C1E—C2E—C3E—C4E	0.7 (7)	K5—O6—Si6—C1Q	126.2 (2)
C2E—C3E—C4E—C5E	1.9 (7)	K6—O6—Si6—C1Q	5.7 (4)
C3E—C4E—C5E—C6E	−2.1 (9)	K4—O6—Si6—C1Q	−108.1 (2)
C2E—C1E—C6E—C5E	2.9 (7)	K5—O6—Si6—C1P	5.0 (2)
Si2—C1E—C6E—C5E	−173.9 (4)	K6—O6—Si6—C1P	−115.6 (3)
C4E—C5E—C6E—C1E	−0.4 (9)	K4—O6—Si6—C1P	130.66 (19)
O2—Si2—C1F—C6F	−132.5 (4)	K5—O6—Si6—C1R	−114.32 (19)
C1E—Si2—C1F—C6F	102.8 (4)	K6—O6—Si6—C1R	125.2 (3)
C1D—Si2—C1F—C6F	−10.3 (4)	K4—O6—Si6—C1R	11.4 (2)
K1—Si2—C1F—C6F	−75.4 (5)	K6—O6—Si6—K5	−120.5 (4)
K4—Si2—C1F—C6F	−130.4 (4)	K4—O6—Si6—K5	125.7 (2)
K2—Si2—C1F—C6F	−165.7 (3)	K5—O6—Si6—K4	−125.7 (2)
O2—Si2—C1F—C2F	52.7 (4)	K6—O6—Si6—K4	113.8 (3)
C1E—Si2—C1F—C2F	−72.0 (4)	O6—Si6—C1P—C2P	−121.0 (4)
C1D—Si2—C1F—C2F	174.9 (3)	C1Q—Si6—C1P—C2P	114.7 (4)
K1—Si2—C1F—C2F	109.8 (4)	C1R—Si6—C1P—C2P	−0.4 (4)
K4—Si2—C1F—C2F	54.8 (3)	K5—Si6—C1P—C2P	−117.6 (4)
K2—Si2—C1F—C2F	19.5 (4)	K4—Si6—C1P—C2P	−75.9 (4)
C6F—C1F—C2F—C3F	1.1 (7)	O6—Si6—C1P—C6P	56.9 (4)
Si2—C1F—C2F—C3F	176.3 (4)	C1Q—Si6—C1P—C6P	−67.3 (4)
C6F—C1F—C2F—K4	121.7 (4)	C1R—Si6—C1P—C6P	177.6 (4)
Si2—C1F—C2F—K4	−63.1 (3)	K5—Si6—C1P—C6P	60.3 (4)
C1F—C2F—C3F—C4F	−0.2 (8)	K4—Si6—C1P—C6P	102.1 (4)
K4—C2F—C3F—C4F	−109.1 (5)	O6—Si6—C1P—K5	−3.40 (16)
C2F—C3F—C4F—C5F	−0.9 (9)	C1Q—Si6—C1P—K5	−127.68 (16)
C3F—C4F—C5F—C6F	1.0 (9)	C1R—Si6—C1P—K5	117.24 (17)
C4F—C5F—C6F—C1F	0.0 (9)	K4—Si6—C1P—K5	41.74 (19)
C2F—C1F—C6F—C5F	−1.0 (7)	C6P—C1P—C2P—C3P	−1.8 (7)
Si2—C1F—C6F—C5F	−176.0 (4)	Si6—C1P—C2P—C3P	176.2 (4)
K5—O3—Si3—C1H	17.3 (3)	K5—C1P—C2P—C3P	81.0 (5)
K3—O3—Si3—C1H	−132.2 (2)	C1P—C2P—C3P—C4P	0.8 (8)
K6—O3—Si3—C1H	120.4 (2)	C2P—C3P—C4P—C5P	0.2 (8)
K5—O3—Si3—C1G	138.7 (2)	C3P—C4P—C5P—C6P	0.0 (9)
K3—O3—Si3—C1G	−10.8 (2)	C2P—C1P—C6P—C5P	2.0 (7)
K6—O3—Si3—C1G	−118.17 (19)	Si6—C1P—C6P—C5P	−176.1 (4)
K5—O3—Si3—C1I	−104.2 (2)	K5—C1P—C6P—C5P	−112.4 (5)
K3—O3—Si3—C1I	106.3 (2)	C2P—C1P—C6P—K5	114.4 (4)
K6—O3—Si3—C1I	−1.1 (3)	Si6—C1P—C6P—K5	−63.7 (3)
K5—O3—Si3—K3	149.5 (3)	C4P—C5P—C6P—C1P	−1.2 (9)
K6—O3—Si3—K3	−107.4 (2)	C4P—C5P—C6P—K5	−98.6 (5)
K5—O3—Si3—K6	−103.1 (2)	O6—Si6—C1Q—C6Q	−152.6 (4)
K3—O3—Si3—K6	107.4 (2)	C1P—Si6—C1Q—C6Q	−29.2 (5)
K3—O3—Si3—K5	−149.5 (3)	C1R—Si6—C1Q—C6Q	86.3 (5)
K6—O3—Si3—K5	103.1 (2)	K5—Si6—C1Q—C6Q	−109.1 (4)
O3—Si3—C1G—C2G	−130.3 (4)	K4—Si6—C1Q—C6Q	159.6 (4)
C1H—Si3—C1G—C2G	−5.1 (5)	O6—Si6—C1Q—C2Q	30.2 (5)
C1I—Si3—C1G—C2G	107.9 (4)	C1P—Si6—C1Q—C2Q	153.7 (4)
K3—Si3—C1G—C2G	−137.1 (4)	C1R—Si6—C1Q—C2Q	−90.9 (4)
K6—Si3—C1G—C2G	−173.8 (3)	K5—Si6—C1Q—C2Q	73.7 (5)
K5—Si3—C1G—C2G	−100.4 (4)	K4—Si6—C1Q—C2Q	−17.5 (5)
O3—Si3—C1G—C6G	52.5 (4)	C6Q—C1Q—C2Q—C3Q	2.0 (8)
C1H—Si3—C1G—C6G	177.7 (4)	Si6—C1Q—C2Q—C3Q	179.3 (5)
C1I—Si3—C1G—C6G	−69.3 (4)	C1Q—C2Q—C3Q—C4Q	−2.1 (10)
K3—Si3—C1G—C6G	45.7 (3)	C2Q—C3Q—C4Q—C5Q	1.6 (12)
K6—Si3—C1G—C6G	9.0 (4)	C3Q—C4Q—C5Q—C6Q	−1.0 (13)
K5—Si3—C1G—C6G	82.4 (4)	C4Q—C5Q—C6Q—C1Q	1.0 (12)
C6G—C1G—C2G—C3G	0.3 (7)	C2Q—C1Q—C6Q—C5Q	−1.4 (9)
Si3—C1G—C2G—C3G	−177.0 (4)	Si6—C1Q—C6Q—C5Q	−178.7 (6)
C1G—C2G—C3G—C4G	0.9 (9)	O6—Si6—C1R—C2R	53.2 (4)
C2G—C3G—C4G—C5G	−2.0 (9)	C1Q—Si6—C1R—C2R	176.2 (4)
C3G—C4G—C5G—C6G	1.9 (9)	C1P—Si6—C1R—C2R	−68.4 (4)
C4G—C5G—C6G—C1G	−0.7 (8)	K5—Si6—C1R—C2R	9.8 (5)
C4G—C5G—C6G—K3	−121.1 (5)	K4—Si6—C1R—C2R	61.6 (4)
C2G—C1G—C6G—C5G	−0.4 (7)	O6—Si6—C1R—C6R	−121.8 (5)
Si3—C1G—C6G—C5G	177.1 (4)	C1Q—Si6—C1R—C6R	1.2 (5)
C2G—C1G—C6G—K3	132.3 (4)	C1P—Si6—C1R—C6R	116.6 (5)
Si3—C1G—C6G—K3	−50.2 (3)	K5—Si6—C1R—C6R	−165.3 (4)
O3—Si3—C1H—C6H	−143.8 (5)	K4—Si6—C1R—C6R	−113.4 (5)
C1G—Si3—C1H—C6H	90.8 (6)	O6—Si6—C1R—K4	−8.39 (16)
C1I—Si3—C1H—C6H	−19.7 (6)	C1Q—Si6—C1R—K4	114.60 (17)
K3—Si3—C1H—C6H	177.0 (5)	C1P—Si6—C1R—K4	−130.01 (15)
K6—Si3—C1H—C6H	−100.6 (5)	K5—Si6—C1R—K4	−51.83 (13)
K5—Si3—C1H—C6H	−134.6 (5)	C6R—C1R—C2R—C3R	0.5 (8)
O3—Si3—C1H—C2H	37.7 (5)	Si6—C1R—C2R—C3R	−174.9 (4)
C1G—Si3—C1H—C2H	−87.6 (4)	K4—C1R—C2R—C3R	−108.2 (5)
C1I—Si3—C1H—C2H	161.9 (4)	C6R—C1R—C2R—K4	108.7 (4)
K3—Si3—C1H—C2H	−1.4 (5)	Si6—C1R—C2R—K4	−66.6 (3)
K6—Si3—C1H—C2H	80.9 (5)	C1R—C2R—C3R—C4R	−0.3 (9)
K5—Si3—C1H—C2H	47.0 (4)	K4—C2R—C3R—C4R	−95.3 (6)
C6H—C1H—C2H—C3H	−0.9 (8)	C2R—C3R—C4R—C5R	−0.2 (10)
Si3—C1H—C2H—C3H	177.7 (4)	C3R—C4R—C5R—C6R	0.3 (11)
C1H—C2H—C3H—C4H	−1.2 (8)	C4R—C5R—C6R—C1R	−0.1 (11)
C2H—C3H—C4H—C5H	2.6 (11)	C2R—C1R—C6R—C5R	−0.3 (9)
C3H—C4H—C5H—C6H	−1.9 (14)	Si6—C1R—C6R—C5R	174.9 (5)
C4H—C5H—C6H—C1H	−0.2 (14)	K4—C1R—C6R—C5R	79.8 (7)
C2H—C1H—C6H—C5H	1.5 (11)	C6S—C1S—C2S—C3S	0.0
Si3—C1H—C6H—C5H	−177.0 (7)	C7S—C1S—C2S—C3S	−178.7 (11)
O3—Si3—C1I—C2I	−130.9 (4)	C1S—C2S—C3S—C4S	0.0
C1H—Si3—C1I—C2I	104.2 (5)	C2S—C3S—C4S—C5S	0.0
C1G—Si3—C1I—C2I	−8.1 (5)	C3S—C4S—C5S—C6S	0.0
K3—Si3—C1I—C2I	−89.3 (4)	C4S—C5S—C6S—C1S	0.0
K6—Si3—C1I—C2I	−131.6 (5)	C2S—C1S—C6S—C5S	0.0
K5—Si3—C1I—C2I	−166.2 (4)	C7S—C1S—C6S—C5S	178.8 (10)
O3—Si3—C1I—C6I	46.9 (5)	C6X—C1X—C2X—C3X	0.0
C1H—Si3—C1I—C6I	−78.0 (5)	C7X—C1X—C2X—C3X	−178.7 (12)
C1G—Si3—C1I—C6I	169.7 (4)	C1X—C2X—C3X—C4X	0.0
K3—Si3—C1I—C6I	88.5 (4)	C2X—C3X—C4X—C5X	0.0
K6—Si3—C1I—C6I	46.2 (4)	C3X—C4X—C5X—C6X	0.0
K5—Si3—C1I—C6I	11.6 (5)	C4X—C5X—C6X—C1X	0.0
C6I—C1I—C2I—C3I	−1.9 (8)	C2X—C1X—C6X—C5X	0.0
Si3—C1I—C2I—C3I	176.0 (5)	C7X—C1X—C6X—C5X	178.7 (13)
C1I—C2I—C3I—C4I	−0.4 (11)	C6T—C1T—C2T—C3T	0.0
C2I—C3I—C4I—C5I	2.5 (12)	C7T—C1T—C2T—C3T	−178.0 (11)
C3I—C4I—C5I—C6I	−2.1 (13)	C1T—C2T—C3T—C4T	0.0
C4I—C5I—C6I—C1I	−0.4 (11)	C2T—C3T—C4T—C5T	0.0
C4I—C5I—C6I—K6	−113.9 (7)	C3T—C4T—C5T—C6T	0.0
C2I—C1I—C6I—C5I	2.3 (9)	C4T—C5T—C6T—C1T	0.0
Si3—C1I—C6I—C5I	−175.7 (5)	C2T—C1T—C6T—C5T	0.0
C2I—C1I—C6I—K6	124.3 (4)	C7T—C1T—C6T—C5T	178.0 (11)
Si3—C1I—C6I—K6	−53.7 (4)	C6Y—C1Y—C2Y—C3Y	0.0
K4—O4—Si4—C1K	5.4 (3)	C7Y—C1Y—C2Y—C3Y	179.5 (18)
K6—O4—Si4—C1K	−129.6 (3)	C1Y—C2Y—C3Y—C4Y	0.0
K2—O4—Si4—C1K	116.7 (2)	C2Y—C3Y—C4Y—C5Y	0.0
K4—O4—Si4—C1L	123.9 (2)	C3Y—C4Y—C5Y—C6Y	0.0
K6—O4—Si4—C1L	−11.1 (3)	C4Y—C5Y—C6Y—C1Y	0.0
K2—O4—Si4—C1L	−124.86 (18)	C2Y—C1Y—C6Y—C5Y	0.0
K4—O4—Si4—C1J	−115.6 (2)	C7Y—C1Y—C6Y—C5Y	−179 (2)
K6—O4—Si4—C1J	109.4 (3)	K3—O1U—C1U—C2U	30.3 (6)
K2—O4—Si4—C1J	−4.3 (2)	K2—O1U—C1U—C2U	−124.3 (4)
K4—O4—Si4—K2	−111.3 (2)	K6—O1U—C1U—C2U	141.0 (4)
K6—O4—Si4—K2	113.8 (3)	K3—O1U—C1U—C3U	−92.8 (5)
K6—O4—Si4—K4	−134.9 (4)	K2—O1U—C1U—C3U	112.6 (5)
K2—O4—Si4—K4	111.3 (2)	K6—O1U—C1U—C3U	17.9 (6)

Hydrogen-bond geometry (Å, º)

D—H···A	D—H	H···A	D···A	D—H···A
O1W—H1W···O2	0.84	1.87	2.653 (4)	155
O1W—H2W···O5	0.84	1.83	2.654 (4)	168
O1U—H1U···O1	0.84	1.84	2.643 (4)	161

(µ₄-Aqua)(µ₃-aqua)pentakis(µ₃-triphenylsilanolato)(µ₂-triphenylsilanolato)hexapotassium (u777bba)

Crystal data

[K6(C18H15OSi)6(H2O)2]	Z = 2
Mr = 1922.97	F(000) = 2008
Triclinic, P1	Dx = 1.286 Mg m^−3
a = 12.7633 (7) Å	Cu Kα radiation, λ = 1.54184 Å
b = 14.7076 (8) Å	Cell parameters from 144636 reflections
c = 28.183 (3) Å	θ = 3.1–67°
α = 89.61 (2)°	µ = 3.48 mm^−1
β = 78.98 (2)°	T = 100 K
γ = 73.26 (2)°	Needle, colorless
V = 4966.3 (9) Å^3	0.17 × 0.15 × 0.09 mm

Data collection

XtaLAB Synergy R, DW system, HyPix-Arc 150 diffractometer	19325 reflections with I > 2σ(I)
Radiation source: Rotating-anode X-ray tube	Rint = 0.036
Detector resolution: 10.0000 pixels mm^-1	θmax = 75.9°, θmin = 3.1°
Absorption correction: gaussian (CrysAlis PRO; Rigaku OD, 2020)	h = −15→14
Tmin = 0.635, Tmax = 1.000	k = −18→18
243068 measured reflections	l = −35→35
20415 independent reflections

Refinement

Refinement on F^2	0 restraints
Least-squares matrix: full	Hydrogen site location: mixed
R[F^2 > 2σ(F^2)] = 0.052	H atoms treated by a mixture of independent and constrained refinement
wR(F^2) = 0.124	w = 1/[σ^2(Fo^2) + (0.0459P)^2 + 6.6226P] where P = (Fo^2 + 2Fc^2)/3
S = 1.05	(Δ/σ)max = 0.001
20415 reflections	Δρmax = 0.72 e Å^−3
1249 parameters	Δρmin = −1.10 e Å^−3

Special details

Geometry. All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes.

