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5'-azido-5'-deoxy-3'-O-acetylthymidine (C12H15N5O5) is orthorhombic. The crystal data for the primitive space lattice are a = 5.584 (1), b = 14.347 (4), c = 18.021 (4) Å, Dm= 1.41 (1), Dx = 1.422 Mg m-3 and Z = 4. The quantitative figure of merit (FN) is F30 = 96 (0.006, 52). Indexed X-ray powder data are reported.
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