Preparation and structural analysis of (±)-threo-ritalinic acid

S. Wyss, I. A. Werner, W. B. Schweizer, S. M. Ametamey and S. Milicevic Sephton

The preparation, single-crystal X-ray structure and solution-state NMR analysis of (±)-threo-ritalinic acid, obtained from the hydrolysis of the methyl ester (±)-threo-methyl phenidate, are reported.

Keywords: crystal structure; (±)-threo-ritalinic acid; (±)-threo-methyl phenidate; hydrolysis; Ritalin^®; gauche⁺-gauche^- interactions.

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