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A cadmium(II) complex, prepared by reaction of Cd(NO3)2·6H2O with terephthalic acid and 1,4-bis(1,2,4-triazol-1-ylmethyl)benzene in H2O, possesses a three-dimensional framework with 3,8-connected three-dimensional binodal {4.52}2{42.510.612.7.83} topology. The compound exhibits a strong fluorescence emission in the solid state at room temperature.

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The title compound has a fivefold inter­penetrating diamondoid three-dimensional metal-organic framework, with each ZnII centre surrounded by two O-donor atoms from monodentate carboxyl­ate groups belonging to two different benzene-1,4-di­acetate ligands and by two triazole N-donor atoms from two different 1,4-bis­[(1H-1,2,4-triazol-1-yl)methyl]benzene ligands.
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