In situ ultra-small-angle X-ray scattering study of the solution-mediated formation and growth of nanocrystalline ceria

A. J. Allen, V. A. Hackley, P. R. Jemian, J. Ilavsky, J. M. Raitano and S.-W. Chan

A circulating fluid flow cell is described for the in situ ultra-small-angle X-ray scattering study of solution-mediated systems. Results are presented for the real-time formation and growth from homogenous solution of nanocrystalline ceria that reveal new aspects.

Keywords: nucleation and growth; nanocrystalline ceria; ultra-small-angle X-ray scattering (USAXS); real-time studies; fluid flow; nanoparticles.

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