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metal-organic compounds
Crystallization of chloro(2,2′:6′,2′′-terpyridine)platinum(II) chloride from dimethyl sulfoxide yields a red polymorph, [PtCl(C15H11N3)]Cl·C2H6OS, (I), which exhibits stacking along the a axis through pairs of Pt
Pt(−x, −y, −z) interactions of 3.3155 (8) Å. The cations are further associated through close PtPt(1 − x, −y, −z) distances of 3.4360 (8) Å. Recrystallization from water gives a merohedrally twinned yellow–orange dihydrate form, [PtCl(C15H11N3)]Cl·2H2O, (II), with pairwise short PtPt(1 − x, 2 − y, −z) contacts of 3.3903 (5) Å but no long-range stacking through the crystals. Interpair PtPt(−x, 2 − y, −z) distances between cation pairs in the hydrate are 4.3269 (5) Å.
Pt(−x, −y, −z) interactions of 3.3155 (8) Å. The cations are further associated through close PtPt(1 − x, −y, −z) distances of 3.4360 (8) Å. Recrystallization from water gives a merohedrally twinned yellow–orange dihydrate form, [PtCl(C15H11N3)]Cl·2H2O, (II), with pairwise short PtPt(1 − x, 2 − y, −z) contacts of 3.3903 (5) Å but no long-range stacking through the crystals. Interpair PtPt(−x, 2 − y, −z) distances between cation pairs in the hydrate are 4.3269 (5) Å.metal-organic compounds
In the title compound, [PtI(C15H11N3)][AuI2], the [PtI(terpy)]+ cations (terpy is 2,2′:6′,2′′-terpyridine) stack in pairs about inversion centers through PtPt interactions of 3.5279 (5) Å. The [AuI2]− anions also exhibit pairwise stacking, with AuI distances of 3.7713 (5) Å. The [PtI(terpy)]+ cations and [AuI2]− anions aggregate forming infinite arrays of stacked ({[PtI(terpy)]+[PtI(terpy)]+}{[AuI2]−[AuI2]−}) units.
Pt interactions of 3.5279 (5) Å. The [AuI2]− anions also exhibit pairwise stacking, with AuI distances of 3.7713 (5) Å. The [PtI(terpy)]+ cations and [AuI2]− anions aggregate forming infinite arrays of stacked ({[PtI(terpy)]+[PtI(terpy)]+}{[AuI2]−[AuI2]−}) units.
