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The title compound, [Fe2Ni(C5H5)2(C20H20N2O2)]·CH2Cl2, is a four-coordinate square-planar nickel(II) complex with a tetra­dentate 1,1'-diferrocenyl-3,3'-(ethane-1,2-diyldinitrilo)dibutanolate ligand, which crystallizes with a mol­ecule of dichloro­methane. The ferrocene substituents are arranged in a syn conformation with respect to the Ni coordination plane. The complexes stack in an alternating assembly with channels occupied by the solvent mol­ecules.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536806046174/wn2079sup1.cif
Contains datablocks global, I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S1600536806046174/wn2079Isup2.hkl
Contains datablock I

CCDC reference: 630500

Key indicators

  • Single-crystal X-ray study
  • T = 200 K
  • Mean [sigma](C-C) = 0.004 Å
  • R factor = 0.027
  • wR factor = 0.070
  • Data-to-parameter ratio = 15.7

checkCIF/PLATON results

No syntax errors found



Alert level C PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd. # 2 C H2 Cl2
0 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 1 ALERT level C = Check and explain 0 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 0 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check

Computing details top

Data collection: SMART (Siemens, 1995); cell refinement: SAINT (Siemens, 1995); data reduction: SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: ORTEP-3 for Windows (Farrugia, 1997); software used to prepare material for publication: WinGX (Farrugia, 1999).

[1,1'-Diferrocenyl-3,3'-(ethane-1,2-diyldinitrilo)dibutanolato]nickel(II) dichloromethane solvate top
Crystal data top
[Fe2Ni(C5H5)2(C20H20N2O2)]·CH2Cl2Z = 2
Mr = 705.90F(000) = 724
Triclinic, P1Dx = 1.667 Mg m3
a = 7.0218 (1) ÅMo Kα radiation, λ = 0.71073 Å
b = 12.9673 (3) ÅCell parameters from 8192 reflections
c = 16.3207 (3) Åθ = 2–26°
α = 98.143 (1)°µ = 1.90 mm1
β = 101.884 (1)°T = 200 K
γ = 100.312 (1)°Irregular fragment, brown
V = 1405.91 (5) Å30.15 × 0.15 × 0.15 mm
Data collection top
Siemens SMART area-detector
diffractometer
5711 independent reflections
Radiation source: fine-focus sealed tube4934 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.020
ω scansθmax = 26.4°, θmin = 1.3°
Absorption correction: empirical (using intensity measurements)
(XABS2; Parkin et al., 1995)
h = 88
Tmin = 0.729, Tmax = 0.752k = 1616
13215 measured reflectionsl = 020
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.027Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.070H-atom parameters constrained
S = 0.90 w = 1/[σ2(Fo2) + (0.0324P)2 + 1.8447P]
where P = (Fo2 + 2Fc2)/3
5711 reflections(Δ/σ)max = 0.002
363 parametersΔρmax = 0.42 e Å3
0 restraintsΔρmin = 0.34 e Å3
Special details top

