organic compounds
The title compound, C33H25N·0.25C6H14, was synthesized via the Ullmann reaction. The dihedral angles between the planes of the phenyl rings of the diphenylamine group and the plane of the central benzene ring are 109.2 (3) and 114.1 (8)°.
organic compounds
Two compounds were obtained via the addition of N-methylhydroxylamine to 1-phenyl-2-nitropropene. The structure of the major product, the title compound, (I), C17H17N3O6, is reported here. Both asymmetric C atoms (C1 and C2) have the same chirality, either R,R or S,S.
organic compounds
The title compound, C22H20N2O3, was prepared by the reaction of 4-benzyloxy-3-methoxybenzaldehyde and benzohydrazide. The central vanillin system makes dihedral angles of 18.2 (1) and 14.3 (1)° with the planes of the benzohydrazide and benzyl groups, respectively. The crystal structure is stabilized by intermolecular N—HO hydrogen bonding.
organic compounds
The title compound, C17H19Cl2N2OS+·Cl−, was synthesized from 2-acetothiophene, 1-(2,3-dichlorophenyl)piperazine and paraformaldehyde. In the cation, the thienyl ring is coplanar with the oxopropyl group. The protonated piperazine ring exhibits a chair conformation. In the crystal packing the cations are connected by C—HO and C—HCl hydrogen bonds.