Refinement. Diffraction data for 1 and 2 were collected at 100 K on an XCALIBUR PX monocrystalline diffractometer with a large CCD camera using Cu Kα radiation (λ = 1.54184 Å). The CrysAlisPro software from Oxford Diffraction was used to determine cell parameters, data reduction, and absorption correction. The structures were solved by direct methods (SHELXS97) and refined using the least-squares technique (SHELXL2013).

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Ų)

	x	y	z	Uiso*/Ueq	Occ. (<1)
O1W	0.43080 (19)	0.79185 (15)	0.24023 (7)	0.0511 (5)
H1W1	0.424231	0.836155	0.221030	0.083 (13)*
H1W2	0.475471	0.739177	0.228983	0.119 (19)*
O2W	0.1908 (3)	0.6764 (2)	0.25737 (13)	0.0458 (9)	0.574 (4)
H2W1	0.240267	0.645048	0.271856	0.069*	0.574 (4)
H2W2	0.140666	0.651461	0.254560	0.069*	0.574 (4)
O3W	0.1639 (4)	0.7198 (3)	0.23145 (17)	0.0439 (12)	0.426 (4)
H3W1	0.095450	0.724851	0.236133	0.066*	0.426 (4)
H3W2	0.200789	0.707468	0.203001	0.066*	0.426 (4)
K1	0.50947 (4)	0.66425 (4)	0.30678 (2)	0.04343 (13)
K2	0.19822 (9)	0.76850 (6)	0.34709 (7)	0.0274 (3)	0.574 (4)
K21	0.22228 (14)	0.76730 (9)	0.32095 (11)	0.0340 (5)	0.426 (4)
K3	0.38532 (5)	0.57842 (5)	0.20134 (3)	0.0640 (2)
K4	0.35715 (4)	0.93972 (4)	0.30889 (2)	0.03498 (12)
K5	0.49925 (4)	0.75981 (3)	0.12282 (2)	0.03637 (12)
K6	0.22192 (10)	0.84378 (15)	0.20967 (3)	0.0324 (4)	0.574 (4)
K61	0.19469 (13)	0.89592 (19)	0.20633 (5)	0.0298 (4)	0.426 (4)
O1	0.34112 (15)	0.59412 (11)	0.30849 (6)	0.0365 (4)
Si1	0.34963 (5)	0.48972 (4)	0.32563 (2)	0.02871 (13)
C1A	0.46819 (19)	0.44007 (16)	0.35821 (8)	0.0313 (5)
C2A	0.4965 (2)	0.5001 (2)	0.38870 (9)	0.0412 (6)
H2A	0.457344	0.566054	0.391526	0.049*
C3A	0.5800 (2)	0.4660 (2)	0.41483 (10)	0.0516 (7)
H3A	0.598262	0.508553	0.434841	0.062*
C4A	0.6368 (2)	0.3703 (2)	0.41183 (10)	0.0521 (7)
H4A	0.694008	0.346790	0.429810	0.062*
C5A	0.6102 (2)	0.3090 (2)	0.38266 (10)	0.0469 (7)
H5A	0.648600	0.242984	0.380781	0.056*
C6A	0.5271 (2)	0.34350 (18)	0.35590 (9)	0.0367 (5)
H6A	0.510210	0.300517	0.335668	0.044*
C1B	0.3706 (2)	0.40926 (16)	0.27038 (8)	0.0343 (5)
C2B	0.2802 (3)	0.40052 (19)	0.25148 (10)	0.0442 (6)
H2B	0.206687	0.424234	0.270092	0.053*
C3B	0.2966 (3)	0.3569 (2)	0.20502 (12)	0.0574 (8)
H3B	0.234338	0.351684	0.192544	0.069*
C4B	0.4023 (3)	0.3220 (2)	0.17800 (12)	0.0628 (9)
H4B	0.412899	0.293233	0.146690	0.075*
C5B	0.4924 (3)	0.3282 (2)	0.19561 (11)	0.0555 (8)
H5B	0.565515	0.303322	0.176776	0.067*
C6B	0.4770 (2)	0.37112 (17)	0.24135 (9)	0.0414 (6)
H6B	0.540524	0.374706	0.253271	0.050*
C1C	0.21941 (19)	0.48377 (16)	0.36885 (8)	0.0316 (5)
C2C	0.2195 (2)	0.41001 (18)	0.40007 (9)	0.0362 (5)
H2C	0.287044	0.360737	0.399292	0.043*
C3C	0.1241 (2)	0.40601 (19)	0.43231 (9)	0.0407 (6)
H3C	0.126780	0.353923	0.452632	0.049*
C4C	0.0258 (2)	0.4774 (2)	0.43481 (10)	0.0436 (6)
H4C	−0.039692	0.475032	0.456786	0.052*
C5C	0.0234 (2)	0.5523 (2)	0.40518 (13)	0.0599 (9)
H5C	−0.043609	0.602823	0.407249	0.072*
C6C	0.1184 (2)	0.5543 (2)	0.37229 (12)	0.0527 (8)
H6C	0.114299	0.605556	0.351373	0.063*
O2	0.37440 (13)	0.79905 (12)	0.36628 (5)	0.0322 (3)
Si2	0.37274 (5)	0.82359 (4)	0.42125 (2)	0.02745 (12)
C1D	0.25690 (18)	0.79322 (16)	0.46488 (8)	0.0293 (4)
C2D	0.2311 (2)	0.70898 (17)	0.45698 (9)	0.0339 (5)
H2D	0.268023	0.670702	0.428239	0.041*
C3D	0.1532 (2)	0.67986 (19)	0.48994 (9)	0.0398 (6)
H3D	0.136973	0.622522	0.483583	0.048*
C4D	0.0989 (2)	0.7346 (2)	0.53221 (10)	0.0425 (6)
H4D	0.046360	0.714384	0.555140	0.051*
C5D	0.1215 (2)	0.8186 (2)	0.54082 (10)	0.0425 (6)
H5D	0.083920	0.856624	0.569584	0.051*
C6D	0.1993 (2)	0.84778 (17)	0.50732 (9)	0.0358 (5)
H6D	0.213564	0.906089	0.513492	0.043*
C1E	0.50638 (19)	0.75451 (17)	0.44012 (8)	0.0330 (5)
C2E	0.5085 (2)	0.70992 (17)	0.48409 (9)	0.0358 (5)
H2E	0.440142	0.715761	0.506007	0.043*
C3E	0.6078 (2)	0.6573 (2)	0.49665 (10)	0.0470 (6)
H3E	0.606799	0.627206	0.526585	0.056*
C4E	0.7076 (3)	0.6491 (3)	0.46548 (12)	0.0656 (10)
H4E	0.775793	0.613003	0.473692	0.079*
C5E	0.7081 (3)	0.6940 (3)	0.42189 (12)	0.0772 (12)
H5E	0.776863	0.689917	0.400620	0.093*
C6E	0.6088 (2)	0.7446 (3)	0.40950 (10)	0.0576 (8)
H6E	0.610401	0.773421	0.379207	0.069*
C1F	0.35771 (19)	0.95476 (17)	0.43092 (8)	0.0301 (5)
C2F	0.2651 (2)	1.02418 (18)	0.42053 (9)	0.0377 (5)
H2F	0.206474	1.004798	0.411476	0.045*
C3F	0.2561 (3)	1.12036 (19)	0.42304 (9)	0.0434 (6)
H3F	0.192349	1.165700	0.415523	0.052*
C4F	0.3402 (2)	1.15016 (19)	0.43653 (9)	0.0421 (6)
H4F	0.334624	1.215935	0.438156	0.051*
C5F	0.4321 (2)	1.08391 (19)	0.44758 (9)	0.0408 (6)
H5F	0.489606	1.104154	0.457150	0.049*
C6F	0.4410 (2)	0.98716 (18)	0.44478 (8)	0.0345 (5)
H6F	0.504930	0.942324	0.452431	0.041*
O3	0.30574 (17)	0.71395 (12)	0.14289 (7)	0.0462 (5)
Si3	0.26424 (5)	0.71846 (4)	0.09310 (2)	0.03067 (13)
C1G	0.19033 (18)	0.62712 (15)	0.08564 (8)	0.0284 (4)
C2G	0.1678 (2)	0.60519 (17)	0.04104 (9)	0.0335 (5)
H2G	0.192997	0.635597	0.013155	0.040*
C3G	0.1098 (2)	0.54033 (18)	0.03656 (10)	0.0387 (5)
H3G	0.094355	0.527710	0.006012	0.046*
C4G	0.0744 (2)	0.49410 (18)	0.07639 (11)	0.0440 (6)
H4G	0.034872	0.449370	0.073418	0.053*
C5G	0.0967 (2)	0.5132 (2)	0.12043 (11)	0.0499 (7)
H5G	0.073122	0.481050	0.147925	0.060*
C6G	0.1536 (2)	0.57919 (18)	0.12501 (9)	0.0383 (5)
H6G	0.167715	0.591850	0.155825	0.046*
C1H	0.3869 (2)	0.69672 (18)	0.04084 (11)	0.0410 (6)
C2H	0.4741 (2)	0.6126 (2)	0.03571 (14)	0.0570 (8)
H2H	0.469012	0.564620	0.058021	0.068*
C3H	0.5687 (3)	0.5963 (3)	−0.00102 (18)	0.0784 (12)
H3H	0.626400	0.537813	−0.003573	0.094*
C4H	0.5783 (3)	0.6645 (4)	−0.0333 (2)	0.0999 (16)
H4H	0.642088	0.653474	−0.058645	0.120*
C5H	0.4946 (3)	0.7497 (4)	−0.02886 (18)	0.1018 (17)
H5H	0.501307	0.797729	−0.050953	0.122*
C6H	0.4004 (3)	0.7655 (3)	0.00784 (13)	0.0654 (9)
H6H	0.343789	0.824672	0.010472	0.078*
C1I	0.16806 (19)	0.83911 (16)	0.08396 (8)	0.0291 (4)
C2I	0.18892 (18)	0.92213 (15)	0.09793 (8)	0.0277 (4)
H2I	0.251411	0.917178	0.112536	0.033*
C3I	0.12115 (19)	1.01135 (16)	0.09111 (9)	0.0326 (5)
H3I	0.136610	1.066560	0.101548	0.039*
C4I	0.0312 (2)	1.02025 (16)	0.06917 (9)	0.0342 (5)
H4I	−0.015409	1.081426	0.064357	0.041*
C5I	0.0096 (2)	0.93997 (19)	0.05436 (11)	0.0471 (7)
H5I	−0.051363	0.945534	0.038621	0.057*
C6I	0.0763 (3)	0.85085 (19)	0.06228 (12)	0.0521 (8)
H6I	0.058740	0.796107	0.052609	0.063*
O4	0.15694 (13)	0.93752 (14)	0.30131 (6)	0.0390 (4)
Si4	0.02932 (5)	0.99735 (5)	0.31157 (2)	0.03125 (13)
C1J	−0.0554 (2)	0.96028 (19)	0.36662 (10)	0.0392 (6)
C2J	−0.0100 (2)	0.92252 (19)	0.40552 (9)	0.0401 (6)
H2J	0.065781	0.917905	0.405506	0.048*
C3J	−0.0718 (3)	0.8909 (2)	0.44491 (10)	0.0567 (8)
H3J	−0.037872	0.865056	0.471137	0.068*
C4J	−0.1804 (3)	0.8967 (3)	0.44597 (13)	0.0724 (11)
H4J	−0.221415	0.872078	0.471992	0.087*
C5J	−0.2304 (3)	0.9388 (4)	0.4090 (2)	0.115 (2)
H5J	−0.307590	0.947217	0.410493	0.138*
C6J	−0.1680 (3)	0.9687 (4)	0.36962 (18)	0.1020 (19)
H6J	−0.203050	0.995750	0.343878	0.122*
C1K	0.0083 (2)	1.12825 (19)	0.31879 (8)	0.0385 (6)
C2K	−0.0957 (3)	1.1962 (2)	0.31947 (10)	0.0513 (7)
H2K	−0.158008	1.175437	0.316280	0.062*
C3K	−0.1089 (4)	1.2931 (2)	0.32472 (12)	0.0689 (10)
H3K	−0.179163	1.338175	0.324546	0.083*
C4K	−0.0168 (4)	1.3234 (3)	0.33028 (12)	0.0738 (9)
H4K	−0.025332	1.389287	0.334591	0.089*
C5K	0.0867 (4)	1.2577 (3)	0.32954 (12)	0.0738 (9)
H5K	0.149094	1.278188	0.333001	0.089*
C6K	0.0974 (3)	1.1621 (2)	0.32370 (10)	0.0532 (8)
H6K	0.168353	1.117435	0.322988	0.064*
C1L	−0.0399 (2)	0.97447 (19)	0.26070 (11)	0.0428 (6)
C2L	−0.0516 (4)	0.8847 (3)	0.2544 (2)	0.124 (2)
H2L	−0.030546	0.839191	0.277588	0.149*
C3L	−0.0921 (5)	0.8577 (3)	0.2166 (3)	0.153 (3)
H3L	−0.097803	0.795047	0.213968	0.184*
C4L	−0.1232 (3)	0.9204 (4)	0.18366 (17)	0.0999 (19)
H4L	−0.150893	0.902622	0.157266	0.120*
C5L	−0.1149 (4)	1.0089 (4)	0.18833 (12)	0.0899 (15)
H5L	−0.138524	1.054127	0.165449	0.108*
C6L	−0.0721 (2)	1.0350 (2)	0.22626 (9)	0.0493 (7)
H6L	−0.065256	1.097472	0.228036	0.059*
O5	0.56570 (14)	0.63134 (12)	0.19646 (6)	0.0390 (4)
Si5	0.69600 (6)	0.58294 (5)	0.17856 (3)	0.03877 (15)
C1M	0.7617 (3)	0.6402 (3)	0.12434 (13)	0.0296 (6)	0.5
C2M	0.7319 (3)	0.6291 (3)	0.08028 (16)	0.0431 (14)	0.5
H2M	0.686058	0.589553	0.077369	0.052*	0.5
C3M	0.7691 (4)	0.6759 (4)	0.04049 (13)	0.0494 (19)	0.5
H3M	0.748769	0.668361	0.010378	0.059*	0.5
C4M	0.8362 (4)	0.7338 (3)	0.04475 (13)	0.052 (2)	0.5
H4M	0.861670	0.765789	0.017556	0.062*	0.5
C5M	0.8660 (4)	0.7449 (3)	0.08881 (15)	0.0600 (17)	0.5
H5M	0.911863	0.784410	0.091725	0.072*	0.5
C6M	0.8288 (3)	0.6980 (3)	0.12860 (12)	0.0496 (14)	0.5
H6M	0.849153	0.705603	0.158716	0.059*	0.5
C1MM	0.7470 (3)	0.6545 (2)	0.12617 (13)	0.0296 (6)	0.5
C2MM	0.7878 (3)	0.61598 (18)	0.07905 (15)	0.0369 (13)	0.5
H2MM	0.795126	0.551116	0.072000	0.044*	0.5
C3MM	0.8179 (3)	0.6724 (3)	0.04223 (11)	0.0448 (18)	0.5
H3MM	0.845825	0.646062	0.010015	0.054*	0.5
C4MM	0.8072 (3)	0.7673 (2)	0.05253 (11)	0.0359 (15)	0.5
H4MM	0.827827	0.805833	0.027370	0.043*	0.5
C5MM	0.7664 (3)	0.80580 (17)	0.09966 (12)	0.0307 (9)	0.5
H5MM	0.759128	0.870661	0.106709	0.037*	0.5
C6MM	0.7363 (3)	0.7494 (2)	0.13648 (9)	0.0285 (9)	0.5
H6MM	0.708427	0.775717	0.168694	0.034*	0.5
C1N	0.7112 (3)	0.45838 (19)	0.14585 (13)	0.0401 (8)	0.5
C2N	0.6468 (3)	0.45266 (19)	0.11202 (13)	0.0371 (10)	0.5
H2N	0.589147	0.506959	0.106741	0.045*	0.5
C3N	0.6667 (3)	0.3675 (2)	0.08592 (11)	0.0423 (12)	0.5
H3N	0.622638	0.363606	0.062801	0.051*	0.5
C4N	0.7510 (3)	0.2881 (2)	0.09365 (15)	0.0543 (16)	0.5
H4N	0.764548	0.229869	0.075806	0.065*	0.5
C5N	0.8154 (3)	0.2938 (2)	0.12747 (18)	0.057 (2)	0.5
H5N	0.872969	0.239484	0.132753	0.069*	0.5
C6N	0.7955 (3)	0.3789 (2)	0.15357 (15)	0.0484 (14)	0.5
H6N	0.839479	0.382837	0.176694	0.058*	0.5
C1NN	0.7722 (3)	0.2939 (2)	0.20171 (13)	0.0401 (8)	0.5
C2NN	0.7457 (3)	0.3920 (2)	0.20874 (10)	0.0432 (12)	0.5
H2NN	0.724003	0.420450	0.240625	0.052*	0.5
C3NN	0.7511 (3)	0.44847 (19)	0.16912 (13)	0.0435 (12)	0.5
H3NN	0.732977	0.515510	0.173926	0.052*	0.5
C4NN	0.7829 (4)	0.4069 (3)	0.12246 (11)	0.0529 (14)	0.5
H4NN	0.786517	0.445446	0.095385	0.064*	0.5
C5NN	0.8093 (4)	0.3088 (3)	0.11543 (12)	0.068 (3)	0.5
H5NN	0.831083	0.280323	0.083544	0.082*	0.5
C6NN	0.8040 (4)	0.2523 (2)	0.15505 (16)	0.0616 (17)	0.5
H6NN	0.822109	0.185262	0.150243	0.074*	0.5
C1O	0.7760 (3)	0.6142 (2)	0.23128 (11)	0.0369 (9)	0.5
C2O	0.7335 (2)	0.7036 (2)	0.25498 (12)	0.0373 (11)	0.5
H2O	0.666979	0.746562	0.248499	0.045*	0.5
C3O	0.7884 (3)	0.73019 (19)	0.28817 (11)	0.0398 (11)	0.5
H3O	0.759410	0.791298	0.304371	0.048*	0.5
C4O	0.8858 (3)	0.6674 (2)	0.29766 (12)	0.0417 (12)	0.5
H4O	0.923325	0.685519	0.320346	0.050*	0.5
C5O	0.9283 (2)	0.5779 (2)	0.27396 (14)	0.0401 (15)	0.5
H5O	0.994811	0.535003	0.280449	0.048*	0.5
C6O	0.8734 (3)	0.55137 (19)	0.24077 (13)	0.0391 (11)	0.5
H6O	0.902381	0.490264	0.224577	0.047*	0.5
C1OO	0.7780 (3)	0.5671 (3)	0.22471 (12)	0.0369 (9)	0.5
C2OO	0.7414 (3)	0.5320 (3)	0.26875 (13)	0.0484 (13)	0.5
H2OO	0.676819	0.510747	0.273324	0.058*	0.5
C3OO	0.7994 (4)	0.5282 (3)	0.30611 (11)	0.0581 (16)	0.5
H3OO	0.774421	0.504260	0.336212	0.070*	0.5
C4OO	0.8940 (4)	0.5594 (3)	0.29942 (16)	0.073 (2)	0.5
H4OO	0.933578	0.556720	0.324955	0.088*	0.5
C5OO	0.9305 (3)	0.5944 (3)	0.25538 (19)	0.079 (3)	0.5
H5OO	0.995135	0.615665	0.250809	0.094*	0.5
C6OO	0.8725 (3)	0.5982 (3)	0.21802 (14)	0.0537 (15)	0.5
H6OO	0.897535	0.622152	0.187920	0.064*	0.5
O6	0.39222 (13)	0.91769 (11)	0.17483 (6)	0.0323 (3)
Si6	0.41582 (5)	1.01814 (4)	0.16886 (2)	0.02685 (12)
C1P	0.28826 (18)	1.11520 (16)	0.15980 (8)	0.0290 (4)
C2P	0.18991 (19)	1.13726 (16)	0.19502 (9)	0.0326 (5)
H2P	0.187778	1.101685	0.223261	0.039*
C3P	0.0954 (2)	1.20941 (17)	0.19002 (10)	0.0379 (5)
H3P	0.030583	1.223812	0.214979	0.045*
C4P	0.0960 (2)	1.26039 (17)	0.14844 (10)	0.0404 (6)
H4P	0.031481	1.309686	0.144707	0.048*
C5P	0.1910 (2)	1.23906 (18)	0.11242 (10)	0.0389 (6)
H5P	0.191292	1.273032	0.083627	0.047*
C6P	0.2860 (2)	1.16801 (17)	0.11827 (9)	0.0332 (5)
H6P	0.350978	1.154946	0.093457	0.040*
C1R	0.53063 (19)	1.0159 (2)	0.11530 (8)	0.0368 (5)
C2R	0.6164 (2)	1.0563 (3)	0.11742 (10)	0.0518 (8)
H2R	0.616970	1.087484	0.146741	0.062*
C3R	0.7010 (3)	1.0517 (4)	0.07733 (12)	0.0789 (13)
H3R	0.758693	1.079489	0.079481	0.095*
C4R	0.7011 (3)	1.0068 (4)	0.03448 (11)	0.0839 (15)
H4R	0.759223	1.003114	0.007236	0.101*
C5R	0.6169 (3)	0.9672 (3)	0.03117 (10)	0.0694 (11)
H5R	0.616621	0.936950	0.001551	0.083*
C6R	0.5326 (2)	0.9716 (2)	0.07118 (9)	0.0469 (7)
H6R	0.475048	0.943949	0.068539	0.056*
C1S	0.46237 (19)	1.05175 (17)	0.22442 (8)	0.0295 (5)
C2S	0.4006 (2)	1.12727 (17)	0.25745 (8)	0.0327 (5)
H2S	0.334464	1.169877	0.250410	0.039*
C3S	0.4335 (2)	1.14169 (19)	0.30044 (9)	0.0400 (6)
H3S	0.388920	1.192688	0.322639	0.048*
C4S	0.5306 (3)	1.0822 (2)	0.31087 (9)	0.0450 (6)
H4S	0.552995	1.092059	0.340219	0.054*
C5S	0.5956 (2)	1.0078 (2)	0.27840 (9)	0.0436 (6)
H5S	0.663313	0.967428	0.285183	0.052*
C6S	0.5615 (2)	0.99241 (19)	0.23579 (8)	0.0349 (5)
H6S	0.606151	0.940773	0.213975	0.042*