Experimental. 1H NMR (CDCl3, δ, p.p.m.): 1.93 (s, 6H, CH3), 3.04 (m, 3H, CH2), 4.21 (m, 10H, Cp), 4.24 (t, 4H, Cp), 4.63 (t, 4H, Cp), 5.26 (s, 2H, CH); HR—MS (FAB), calculated for C30H30N2O2Fe258Ni (M+) m/z 620.03595; found: 620.03567.

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
Ni0.17718 (4)0.99380 (2)0.391416 (17)0.01840 (7)
Fe10.10423 (5)0.72007 (2)0.07639 (2)0.02042 (8)
Fe20.40449 (5)1.37870 (2)0.27434 (2)0.02070 (8)
O10.1724 (2)1.11294 (12)0.34046 (10)0.0238 (3)
O20.0839 (2)0.92090 (12)0.28018 (10)0.0243 (3)
N10.2734 (3)1.07140 (15)0.50123 (11)0.0212 (4)
N20.1697 (3)0.87205 (15)0.43901 (11)0.0209 (4)
C10.2282 (3)1.21170 (17)0.37829 (14)0.0215 (4)
C20.3053 (3)1.24503 (18)0.46454 (15)0.0253 (5)
H2A0.34801.31960.48560.030*
C30.3255 (3)1.17611 (18)0.52382 (14)0.0234 (5)
C40.3008 (4)1.00805 (19)0.56857 (14)0.0262 (5)
H4A0.22671.02940.61130.031*
H4B0.44391.02250.59760.031*
C50.2282 (4)0.89072 (19)0.53288 (14)0.0271 (5)
H5A0.33510.85260.55130.033*
H5B0.11250.86220.55510.033*
C60.1119 (3)0.77224 (18)0.39741 (15)0.0226 (5)
C70.0482 (3)0.74516 (18)0.30801 (15)0.0236 (5)
H7A0.01110.67160.28280.028*
C80.0362 (3)0.81842 (17)0.25465 (14)0.0209 (4)
C90.4068 (4)1.2265 (2)0.61664 (15)0.0300 (5)
H9A0.30161.21320.64750.045*
H9B0.45351.30360.62180.045*
H9C0.51821.19550.64090.045*
C100.1152 (4)0.68118 (19)0.44608 (16)0.0308 (5)
H10A0.25250.68390.47630.046*
H10B0.06290.61320.40610.046*
H10C0.03240.68760.48730.046*
C110.1967 (3)1.29008 (18)0.32211 (15)0.0239 (5)
C120.1453 (3)1.26597 (19)0.23109 (15)0.0266 (5)
H12A0.12911.19430.19520.032*
C130.1226 (4)1.3611 (2)0.20043 (17)0.0313 (5)
H13A0.08781.36830.13920.038*
C140.1597 (4)1.4443 (2)0.27167 (18)0.0334 (6)
H14A0.15601.52050.26930.040*
C150.2068 (4)1.40173 (19)0.34715 (17)0.0293 (5)
H15A0.24001.44230.40690.035*
C160.6852 (4)1.4426 (3)0.34581 (19)0.0457 (7)
H16A0.72191.47630.40750.055*
C170.6680 (4)1.3341 (3)0.31293 (19)0.0417 (7)
H17A0.68981.27720.34710.050*
C180.6150 (4)1.3197 (2)0.22368 (18)0.0341 (6)
H18A0.59151.25060.18330.041*
C190.5992 (4)1.4194 (2)0.20073 (17)0.0302 (5)
H19A0.56271.43320.14130.036*
C200.6428 (4)1.4960 (2)0.27613 (19)0.0378 (6)
H20A0.64411.57380.27990.045*
C210.0399 (3)0.78317 (18)0.16180 (15)0.0230 (5)
C220.1495 (3)0.67924 (19)0.11753 (15)0.0267 (5)
H22A0.18590.61590.14420.032*
C230.1991 (4)0.6825 (2)0.02943 (16)0.0306 (5)
H23A0.27510.62140.01710.037*
C240.1192 (4)0.7866 (2)0.01827 (16)0.0316 (6)
H24A0.12940.81150.03740.038*
C250.0207 (4)0.84902 (19)0.09943 (15)0.0279 (5)
H25A0.04980.92560.11110.033*
C260.3885 (4)0.7253 (3)0.14014 (18)0.0409 (7)
H26A0.44930.75700.20150.049*
C270.2864 (4)0.6178 (2)0.10714 (19)0.0394 (7)
H27A0.26230.56040.14100.047*
C280.2254 (4)0.60666 (19)0.01726 (17)0.0314 (5)
H28A0.14980.54000.02350.038*
C290.2908 (4)0.70639 (19)0.00417 (16)0.0285 (5)
H29A0.26840.72270.06300.034*
C300.3905 (4)0.7793 (2)0.07102 (17)0.0345 (6)
