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A novel two-dimensional small-angle X-ray scattering pattern analysis method is presented which extracts parameters characterizing the radius, length and polydispersity of scatterers in heat-treated and precursor poly(p-phenylene terephtalamide) fibres.

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Combined in situ small- and wide-angle X-ray scattering was applied to investigate the dynamical properties of dry oleic acid-capped titanium dioxide nanorods during annealing in an inert gas stream, using a recently developed laboratory setup.
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