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Acetonitrilediaqua-κ1O-nitrato-κ2O-nitratonickel(II) 15-crown-5 acetonitrile solvate was studied by single-crystal X-ray diffraction at intervals of 10 K in the range 90–273 K as the crystal passed, without obvious damage, through three phase transitions. The phase sequence includes an intermediate modulated phase that seems to be a kind of striped hybrid of the phases stable at immediately higher and lower temperatures.
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