H30A0.45230.85600.07490.041*
Cl10.49908 (11)1.03339 (6)0.22953 (5)0.04306 (17)
Cl20.28203 (12)1.06183 (5)0.09701 (4)0.04228 (16)
C310.2715 (4)1.0366 (3)0.2012 (2)0.0480 (8)
H31A0.23280.96740.20510.058*
H31B0.16761.09290.24210.058*
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Ni0.02079 (14)0.01931 (14)0.01543 (14)0.00407 (11)0.00559 (11)0.00272 (10)
Fe10.02327 (17)0.01951 (16)0.01895 (16)0.00541 (13)0.00659 (13)0.00179 (12)
Fe20.02275 (17)0.01720 (15)0.02241 (17)0.00239 (12)0.00837 (13)0.00255 (12)
O10.0323 (9)0.0204 (8)0.0176 (8)0.0030 (7)0.0064 (7)0.0029 (6)
O20.0328 (9)0.0199 (8)0.0188 (8)0.0046 (7)0.0055 (7)0.0015 (6)
N10.0193 (9)0.0271 (10)0.0176 (9)0.0052 (8)0.0056 (7)0.0036 (7)
N20.0203 (9)0.0260 (9)0.0182 (9)0.0068 (8)0.0063 (7)0.0053 (7)
C10.0193 (11)0.0208 (11)0.0259 (12)0.0027 (9)0.0105 (9)0.0042 (9)
C20.0264 (12)0.0218 (11)0.0248 (12)0.0015 (9)0.0059 (9)0.0002 (9)
C30.0187 (11)0.0296 (12)0.0207 (11)0.0046 (9)0.0059 (9)0.0008 (9)
C40.0262 (12)0.0338 (13)0.0186 (11)0.0067 (10)0.0048 (9)0.0054 (9)
C50.0311 (13)0.0336 (13)0.0196 (11)0.0076 (10)0.0084 (10)0.0099 (10)
C60.0189 (11)0.0246 (11)0.0280 (12)0.0062 (9)0.0100 (9)0.0089 (9)
C70.0241 (11)0.0215 (11)0.0249 (12)0.0048 (9)0.0071 (9)0.0020 (9)
C80.0180 (10)0.0230 (11)0.0223 (11)0.0051 (9)0.0081 (9)0.0007 (9)
C90.0294 (13)0.0358 (13)0.0213 (12)0.0061 (11)0.0053 (10)0.0038 (10)
C100.0350 (14)0.0266 (12)0.0341 (14)0.0082 (11)0.0094 (11)0.0123 (10)
C110.0222 (11)0.0228 (11)0.0280 (12)0.0032 (9)0.0094 (9)0.0063 (9)
C120.0239 (12)0.0261 (12)0.0262 (12)0.0015 (9)0.0038 (10)0.0049 (9)
C130.0258 (12)0.0345 (13)0.0332 (14)0.0033 (10)0.0046 (10)0.0124 (11)
C140.0358 (14)0.0305 (13)0.0442 (15)0.0165 (11)0.0190 (12)0.0151 (11)
C150.0367 (14)0.0251 (12)0.0332 (13)0.0110 (10)0.0192 (11)0.0073 (10)
C160.0286 (14)0.064 (2)0.0328 (15)0.0107 (13)0.0043 (12)0.0015 (14)
C170.0288 (14)0.0580 (18)0.0473 (17)0.0143 (13)0.0141 (12)0.0258 (14)
C180.0351 (14)0.0321 (13)0.0442 (16)0.0132 (11)0.0228 (12)0.0096 (11)
C190.0292 (13)0.0319 (13)0.0339 (14)0.0050 (10)0.0153 (11)0.0109 (11)
C200.0351 (14)0.0284 (13)0.0472 (17)0.0061 (11)0.0190 (13)0.0005 (11)
C210.0229 (11)0.0225 (11)0.0240 (11)0.0076 (9)0.0066 (9)0.0005 (9)
C220.0228 (12)0.0271 (12)0.0282 (12)0.0033 (9)0.0083 (10)0.0019 (10)
C230.0263 (12)0.0347 (13)0.0260 (12)0.0078 (10)0.0023 (10)0.0061 (10)
C240.0352 (14)0.0367 (14)0.0241 (12)0.0178 (11)0.0031 (10)0.0024 (10)
C250.0358 (13)0.0265 (12)0.0231 (12)0.0149 (10)0.0060 (10)0.0017 (9)
C260.0265 (13)0.0651 (19)0.0287 (14)0.0163 (13)0.0019 (11)0.0005 (13)
C270.0432 (16)0.0490 (16)0.0456 (16)0.0291 (14)0.0244 (13)0.0283 (13)
C280.0347 (14)0.0232 (12)0.0392 (14)0.0081 (10)0.0170 (11)0.0009 (10)
C290.0317 (13)0.0302 (12)0.0282 (13)0.0083 (10)0.0155 (10)0.0061 (10)
C300.0267 (13)0.0335 (13)0.0408 (15)0.0008 (11)0.0126 (11)0.0004 (11)