Atomic displacement parameters (Ų)

	U^11	U^22	U^33	U^12	U^13	U^23
O1W	0.0756 (14)	0.0447 (11)	0.0391 (10)	−0.0158 (10)	−0.0290 (10)	0.0093 (9)
O2W	0.0487 (19)	0.0447 (19)	0.048 (2)	−0.0152 (15)	−0.0166 (16)	0.0135 (16)
O3W	0.041 (2)	0.049 (3)	0.043 (3)	−0.016 (2)	−0.0085 (19)	0.005 (2)
K1	0.0268 (2)	0.0461 (3)	0.0539 (3)	−0.0085 (2)	−0.0031 (2)	0.0058 (2)
K2	0.0277 (5)	0.0281 (4)	0.0280 (7)	−0.0105 (3)	−0.0063 (4)	0.0037 (4)
K21	0.0306 (7)	0.0259 (6)	0.0477 (14)	−0.0089 (5)	−0.0123 (8)	0.0048 (6)
K3	0.0393 (3)	0.0432 (3)	0.1258 (7)	−0.0234 (3)	−0.0393 (4)	0.0432 (4)
K4	0.0330 (2)	0.0475 (3)	0.0341 (2)	−0.0236 (2)	−0.0121 (2)	0.0171 (2)
K5	0.0323 (3)	0.0275 (2)	0.0534 (3)	−0.00812 (19)	−0.0195 (2)	0.0024 (2)
K6	0.0328 (5)	0.0406 (10)	0.0256 (4)	−0.0135 (6)	−0.0056 (3)	0.0004 (4)
K61	0.0280 (7)	0.0318 (11)	0.0301 (6)	−0.0111 (7)	−0.0030 (5)	0.0011 (6)
O1	0.0457 (10)	0.0259 (8)	0.0376 (9)	−0.0103 (7)	−0.0077 (7)	0.0065 (7)
Si1	0.0307 (3)	0.0244 (3)	0.0309 (3)	−0.0070 (2)	−0.0076 (2)	0.0057 (2)
C1A	0.0288 (11)	0.0320 (11)	0.0306 (11)	−0.0064 (9)	−0.0038 (9)	0.0022 (9)
C2A	0.0380 (13)	0.0447 (14)	0.0387 (13)	−0.0083 (11)	−0.0083 (10)	−0.0040 (11)
C3A	0.0445 (15)	0.071 (2)	0.0411 (15)	−0.0159 (14)	−0.0132 (12)	−0.0038 (13)
C4A	0.0336 (14)	0.079 (2)	0.0397 (14)	−0.0078 (14)	−0.0120 (11)	0.0121 (14)
C5A	0.0349 (13)	0.0502 (16)	0.0446 (15)	0.0018 (11)	−0.0038 (11)	0.0127 (12)
C6A	0.0338 (12)	0.0363 (13)	0.0358 (12)	−0.0048 (10)	−0.0048 (10)	0.0049 (10)
C1B	0.0510 (14)	0.0234 (11)	0.0337 (12)	−0.0165 (10)	−0.0130 (10)	0.0101 (9)
C2B	0.0586 (17)	0.0355 (13)	0.0491 (15)	−0.0243 (12)	−0.0200 (13)	0.0098 (11)
C3B	0.090 (2)	0.0475 (16)	0.0585 (18)	−0.0442 (17)	−0.0348 (18)	0.0109 (14)
C4B	0.099 (3)	0.0572 (19)	0.0445 (16)	−0.0476 (19)	−0.0048 (17)	−0.0042 (14)
C5B	0.082 (2)	0.0446 (16)	0.0419 (15)	−0.0326 (16)	0.0036 (15)	−0.0039 (12)
C6B	0.0591 (16)	0.0302 (12)	0.0345 (12)	−0.0170 (11)	−0.0020 (11)	0.0024 (10)
C1C	0.0320 (11)	0.0329 (12)	0.0318 (11)	−0.0099 (9)	−0.0103 (9)	0.0057 (9)
C2C	0.0372 (13)	0.0351 (12)	0.0363 (12)	−0.0094 (10)	−0.0098 (10)	0.0097 (10)
C3C	0.0468 (14)	0.0437 (14)	0.0361 (13)	−0.0190 (12)	−0.0103 (11)	0.0119 (11)
C4C	0.0363 (13)	0.0580 (17)	0.0389 (13)	−0.0191 (12)	−0.0054 (11)	0.0078 (12)
C5C	0.0295 (13)	0.065 (2)	0.075 (2)	−0.0015 (13)	−0.0052 (13)	0.0281 (17)
C6C	0.0339 (14)	0.0524 (17)	0.0648 (18)	−0.0039 (12)	−0.0075 (13)	0.0310 (14)
O2	0.0355 (8)	0.0425 (9)	0.0247 (7)	−0.0196 (7)	−0.0081 (6)	0.0056 (6)
Si2	0.0300 (3)	0.0334 (3)	0.0237 (3)	−0.0153 (2)	−0.0075 (2)	0.0054 (2)
C1D	0.0292 (11)	0.0322 (11)	0.0283 (10)	−0.0102 (9)	−0.0088 (9)	0.0075 (9)
C2D	0.0376 (12)	0.0353 (12)	0.0315 (11)	−0.0149 (10)	−0.0072 (9)	0.0066 (9)
C3D	0.0417 (14)	0.0419 (14)	0.0426 (14)	−0.0217 (11)	−0.0101 (11)	0.0134 (11)
C4D	0.0359 (13)	0.0509 (15)	0.0430 (14)	−0.0190 (12)	−0.0037 (11)	0.0152 (12)
C5D	0.0371 (13)	0.0472 (15)	0.0375 (13)	−0.0099 (11)	0.0029 (10)	0.0031 (11)
C6D	0.0348 (12)	0.0329 (12)	0.0390 (13)	−0.0109 (10)	−0.0038 (10)	0.0038 (10)
C1E	0.0320 (12)	0.0395 (13)	0.0301 (11)	−0.0126 (10)	−0.0092 (9)	−0.0022 (9)
C2E	0.0370 (13)	0.0377 (13)	0.0341 (12)	−0.0092 (10)	−0.0133 (10)	0.0025 (10)
C3E	0.0485 (16)	0.0502 (16)	0.0420 (14)	−0.0053 (12)	−0.0226 (12)	−0.0015 (12)
C4E	0.0378 (15)	0.096 (3)	0.0526 (18)	0.0070 (16)	−0.0235 (14)	−0.0126 (17)
C5E	0.0305 (15)	0.141 (4)	0.0473 (18)	−0.0053 (18)	−0.0082 (13)	−0.004 (2)
C6E	0.0331 (14)	0.103 (3)	0.0353 (14)	−0.0157 (15)	−0.0088 (11)	0.0048 (15)
C1F	0.0368 (12)	0.0376 (12)	0.0217 (10)	−0.0194 (10)	−0.0063 (9)	0.0066 (8)
C2F	0.0458 (14)	0.0378 (13)	0.0377 (13)	−0.0194 (11)	−0.0177 (11)	0.0078 (10)
C3F	0.0592 (17)	0.0387 (14)	0.0391 (13)	−0.0180 (12)	−0.0207 (12)	0.0099 (11)
C4F	0.0669 (18)	0.0387 (13)	0.0307 (12)	−0.0280 (13)	−0.0142 (12)	0.0105 (10)
C5F	0.0543 (16)	0.0481 (15)	0.0336 (12)	−0.0339 (13)	−0.0126 (11)	0.0083 (11)
C6F	0.0396 (13)	0.0427 (13)	0.0287 (11)	−0.0221 (11)	−0.0095 (9)	0.0086 (9)
O3	0.0692 (13)	0.0322 (9)	0.0559 (11)	−0.0234 (9)	−0.0445 (10)	0.0166 (8)
Si3	0.0360 (3)	0.0246 (3)	0.0390 (3)	−0.0124 (2)	−0.0204 (3)	0.0075 (2)
C1G	0.0259 (10)	0.0223 (10)	0.0378 (12)	−0.0062 (8)	−0.0093 (9)	0.0032 (8)
C2G	0.0336 (12)	0.0353 (12)	0.0349 (12)	−0.0141 (10)	−0.0084 (9)	0.0017 (9)
C3G	0.0363 (13)	0.0356 (13)	0.0477 (14)	−0.0122 (10)	−0.0138 (11)	−0.0043 (11)
C4G	0.0374 (13)	0.0328 (13)	0.0696 (18)	−0.0184 (11)	−0.0168 (12)	0.0058 (12)
C5G	0.0512 (16)	0.0516 (16)	0.0562 (17)	−0.0290 (14)	−0.0121 (13)	0.0203 (13)
C6G	0.0408 (13)	0.0396 (13)	0.0390 (13)	−0.0164 (11)	−0.0120 (10)	0.0066 (10)
C1H	0.0284 (12)	0.0372 (13)	0.0651 (17)	−0.0148 (10)	−0.0195 (11)	0.0059 (12)
C2H	0.0409 (15)	0.0367 (14)	0.096 (3)	−0.0100 (12)	−0.0224 (16)	0.0002 (15)
C3H	0.0297 (15)	0.064 (2)	0.135 (4)	−0.0042 (15)	−0.0140 (19)	−0.025 (2)
C4H	0.0391 (19)	0.114 (4)	0.126 (4)	−0.013 (2)	0.018 (2)	0.004 (3)
C5H	0.050 (2)	0.126 (4)	0.105 (3)	−0.008 (2)	0.017 (2)	0.035 (3)
C6H	0.0370 (15)	0.074 (2)	0.074 (2)	−0.0066 (15)	0.0007 (15)	0.0243 (18)
C1I	0.0344 (11)	0.0276 (11)	0.0293 (11)	−0.0115 (9)	−0.0127 (9)	0.0048 (8)
C2I	0.0260 (10)	0.0296 (11)	0.0287 (10)	−0.0103 (9)	−0.0050 (8)	0.0012 (8)
C3I	0.0323 (12)	0.0280 (11)	0.0374 (12)	−0.0098 (9)	−0.0051 (9)	−0.0023 (9)
C4I	0.0345 (12)	0.0279 (11)	0.0374 (12)	−0.0031 (9)	−0.0096 (10)	0.0029 (9)
C5I	0.0535 (16)	0.0346 (13)	0.0613 (17)	−0.0080 (12)	−0.0386 (14)	0.0055 (12)
C6I	0.0666 (19)	0.0293 (13)	0.076 (2)	−0.0137 (12)	−0.0519 (17)	0.0047 (12)
O4	0.0272 (8)	0.0607 (11)	0.0337 (9)	−0.0208 (8)	−0.0049 (7)	0.0027 (8)
Si4	0.0269 (3)	0.0423 (3)	0.0314 (3)	−0.0177 (3)	−0.0106 (2)	0.0113 (3)
C1J	0.0270 (11)	0.0437 (14)	0.0464 (14)	−0.0116 (10)	−0.0042 (10)	0.0156 (11)
C2J	0.0433 (14)	0.0446 (14)	0.0350 (12)	−0.0177 (11)	−0.0063 (10)	0.0042 (10)
C3J	0.080 (2)	0.0598 (19)	0.0346 (14)	−0.0316 (17)	−0.0045 (14)	0.0092 (13)
C4J	0.079 (2)	0.073 (2)	0.062 (2)	−0.041 (2)	0.0215 (18)	0.0127 (18)
C5J	0.045 (2)	0.150 (5)	0.149 (5)	−0.042 (3)	0.002 (2)	0.082 (4)
C6J	0.0361 (17)	0.158 (4)	0.124 (4)	−0.043 (2)	−0.023 (2)	0.097 (3)
C1K	0.0519 (15)	0.0470 (14)	0.0230 (11)	−0.0274 (12)	−0.0025 (10)	0.0051 (10)
C2K	0.0584 (18)	0.0463 (16)	0.0455 (15)	−0.0245 (14)	0.0130 (13)	−0.0054 (12)
C3K	0.093 (3)	0.0459 (17)	0.0556 (19)	−0.0252 (17)	0.0232 (18)	−0.0080 (14)
C4K	0.138 (3)	0.0657 (17)	0.0425 (11)	−0.0692 (16)	−0.0167 (16)	0.0097 (12)
C5K	0.138 (3)	0.0657 (17)	0.0425 (11)	−0.0692 (16)	−0.0167 (16)	0.0097 (12)
C6K	0.081 (2)	0.0630 (18)	0.0388 (14)	−0.0473 (17)	−0.0277 (14)	0.0172 (13)
C1L	0.0353 (13)	0.0408 (14)	0.0571 (16)	−0.0116 (11)	−0.0201 (12)	−0.0008 (12)
C2L	0.143 (4)	0.0430 (19)	0.239 (7)	−0.032 (2)	−0.156 (5)	0.017 (3)
C3L	0.129 (5)	0.061 (3)	0.305 (9)	−0.003 (3)	−0.162 (6)	−0.043 (4)
C4L	0.050 (2)	0.164 (5)	0.091 (3)	−0.047 (3)	0.000 (2)	−0.071 (3)
C5L	0.100 (3)	0.175 (5)	0.0352 (16)	−0.097 (3)	−0.0252 (18)	0.024 (2)
C6L	0.0511 (16)	0.078 (2)	0.0334 (13)	−0.0393 (15)	−0.0133 (12)	0.0132 (13)
O5	0.0323 (9)	0.0417 (9)	0.0469 (10)	−0.0154 (7)	−0.0105 (7)	0.0129 (8)
Si5	0.0338 (3)	0.0310 (3)	0.0484 (4)	−0.0079 (3)	−0.0036 (3)	0.0117 (3)
C1M	0.0214 (13)	0.0259 (14)	0.0415 (13)	−0.0047 (11)	−0.0093 (10)	0.0048 (11)
C2M	0.038 (3)	0.046 (3)	0.046 (3)	−0.012 (3)	−0.012 (3)	0.010 (2)
C3M	0.052 (5)	0.052 (4)	0.037 (3)	−0.007 (3)	−0.006 (3)	0.006 (3)
C4M	0.048 (4)	0.057 (5)	0.039 (3)	−0.008 (4)	0.007 (3)	0.010 (3)
C5M	0.075 (4)	0.053 (4)	0.057 (4)	−0.041 (3)	0.009 (3)	−0.002 (3)
C6M	0.058 (4)	0.052 (3)	0.045 (3)	−0.030 (3)	−0.003 (3)	−0.001 (2)
C1MM	0.0214 (13)	0.0259 (14)	0.0415 (13)	−0.0047 (11)	−0.0093 (10)	0.0048 (11)
C2MM	0.036 (3)	0.021 (2)	0.050 (3)	−0.010 (2)	0.005 (3)	0.000 (2)
C3MM	0.056 (5)	0.024 (3)	0.051 (4)	−0.018 (3)	0.009 (3)	0.000 (2)
C4MM	0.027 (3)	0.030 (3)	0.049 (3)	−0.010 (3)	−0.003 (2)	0.012 (2)
C5MM	0.027 (2)	0.022 (2)	0.048 (3)	−0.0115 (17)	−0.0156 (19)	0.0047 (18)
C6MM	0.023 (2)	0.027 (2)	0.040 (2)	−0.0095 (17)	−0.0136 (18)	0.0028 (18)
C1N	0.0334 (18)	0.0329 (18)	0.056 (2)	−0.0113 (15)	−0.0115 (17)	0.0082 (16)
C2N	0.038 (3)	0.034 (2)	0.042 (3)	−0.016 (2)	−0.006 (2)	0.006 (2)
C3N	0.049 (3)	0.043 (3)	0.041 (3)	−0.027 (2)	−0.003 (2)	0.000 (2)
C4N	0.047 (3)	0.036 (3)	0.080 (4)	−0.022 (3)	0.001 (3)	−0.017 (3)
C5N	0.033 (4)	0.033 (3)	0.106 (6)	−0.008 (3)	−0.017 (4)	−0.003 (4)
C6N	0.031 (3)	0.023 (3)	0.089 (5)	−0.004 (2)	−0.013 (3)	−0.009 (3)
C1NN	0.0334 (18)	0.0329 (18)	0.056 (2)	−0.0113 (15)	−0.0115 (17)	0.0082 (16)
C2NN	0.040 (3)	0.043 (3)	0.052 (3)	−0.015 (2)	−0.018 (2)	0.013 (2)
C3NN	0.043 (3)	0.046 (3)	0.053 (3)	−0.027 (3)	−0.017 (3)	0.016 (3)
C4NN	0.062 (4)	0.045 (3)	0.057 (4)	−0.017 (3)	−0.020 (3)	0.008 (3)
C5NN	0.090 (7)	0.044 (4)	0.070 (5)	−0.007 (4)	−0.036 (5)	0.000 (4)
C6NN	0.072 (5)	0.046 (4)	0.076 (5)	−0.021 (3)	−0.032 (4)	0.005 (3)
C1O	0.0328 (15)	0.032 (2)	0.0418 (19)	−0.004 (2)	−0.0074 (14)	0.013 (2)
C2O	0.030 (2)	0.048 (3)	0.038 (2)	−0.016 (2)	−0.0090 (19)	0.015 (2)
C3O	0.041 (3)	0.046 (3)	0.036 (2)	−0.018 (2)	−0.007 (2)	0.011 (2)
C4O	0.045 (3)	0.053 (3)	0.036 (3)	−0.023 (2)	−0.017 (2)	0.012 (2)
C5O	0.036 (3)	0.036 (3)	0.056 (4)	−0.012 (2)	−0.026 (3)	0.023 (3)
C6O	0.034 (3)	0.046 (3)	0.043 (3)	−0.016 (2)	−0.015 (2)	0.008 (2)
C1OO	0.0328 (15)	0.032 (2)	0.0418 (19)	−0.004 (2)	−0.0074 (14)	0.013 (2)
C2OO	0.041 (3)	0.041 (3)	0.056 (3)	0.001 (2)	−0.011 (2)	0.004 (2)
C3OO	0.069 (4)	0.042 (3)	0.053 (3)	0.004 (3)	−0.019 (3)	0.010 (3)
C4OO	0.094 (6)	0.052 (4)	0.094 (6)	−0.023 (4)	−0.064 (5)	0.017 (4)
C5OO	0.088 (6)	0.061 (5)	0.117 (8)	−0.038 (4)	−0.070 (6)	0.050 (5)
C6OO	0.049 (3)	0.047 (3)	0.079 (4)	−0.022 (3)	−0.033 (3)	0.021 (3)
O6	0.0296 (8)	0.0317 (8)	0.0400 (9)	−0.0112 (6)	−0.0139 (7)	0.0035 (7)
Si6	0.0251 (3)	0.0344 (3)	0.0250 (3)	−0.0132 (2)	−0.0077 (2)	0.0047 (2)
C1P	0.0301 (11)	0.0309 (11)	0.0337 (11)	−0.0173 (9)	−0.0117 (9)	0.0051 (9)
C2P	0.0318 (11)	0.0311 (11)	0.0396 (12)	−0.0157 (9)	−0.0085 (9)	0.0062 (9)
C3P	0.0316 (12)	0.0319 (12)	0.0533 (15)	−0.0147 (10)	−0.0078 (11)	0.0036 (11)
C4P	0.0362 (13)	0.0277 (12)	0.0643 (17)	−0.0139 (10)	−0.0204 (12)	0.0085 (11)
C5P	0.0461 (14)	0.0350 (12)	0.0470 (14)	−0.0210 (11)	−0.0228 (11)	0.0141 (11)
C6P	0.0358 (12)	0.0361 (12)	0.0361 (12)	−0.0194 (10)	−0.0135 (10)	0.0084 (9)
C1R	0.0270 (11)	0.0567 (15)	0.0257 (11)	−0.0085 (10)	−0.0088 (9)	0.0086 (10)
C2R	0.0351 (14)	0.098 (2)	0.0300 (12)	−0.0310 (15)	−0.0087 (10)	0.0201 (14)
C3R	0.0334 (15)	0.163 (4)	0.0445 (17)	−0.036 (2)	−0.0075 (13)	0.041 (2)
C4R	0.0305 (15)	0.165 (4)	0.0312 (15)	0.0037 (19)	0.0019 (12)	0.032 (2)
C5R	0.0422 (17)	0.115 (3)	0.0243 (13)	0.0198 (17)	−0.0095 (11)	0.0023 (15)
C6R	0.0348 (13)	0.0686 (19)	0.0278 (12)	0.0043 (12)	−0.0129 (10)	0.0017 (12)
C1S	0.0327 (11)	0.0400 (12)	0.0243 (10)	−0.0224 (10)	−0.0077 (8)	0.0096 (9)
C2S	0.0403 (13)	0.0365 (12)	0.0296 (11)	−0.0232 (10)	−0.0082 (9)	0.0084 (9)
C3S	0.0584 (16)	0.0428 (14)	0.0305 (12)	−0.0314 (12)	−0.0114 (11)	0.0066 (10)
C4S	0.0662 (18)	0.0550 (16)	0.0314 (12)	−0.0378 (14)	−0.0216 (12)	0.0112 (11)
C5S	0.0461 (15)	0.0592 (17)	0.0386 (13)	−0.0267 (13)	−0.0228 (11)	0.0159 (12)
C6S	0.0346 (12)	0.0465 (14)	0.0304 (11)	−0.0191 (11)	−0.0115 (9)	0.0093 (10)

