Side-chain conformations in the isomorphous polyfluorinated {4,4′-bis[(2,2-difluoroethoxy)methyl]-2,2′-bipyridine-κ²N,N′}dichloridopalladium and -platinum complexes

N. Lu, J.-H. Zheng, Y.-J. Lu, H.-F. Chiang, C.-W. Chu, J. S. Thrasher, Y.-S. Wen and L.-K. Liu

The structures of the palladium and platinum complexes of 4,4′-bis[(2,2-difluoroethoxy)methyl]-2,2′-bipyridine are isomorphous and have –C(H_α)₂OC(H_β)₂CF₂H side chains with H-atom donors at the α and β sites. Molecules are associated into dimers and the dimers form columns, with alternating dimers reinforced by C—H

Cl hydrogen bonds and C—H_β

F(—C) interactions.

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Side-chain conformations in the isomorphous polyfluorinated {4,4′-bis[(2,2-difluoroethoxy)methyl]-2,2′-bipyridine-κ²N,N′}dichloridopalladium and -platinum complexes

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results of search on CRYSTALLOGRAPHY JOURNALS ONLINE

Side-chain conformations in the isomorphous polyfluorinated {4,4′-bis[(2,2-di­fluoro­eth­oxy)meth­yl]-2,2′-bi­pyridine-κ2N,N′}di­chlorido­palladium and -platinum complexes

Side-chain conformations in the isomorphous polyfluorinated {4,4′-bis[(2,2-difluoroethoxy)methyl]-2,2′-bipyridine-κ²N,N′}dichloridopalladium and -platinum complexes