Cl10.0424 (4)0.0487 (4)0.0397 (4)0.0090 (3)0.0107 (3)0.0130 (3)
Cl20.0542 (4)0.0370 (3)0.0376 (4)0.0091 (3)0.0128 (3)0.0116 (3)
C310.0332 (15)0.070 (2)0.0434 (17)0.0133 (15)0.0045 (13)0.0244 (16)
Geometric parameters (Å, º) top
Ni—O21.8496 (15)C9—H9C0.9800
Ni—N11.8515 (18)C10—H10A0.9800
Ni—N21.8529 (18)C10—H10B0.9800
Ni—O11.8575 (15)C10—H10C0.9800
Fe1—C262.037 (3)C11—C121.429 (3)
Fe1—C222.040 (2)C11—C151.432 (3)
Fe1—C272.044 (2)C12—C131.417 (3)
Fe1—C302.044 (3)C12—H12A1.0000
Fe1—C252.047 (2)C13—C141.415 (4)
Fe1—C212.048 (2)C13—H13A1.0000
Fe1—C282.050 (2)C14—C151.422 (4)
Fe1—C242.052 (2)C14—H14A1.0000
Fe1—C292.050 (2)C15—H15A1.0000
Fe1—C232.052 (2)C16—C171.407 (4)
Fe2—C162.032 (3)C16—C201.421 (4)
Fe2—C152.038 (2)C16—H16A1.0000
Fe2—C172.040 (3)C17—C181.403 (4)
Fe2—C112.044 (2)C17—H17A1.0000
Fe2—C122.043 (2)C18—C191.413 (3)
Fe2—C202.042 (3)C18—H18A1.0000
Fe2—C142.045 (2)C19—C201.409 (4)
Fe2—C182.046 (2)C19—H19A1.0000
Fe2—C192.047 (2)C20—H20A1.0000
Fe2—C132.050 (3)C21—C251.430 (3)
O1—C11.293 (3)C21—C221.433 (3)
O2—C81.295 (3)C22—C231.416 (3)
N1—C31.318 (3)C22—H22A1.0000
N1—C41.465 (3)C23—C241.419 (4)
N2—C61.323 (3)C23—H23A1.0000
N2—C51.475 (3)C24—C251.416 (3)
C1—C21.375 (3)C24—H24A1.0000
C1—C111.478 (3)C25—H25A1.0000
C2—C31.410 (3)C26—C301.410 (4)
C2—H2A0.9500C26—C271.421 (4)
C3—C91.509 (3)C26—H26A1.0000
C4—C51.504 (3)C27—C281.419 (4)
C4—H4A0.9900C27—H27A1.0000
C4—H4B0.9900C28—C291.410 (3)
C5—H5A0.9900C28—H28A1.0000
C5—H5B0.9900C29—C301.403 (4)
C6—C71.408 (3)C29—H29A1.0000
C6—C101.515 (3)C30—H30A1.0000
C7—C81.379 (3)Cl1—C311.748 (3)
C7—H7A0.9500Cl2—C311.766 (3)
C8—C211.474 (3)C31—H31A0.9900
C9—H9A0.9800C31—H31B0.9900
C9—H9B0.9800
O2—Ni—N1177.85 (8)H9A—C9—H9B109.5
O2—Ni—N294.93 (7)C3—C9—H9C109.5
N1—Ni—N287.16 (8)H9A—C9—H9C109.5
O2—Ni—O183.18 (7)H9B—C9—H9C109.5
N1—Ni—O194.75 (8)C6—C10—H10A109.5
N2—Ni—O1177.23 (8)C6—C10—H10B109.5
C26—Fe1—C22127.10 (11)H10A—C10—H10B109.5
C26—Fe1—C2740.74 (12)C6—C10—H10C109.5
C22—Fe1—C27109.20 (10)H10A—C10—H10C109.5
C26—Fe1—C3040.43 (11)H10B—C10—H10C109.5
C22—Fe1—C30163.68 (10)C12—C11—C15107.4 (2)
C27—Fe1—C3068.13 (11)C12—C11—C1125.1 (2)
C26—Fe1—C25119.45 (11)C15—C11—C1127.4 (2)
C22—Fe1—C2568.81 (10)C12—C11—Fe269.49 (13)
C27—Fe1—C25155.22 (11)C15—C11—Fe269.24 (13)
C30—Fe1—C25106.47 (11)C1—C11—Fe2127.58 (16)
C26—Fe1—C21107.95 (10)C13—C12—C11108.3 (2)
C22—Fe1—C2141.05 (9)C13—C12—Fe270.00 (14)
C27—Fe1—C21121.18 (10)C11—C12—Fe269.58 (13)
C30—Fe1—C21125.35 (10)C13—C12—H12A125.8
C25—Fe1—C2140.89 (9)C11—C12—H12A125.8
C26—Fe1—C2868.21 (11)Fe2—C12—H12A125.8
C22—Fe1—C28121.39 (10)C12—C13—C14108.0 (2)
C27—Fe1—C2840.57 (11)C12—C13—Fe269.47 (14)
C30—Fe1—C2867.84 (10)C14—C13—Fe269.59 (15)
C25—Fe1—C28161.86 (10)C12—C13—H13A126.0
C21—Fe1—C28156.33 (10)C14—C13—H13A126.0
C26—Fe1—C24153.55 (12)Fe2—C13—H13A126.0
