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Non-ambient conditions are used with increasing regularity in structural studies of crystals and functional materials - this editorial summarizes very briefly the history of environment devices and describes selected recent achievements in this field.
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It is well known that pre-treatment procedures affect catalyst performance. In situ X-ray diffraction was used in this study to monitor the changes in phase composition and crystallite size during the pre-treatment of Fe/TiO2 catalysts, yielding insight into crystalline and non-crystalline phase changes and metal-support interactions.
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