Geometric parameters (Å, º)

O1W—K4	2.746 (2)	Si3—C1G	1.884 (2)
O1W—K1	2.763 (2)	Si3—C1H	1.887 (3)
O1W—K6	2.851 (2)	Si3—C1I	1.893 (2)
O1W—K21	3.258 (4)	C1G—C6G	1.389 (3)
O1W—K5	3.258 (2)	C1G—C2G	1.401 (3)
O1W—K61	3.280 (3)	C2G—C3G	1.385 (3)
O1W—H1W1	0.8400	C2G—H2G	0.9500
O1W—H1W2	0.8400	C3G—C4G	1.378 (4)
O2W—K3	2.684 (4)	C3G—H3G	0.9500
O2W—K6	2.888 (4)	C4G—C5G	1.373 (4)
O2W—K2	2.907 (4)	C4G—H4G	0.9500
O2W—H2W1	0.8400	C5G—C6G	1.389 (4)
O2W—H2W2	0.8400	C5G—H5G	0.9500
O3W—K61	2.796 (5)	C6G—H6G	0.9500
O3W—K21	2.906 (5)	C1H—C2H	1.392 (4)
O3W—K3	2.958 (5)	C1H—C6H	1.395 (4)
O3W—H3W1	0.8400	C2H—C3H	1.395 (5)
O3W—H3W2	0.8400	C2H—H2H	0.9500
K1—O2	2.5857 (19)	C3H—C4H	1.366 (7)
K1—O1	2.6305 (18)	C3H—H3H	0.9500
K1—C2OO	3.032 (4)	C4H—C5H	1.381 (6)
K1—O5	3.063 (2)	C4H—H4H	0.9500
K1—C2O	3.161 (3)	C5H—C6H	1.391 (5)
K1—C2A	3.345 (3)	C5H—H5H	0.9500
K1—K21	3.4843 (17)	C6H—H6H	0.9500
K1—C1O	3.529 (4)	C1I—C6I	1.390 (3)
K1—Si1	3.6902 (10)	C1I—C2I	1.397 (3)
K1—K2	3.7699 (15)	C2I—C3I	1.383 (3)
K1—Si2	3.8132 (13)	C2I—H2I	0.9500
K1—H1W2	2.5030	C3I—C4I	1.379 (3)
K2—O2	2.5692 (18)	C3I—H3I	0.9500
K2—O4	2.754 (2)	C4I—C5I	1.372 (4)
K2—O1	2.770 (2)	C4I—H4I	0.9500
K2—C2J	3.133 (3)	C5I—C6I	1.385 (4)
K2—C2D	3.284 (3)	C5I—H5I	0.9500
K2—Si2	3.5819 (13)	C6I—H6I	0.9500
K2—Si4	3.6847 (14)	O4—Si4	1.5839 (18)
K2—K4	3.6993 (14)	Si4—C1K	1.873 (3)
K2—K6	4.0004 (17)	Si4—C1J	1.887 (2)
K2—K3	4.791 (2)	Si4—C1L	1.900 (3)
K2—H2W1	2.6714	C1J—C2J	1.377 (4)
K21—O4	2.495 (2)	C1J—C6J	1.392 (4)
K21—O1	2.548 (2)	C2J—C3J	1.393 (4)
K21—O2	2.664 (2)	C2J—H2J	0.9500
K21—K4	3.4334 (16)	C3J—C4J	1.357 (5)
K21—Si4	3.6083 (16)	C3J—H3J	0.9500
K21—K61	3.756 (2)	C4J—C5J	1.376 (6)
K21—Si2	3.923 (2)	C4J—H4J	0.9500
K21—K3	4.186 (3)	C5J—C6J	1.384 (5)
K3—O5	2.6143 (18)	C5J—H5J	0.9500
K3—O3	2.6735 (18)	C6J—H6J	0.9500
K3—O1	2.9621 (19)	C1K—C6K	1.395 (4)
K3—C1B	3.174 (2)	C1K—C2K	1.410 (4)
K3—C6B	3.215 (3)	C2K—C3K	1.391 (4)
K3—C2B	3.448 (3)	C2K—H2K	0.9500
K3—C5B	3.531 (3)	C3K—C4K	1.407 (6)
K3—Si1	3.7215 (11)	C3K—H3K	0.9500
K3—K6	3.844 (2)	C4K—C5K	1.391 (6)
K3—K5	3.8799 (11)	C4K—H4K	0.9500
K3—H1W2	3.0751	C5K—C6K	1.381 (4)
K3—H2W1	2.4314	C5K—H5K	0.9500
K3—H2W2	3.0746	C6K—H6K	0.9500
K3—H3W2	2.5565	C1L—C6L	1.354 (4)
K4—O2	2.6025 (17)	C1L—C2L	1.388 (4)
K4—O4	2.6139 (16)	C2L—C3L	1.375 (7)
K4—C1S	3.191 (2)	C2L—H2L	0.9500
K4—C2S	3.246 (2)	C3L—C4L	1.338 (8)
K4—C2F	3.259 (3)	C3L—H3L	0.9500
K4—C6S	3.277 (2)	C4L—C5L	1.345 (7)
K4—C3S	3.376 (2)	C4L—H4L	0.9500
K4—C5S	3.428 (3)	C5L—C6L	1.392 (4)
K4—C1F	3.449 (2)	C5L—H5L	0.9500
K4—C4S	3.467 (3)	C6L—H6L	0.9500
K4—H1W1	2.7702	O5—Si5	1.5904 (18)
K5—O6	2.6192 (18)	Si5—C1OO	1.794 (3)
K5—O3	2.701 (2)	Si5—C3NN	1.900 (3)
K5—O5	2.8798 (19)	Si5—C1M	1.909 (3)
K5—C2M	3.055 (4)	Si5—C1MM	1.928 (3)
K5—C6MM	3.083 (3)	Si5—C1N	1.998 (2)
K5—C1MM	3.114 (4)	Si5—C1O	2.079 (2)
K5—C1H	3.212 (3)	C1M—C2M	1.3900
K5—C1M	3.313 (4)	C1M—C6M	1.3900
K5—C2H	3.404 (3)	C2M—C3M	1.3900
K5—Si3	3.4766 (8)	C2M—H2M	0.9500
K5—C6R	3.530 (3)	C3M—C4M	1.3900
K5—H1W1	2.8720	C3M—H3M	0.9500
K5—H1W2	2.9715	C4M—C5M	1.3900
K6—O3	2.537 (3)	C4M—H4M	0.9500
K6—O6	2.7205 (19)	C5M—C6M	1.3900
K6—O4	2.798 (2)	C5M—H5M	0.9500
K6—C2L	3.356 (6)	C6M—H6M	0.9500
K6—C1L	3.381 (3)	C1MM—C2MM	1.3900
K6—C2I	3.406 (3)	C1MM—C6MM	1.3900
K6—Si3	3.6486 (14)	C2MM—C3MM	1.3900
K6—Si4	3.6855 (19)	C2MM—H2MM	0.9500
K6—H1W1	2.6328	C3MM—C4MM	1.3900
K61—O6	2.618 (2)	C3MM—H3MM	0.9500
K61—O4	2.670 (2)	C4MM—C5MM	1.3900
K61—C1L	2.988 (3)	C4MM—H4MM	0.9500
K61—O3	3.046 (3)	C5MM—C6MM	1.3900
K61—C2I	3.089 (3)	C5MM—H5MM	0.9500
K61—C2L	3.228 (6)	C6MM—H6MM	0.9500
K61—Si4	3.3660 (18)	C1N—C2N	1.3900
K61—C6L	3.372 (4)	C1N—C6N	1.3900
K61—C2P	3.546 (3)	C2N—C3N	1.3900
K61—Si6	3.7509 (16)	C2N—H2N	0.9500
K61—H1W1	2.9159	C3N—C4N	1.3900
K61—H3W2	2.7520	C3N—H3N	0.9500
O1—Si1	1.5864 (16)	C4N—C5N	1.3900
Si1—C1A	1.885 (2)	C4N—H4N	0.9500
Si1—C1C	1.887 (2)	C5N—C6N	1.3900
Si1—C1B	1.892 (2)	C5N—H5N	0.9500
C1A—C6A	1.398 (3)	C6N—H6N	0.9500
C1A—C2A	1.401 (3)	C1NN—C2NN	1.3900
C2A—C3A	1.385 (4)	C1NN—C6NN	1.3900
C2A—H2A	0.9500	C2NN—C3NN	1.3900
C3A—C4A	1.380 (5)	C2NN—H2NN	0.9500
C3A—H3A	0.9500	C3NN—C4NN	1.3900
C4A—C5A	1.378 (4)	C3NN—H3NN	0.9500
C4A—H4A	0.9500	C4NN—C5NN	1.3900
C5A—C6A	1.393 (4)	C4NN—H4NN	0.9500
C5A—H5A	0.9500	C5NN—C6NN	1.3900
C6A—H6A	0.9500	C5NN—H5NN	0.9500
C1B—C2B	1.398 (4)	C6NN—H6NN	0.9500
C1B—C6B	1.404 (4)	C1O—C2O	1.3900
C2B—C3B	1.414 (4)	C1O—C6O	1.3900
C2B—H2B	0.9500	C2O—C3O	1.3900
C3B—C4B	1.370 (5)	C2O—H2O	0.9500
C3B—H3B	0.9500	C3O—C4O	1.3900
C4B—C5B	1.363 (5)	C3O—H3O	0.9500
C4B—H4B	0.9500	C4O—C5O	1.3900
C5B—C6B	1.393 (4)	C4O—H4O	0.9500
C5B—H5B	0.9500	C5O—C6O	1.3900
C6B—H6B	0.9500	C5O—H5O	0.9500
C1C—C6C	1.389 (3)	C6O—H6O	0.9500
C1C—C2C	1.392 (3)	C1OO—C2OO	1.3900
C2C—C3C	1.389 (4)	C1OO—C6OO	1.3900
C2C—H2C	0.9500	C2OO—C3OO	1.3900
C3C—C4C	1.375 (4)	C2OO—H2OO	0.9500
C3C—H3C	0.9500	C3OO—C4OO	1.3900
C4C—C5C	1.374 (4)	C3OO—H3OO	0.9500
C4C—H4C	0.9500	C4OO—C5OO	1.3900
C5C—C6C	1.386 (4)	C4OO—H4OO	0.9500
C5C—H5C	0.9500	C5OO—C6OO	1.3900
C6C—H6C	0.9500	C5OO—H5OO	0.9500
O2—Si2	1.5880 (16)	C6OO—H6OO	0.9500
Si2—C1E	1.888 (2)	O6—Si6	1.5922 (16)
Si2—C1D	1.891 (2)	Si6—C1R	1.885 (2)
Si2—C1F	1.899 (2)	Si6—C1P	1.889 (2)
C1D—C6D	1.397 (3)	Si6—C1S	1.893 (2)
C1D—C2D	1.400 (3)	C1P—C2P	1.400 (3)
C2D—C3D	1.387 (3)	C1P—C6P	1.401 (3)
C2D—H2D	0.9500	C2P—C3P	1.388 (3)
C3D—C4D	1.387 (4)	C2P—H2P	0.9500
C3D—H3D	0.9500	C3P—C4P	1.387 (4)
C4D—C5D	1.380 (4)	C3P—H3P	0.9500
C4D—H4D	0.9500	C4P—C5P	1.383 (4)
C5D—C6D	1.394 (3)	C4P—H4P	0.9500
C5D—H5D	0.9500	C5P—C6P	1.391 (4)
C6D—H6D	0.9500	C5P—H5P	0.9500
C1E—C6E	1.391 (4)	C6P—H6P	0.9500
C1E—C2E	1.399 (3)	C1R—C2R	1.399 (4)
C2E—C3E	1.390 (4)	C1R—C6R	1.400 (4)
C2E—H2E	0.9500	C2R—C3R	1.393 (4)
C3E—C4E	1.376 (5)	C2R—H2R	0.9500
C3E—H3E	0.9500	C3R—C4R	1.380 (6)
C4E—C5E	1.390 (5)	C3R—H3R	0.9500
C4E—H4E	0.9500	C4R—C5R	1.379 (6)
C5E—C6E	1.380 (4)	C4R—H4R	0.9500
C5E—H5E	0.9500	C5R—C6R	1.390 (4)
C6E—H6E	0.9500	C5R—H5R	0.9500
C1F—C2F	1.400 (3)	C6R—H6R	0.9500
C1F—C6F	1.401 (3)	C1S—C2S	1.397 (3)
C2F—C3F	1.387 (4)	C1S—C6S	1.408 (3)
C2F—H2F	0.9500	C2S—C3S	1.392 (3)
C3F—C4F	1.386 (4)	C2S—H2S	0.9500
C3F—H3F	0.9500	C3S—C4S	1.378 (4)
C4F—C5F	1.378 (4)	C3S—H3S	0.9500
C4F—H4F	0.9500	C4S—C5S	1.386 (4)
C5F—C6F	1.396 (3)	C4S—H4S	0.9500
C5F—H5F	0.9500	C5S—C6S	1.394 (3)
C6F—H6F	0.9500	C5S—H5S	0.9500
O3—Si3	1.5865 (17)	C6S—H6S	0.9500
K4—O1W—K1	91.68 (6)	C2L—K61—H1W1	141.3
K4—O1W—K6	91.54 (8)	O1W—K61—H1W1	14.1
K1—O1W—K6	130.96 (9)	Si4—K61—H1W1	107.8
K4—O1W—K21	69.15 (6)	C6L—K61—H1W1	154.9
K1—O1W—K21	70.17 (6)	C2P—K61—H1W1	93.3
K4—O1W—K5	138.60 (7)	Si6—K61—H1W1	52.2
K1—O1W—K5	126.38 (8)	O6—K61—H3W2	111.6
K6—O1W—K5	76.02 (5)	O4—K61—H3W2	102.5
K21—O1W—K5	133.80 (7)	O3W—K61—H3W2	17.4
K4—O1W—K61	83.15 (7)	C1L—K61—H3W2	97.8
K1—O1W—K61	139.10 (9)	O3—K61—H3W2	39.3
K21—O1W—K61	70.11 (6)	C2I—K61—H3W2	94.8
K5—O1W—K61	77.48 (5)	C2L—K61—H3W2	72.7
K4—O1W—H1W1	82.9	O1W—K61—H3W2	77.9
K1—O1W—H1W1	162.0	Si4—K61—H3W2	107.8