C22—Fe1—C2468.36 (10)C15—C14—C13108.6 (2)
C27—Fe1—C24163.68 (12)C15—C14—Fe269.38 (14)
C30—Fe1—C24118.88 (11)C13—C14—Fe269.98 (14)
C25—Fe1—C2440.43 (10)C15—C14—H14A125.7
C21—Fe1—C2468.34 (9)C13—C14—H14A125.7
C28—Fe1—C24125.77 (10)Fe2—C14—H14A125.7
C26—Fe1—C2967.75 (11)C14—C15—C11107.6 (2)
C22—Fe1—C29155.34 (10)C14—C15—Fe269.87 (14)
C27—Fe1—C2967.85 (10)C11—C15—Fe269.68 (13)
C30—Fe1—C2940.10 (10)C14—C15—H15A126.2
C25—Fe1—C29124.53 (10)C11—C15—H15A126.2
C21—Fe1—C29161.95 (10)Fe2—C15—H15A126.2
C28—Fe1—C2940.22 (10)C17—C16—C20108.2 (3)
C24—Fe1—C29107.22 (10)C17—C16—Fe270.11 (16)
C26—Fe1—C23164.70 (12)C20—C16—Fe270.00 (16)
C22—Fe1—C2340.50 (10)C17—C16—H16A125.9
C27—Fe1—C23127.33 (12)C20—C16—H16A125.9
C30—Fe1—C23153.84 (11)Fe2—C16—H16A125.9
C25—Fe1—C2368.20 (10)C16—C17—C18108.0 (2)
C21—Fe1—C2368.37 (9)C16—C17—Fe269.44 (16)
C28—Fe1—C23108.82 (10)C18—C17—Fe270.12 (15)
C24—Fe1—C2340.45 (10)C16—C17—H17A126.0
C29—Fe1—C23120.40 (10)C18—C17—H17A126.0
C16—Fe2—C15108.87 (12)Fe2—C17—H17A126.0
C16—Fe2—C1740.44 (13)C17—C18—C19108.3 (2)
C15—Fe2—C17125.88 (11)C17—C18—Fe269.71 (15)
C16—Fe2—C11121.40 (11)C19—C18—Fe269.83 (14)
C15—Fe2—C1141.08 (9)C17—C18—H18A125.9
C17—Fe2—C11107.52 (10)C19—C18—H18A125.9
C16—Fe2—C12155.88 (12)Fe2—C18—H18A125.9
C15—Fe2—C1268.82 (10)C20—C19—C18108.1 (2)
C17—Fe2—C12120.15 (11)C20—C19—Fe269.69 (14)
C11—Fe2—C1240.93 (9)C18—C19—Fe269.76 (14)
C16—Fe2—C2040.83 (12)C20—C19—H19A126.0
C15—Fe2—C20121.96 (11)C18—C19—H19A126.0
C17—Fe2—C2068.27 (12)Fe2—C19—H19A126.0
C11—Fe2—C20157.18 (11)C19—C20—C16107.5 (2)
C12—Fe2—C20160.96 (11)C19—C20—Fe270.01 (14)
C16—Fe2—C14126.73 (13)C16—C20—Fe269.17 (15)
C15—Fe2—C1440.75 (10)C19—C20—H20A126.3
C17—Fe2—C14163.46 (12)C16—C20—H20A126.3
C11—Fe2—C1468.58 (10)Fe2—C20—H20A126.3
C12—Fe2—C1468.18 (10)C25—C21—C22107.5 (2)
C20—Fe2—C14108.70 (11)C25—C21—C8125.4 (2)
C16—Fe2—C1867.79 (12)C22—C21—C8127.1 (2)
C15—Fe2—C18162.03 (10)C25—C21—Fe169.54 (13)
C17—Fe2—C1840.18 (11)C22—C21—Fe169.19 (13)
C11—Fe2—C18124.24 (10)C8—C21—Fe1127.71 (16)
C12—Fe2—C18106.59 (11)C23—C22—C21107.9 (2)
C20—Fe2—C1867.94 (11)C23—C22—Fe170.20 (14)
C14—Fe2—C18155.32 (11)C21—C22—Fe169.75 (13)
C16—Fe2—C1968.04 (11)C23—C22—H22A126.1
C15—Fe2—C19156.48 (10)C21—C22—H22A126.1
C17—Fe2—C1967.93 (11)Fe1—C22—H22A126.1
C11—Fe2—C19160.88 (10)C22—C23—C24108.3 (2)
C12—Fe2—C19123.87 (10)C22—C23—Fe169.29 (14)
C20—Fe2—C1940.30 (10)C24—C23—Fe169.76 (14)
C14—Fe2—C19121.06 (10)C22—C23—H23A125.8
C18—Fe2—C1940.41 (10)C24—C23—H23A125.8
C16—Fe2—C13162.87 (12)Fe1—C23—H23A125.8
C15—Fe2—C1368.61 (11)C25—C24—C23108.3 (2)
C17—Fe2—C13154.73 (12)C25—C24—Fe169.61 (13)
C11—Fe2—C1368.62 (10)C23—C24—Fe169.79 (14)
C12—Fe2—C1340.52 (9)C25—C24—H24A125.8
C20—Fe2—C13124.97 (11)C23—C24—H24A125.8
C14—Fe2—C1340.44 (11)Fe1—C24—H24A125.8
C18—Fe2—C13119.94 (11)C24—C25—C21108.0 (2)
C19—Fe2—C13107.10 (10)C24—C25—Fe169.96 (13)
