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For the first time, a high-resolution far-field detector has been used to study the initial and evolving structure of individual metastable austenite grains during uniaxial tensile deformation of a transformation-induced plasticity (TRIP) steel sample. The orientation, position and lattice parameters of the selected grains were reconstructed from additional measurements with a lower-resolution medium-field detector.

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A high-precision method for tilt calibration of area detectors is presented. The procedure takes into account continuously varying spatial distortions.
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