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Search query: GISAXS/GIWAXS

41 articles match your search "GISAXS/GIWAXS"

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INSIGHT is a Python-based software tool for reducing and batch processing large grazing-incidence wide- and small-angle X-ray scattering data sets and extracting structural, orientational and morphological information on thin films.

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A description of a flexible sample cell for time-resolved grazing-incidence X-ray scattering and X-ray reflectivity measurements is presented. The cell is especially designed for studying drying kinetics, solvent vapor annealing and hydration processes.

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Advanced grazing-incidence techniques have developed significantly during recent years. With the ongoing progress in instrumentation, novel methods have emerged which allow for an in-depth morphology characterization of modern soft-matter materials. Examples are in situ and in operando grazing-incidence small-angle X-ray scattering (GISAXS), micro- and nanofocused GISAXS, time-of-flight (TOF) grazing-incidence small-angle neutron scattering (GISANS) and surface-sensitive resonant soft X-ray scattering techniques, including the potential to investigate polarization. Progress in software for data analysis is another important aspect.

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The program SUNBIM, here presented, is a novel suite of programs designed for scientists who make use of small- and wide-angle X-ray scattering (SAXS/WAXS) and grazing-incidence SAXS/WAXS (GISAXS/GIWAXS) techniques for the structural characterization of artificial or natural materials. It consists of four sections: (1) Calibration; (2) Batch Script & 2D Mesh Composite; (3) multi-scan SAXS and WAXS data analysis (M-SAWANA); (4) single-scan SAXS and WAXS data analysis (S-SAWANA).

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Combined 100 ms-resolved grazing-incidence small/wide-angle X-ray scattering and optical interferometry reveal that the additive diiodooctane can double the solvent evaporation rate, thereby effectively suppressing the rapid spinodal decomposition process in the early stage of spin-coating, favouring slow phase segregation kinetics with nucleation and growth.

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The design and performance of a novel micro-reactor in situ flow cell permitting investigation of model catalysts with grazing-incidence small- and wide-angle X-ray scattering is presented.

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The main characteristics of the beamline SIRIUS at Synchrotron SOLEIL relevant for soft matter science are presented, as well as recent developments of new sample environments and of X-ray focusing with compound refractive lenses.

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The status, opportunities, challenges and limitations of machine learning are discussed as applied to X-ray and neutron scattering techniques, with an emphasis on surface scattering.

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This work describes the application of X-ray ptychography for the inspection of complex assemblies of CdSe/CdS octapod nanocrystals embedded in 24 ± 4 µm-thick polymethyl methacrylate and polystyrene matrices.

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A computational method that directly translates the scattering peak information to crystalline domain shapes and orientations is presented. The method is demonstrated at a synchrotron beamline with a standard X-ray scattering setup.
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