C1—O1—Ni126.80 (14)C21—C25—Fe169.58 (13)
C8—O2—Ni126.96 (14)C24—C25—H25A126.0
C3—N1—C4117.74 (19)C21—C25—H25A126.0
C3—N1—Ni126.75 (16)Fe1—C25—H25A126.0
C4—N1—Ni115.46 (14)C30—C26—C27108.0 (2)
C6—N2—C5118.06 (18)C30—C26—Fe170.06 (15)
C6—N2—Ni126.51 (15)C27—C26—Fe169.91 (15)
C5—N2—Ni115.39 (15)C30—C26—H26A126.0
O1—C1—C2124.4 (2)C27—C26—H26A126.0
O1—C1—C11115.0 (2)Fe1—C26—H26A126.0
C2—C1—C11120.5 (2)C28—C27—C26107.6 (2)
C1—C2—C3124.5 (2)C28—C27—Fe169.92 (14)
C1—C2—H2A117.8C26—C27—Fe169.34 (15)
C3—C2—H2A117.8C28—C27—H27A126.2
N1—C3—C2122.7 (2)C26—C27—H27A126.2
N1—C3—C9119.8 (2)Fe1—C27—H27A126.2
C2—C3—C9117.5 (2)C29—C28—C27107.7 (2)
N1—C4—C5111.20 (18)C29—C28—Fe169.90 (13)
N1—C4—H4A109.4C27—C28—Fe169.50 (14)
C5—C4—H4A109.4C29—C28—H28A126.1
N1—C4—H4B109.4C27—C28—H28A126.1
C5—C4—H4B109.4Fe1—C28—H28A126.1
H4A—C4—H4B108.0C30—C29—C28108.6 (2)
N2—C5—C4110.47 (18)C30—C29—Fe169.71 (14)
N2—C5—H5A109.6C28—C29—Fe169.88 (14)
C4—C5—H5A109.6C30—C29—H29A125.7
N2—C5—H5B109.6C28—C29—H29A125.7
C4—C5—H5B109.6Fe1—C29—H29A125.7
H5A—C5—H5B108.1C29—C30—C26108.1 (2)
N2—C6—C7122.9 (2)C29—C30—Fe170.19 (14)
N2—C6—C10120.0 (2)C26—C30—Fe169.51 (15)
C7—C6—C10117.1 (2)C29—C30—H30A125.9
C8—C7—C6124.3 (2)C26—C30—H30A125.9
C8—C7—H7A117.9Fe1—C30—H30A125.9
C6—C7—H7A117.9Cl1—C31—Cl2112.34 (16)
O2—C8—C7124.4 (2)Cl1—C31—H31A109.1
O2—C8—C21114.78 (19)Cl2—C31—H31A109.1
C7—C8—C21120.8 (2)Cl1—C31—H31B109.1
C3—C9—H9A109.5Cl2—C31—H31B109.1
C3—C9—H9B109.5H31A—C31—H31B107.9
O2—Ni—O1—C1177.83 (19)Fe2—C16—C20—C1959.79 (18)
N1—Ni—O1—C11.58 (19)C17—C16—C20—Fe259.96 (19)
N2—Ni—O2—C80.13 (19)C16—Fe2—C20—C19118.7 (2)
O1—Ni—O2—C8178.10 (19)C15—Fe2—C20—C19159.28 (15)
N2—Ni—N1—C3178.41 (19)C17—Fe2—C20—C1981.05 (17)
O1—Ni—N1—C33.60 (19)C11—Fe2—C20—C19164.6 (2)
N2—Ni—N1—C41.07 (16)C12—Fe2—C20—C1939.1 (4)
O1—Ni—N1—C4179.07 (15)C14—Fe2—C20—C19116.29 (16)
O2—Ni—N2—C60.13 (19)C18—Fe2—C20—C1937.60 (16)
N1—Ni—N2—C6179.61 (19)C13—Fe2—C20—C1974.34 (19)
O2—Ni—N2—C5177.92 (15)C15—Fe2—C20—C1682.0 (2)
N1—Ni—N2—C52.60 (16)C17—Fe2—C20—C1637.65 (18)
Ni—O1—C1—C21.2 (3)C11—Fe2—C20—C1645.9 (3)
Ni—O1—C1—C11176.59 (14)C12—Fe2—C20—C16157.8 (3)
O1—C1—C2—C33.1 (4)C14—Fe2—C20—C16125.02 (18)
C11—C1—C2—C3174.7 (2)C18—Fe2—C20—C1681.10 (19)
C4—N1—C3—C2179.8 (2)C19—Fe2—C20—C16118.7 (2)
Ni—N1—C3—C22.9 (3)C13—Fe2—C20—C16166.96 (17)
C4—N1—C3—C91.0 (3)O2—C8—C21—C2515.5 (3)
Ni—N1—C3—C9178.32 (16)C7—C8—C21—C25166.1 (2)
C1—C2—C3—N10.9 (4)O2—C8—C21—C22162.9 (2)
C1—C2—C3—C9177.9 (2)C7—C8—C21—C2215.5 (3)
C3—N1—C4—C5178.1 (2)O2—C8—C21—Fe1105.9 (2)
Ni—N1—C4—C54.3 (2)C7—C8—C21—Fe175.7 (3)
C6—N2—C5—C4176.6 (2)C26—Fe1—C21—C25114.55 (16)
Ni—N2—C5—C45.5 (2)C22—Fe1—C21—C25119.0 (2)
N1—C4—C5—N26.0 (3)C27—Fe1—C21—C25157.26 (16)
C5—N2—C6—C7178.4 (2)C30—Fe1—C21—C2573.25 (18)
Ni—N2—C6—C70.7 (3)C28—Fe1—C21—C25168.9 (2)
C5—N2—C6—C102.4 (3)C24—Fe1—C21—C2537.57 (15)