K6—O1W—H1W1	66.6	C6L—K61—H3W2	110.0
K21—O1W—H1W1	122.8	C2P—K61—H3W2	173.0
K5—O1W—H1W1	55.9	Si6—K61—H3W2	132.1
K61—O1W—H1W1	57.5	H1W1—K61—H3W2	88.5
K4—O1W—H1W2	150.8	Si1—O1—K21	144.31 (12)
K1—O1W—H1W2	63.5	Si1—O1—K1	120.06 (9)
K6—O1W—H1W2	115.9	K21—O1—K1	84.55 (6)
K21—O1W—H1W2	112.0	Si1—O1—K2	130.82 (10)
K5—O1W—H1W2	62.9	K1—O1—K2	88.51 (5)
K61—O1W—H1W2	125.4	Si1—O1—K3	105.80 (8)
H1W1—O1W—H1W2	115.9	K21—O1—K3	98.60 (9)
K3—O2W—K6	87.15 (11)	K1—O1—K3	90.90 (6)
K3—O2W—K2	117.89 (13)	K2—O1—K3	113.35 (7)
K6—O2W—K2	87.32 (10)	O1—Si1—C1A	113.33 (10)
K3—O2W—H2W1	63.7	O1—Si1—C1C	112.24 (10)
K6—O2W—H2W1	118.5	C1A—Si1—C1C	105.79 (10)
K2—O2W—H2W1	65.6	O1—Si1—C1B	108.32 (9)
K3—O2W—H2W2	110.0	C1A—Si1—C1B	108.57 (11)
K6—O2W—H2W2	124.8	C1C—Si1—C1B	108.45 (11)
K2—O2W—H2W2	123.1	O1—Si1—K1	38.09 (7)
H2W1—O2W—H2W2	116.0	C1A—Si1—K1	76.38 (7)
K61—O3W—K21	82.36 (12)	C1C—Si1—K1	134.45 (8)
K61—O3W—K3	105.82 (15)	C1B—Si1—K1	113.81 (8)
K21—O3W—K3	91.09 (14)	O1—Si1—K3	49.98 (7)
K61—O3W—H3W1	108.8	C1A—Si1—K3	123.92 (7)
K21—O3W—H3W1	109.8	C1C—Si1—K3	130.29 (7)
K3—O3W—H3W1	141.4	C1B—Si1—K3	58.51 (7)
K61—O3W—H3W2	78.3	K1—Si1—K3	65.18 (2)
K21—O3W—H3W2	132.1	C6A—C1A—C2A	116.9 (2)
K3—O3W—H3W2	54.0	C6A—C1A—Si1	123.23 (19)
H3W1—O3W—H3W2	117.8	C2A—C1A—Si1	119.82 (18)
O2—K1—O1	87.39 (5)	C3A—C2A—C1A	121.8 (3)
O2—K1—O1W	81.19 (6)	C3A—C2A—K1	121.9 (2)
O1—K1—O1W	89.67 (6)	C1A—C2A—K1	94.52 (16)
O2—K1—C2OO	150.66 (8)	C3A—C2A—H2A	119.1
O1—K1—C2OO	116.91 (8)	C1A—C2A—H2A	119.1
O1W—K1—C2OO	113.15 (8)	K1—C2A—H2A	51.4
O2—K1—O5	134.52 (5)	C4A—C3A—C2A	120.1 (3)
O1—K1—O5	88.59 (5)	C4A—C3A—H3A	120.0
O1W—K1—O5	53.49 (6)	C2A—C3A—H3A	120.0
C2OO—K1—O5	66.38 (8)	C5A—C4A—C3A	119.7 (3)
O2—K1—C2O	115.36 (7)	C5A—C4A—H4A	120.2
O1—K1—C2O	152.64 (7)	C3A—C4A—H4A	120.2
O1W—K1—C2O	79.71 (7)	C4A—C5A—C6A	120.2 (3)
O5—K1—C2O	64.79 (7)	C4A—C5A—H5A	119.9
O2—K1—C2A	92.21 (6)	C6A—C5A—H5A	119.9
O1—K1—C2A	66.33 (6)	C5A—C6A—C1A	121.4 (3)
O1W—K1—C2A	155.46 (7)	C5A—C6A—H6A	119.3
C2OO—K1—C2A	83.83 (8)	C1A—C6A—H6A	119.3
O5—K1—C2A	126.85 (6)	C2B—C1B—C6B	116.6 (2)
C2O—K1—C2A	124.01 (7)	C2B—C1B—Si1	121.4 (2)
O2—K1—K21	49.39 (5)	C6B—C1B—Si1	120.85 (19)
O1—K1—K21	46.73 (4)	C2B—C1B—K3	89.11 (14)
O1W—K1—K21	61.60 (7)	C6B—C1B—K3	78.96 (14)
O5—K1—K21	98.52 (6)	Si1—C1B—K3	90.93 (8)
C2A—K1—K21	96.24 (6)	C1B—C2B—C3B	120.9 (3)
O2—K1—C1O	138.46 (6)	C1B—C2B—K3	66.98 (13)
O1—K1—C1O	132.64 (6)	C3B—C2B—K3	90.58 (17)
O1W—K1—C1O	87.55 (7)	C1B—C2B—H2B	119.6
O5—K1—C1O	53.07 (5)	C3B—C2B—H2B	119.6
C2O—K1—C1O	23.2	K3—C2B—H2B	112.7
C2A—K1—C1O	112.07 (7)	C4B—C3B—C2B	120.0 (3)
O2—K1—Si1	98.57 (4)	C4B—C3B—H3B	120.0
O1—K1—Si1	21.84 (4)	C2B—C3B—H3B	120.0
O1W—K1—Si1	109.82 (5)	C5B—C4B—C3B	120.6 (3)
C2OO—K1—Si1	99.95 (7)	C5B—C4B—H4B	119.7
O5—K1—Si1	93.97 (4)	C3B—C4B—H4B	119.7
C2O—K1—Si1	145.94 (6)	C4B—C5B—C6B	119.8 (3)
C2A—K1—Si1	47.53 (5)	C4B—C5B—K3	89.3 (2)
K21—K1—Si1	66.68 (3)	C6B—C5B—K3	65.57 (16)
C1O—K1—Si1	122.80 (5)	C4B—C5B—H5B	120.1
O2—K1—K2	42.83 (4)	C6B—C5B—H5B	120.1
O1—K1—K2	47.26 (4)	K3—C5B—H5B	115.1
O1W—K1—K2	71.26 (6)	C5B—C6B—C1B	122.2 (3)
O5—K1—K2	109.07 (5)	C5B—C6B—K3	91.19 (18)
C2A—K1—K2	87.80 (6)	C1B—C6B—K3	75.67 (14)
Si1—K1—K2	64.69 (2)	C5B—C6B—H6B	118.9
O2—K1—Si2	18.46 (4)	C1B—C6B—H6B	118.9
O1—K1—Si2	94.61 (4)	K3—C6B—H6B	103.6
O1W—K1—Si2	98.21 (5)	C6C—C1C—C2C	116.0 (2)
C2OO—K1—Si2	134.34 (8)	C6C—C1C—Si1	121.86 (18)
O5—K1—Si2	151.55 (4)	C2C—C1C—Si1	122.09 (18)
C2O—K1—Si2	111.74 (6)	C3C—C2C—C1C	122.2 (2)
C2A—K1—Si2	79.64 (5)	C3C—C2C—H2C	118.9
K21—K1—Si2	64.85 (5)	C1C—C2C—H2C	118.9
C1O—K1—Si2	132.56 (5)	C4C—C3C—C2C	120.0 (2)
Si1—K1—Si2	99.45 (2)	C4C—C3C—H3C	120.0
K2—K1—Si2	56.37 (3)	C2C—C3C—H3C	120.0
O2—K1—H1W2	98.6	C5C—C4C—C3C	119.3 (2)
O1—K1—H1W2	89.6	C5C—C4C—H4C	120.4
O1W—K1—H1W2	17.5	C3C—C4C—H4C	120.4
C2OO—K1—H1W2	97.8	C4C—C5C—C6C	120.2 (3)
O5—K1—H1W2	36.0	C4C—C5C—H5C	119.9
C2O—K1—H1W2	72.8	C6C—C5C—H5C	119.9
C2A—K1—H1W2	153.1	C5C—C6C—C1C	122.3 (3)
K21—K1—H1W2	73.2	C5C—C6C—H6C	118.9
C1O—K1—H1W2	74.9	C1C—C6C—H6C	118.9
Si1—K1—H1W2	106.2	Si2—O2—K2	117.02 (9)
K2—K1—H1W2	83.8	Si2—O2—K1	130.50 (9)
Si2—K1—H1W2	115.6	K2—O2—K1	93.99 (6)
O2—K2—O4	88.61 (6)	Si2—O2—K4	116.30 (9)
O2—K2—O1	84.81 (6)	K2—O2—K4	91.33 (6)
O4—K2—O1	126.85 (9)	K1—O2—K4	99.23 (6)
O2—K2—O2W	124.11 (10)	Si2—O2—K21	132.97 (11)
O4—K2—O2W	87.65 (8)	K1—O2—K21	83.15 (7)
O1—K2—O2W	55.13 (9)	K4—O2—K21	81.36 (6)
O2—K2—C2J	108.08 (7)	O2—Si2—C1E	111.48 (10)
O4—K2—C2J	68.53 (6)	O2—Si2—C1D	113.13 (9)
O1—K2—C2J	161.16 (8)	C1E—Si2—C1D	105.61 (10)
O2W—K2—C2J	121.85 (9)	O2—Si2—C1F	110.45 (9)
O2—K2—C2D	68.49 (6)	C1E—Si2—C1F	107.27 (10)
O4—K2—C2D	134.30 (7)	C1D—Si2—C1F	108.63 (10)
O1—K2—C2D	91.15 (7)	O2—Si2—K2	39.72 (7)
O2W—K2—C2D	138.03 (8)	C1E—Si2—K2	134.37 (8)
C2J—K2—C2D	81.38 (8)	C1D—Si2—K2	74.73 (7)
O2—K2—Si2	23.26 (4)	C1F—Si2—K2	115.85 (7)
O4—K2—Si2	96.50 (4)	O2—Si2—K4	40.40 (6)
O1—K2—Si2	97.45 (5)	C1E—Si2—K4	124.87 (8)
O2W—K2—Si2	146.00 (9)	C1D—Si2—K4	128.01 (7)
C2J—K2—Si2	90.66 (6)	C1F—Si2—K4	70.04 (7)
C2D—K2—Si2	48.93 (5)	K2—Si2—K4	62.01 (3)
O2—K2—Si4	106.07 (5)	O2—Si2—K1	31.04 (6)
O4—K2—Si4	23.21 (4)	C1E—Si2—K1	81.05 (7)
O1—K2—Si4	141.82 (7)	C1D—Si2—K1	118.27 (8)
O2W—K2—Si4	90.35 (7)	C1F—Si2—K1	128.14 (7)
C2J—K2—Si4	49.00 (5)	K2—Si2—K1	61.20 (3)
C2D—K2—Si4	126.99 (7)	K4—Si2—K1	64.360 (19)
Si2—K2—Si4	106.54 (3)	O2—Si2—K21	29.80 (7)
O2—K2—K4	44.70 (4)	C1E—Si2—K21	131.23 (8)
O4—K2—K4	44.89 (4)	C1D—Si2—K21	84.72 (8)
O1—K2—K4	104.47 (6)	C1F—Si2—K21	114.21 (7)
O2W—K2—K4	104.74 (8)	K4—Si2—K21	54.11 (4)
C2J—K2—K4	94.29 (5)	K1—Si2—K21	53.52 (4)
C2D—K2—K4	107.84 (5)	C6D—C1D—C2D	117.0 (2)
Si2—K2—K4	59.23 (2)	C6D—C1D—Si2	123.12 (18)
Si4—K2—K4	65.76 (2)	C2D—C1D—Si2	119.72 (17)
O2—K2—K1	43.17 (4)	C3D—C2D—C1D	121.8 (2)
O4—K2—K1	102.42 (6)	C3D—C2D—K2	123.37 (17)
O1—K2—K1	44.23 (4)	C1D—C2D—K2	90.59 (14)
O2W—K2—K1	83.69 (8)	C3D—C2D—H2D	119.1
C2J—K2—K1	151.13 (6)	C1D—C2D—H2D	119.1
C2D—K2—K1	87.50 (5)	K2—C2D—H2D	54.8
Si2—K2—K1	62.43 (2)	C2D—C3D—C4D	119.9 (2)
Si4—K2—K1	125.63 (5)	C2D—C3D—H3D	120.1
K4—K2—K1	63.88 (3)	C4D—C3D—H3D	120.1
O2—K2—K6	100.10 (6)	C5D—C4D—C3D	119.8 (2)
O4—K2—K6	44.35 (5)	C5D—C4D—H4D	120.1
O1—K2—K6	85.19 (8)	C3D—C4D—H4D	120.1
O2W—K2—K6	46.15 (7)	C4D—C5D—C6D	120.0 (2)
C2J—K2—K6	105.31 (6)	C4D—C5D—H5D	120.0
C2D—K2—K6	168.33 (6)	C6D—C5D—H5D	120.0
Si2—K2—K6	120.53 (4)	C5D—C6D—C1D	121.5 (2)
Si4—K2—K6	57.14 (3)	C5D—C6D—H6D	119.2
K4—K2—K6	62.65 (3)	C1D—C6D—H6D	119.2
K1—K2—K6	82.14 (5)	C6E—C1E—C2E	116.8 (2)
O2—K2—K3	95.37 (6)	C6E—C1E—Si2	120.2 (2)
O4—K2—K3	94.33 (6)	C2E—C1E—Si2	122.97 (18)
O1—K2—K3	34.59 (4)	C3E—C2E—C1E	121.9 (2)
O2W—K2—K3	29.68 (7)	C3E—C2E—H2E	119.0
C2J—K2—K3	150.02 (6)	C1E—C2E—H2E	119.0
C2D—K2—K3	125.62 (5)	C4E—C3E—C2E	119.6 (3)
Si2—K2—K3	116.38 (3)	C4E—C3E—H3E	120.2
Si4—K2—K3	107.25 (4)	C2E—C3E—H3E	120.2
K4—K2—K3	89.39 (4)	C3E—C4E—C5E	119.6 (3)
K1—K2—K3	54.01 (3)	C3E—C4E—H4E	120.2
K6—K2—K3	50.89 (5)	C5E—C4E—H4E	120.2
O2—K2—H2W1	113.5	C6E—C5E—C4E	120.1 (3)
O4—K2—H2W1	100.5	C6E—C5E—H5E	120.0
