Journal of Synchrotron Radiation
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J. Synchrotron Rad.
(2014).
21
,
1275-1281
https://doi.org/10.1107/S1600577514014891
Download PDF of article
Download citation
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An unconventional method for measuring the Tc
L
3
-edge of technetium compounds
P. E. R. Blanchard
,
E. Reynolds
,
B. J. Kennedy
,
C. D. Ling
,
Z. Zhang
,
G. Thorogood
,
B. C. C. Cowie
and
L. Thomsen
Embedding Tc oxides in epoxy allows measurement of the Tc
L
-edge spectra under UHV conditions. Changes in the Tc
L
-edge XANES spectra provide information on the oxidation state, crystal field splitting and coordination environment.
Keywords:
XANES
;
Tc
L
3
-edge
;
technetium oxides
;
radioactive materials
;
crystal field splitting
.
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