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This paper describes the design and construction of a new molten salt cell and furnace, which together allow individual cell components such as anodes and cathodes to be studied in situ using synchrotron-based energy-dispersive X-ray diffraction. The performance of this equipment is demonstrated by an in situ study of a model inert anode within an operational Fray-Farthing-Chen Cambridge titanium electrowinning cell, using the JEEP beamline at the Diamond Light Source.
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