Ni—N2—C6—C10179.83 (16)C29—Fe1—C21—C2541.5 (4)
N2—C6—C7—C81.0 (4)C23—Fe1—C21—C2581.24 (15)
C10—C6—C7—C8179.8 (2)C26—Fe1—C21—C22126.40 (16)
Ni—O2—C8—C70.2 (3)C27—Fe1—C21—C2283.70 (17)
Ni—O2—C8—C21178.16 (14)C30—Fe1—C21—C22167.71 (15)
C6—C7—C8—O20.7 (4)C25—Fe1—C21—C22119.0 (2)
C6—C7—C8—C21177.5 (2)C28—Fe1—C21—C2249.9 (3)
O1—C1—C11—C1211.6 (3)C24—Fe1—C21—C2281.47 (15)
C2—C1—C11—C12170.5 (2)C29—Fe1—C21—C22160.5 (3)
O1—C1—C11—C15166.9 (2)C23—Fe1—C21—C2237.80 (14)
C2—C1—C11—C1511.1 (4)C26—Fe1—C21—C84.9 (2)
O1—C1—C11—Fe2101.6 (2)C22—Fe1—C21—C8121.5 (3)
C2—C1—C11—Fe280.4 (3)C27—Fe1—C21—C837.8 (2)
C16—Fe2—C11—C12158.17 (16)C30—Fe1—C21—C846.2 (2)
C15—Fe2—C11—C12118.9 (2)C25—Fe1—C21—C8119.5 (3)
C17—Fe2—C11—C12116.10 (16)C28—Fe1—C21—C871.6 (3)
C20—Fe2—C11—C12168.4 (3)C24—Fe1—C21—C8157.1 (2)
C14—Fe2—C11—C1280.96 (15)C29—Fe1—C21—C878.0 (4)
C18—Fe2—C11—C1275.07 (17)C23—Fe1—C21—C8159.3 (2)
C19—Fe2—C11—C1243.1 (3)C25—C21—C22—C230.9 (3)
C13—Fe2—C11—C1237.38 (14)C8—C21—C22—C23177.7 (2)
C16—Fe2—C11—C1582.90 (18)Fe1—C21—C22—C2360.13 (16)
C17—Fe2—C11—C15124.97 (16)C25—C21—C22—Fe159.20 (16)
C12—Fe2—C11—C15118.9 (2)C8—C21—C22—Fe1122.2 (2)
C20—Fe2—C11—C1549.5 (3)C26—Fe1—C22—C23167.58 (16)
C14—Fe2—C11—C1537.97 (15)C27—Fe1—C22—C23125.52 (16)
C18—Fe2—C11—C15166.00 (16)C30—Fe1—C22—C23156.9 (3)
C19—Fe2—C11—C15162.1 (3)C25—Fe1—C22—C2380.83 (15)
C13—Fe2—C11—C1581.55 (16)C21—Fe1—C22—C23118.7 (2)
C16—Fe2—C11—C139.0 (2)C28—Fe1—C22—C2382.39 (17)
C15—Fe2—C11—C1121.9 (3)C24—Fe1—C22—C2337.25 (14)
C17—Fe2—C11—C13.1 (2)C29—Fe1—C22—C2347.0 (3)
C12—Fe2—C11—C1119.2 (3)C26—Fe1—C22—C2173.74 (18)
C20—Fe2—C11—C172.4 (3)C27—Fe1—C22—C21115.79 (15)
C14—Fe2—C11—C1159.9 (2)C30—Fe1—C22—C2138.2 (4)
C18—Fe2—C11—C144.1 (2)C25—Fe1—C22—C2137.86 (13)
C19—Fe2—C11—C176.0 (4)C28—Fe1—C22—C21158.92 (14)
C13—Fe2—C11—C1156.5 (2)C24—Fe1—C22—C2181.44 (15)
C15—C11—C12—C130.4 (3)C29—Fe1—C22—C21165.7 (2)
C1—C11—C12—C13178.3 (2)C23—Fe1—C22—C21118.7 (2)
Fe2—C11—C12—C1359.48 (17)C21—C22—C23—C240.8 (3)
C15—C11—C12—Fe259.07 (16)Fe1—C22—C23—C2459.01 (17)
C1—C11—C12—Fe2122.2 (2)C21—C22—C23—Fe159.85 (16)
C16—Fe2—C12—C13170.5 (3)C26—Fe1—C23—C2240.6 (4)
C15—Fe2—C12—C1381.45 (16)C27—Fe1—C23—C2275.16 (18)
C17—Fe2—C12—C13158.43 (16)C30—Fe1—C23—C22165.5 (2)
C11—Fe2—C12—C13119.5 (2)C25—Fe1—C23—C2282.47 (15)
C20—Fe2—C12—C1346.7 (4)C21—Fe1—C23—C2238.30 (14)
C14—Fe2—C12—C1337.50 (15)C28—Fe1—C23—C22116.63 (15)
C18—Fe2—C12—C13116.92 (16)C24—Fe1—C23—C22119.9 (2)
C19—Fe2—C12—C1376.11 (18)C29—Fe1—C23—C22159.29 (14)
C16—Fe2—C12—C1151.0 (3)C26—Fe1—C23—C24160.4 (4)
C15—Fe2—C12—C1138.08 (14)C22—Fe1—C23—C24119.9 (2)
C17—Fe2—C12—C1182.04 (17)C27—Fe1—C23—C24164.98 (15)
C20—Fe2—C12—C11166.2 (3)C30—Fe1—C23—C2445.6 (3)
C14—Fe2—C12—C1182.03 (15)C25—Fe1—C23—C2437.40 (14)
C18—Fe2—C12—C11123.54 (14)C21—Fe1—C23—C2481.56 (15)
C19—Fe2—C12—C11164.36 (13)C28—Fe1—C23—C24123.51 (15)
