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A neutron diffraction study of the nuclear and magnetic structure of goethite (\alpha-FeOOH) with varying crystallinity and temperature is presented. The antiferromagnetic structure in the Pbnm color space group suggests spins aligned parallel to the c axis. A significant reduction in the Néel temperature was found for a nanocrystalline sample.

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A new six-axis robotic sample changer for neutron powder diffraction experiments, including texture measurements, has enabled a novel set of experiments to be performed at the High-Pressure Preferred Orientation diffractometer at the Lujan Neutron Scattering Center.
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