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The cross-coupling reaction of (benzo[b]thiophen-2-yl)tributylstannane and 2-chloro-3-methylpyridine using a palladium catalyst gave the desired product in excellent yield, but resulted in the unexpected isolation of the benzo[b]thiophene dimer present in trace quantities (2-3 mol%) during recrystallization. Two independent half-molecules of this dimer comprise the symmetric unit, and the dimers exhibit ring disorder.
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