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7 citations found for Seo, D
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Ferredoxin-NADP+ oxidoreductase from B. subtilis has been crystallized by the sitting-drop vapour-diffusion method. Diffraction data were collected to 1.8 Å resolution.
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Ferredoxin-NAD(P)+ reductase from C. tepidum has been overexpressed in E. coli, purified and crystallized. Diffraction data were collected to 2.4 Å resolution.
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The structure of the title compound, [Li(BF4)(CH3CN)]n, consists of a layered arrangement parallel to (100) in which the Li+ cations are coordinated by three F atoms from three tetrafluoridoborate (BF4−) anions and an N atom from an acetonitrile molecule. The BF4− anion is coordinated to three different Li+ cations though three F atoms. The structure can be described as being built from vertex-shared BF4 and LiF3(NCCH3) tetrahedra. These tetrahedra reside around a crystallographic inversion center and form 8-membered rings.
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In the title compound, [Li(CH3CN)4]PF6·CH3CN, the asymmetric unit consists of three independent tetrahedral [Li(CH3CN)4]+ cations, three uncoordinated PF6− anions and three uncoordinated CH3CN solvent molecules. The three anions are disordered over two sites through a rotation along one of the F—P—F axes. The relative occupancies of the two sites for the F atoms are 0.643 (16):0.357 (16), 0.677 (10):0.323 (10) and 0.723 (13):0.277 (13). The crystal used was a racemic twin, with approximately equal twin components.
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In the title compound, [Li2(CF3SO2NSO2CF3)2(CH3CN)2]n, two Li+ cations reside on crystallographic inversion centers, each coordinated by six O atoms from bis(trifluoromethanesulfonyl)imide (TFSI−) anions. The third Li+ cation on a general position is four-coordinated by two anion O atoms and two N atoms from acetonitrile molecules in a tetrahedral geometry.
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