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The crystal structure of a new quenchable high-pressure–high-temperature modification of antimony(III) oxide, γ-Sb2O3, with rare 3,3T8 topology has been determined from high-resolution synchrotron powder diffraction data.

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The crystal structures of two polymorphs of dimeric toluene-2,4-diisocyanate have been solved from high-resolution laboratory X-ray powder diffraction data. A study of their intermolecular energies highlighted the differences in physical properties observed between the two forms.

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