organic compounds
Open access
The title compound, C30H26O4, contains an oxo-cyclohexane ring in a distorted half-chair configuration, with disorder of two C atoms in a 0.859 (4):0.141 (4) ratio. The dihedral angle between the mean planes of the two napthalene ring systems is 58.6 (8)°.
organic compounds
Open access
In the title compound, C16H15FN2O, the dihedral angles between the benzene rings are74.7(8), 74.1 (1), 74.2 (7) and 74.3 (5)° in the four independent molecules in the asymmetric unit. In the crystal, N-H-O hydrogen bonds involving the hydrazide and acetyl groups, which form R22(18) ring motifs, link the molecules into dimers, which form columns along [010].
organic compounds
Open access
A new polymorph of the title compound, C8H8BrNO, has been determined at 173 K in the space group P21/c. The previous room-temperature structure was reported to crystallize in the orthorhombic space group Pna21 [Andreetti et al. (1968). Acta Cryst. B24, 1195–1198]. In the crystal, molecules are linked by N—HO hydrogen bonds forming chains along [010]. Weak C—Hπ interactions are also present.