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106 citations found for Jones, D.
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The beneficial engineered single-amino-acid deletion variants EGFPD190Δ and EGFPA227Δ have been studied.
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In the crystal structure of the title compound, C11H10N2O3, inversion-related molecules are connected by pairs of O—H
O hydrogen bonds. With the exception of the atoms in the carboxylic acid group, the non-H atoms are roughly coplanar with a maximum deviation from the mean plane of 0.270 (1) Å for the C atom to which the carboxylic group is attached. The C atom of the carboxylic group lies 1.730 (2) Å from the mean plane.
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The title compound, C44H60Si, was prepared as an internal standard for diffusion-ordered NMR spectroscopy. The Si atom lies on a special position with
site symmetry.
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The title compound, [Ni(C15H19BCl3N6)2] or Ni(Tp*Cl)2, adds to the list of structurally characterized bis(trispyrazolyl)borate-nickel(II) complexes. The two facially coordinating N-donor Tp*Cl ligands impose pseudo-octahedral coordination on the nickel(II) center. The asymmetric unit consists of two half molecules, primarily differing in the torsion angles of the coordinated pyrazole rings relative to the central B-Ni-B axis of the molecules; each molecule is centrosymmetric. An average overall Ni-N distance of 2.104 (15) Å is observed, typical of octahedral NiN6 coordination spheres and this class of compound. The title compound readily forms good quality crystals, while its 4-H analog, Ni(Tp*)2, does not. This characteristic is attributed to close contacts between the pyrazole 4-chloro-substituents on adjacent molecules.
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The title compound, [PtCl2(C14H16)], contains a square-planar d8 platinum(II) center which is coordinated by two Cl atoms and the double bonds of a rigid polycyclic ligand containing a 1,4-cyclooctadiene subunit. This compound is an interesting substrate for additional mechanistic studies of catalytically active metal complexes.
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The title compound, C32H26Si, is a benzosilacyclopentene in which the silacyclopentene ring assumes an envelope conformation, with the Si atom displaced by 0.953 (2) Å from the mean plane of the four C atoms. The Si atom is bonded to two phenyl rings and to two Csp3 atoms in the silacyclopentene ring; one phenyl ring is attached to each of these two Csp3 atoms in the cis configuration.
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In the title compound, C20H21N3O2·H2O (EQR·H2O), the quinazoline ring system forms dihedral angles of 53.1 (1) and 85.6 (1)° with the phenyl ring and the amide link, respectively. In the crystal, O—H
O hydrogen bonds link two EQR and two water molecules into a centrosymmetric R44(18) ring motif. N—H
O hydrogen bonds further link these hydrogen-bonded fragments into columns extending in [010].
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The crystal structure of the title compound, C26H39BO2, which contains no strong hydrogen bond donors, displays only long C—H
O contacts between inversion-related pairs of molecules. The structure contains layers rich in oxygen and boron parallel to the ac plane. The dioxaborinane ring adopts an envelope conformation with the C atom attached to the two methyl groups as the flap .
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In the title compound, C19H21ClN2O2, the aromatic rings are approximately perpendicular to each other, subtending a dihedral angle of 87.7 (1)°. In the crystal, the 4-nitrophenyl groups of pairs of neighbouring molecules are parallel and oriented head-to-tail with a ring centroid–centroid distance of 3.9247 (12) Å, leading to a π–π interaction between the pair. The faces of each phenyl ring of the 2,6-diisopropylphenyl group interact with two different groups, viz. a chloro group of an adjacent molecule on one side and the edge of the 4-nitrophenyl ring of a second molecule on the other side.