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The ordering of carbon vacancies induces the reduction of twinning interfacial energy and leads to the presence of {111} twinning structures in nonstoichiometric ZrC0.6. Two types of twinning boundaries, i.e. {111}C and {111}Zr, can be recognized.

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The performance of confocal energy-dispersive small-angle X-ray scattering based on polycapillary optics is presented. This confocal small-angle X-ray scattering technology could be used to perform nondestructive and in situ analysis of samples such as milk powder in its packaging.
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