O1—K2—H2W1	38.5	C4E—C5E—H5E	120.0
O2W—K2—H2W1	16.6	C5E—C6E—C1E	121.8 (3)
C2J—K2—H2W1	136.8	C5E—C6E—H6E	119.1
C2D—K2—H2W1	124.6	C1E—C6E—H6E	119.1
Si2—K2—H2W1	132.6	C2F—C1F—C6F	116.7 (2)
Si4—K2—H2W1	106.3	C2F—C1F—Si2	120.54 (17)
K4—K2—H2W1	106.6	C6F—C1F—Si2	122.59 (19)
K1—K2—H2W1	70.8	C2F—C1F—K4	70.44 (13)
K6—K2—H2W1	56.6	C6F—C1F—K4	117.57 (14)
K3—K2—H2W1	19.2	Si2—C1F—K4	78.79 (7)
O4—K21—O1	156.78 (14)	C3F—C2F—C1F	122.1 (2)
O4—K21—O2	92.23 (7)	C3F—C2F—K4	109.92 (17)
O1—K21—O2	87.44 (7)	C1F—C2F—K4	85.70 (15)
O4—K21—O3W	87.31 (11)	C3F—C2F—H2F	118.9
O1—K21—O3W	81.15 (13)	C1F—C2F—H2F	118.9
O2—K21—O3W	148.72 (14)	K4—C2F—H2F	74.1
O4—K21—O1W	77.09 (8)	C4F—C3F—C2F	119.8 (3)
O1—K21—O1W	80.85 (9)	C4F—C3F—H3F	120.1
O2—K21—O1W	71.24 (6)	C2F—C3F—H3F	120.1
O3W—K21—O1W	78.20 (12)	C5F—C4F—C3F	119.7 (2)
O4—K21—K4	49.26 (5)	C5F—C4F—H4F	120.2
O1—K21—K4	117.93 (7)	C3F—C4F—H4F	120.2
O2—K21—K4	48.54 (4)	C4F—C5F—C6F	120.3 (2)
O3W—K21—K4	113.07 (12)	C4F—C5F—H5F	119.9
O1W—K21—K4	48.37 (5)	C6F—C5F—H5F	119.9
O4—K21—K1	117.01 (8)	C5F—C6F—C1F	121.4 (2)
O1—K21—K1	48.72 (5)	C5F—C6F—H6F	119.3
O2—K21—K1	47.46 (4)	C1F—C6F—H6F	119.3
O3W—K21—K1	105.81 (12)	Si3—O3—K6	122.81 (11)
O1W—K21—K1	48.24 (5)	Si3—O3—K3	136.52 (10)
K4—K21—K1	69.68 (3)	K6—O3—K3	95.04 (8)
O4—K21—Si4	21.64 (4)	Si3—O3—K5	105.39 (10)
O1—K21—Si4	165.21 (10)	K6—O3—K5	92.20 (6)
O2—K21—Si4	106.00 (6)	K3—O3—K5	92.42 (6)
O3W—K21—Si4	84.11 (10)	Si3—O3—K61	112.40 (10)
O1W—K21—Si4	97.38 (7)	K3—O3—K61	106.59 (8)
K4—K21—Si4	69.35 (3)	K5—O3—K61	90.58 (6)
K1—K21—Si4	138.43 (5)	O3—Si3—C1G	113.25 (10)
O4—K21—K61	45.23 (5)	O3—Si3—C1H	110.05 (12)
O1—K21—K61	114.67 (13)	C1G—Si3—C1H	107.03 (11)
O2—K21—K61	114.79 (7)	O3—Si3—C1I	113.00 (10)
O3W—K21—K61	47.55 (10)	C1G—Si3—C1I	107.69 (10)
O1W—K21—K61	55.22 (7)	C1H—Si3—C1I	105.36 (11)
K4—K21—K61	67.81 (4)	O3—Si3—K5	48.51 (8)
K1—K21—K61	102.92 (9)	C1G—Si3—K5	145.99 (7)
Si4—K21—K61	54.36 (4)	C1H—Si3—K5	66.02 (8)
O4—K21—Si2	93.02 (6)	C1I—Si3—K5	106.20 (7)
O1—K21—Si2	93.41 (6)	O3—Si3—K6	35.76 (8)
O2—K21—Si2	17.23 (4)	C1G—Si3—K6	121.12 (8)
O3W—K21—Si2	165.93 (12)	C1H—Si3—K6	128.46 (8)
O1W—K21—Si2	88.16 (4)	C1I—Si3—K6	77.86 (8)
K4—K21—Si2	58.14 (3)	K5—Si3—K6	63.94 (3)
K1—K21—Si2	61.63 (3)	O3—Si3—K61	45.71 (8)
Si4—K21—Si2	101.23 (5)	C1G—Si3—K61	125.26 (8)
K61—K21—Si2	125.89 (4)	C1H—Si3—K61	127.25 (8)
O4—K21—K3	114.84 (10)	C1I—Si3—K61	67.48 (8)
O1—K21—K3	44.40 (6)	K5—Si3—K61	66.69 (3)
O2—K21—K3	108.91 (7)	C6G—C1G—C2G	116.7 (2)
O3W—K21—K3	44.95 (10)	C6G—C1G—Si3	120.76 (18)
O1W—K21—K3	55.61 (6)	C2G—C1G—Si3	122.48 (17)
K4—K21—K3	103.97 (7)	C3G—C2G—C1G	121.7 (2)
K1—K21—K3	61.93 (4)	C3G—C2G—H2G	119.1
Si4—K21—K3	122.99 (7)	C1G—C2G—H2G	119.1
K61—K21—K3	70.39 (8)	C4G—C3G—C2G	120.0 (2)
Si2—K21—K3	123.48 (4)	C4G—C3G—H3G	120.0
O5—K3—O3	91.43 (6)	C2G—C3G—H3G	120.0
O5—K3—O2W	121.29 (9)	C5G—C4G—C3G	119.5 (2)
O3—K3—O2W	78.54 (9)	C5G—C4G—H4G	120.3
O5—K3—O3W	119.49 (10)	C3G—C4G—H4G	120.3
O3—K3—O3W	58.77 (11)	C4G—C5G—C6G	120.4 (2)
O5—K3—O1	91.10 (6)	C4G—C5G—H5G	119.8
O3—K3—O1	126.43 (6)	C6G—C5G—H5G	119.8
O2W—K3—O1	55.25 (9)	C5G—C6G—C1G	121.6 (2)
O3W—K3—O1	73.89 (10)	C5G—C6G—H6G	119.2
O5—K3—C1B	114.60 (6)	C1G—C6G—H6G	119.2
O3—K3—C1B	153.87 (7)	C2H—C1H—C6H	116.3 (3)
O2W—K3—C1B	85.51 (9)	C2H—C1H—Si3	120.9 (2)
O3W—K3—C1B	103.23 (11)	C6H—C1H—Si3	122.7 (2)
O1—K3—C1B	54.70 (6)	C2H—C1H—K5	85.75 (18)
O5—K3—C6B	97.66 (7)	C6H—C1H—K5	98.6 (2)
O3—K3—C6B	160.39 (7)	Si3—C1H—K5	81.52 (10)
O2W—K3—C6B	110.73 (9)	C1H—C2H—C3H	122.3 (3)
O3W—K3—C6B	128.56 (11)	C1H—C2H—K5	70.18 (17)
O1—K3—C6B	70.96 (6)	C3H—C2H—K5	107.9 (2)
C1B—K3—C6B	25.37 (7)	C1H—C2H—H2H	118.8
O5—K3—C2B	137.91 (7)	C3H—C2H—H2H	118.8
O3—K3—C2B	130.51 (7)	K5—C2H—H2H	91.9
O2W—K3—C2B	77.42 (9)	C4H—C3H—C2H	119.9 (3)
O3W—K3—C2B	90.57 (10)	C4H—C3H—H3H	120.1
O1—K3—C2B	68.30 (6)	C2H—C3H—H3H	120.1
C1B—K3—C2B	23.91 (6)	C3H—C4H—C5H	119.5 (4)
C6B—K3—C2B	41.73 (7)	C3H—C4H—H4H	120.2
O5—K3—C5B	102.09 (7)	C5H—C4H—H4H	120.2
O3—K3—C5B	137.48 (7)	C4H—C5H—C6H	120.3 (4)
O2W—K3—C5B	124.04 (9)	C4H—C5H—H5H	119.9
O3W—K3—C5B	136.33 (11)	C6H—C5H—H5H	119.9
O1—K3—C5B	93.78 (6)	C5H—C6H—C1H	121.7 (3)
C1B—K3—C5B	42.42 (7)	C5H—C6H—H6H	119.2
C6B—K3—C5B	23.24 (7)	C1H—C6H—H6H	119.2
C2B—K3—C5B	46.78 (7)	C6I—C1I—C2I	116.4 (2)
O5—K3—Si1	101.50 (5)	C6I—C1I—Si3	123.07 (18)
O3—K3—Si1	146.15 (6)	C2I—C1I—Si3	120.46 (16)
O2W—K3—Si1	67.97 (8)	C3I—C2I—C1I	121.9 (2)
O3W—K3—Si1	87.86 (10)	C3I—C2I—K61	110.74 (16)
O1—K3—Si1	24.22 (3)	C1I—C2I—K61	102.50 (14)
C1B—K3—Si1	30.55 (5)	C3I—C2I—K6	122.66 (15)
C6B—K3—Si1	48.32 (5)	C1I—C2I—K6	92.65 (13)
C2B—K3—Si1	47.17 (5)	C3I—C2I—H2I	119.1
C5B—K3—Si1	70.32 (5)	C1I—C2I—H2I	119.1
O5—K3—K6	87.26 (5)	K6—C2I—H2I	52.9
O3—K3—K6	41.10 (5)	C4I—C3I—C2I	120.1 (2)
O2W—K3—K6	48.63 (8)	C4I—C3I—H3I	120.0
O1—K3—K6	85.64 (5)	C2I—C3I—H3I	120.0
C1B—K3—K6	132.97 (6)	C5I—C4I—C3I	119.4 (2)
C6B—K3—K6	156.12 (6)	C5I—C4I—H4I	120.3
C2B—K3—K6	125.03 (6)	C3I—C4I—H4I	120.3
C5B—K3—K6	170.64 (6)	C4I—C5I—C6I	120.2 (2)
Si1—K3—K6	107.81 (4)	C4I—C5I—H5I	119.9
O5—K3—K5	47.92 (4)	C6I—C5I—H5I	119.9
O3—K3—K5	44.07 (4)	C5I—C6I—C1I	122.0 (2)
O2W—K3—K5	107.13 (8)	C5I—C6I—H6I	119.0
O3W—K3—K5	91.61 (9)	C1I—C6I—H6I	119.0
O1—K3—K5	122.03 (4)	Si4—O4—K21	122.85 (10)
C1B—K3—K5	161.96 (5)	Si4—O4—K4	144.33 (10)
C6B—K3—K5	139.04 (6)	K21—O4—K4	84.42 (6)
C2B—K3—K5	169.62 (5)	Si4—O4—K61	101.53 (9)
C5B—K3—K5	128.54 (6)	K21—O4—K61	93.22 (8)
Si1—K3—K5	143.07 (3)	K4—O4—K61	99.03 (6)
K6—K3—K5	58.53 (2)	Si4—O4—K2	113.55 (9)
O5—K3—H1W2	35.8	K4—O4—K2	87.09 (6)
O3—K3—H1W2	78.1	Si4—O4—K6	111.46 (9)
O2W—K3—H1W2	86.0	K4—O4—K6	95.60 (6)
O3W—K3—H1W2	84.4	K2—O4—K6	92.19 (7)
O1—K3—H1W2	73.6	O4—Si4—C1K	112.72 (11)
C1B—K3—H1W2	121.6	O4—Si4—C1J	113.20 (10)
C6B—K3—H1W2	118.9	C1K—Si4—C1J	108.19 (12)
C2B—K3—H1W2	141.4	O4—Si4—C1L	110.44 (11)
C5B—K3—H1W2	132.9	C1K—Si4—C1L	108.80 (12)
Si1—K3—H1W2	94.4	C1J—Si4—C1L	102.98 (12)
K6—K3—H1W2	55.8	O4—Si4—K61	51.02 (7)
K5—K3—H1W2	48.9	C1K—Si4—K61	114.00 (9)
O5—K3—H2W1	114.2	C1J—Si4—K61	137.77 (10)
O3—K3—H2W1	95.1	C1L—Si4—K61	61.95 (9)
O2W—K3—H2W1	18.0	O4—Si4—K21	35.51 (8)
O1—K3—H2W1	37.3	C1K—Si4—K21	143.23 (9)
C1B—K3—H2W1	72.9	C1J—Si4—K21	82.43 (9)
C6B—K3—H2W1	96.9	C1L—Si4—K21	102.48 (9)
C2B—K3—H2W1	71.2	K61—Si4—K21	65.05 (5)
C5B—K3—H2W1	114.7	O4—Si4—K6	44.96 (7)
Si1—K3—H2W1	51.1	C1K—Si4—K6	123.94 (8)
K6—K3—H2W1	60.1	C1J—Si4—K6	127.73 (9)
K5—K3—H2W1	116.0	C1L—Si4—K6	65.70 (9)
H1W2—K3—H2W1	82.3	O4—Si4—K2	43.24 (7)
O5—K3—H2W2	136.2	C1K—Si4—K2	140.94 (9)
O3—K3—H2W2	79.9	C1J—Si4—K2	71.90 (9)
O2W—K3—H2W2	14.9	C1L—Si4—K2	109.08 (9)
O1—K3—H2W2	62.4	K6—Si4—K2	65.75 (3)
C1B—K3—H2W2	79.5	C2J—C1J—C6J	116.3 (3)
C6B—K3—H2W2	104.6	C2J—C1J—Si4	122.46 (19)
C2B—K3—H2W2	66.7	C6J—C1J—Si4	121.2 (2)
C5B—K3—H2W2	113.2	C1J—C2J—C3J	122.0 (3)
Si1—K3—H2W2	69.0	C1J—C2J—K2	97.37 (17)
K6—K3—H2W2	58.3	C3J—C2J—K2	116.0 (2)
K5—K3—H2W2	115.8	C1J—C2J—H2J	119.0
H1W2—K3—H2W2	100.7	C3J—C2J—H2J	119.0
H2W1—K3—H2W2	26.9	K2—C2J—H2J	54.3
O5—K3—H3W2	118.0	C4J—C3J—C2J	120.3 (3)
