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Improvements to the experimental setup, the data collection strategy and the data analysis procedure have simplified the method for exploiting preferred orientation in the structure analysis of polycrystalline materials.

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The proof of concept for using a 4% broad-bandpass beam, which is planned for the new SwissFEL facility, for the structural characterization of nonbiological materials is shown.

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The zeolite-specific structure solution program FOCUS has been modified to work with three-dimensional electron diffraction data. The method was applied successfully to five different zeolite materials using data sets collected with either automated diffraction tomography or the rotation electron diffraction technique.

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The feasibility of exploiting the features of Laue microdiffraction to characterize the structures of inorganic materials by using data collected on several randomly oriented stationary microcrystals is demonstrated.
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