organic compounds
Open access
In the title compound, C16H14O4, there is an intramolecular O—HO hydrogen bond. The benzene rings are inclined to one another by 13.89 (9)°. The prop-2-en-1-one group is twisted slightly, the O=C—Car—Car (ar = aromatic) and C=C—C=O torsion angles being −10.4 (3) and −7.4 (3)°, respectively. In the crystal, molecules are linked by O—HO hydrogen bonds, forming chains along [100]. These chains are further linked by O—HO hydrogen bonds, forming corrugated sheets lying parallel to (010). There are C—Hπ interactions present within the sheets.
data reports
Open access
In the title compound, C23H18O4, the methoxybenzene ring and attached C=C grouping are disordered over two sets of sites in a 0.823 (5):0.177 (5) ratio. The dihedral angles between the central benzene ring and the pendant phenyl and methoxybenzene ring (major orientation) are 51.21 (1) and 51.6 (1)°, respectively. In the crystal, inversion dimers linked by pairs of C—HO hydrogen bonds generate R22(28) loops.
data reports
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In the title compound, C20H20Cl2N2O2·H2O, the piperidine ring adopts a chair conformation with the two substituent benzene rings inclined to one another [dihedral angle 84.63 (9)°]. In the crystal, the components are linked by Ow—HO, N—HOw (w = water) and C—HO hydrogen bonds, generating a sheet structure lying parallel to (101).
data reports
Open access
In the title moleclue, C16H14O4, the dihedral angle between the benzene rings is 16.1 (3)°. The methoxy group is essentially coplanar with the benzene ring to which it is attached, with a C—O—CC torsion angle of 5.5 (9)°. In the crystal, molecules are linked by O—HO and bifurcated O—H(O,O) hydrogen bonds, forming a three-dimensional network. The structure was refined as a two-component inversion twin.