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A lead(II) complex has been prepared by reaction of Pb(OAc)2·2H2O (OAc is acetate) with 2,2'-(diazene-1,2-di­yl)di­benzoic acid and 4,4'-bi­pyridine in MeOH-H2O at 363 K. Single-crystal X-ray diffraction analysis reveals that the complex possesses a three-dimensional framework with a 41263 topology.
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