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17 citations found for Jensen, R.
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In the title compound, [VO(C16H16N2O2)(H2O)]NO3·0.76H2O, the V atom has a distorted octahedral coordination geometry with a long V—O(water) bond, 2.225 (1) Å, trans to V=O, 1.594 (1) Å. The V atom is 0.260 Å out of the plane defined by the N and O atoms of the bis(salicylidene)ethylenediaminate ligand and is displaced towards the vanadyl O atom. The coordinated water molecule is hydrogen bonded to one O atom of the nitrate ion so that pairs of cations are linked by two O—H
O
H—O bridges to give neutral centrosymmetric dimers. This is a different bridging arrangement from that found in either of the polymorphs of the anhydrous compound. There is also a weak hydrogen bond between a nitrate O and the partially occupied water of crystallization.
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Three in situ X-ray diffraction sample environments for gas–solid and gas–solid–liquid reactions at elevated pressure and temperature are described. The environments can be used in a wide range of fields and can withstand up to 1000 bar (1 bar = 105 Pa).
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The therapeutic antibody omalizumab inhibits the binding of IgE to its receptors. Two crystal structures of the omalizumab Fab fragment have been determined at 1.9 and 3.0 Å resolution.
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Two multipurpose sample cells of quartz (SiO2) or sapphire (Al2O3) capillaries, developed for the study of solid–gas reactions in dosing or flow mode, are presented. They allow fast change of pressure up to 100 or 300 bar (1 bar = 100 000 Pa) and can also handle solid–liquid–gas studies.
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Cyclohexadienyl dehydratase from P. aeruginosa has been crystallized in a new crystal form, which diffracts beyond 1.6 Å at the Cornell High Energy Synchrotron Source (CHESS) A1 beamline.
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Even though they contain isosteric and isoelectronic molecules that both form C=O
Br contacts, the cyanide and isocyanide crystals are not isomorphous in any dimension.
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The title microbial antibiotic, C26H33Cl3O6, is an unusual trichlorinated dihydroquinone with cyclized prenyl and geranyl terpene substitution. The crystal structure provides an unambiguous assignment for this compound including its absolute stereochemistry, and shows the favored configuration of the chlorocyclohexane substituent.
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Crystal structures of MauG in complexes with MADH with its TTQ cofactor in the quinone and quinol forms are reported.