O3—K3—H3W2	44.2	C4J—C3J—H3J	119.8
O3W—K3—H3W2	15.4	C2J—C3J—H3J	119.8
O1—K3—H3W2	89.1	C3J—C4J—C5J	119.3 (3)
C1B—K3—H3W2	115.2	C3J—C4J—H4J	120.3
C6B—K3—H3W2	139.7	C5J—C4J—H4J	120.3
C2B—K3—H3W2	98.7	C4J—C5J—C6J	119.9 (4)
C5B—K3—H3W2	139.7	C4J—C5J—H5J	120.0
Si1—K3—H3W2	103.0	C6J—C5J—H5J	120.0
K5—K3—H3W2	81.3	C5J—C6J—C1J	121.9 (4)
H1W2—K3—H3W2	86.3	C5J—C6J—H6J	119.0
O2—K4—O4	90.99 (6)	C1J—C6J—H6J	119.0
O2—K4—O1W	81.22 (6)	C6K—C1K—C2K	117.3 (3)
O4—K4—O1W	85.34 (7)	C6K—C1K—Si4	120.1 (2)
O2—K4—C1S	151.41 (6)	C2K—C1K—Si4	122.6 (2)
O4—K4—C1S	111.78 (6)	C3K—C2K—C1K	121.4 (3)
O1W—K4—C1S	83.58 (6)	C3K—C2K—H2K	119.3
O2—K4—C2S	159.70 (6)	C1K—C2K—H2K	119.3
O4—K4—C2S	107.49 (6)	C2K—C3K—C4K	119.0 (4)
O1W—K4—C2S	107.99 (6)	C2K—C3K—H3K	120.5
C1S—K4—C2S	25.04 (6)	C4K—C3K—H3K	120.5
O2—K4—C2F	70.88 (6)	C5K—C4K—C3K	120.6 (3)
O4—K4—C2F	90.70 (6)	C5K—C4K—H4K	119.7
O1W—K4—C2F	151.75 (6)	C3K—C4K—H4K	119.7
C1S—K4—C2F	123.50 (6)	C6K—C5K—C4K	118.9 (4)
C2S—K4—C2F	99.88 (6)	C6K—C5K—H5K	120.6
O2—K4—C6S	126.80 (6)	C4K—C5K—H5K	120.6
O4—K4—C6S	133.97 (6)	C5K—C6K—C1K	122.8 (4)
O1W—K4—C6S	77.07 (7)	C5K—C6K—H6K	118.6
C1S—K4—C6S	25.09 (6)	C1K—C6K—H6K	118.6
C2S—K4—C6S	43.00 (7)	C6L—C1L—C2L	114.4 (3)
C2F—K4—C6S	123.43 (7)	C6L—C1L—Si4	126.7 (2)
O2—K4—C3S	136.57 (6)	C2L—C1L—Si4	118.7 (3)
O4—K4—C3S	121.86 (7)	C6L—C1L—K61	94.3 (2)
O1W—K4—C3S	125.07 (7)	C2L—C1L—K61	87.0 (3)
C1S—K4—C3S	43.42 (6)	Si4—C1L—K61	83.90 (9)
C2S—K4—C3S	24.17 (6)	C6L—C1L—K6	104.0 (2)
C2F—K4—C3S	80.38 (6)	C2L—C1L—K6	77.1 (3)
C6S—K4—C3S	49.13 (7)	Si4—C1L—K6	83.48 (9)
O2—K4—C5S	113.90 (6)	C3L—C2L—C1L	123.7 (5)
O4—K4—C5S	154.65 (6)	C3L—C2L—K61	104.8 (5)
O1W—K4—C5S	93.48 (7)	C1L—C2L—K61	67.6 (3)
C1S—K4—C5S	43.13 (6)	C3L—C2L—K6	103.9 (5)
C2S—K4—C5S	48.90 (7)	C1L—C2L—K6	79.1 (3)
C2F—K4—C5S	101.61 (7)	C3L—C2L—H2L	118.1
C6S—K4—C5S	23.86 (6)	C1L—C2L—H2L	118.1
C3S—K4—C5S	41.15 (7)	K6—C2L—H2L	86.9
O2—K4—K21	50.10 (5)	C4L—C3L—C2L	119.5 (4)
O4—K4—K21	46.32 (5)	C4L—C3L—H3L	120.2
O1W—K4—K21	62.48 (7)	C2L—C3L—H3L	120.2
C1S—K4—K21	138.30 (7)	C3L—C4L—C5L	119.2 (4)
C2S—K4—K21	150.19 (6)	C3L—C4L—H4L	120.4
C2F—K4—K21	95.02 (7)	C5L—C4L—H4L	120.4
C6S—K4—K21	139.54 (7)	C4L—C5L—C6L	120.9 (4)
C3S—K4—K21	167.63 (6)	C4L—C5L—H5L	119.6
C5S—K4—K21	151.00 (6)	C6L—C5L—H5L	119.6
O2—K4—C1F	54.47 (5)	C1L—C6L—C5L	122.3 (3)
O4—K4—C1F	106.79 (6)	C1L—C6L—K61	62.08 (17)
O1W—K4—C1F	133.43 (6)	C5L—C6L—K61	104.2 (3)
C1S—K4—C1F	128.21 (6)	C1L—C6L—H6L	118.9
C2S—K4—C1F	110.41 (6)	C5L—C6L—H6L	118.9
C2F—K4—C1F	23.87 (6)	K61—C6L—H6L	103.4
C6S—K4—C1F	116.26 (6)	Si5—O5—K3	135.73 (10)
C3S—K4—C1F	86.93 (6)	Si5—O5—K5	105.24 (8)
C5S—K4—C1F	92.39 (6)	K3—O5—K5	89.72 (5)
K21—K4—C1F	93.44 (6)	Si5—O5—K1	110.26 (9)
O2—K4—C4S	117.99 (6)	K3—O5—K1	89.00 (6)
O4—K4—C4S	144.99 (7)	K5—O5—K1	129.61 (7)
O1W—K4—C4S	116.45 (7)	O5—Si5—C1OO	115.56 (15)
C1S—K4—C4S	49.89 (6)	O5—Si5—C3NN	119.22 (14)
C2S—K4—C4S	41.77 (6)	O5—Si5—C1M	114.01 (14)
C2F—K4—C4S	81.74 (7)	O5—Si5—C1MM	107.47 (13)
C6S—K4—C4S	41.71 (6)	O5—Si5—C1N	105.94 (12)
C3S—K4—C4S	23.19 (7)	O5—Si5—C1O	107.55 (12)
C5S—K4—C4S	23.19 (7)	O5—Si5—K5	49.81 (7)
K21—K4—C4S	167.78 (6)	C1OO—Si5—K5	143.42 (13)
C1F—K4—C4S	78.80 (6)	C3NN—Si5—K5	131.74 (12)
O2—K4—H1W1	98.7	C1M—Si5—K5	64.88 (12)
O4—K4—H1W1	84.6	C1MM—Si5—K5	58.88 (11)
O1W—K4—H1W1	17.5	C1N—Si5—K5	105.53 (10)
C1S—K4—H1W1	67.9	C1O—Si5—K5	124.36 (9)
C2S—K4—H1W1	91.5	O5—Si5—K1	47.30 (7)
C2F—K4—H1W1	168.6	C1OO—Si5—K1	68.36 (12)
C6S—K4—H1W1	66.4	C3NN—Si5—K1	112.52 (11)
C3S—K4—H1W1	110.9	C1M—Si5—K1	137.65 (13)
C5S—K4—H1W1	86.8	C1MM—Si5—K1	131.44 (10)
K21—K4—H1W1	74.2	C1N—Si5—K1	122.16 (11)
C1F—K4—H1W1	150.0	C1O—Si5—K1	63.88 (10)
C4S—K4—H1W1	108.0	K5—Si5—K1	90.82 (3)
O6—K5—O3	86.65 (6)	O5—Si5—K3	27.79 (7)
O6—K5—O5	101.34 (6)	C1OO—Si5—K3	123.86 (12)
O3—K5—O5	85.37 (5)	C3NN—Si5—K3	92.33 (12)
O6—K5—C2M	143.46 (7)	C1M—Si5—K3	123.04 (12)
O3—K5—C2M	127.65 (7)	C1MM—Si5—K3	118.58 (12)
O5—K5—C2M	73.16 (9)	C1N—Si5—K3	78.45 (10)
O6—K5—C6MM	97.75 (7)	C1O—Si5—K3	125.02 (10)
O3—K5—C6MM	154.05 (7)	K5—Si5—K3	61.71 (2)
O5—K5—C6MM	68.69 (7)	K1—Si5—K3	61.36 (2)
O6—K5—C1MM	121.04 (8)	C2M—C1M—C6M	120.0
O3—K5—C1MM	134.86 (6)	C2M—C1M—Si5	117.3 (2)
O5—K5—C1MM	56.48 (6)	C6M—C1M—Si5	122.5 (2)
C6MM—K5—C1MM	25.9	C2M—C1M—K5	67.14 (17)
O6—K5—C1H	118.56 (6)	C6M—C1M—K5	113.62 (18)
O3—K5—C1H	56.87 (6)	Si5—C1M—K5	83.68 (13)
O5—K5—C1H	120.04 (6)	C3M—C2M—C1M	120.0
C2M—K5—C1H	93.79 (8)	C3M—C2M—K5	103.92 (18)
C6MM—K5—C1H	137.26 (7)	C1M—C2M—K5	88.07 (18)
C1MM—K5—C1H	119.45 (9)	C3M—C2M—H2M	120.0
O6—K5—O1W	51.46 (5)	C1M—C2M—H2M	120.0
O3—K5—O1W	77.69 (6)	K5—C2M—H2M	78.1
O5—K5—O1W	50.40 (5)	C2M—C3M—C4M	120.0
C2M—K5—O1W	117.20 (9)	C2M—C3M—H3M	120.0
C6MM—K5—O1W	85.11 (7)	C4M—C3M—H3M	120.0
C1MM—K5—O1W	92.32 (8)	C5M—C4M—C3M	120.0
C1H—K5—O1W	134.55 (6)	C5M—C4M—H4M	120.0
O6—K5—C1M	123.23 (8)	C3M—C4M—H4M	120.0
O3—K5—C1M	133.20 (6)	C4M—C5M—C6M	120.0
O5—K5—C1M	56.17 (6)	C4M—C5M—H5M	120.0
C2M—K5—C1M	24.8	C6M—C5M—H5M	120.0
C1H—K5—C1M	117.42 (9)	C5M—C6M—C1M	120.0
O1W—K5—C1M	93.42 (8)	C5M—C6M—H6M	120.0
O6—K5—C2H	142.35 (6)	C1M—C6M—H6M	120.0
O3—K5—C2H	67.00 (7)	C2MM—C1MM—C6MM	120.0
O5—K5—C2H	102.70 (7)	C2MM—C1MM—Si5	122.49 (19)
C2M—K5—C2H	72.03 (8)	C6MM—C1MM—Si5	117.43 (19)
C6MM—K5—C2H	117.85 (7)	C2MM—C1MM—K5	101.60 (14)
C1MM—K5—C2H	96.43 (9)	C6MM—C1MM—K5	75.78 (12)
C1H—K5—C2H	24.06 (7)	Si5—C1MM—K5	89.11 (12)
O1W—K5—C2H	137.77 (7)	C3MM—C2MM—C1MM	120.0
C1M—K5—C2H	94.28 (9)	C3MM—C2MM—H2MM	120.0
O6—K5—Si3	95.99 (4)	C1MM—C2MM—H2MM	120.0
O3—K5—Si3	26.10 (4)	C4MM—C3MM—C2MM	120.0
O5—K5—Si3	107.27 (4)	C4MM—C3MM—H3MM	120.0
C2M—K5—Si3	120.34 (6)	C2MM—C3MM—H3MM	120.0
C6MM—K5—Si3	166.20 (6)	C3MM—C4MM—C5MM	120.0
C1MM—K5—Si3	140.80 (6)	C3MM—C4MM—H4MM	120.0
C1H—K5—Si3	32.46 (5)	C5MM—C4MM—H4MM	120.0
O1W—K5—Si3	102.58 (5)	C6MM—C5MM—C4MM	120.0
C1M—K5—Si3	138.53 (7)	C6MM—C5MM—H5MM	120.0
C2H—K5—Si3	49.14 (5)	C4MM—C5MM—H5MM	120.0
O6—K5—C6R	63.79 (6)	C5MM—C6MM—C1MM	120.0
O3—K5—C6R	125.38 (6)	C5MM—C6MM—K5	100.40 (15)
O5—K5—C6R	142.07 (6)	C1MM—C6MM—K5	78.30 (13)
C2M—K5—C6R	97.90 (9)	C5MM—C6MM—H6MM	120.0
C6MM—K5—C6R	78.64 (7)	C1MM—C6MM—H6MM	120.0
C1MM—K5—C6R	99.56 (6)	K5—C6MM—H6MM	91.3
C1H—K5—C6R	96.92 (7)	C2N—C1N—C6N	120.0
O1W—K5—C6R	109.65 (6)	C2N—C1N—Si5	120.85 (18)
C1M—K5—C6R	101.04 (7)	C6N—C1N—Si5	118.80 (18)
C2H—K5—C6R	109.44 (8)	C3N—C2N—C1N	120.0
Si3—K5—C6R	108.83 (5)	C3N—C2N—H2N	120.0
O6—K5—H1W1	37.7	C1N—C2N—H2N	120.0
O3—K5—H1W1	81.5	C4N—C3N—C2N	120.0
O5—K5—H1W1	63.8	C4N—C3N—H3N	120.0
C2M—K5—H1W1	125.4	C2N—C3N—H3N	120.0
C6MM—K5—H1W1	86.5	C3N—C4N—C5N	120.0
C1MM—K5—H1W1	99.2	C3N—C4N—H4N	120.0
C1H—K5—H1W1	136.1	C5N—C4N—H4N	120.0
O1W—K5—H1W1	14.0	C6N—C5N—C4N	120.0
C1M—K5—H1W1	100.7	C6N—C5N—H5N	120.0
C2H—K5—H1W1	147.1	C4N—C5N—H5N	120.0
Si3—K5—H1W1	103.8	C5N—C6N—C1N	120.0
C6R—K5—H1W1	96.3	C5N—C6N—H6N	120.0
O6—K5—H1W2	65.8	C1N—C6N—H6N	120.0
O3—K5—H1W2	79.5	C2NN—C1NN—C6NN	120.0
O5—K5—H1W2	35.8	C1NN—C2NN—C3NN	120.0
C2M—K5—H1W2	104.4	C1NN—C2NN—H2NN	120.0
C6MM—K5—H1W2	79.1	C3NN—C2NN—H2NN	120.0
