research papers
A versatile setup for in situ synchrotron small/wide-angle X-ray scattering (SAXS/WAXS) and pair distribution function (PDF) measurements of supercritical fluid reactions has been developed.
research papers
Nanocrystalline boehmite (AlOOH) was synthesized under continuous flow in sub- and supercritical water. The reaction temperature- and pressure-dependent particle size and morphology were studied using powder X-ray diffraction and transmission electron microscopy.