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The title zinc(II) complex, prepared by the reaction of Zn(OAc)2·2H2O with 2,2'-(diazene-1,2-diyl)di­benzoic acid and 1,2-bis­(pyridin-4-yl)ethene in MeOH/H2O at 393 K, possesses a three-dimensional framework with a 4664 topology. Powder X-ray diffraction and solid-state photoluminescent properties were also measured.

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A lead(II) complex has been prepared by reaction of Pb(OAc)2·2H2O (OAc is acetate) with 2,2'-(diazene-1,2-di­yl)di­benzoic acid and 4,4'-bi­pyridine in MeOH-H2O at 363 K. Single-crystal X-ray diffraction analysis reveals that the complex possesses a three-dimensional framework with a 41263 topology.
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