C1MM—K5—H1W2	81.1	C4NN—C3NN—C2NN	120.0
C1H—K5—H1W2	134.5	C4NN—C3NN—Si5	119.8 (2)
O1W—K5—H1W2	14.6	C2NN—C3NN—Si5	119.7 (2)
C1M—K5—H1W2	81.9	C4NN—C3NN—H3NN	120.0
C2H—K5—H1W2	129.6	C2NN—C3NN—H3NN	120.0
Si3—K5—H1W2	105.6	Si5—C3NN—H3NN	7.3
C6R—K5—H1W2	120.6	C5NN—C4NN—C3NN	120.0
H1W1—K5—H1W2	28.1	C5NN—C4NN—H4NN	120.0
O3—K6—O6	87.90 (7)	C3NN—C4NN—H4NN	120.0
O3—K6—O4	161.31 (10)	C6NN—C5NN—C4NN	120.0
O6—K6—O4	97.53 (6)	C6NN—C5NN—H5NN	120.0
O3—K6—O1W	88.39 (8)	C4NN—C5NN—H5NN	120.0
O6—K6—O1W	55.94 (6)	C5NN—C6NN—C1NN	120.0
O4—K6—O1W	80.06 (6)	C5NN—C6NN—H6NN	120.0
O3—K6—O2W	77.08 (10)	C1NN—C6NN—H6NN	120.0
O6—K6—O2W	138.29 (10)	C2O—C1O—C6O	120.0
O4—K6—O2W	87.18 (8)	C2O—C1O—Si5	117.87 (17)
O1W—K6—O2W	84.59 (9)	C6O—C1O—Si5	121.99 (17)
O3—K6—C2L	115.48 (9)	C2O—C1O—K1	63.39 (13)
O6—K6—C2L	147.58 (11)	C6O—C1O—K1	125.53 (14)
O4—K6—C2L	67.77 (10)	Si5—C1O—K1	84.18 (10)
O1W—K6—C2L	140.52 (11)	C1O—C2O—C3O	120.0
O2W—K6—C2L	71.96 (11)	C1O—C2O—K1	93.46 (14)
O3—K6—C1L	135.04 (7)	C3O—C2O—K1	111.63 (15)
O6—K6—C1L	124.48 (9)	C1O—C2O—H2O	120.0
O4—K6—C1L	54.31 (6)	C3O—C2O—H2O	120.0
O1W—K6—C1L	134.36 (7)	K1—C2O—H2O	64.6
O2W—K6—C1L	91.74 (9)	C2O—C3O—C4O	120.0
C2L—K6—C1L	23.77 (8)	C2O—C3O—H3O	120.0
O3—K6—C2I	66.86 (6)	C4O—C3O—H3O	120.0
O6—K6—C2I	72.68 (6)	C5O—C4O—C3O	120.0
O4—K6—C2I	131.83 (9)	C5O—C4O—H4O	120.0
O1W—K6—C2I	123.71 (6)	C3O—C4O—H4O	120.0
O2W—K6—C2I	131.70 (9)	C4O—C5O—C6O	120.0
C2L—K6—C2I	95.25 (11)	C4O—C5O—H5O	120.0
C1L—K6—C2I	91.91 (8)	C6O—C5O—H5O	120.0
O3—K6—Si3	21.44 (4)	C5O—C6O—C1O	120.0
O6—K6—Si3	90.39 (5)	C5O—C6O—H6O	120.0
O4—K6—Si3	171.41 (5)	C1O—C6O—H6O	120.0
O1W—K6—Si3	107.31 (7)	C2OO—C1OO—C6OO	120.0
O2W—K6—Si3	89.13 (9)	C2OO—C1OO—Si5	120.0 (2)
C2L—K6—Si3	103.70 (9)	C6OO—C1OO—Si5	119.7 (2)
C1L—K6—Si3	118.12 (6)	C1OO—C2OO—C3OO	120.0
C2I—K6—Si3	47.78 (4)	C1OO—C2OO—K1	105.17 (17)
O3—K6—Si4	162.05 (6)	C3OO—C2OO—K1	105.70 (19)
O6—K6—Si4	109.84 (6)	C1OO—C2OO—H2OO	120.0
O4—K6—Si4	23.58 (4)	C3OO—C2OO—H2OO	120.0
O1W—K6—Si4	103.61 (5)	K1—C2OO—H2OO	57.8
O2W—K6—Si4	90.63 (7)	C4OO—C3OO—C2OO	120.0
C2L—K6—Si4	47.29 (8)	C4OO—C3OO—H3OO	120.0
C1L—K6—Si4	30.81 (5)	C2OO—C3OO—H3OO	120.0
C2I—K6—Si4	114.84 (7)	C3OO—C4OO—C5OO	120.0
Si3—K6—Si4	148.91 (4)	C3OO—C4OO—H4OO	120.0
O3—K6—K5	45.63 (5)	C5OO—C4OO—H4OO	120.0
O6—K6—K5	43.92 (4)	C6OO—C5OO—C4OO	120.0
O4—K6—K5	132.72 (5)	C6OO—C5OO—H5OO	120.0
O1W—K6—K5	56.86 (5)	C4OO—C5OO—H5OO	120.0
O2W—K6—K5	105.41 (9)	C5OO—C6OO—C1OO	120.0
C2L—K6—K5	159.50 (9)	C5OO—C6OO—H6OO	120.0
C1L—K6—K5	161.17 (8)	C1OO—C6OO—H6OO	120.0
C2I—K6—K5	70.97 (4)	Si6—O6—K61	124.17 (10)
Si3—K6—K5	55.81 (3)	Si6—O6—K5	127.40 (9)
Si4—K6—K5	152.22 (4)	K61—O6—K5	102.76 (7)
O3—K6—K3	43.86 (5)	Si6—O6—K6	139.78 (10)
O6—K6—K3	99.55 (6)	K5—O6—K6	89.98 (6)
O4—K6—K3	117.46 (7)	O6—Si6—C1R	111.85 (11)
O1W—K6—K3	62.35 (6)	O6—Si6—C1P	111.98 (9)
O2W—K6—K3	44.22 (8)	C1R—Si6—C1P	107.09 (10)
C2L—K6—K3	112.87 (8)	O6—Si6—C1S	109.94 (9)
C1L—K6—K3	135.17 (7)	C1R—Si6—C1S	107.02 (10)
C2I—K6—K3	110.69 (6)	C1P—Si6—C1S	108.76 (10)
Si3—K6—K3	64.07 (4)	O6—Si6—K61	35.27 (7)
Si4—K6—K3	131.14 (5)	C1R—Si6—K61	138.21 (9)
K5—K6—K3	61.22 (4)	C1P—Si6—K61	79.72 (8)
O3—K6—H1W1	89.5	C1S—Si6—K61	109.43 (7)
O6—K6—H1W1	39.0	O6—Si6—K5	33.17 (6)
O4—K6—H1W1	83.7	C1R—Si6—K5	78.73 (9)
O1W—K6—H1W1	17.0	C1P—Si6—K5	126.38 (7)
O2W—K6—H1W1	101.4	C1S—Si6—K5	120.46 (8)
C2L—K6—H1W1	150.8	K61—Si6—K5	65.59 (4)
C1L—K6—H1W1	135.4	C2P—C1P—C6P	116.6 (2)
C2I—K6—H1W1	109.1	C2P—C1P—Si6	120.62 (17)
Si3—K6—H1W1	104.6	C6P—C1P—Si6	122.76 (18)
Si4—K6—H1W1	105.9	C3P—C2P—C1P	122.2 (2)
K5—K6—H1W1	49.4	C3P—C2P—K61	123.31 (15)
K3—K6—H1W1	74.0	C1P—C2P—K61	93.34 (14)
O6—K61—O4	103.41 (7)	C3P—C2P—H2P	118.9
O6—K61—O3W	122.57 (13)	C1P—C2P—H2P	118.9
O4—K61—O3W	86.32 (11)	K61—C2P—H2P	51.1
O6—K61—C1L	149.43 (11)	C4P—C3P—C2P	119.7 (2)
O4—K61—C1L	60.59 (7)	C4P—C3P—H3P	120.1
O3W—K61—C1L	84.30 (11)	C2P—C3P—H3P	120.1
O6—K61—O3	79.88 (7)	C5P—C4P—C3P	119.6 (2)
O4—K61—O3	134.01 (11)	C5P—C4P—H4P	120.2
O3W—K61—O3	56.51 (11)	C3P—C4P—H4P	120.2
C1L—K61—O3	130.41 (8)	C4P—C5P—C6P	120.1 (2)
O6—K61—C2I	79.64 (7)	C4P—C5P—H5P	119.9
O4—K61—C2I	159.67 (12)	C6P—C5P—H5P	119.9
O3W—K61—C2I	109.24 (12)	C5P—C6P—C1P	121.7 (2)
C1L—K61—C2I	106.79 (9)	C5P—C6P—H6P	119.2
O3—K61—C2I	66.25 (6)	C1P—C6P—H6P	119.2
O6—K61—C2L	173.99 (11)	C2R—C1R—C6R	117.4 (2)
O4—K61—C2L	71.17 (10)	C2R—C1R—Si6	122.83 (19)
O3W—K61—C2L	60.56 (12)	C6R—C1R—Si6	119.8 (2)
C1L—K61—C2L	25.43 (9)	C3R—C2R—C1R	121.2 (3)
O3—K61—C2L	105.71 (10)	C3R—C2R—H2R	119.4
C2I—K61—C2L	104.50 (11)	C1R—C2R—H2R	119.4
O6—K61—O1W	51.15 (6)	C4R—C3R—C2R	120.0 (3)
O4—K61—O1W	74.49 (7)	C4R—C3R—H3R	120.0
O3W—K61—O1W	79.36 (11)	C2R—C3R—H3R	120.0
C1L—K61—O1W	132.95 (8)	C5R—C4R—C3R	120.1 (3)
O3—K61—O1W	72.88 (7)	C5R—C4R—H4R	120.0
C2I—K61—O1W	120.24 (7)	C3R—C4R—H4R	120.0
C2L—K61—O1W	127.81 (11)	C4R—C5R—C6R	120.0 (3)
O6—K61—Si4	123.03 (6)	C4R—C5R—H5R	120.0
O4—K61—Si4	27.46 (4)	C6R—C5R—H5R	120.0
O3W—K61—Si4	90.51 (10)	C5R—C6R—C1R	121.3 (3)
C1L—K61—Si4	34.15 (5)	C5R—C6R—K5	119.9 (2)
O3—K61—Si4	146.99 (8)	C1R—C6R—K5	94.57 (17)
C2I—K61—Si4	135.60 (9)	C5R—C6R—H6R	119.3
C2L—K61—Si4	50.97 (9)	C1R—C6R—H6R	119.3
O1W—K61—Si4	101.93 (6)	K5—C6R—H6R	53.9
O6—K61—C6L	136.67 (11)	C2S—C1S—C6S	117.0 (2)
O4—K61—C6L	78.74 (8)	C2S—C1S—Si6	124.59 (18)
O3W—K61—C6L	100.75 (11)	C6S—C1S—Si6	118.22 (18)
C1L—K61—C6L	23.61 (7)	C2S—C1S—K4	79.67 (12)
O3—K61—C6L	129.73 (7)	C6S—C1S—K4	80.85 (13)
C2I—K61—C6L	85.36 (8)	Si6—C1S—K4	104.38 (8)
C2L—K61—C6L	40.81 (9)	C3S—C2S—C1S	121.7 (2)
O1W—K61—C6L	153.18 (7)	C3S—C2S—K4	83.17 (14)
Si4—K61—C6L	51.35 (6)	C1S—C2S—K4	75.29 (12)
O6—K61—C2P	66.69 (7)	C3S—C2S—H2S	119.2
O4—K61—C2P	84.51 (8)	C1S—C2S—H2S	119.2
O3W—K61—C2P	168.43 (11)	K4—C2S—H2S	112.5
C1L—K61—C2P	85.06 (9)	C4S—C3S—C2S	120.2 (3)
O3—K61—C2P	134.89 (7)	C4S—C3S—K4	82.08 (15)
C2I—K61—C2P	78.25 (8)	C2S—C3S—K4	72.67 (13)
C2L—K61—C2P	109.56 (10)	C4S—C3S—H3S	119.9
O1W—K61—C2P	104.86 (6)	C2S—C3S—H3S	119.9
Si4—K61—C2P	78.12 (7)	K4—C3S—H3S	115.9
C6L—K61—C2P	70.54 (8)	C3S—C4S—C5S	119.8 (2)
O6—K61—Si6	20.56 (4)	C3S—C4S—K4	74.73 (14)
O4—K61—Si6	97.28 (6)	C5S—C4S—K4	76.83 (15)
O3W—K61—Si6	142.60 (11)	C3S—C4S—H4S	120.1
C1L—K61—Si6	129.72 (9)	C5S—C4S—H4S	120.1
O3—K61—Si6	98.14 (5)	K4—C4S—H4S	119.3
C2I—K61—Si6	78.49 (5)	C4S—C5S—C6S	120.0 (3)
C2L—K61—Si6	155.10 (11)	C4S—C5S—K4	79.98 (16)
O1W—K61—Si6	66.07 (4)	C6S—C5S—K4	71.99 (14)
Si4—K61—Si6	109.60 (5)	C4S—C5S—H5S	120.0
C6L—K61—Si6	116.51 (9)	C6S—C5S—H5S	120.0
C2P—K61—Si6	46.17 (5)	K4—C5S—H5S	118.9
O6—K61—H1W1	37.2	C5S—C6S—C1S	121.4 (2)
O4—K61—H1W1	80.8	C5S—C6S—K4	84.15 (15)
O3W—K61—H1W1	92.2	C1S—C6S—K4	74.06 (12)
C1L—K61—H1W1	141.4	C5S—C6S—H6S	119.3
O3—K61—H1W1	75.3	C1S—C6S—H6S	119.3
C2I—K61—H1W1	110.6	K4—C6S—H6S	112.6

Hydrogen-bond geometry (Å, º)

D—H···A	D—H	H···A	D···A	D—H···A
O1W—H1W1···O6	0.84	1.79	2.616 (3)	168
O1W—H1W2···O5	0.84	1.80	2.635 (3)	172
O2W^g—H2^W^1g···O1	0.84	1.80	2.630 (4)	171
O3W^h—H3^W^2h···O3	0.84	1.97	2.775 (5)	160