C13—Fe2—C12—C11119.5 (2)C29—Fe1—C23—C2480.84 (16)
C11—C12—C13—C140.1 (3)C22—C23—C24—C250.4 (3)
Fe2—C12—C13—C1459.14 (17)Fe1—C23—C24—C2559.14 (17)
C11—C12—C13—Fe259.21 (16)C22—C23—C24—Fe158.72 (17)
C16—Fe2—C13—C12166.8 (3)C26—Fe1—C24—C2548.9 (3)
C15—Fe2—C13—C1282.01 (16)C22—Fe1—C24—C2582.31 (16)
C17—Fe2—C13—C1248.1 (3)C27—Fe1—C24—C25166.8 (3)
C11—Fe2—C13—C1237.74 (14)C30—Fe1—C24—C2581.49 (18)
C20—Fe2—C13—C12163.17 (15)C21—Fe1—C24—C2537.98 (15)
C14—Fe2—C13—C12119.4 (2)C28—Fe1—C24—C25163.82 (15)
C18—Fe2—C13—C1280.41 (17)C29—Fe1—C24—C25123.45 (16)
C19—Fe2—C13—C12122.50 (15)C23—Fe1—C24—C25119.6 (2)
C16—Fe2—C13—C1447.4 (4)C26—Fe1—C24—C23168.5 (2)
C15—Fe2—C13—C1437.38 (15)C22—Fe1—C24—C2337.30 (14)
C17—Fe2—C13—C14167.5 (2)C27—Fe1—C24—C2347.2 (4)
C11—Fe2—C13—C1481.65 (16)C30—Fe1—C24—C23158.90 (14)
C12—Fe2—C13—C14119.4 (2)C25—Fe1—C24—C23119.6 (2)
C20—Fe2—C13—C1477.44 (18)C21—Fe1—C24—C2381.63 (15)
C18—Fe2—C13—C14160.20 (15)C28—Fe1—C24—C2376.57 (18)
C19—Fe2—C13—C14118.11 (15)C29—Fe1—C24—C23116.94 (15)
C12—C13—C14—C150.3 (3)C23—C24—C25—C210.2 (3)
Fe2—C13—C14—C1558.77 (18)Fe1—C24—C25—C2159.42 (16)
C12—C13—C14—Fe259.07 (17)C23—C24—C25—Fe159.25 (17)
C16—Fe2—C14—C1575.66 (19)C22—C21—C25—C240.7 (3)
C17—Fe2—C14—C1541.1 (4)C8—C21—C25—C24178.0 (2)
C11—Fe2—C14—C1538.26 (15)Fe1—C21—C25—C2459.65 (17)
C12—Fe2—C14—C1582.45 (16)C22—C21—C25—Fe158.98 (15)
C20—Fe2—C14—C15117.59 (16)C8—C21—C25—Fe1122.4 (2)
C18—Fe2—C14—C15164.7 (2)C26—Fe1—C25—C24157.32 (17)
C19—Fe2—C14—C15160.19 (15)C22—Fe1—C25—C2481.08 (17)
C13—Fe2—C14—C15120.0 (2)C27—Fe1—C25—C24171.2 (2)
C16—Fe2—C14—C13164.31 (16)C30—Fe1—C25—C24115.44 (17)
C15—Fe2—C14—C13120.0 (2)C21—Fe1—C25—C24119.1 (2)
C17—Fe2—C14—C13161.1 (4)C28—Fe1—C25—C2446.6 (4)
C11—Fe2—C14—C1381.76 (15)C29—Fe1—C25—C2475.33 (19)
C12—Fe2—C14—C1337.58 (14)C23—Fe1—C25—C2437.41 (16)
C20—Fe2—C14—C13122.39 (16)C26—Fe1—C25—C2183.59 (17)
C18—Fe2—C14—C1344.7 (3)C22—Fe1—C25—C2138.01 (14)
C19—Fe2—C14—C1379.78 (17)C27—Fe1—C25—C2152.1 (3)
C13—C14—C15—C110.6 (3)C30—Fe1—C25—C21125.47 (15)
Fe2—C14—C15—C1159.69 (16)C28—Fe1—C25—C21165.7 (3)
C13—C14—C15—Fe259.14 (18)C24—Fe1—C25—C21119.1 (2)
C12—C11—C15—C140.6 (3)C29—Fe1—C25—C21165.58 (14)
C1—C11—C15—C14178.1 (2)C23—Fe1—C25—C2181.68 (15)
Fe2—C11—C15—C1459.81 (17)C22—Fe1—C26—C30165.41 (15)
C12—C11—C15—Fe259.22 (16)C27—Fe1—C26—C30118.8 (2)
C1—C11—C15—Fe2122.1 (2)C25—Fe1—C26—C3080.76 (18)
C16—Fe2—C15—C14124.85 (18)C21—Fe1—C26—C30123.90 (16)
C17—Fe2—C15—C14166.66 (17)C28—Fe1—C26—C3080.96 (17)
C11—Fe2—C15—C14118.7 (2)C24—Fe1—C26—C3046.6 (3)
C12—Fe2—C15—C1480.73 (17)C29—Fe1—C26—C3037.42 (15)
C20—Fe2—C15—C1481.67 (19)C23—Fe1—C26—C30162.6 (3)
C18—Fe2—C15—C14159.1 (3)C22—Fe1—C26—C2775.75 (19)
C19—Fe2—C15—C1446.7 (3)C30—Fe1—C26—C27118.8 (2)
C13—Fe2—C15—C1437.09 (15)C25—Fe1—C26—C27160.39 (15)
C16—Fe2—C15—C11116.47 (16)C21—Fe1—C26—C27117.26 (16)
C17—Fe2—C15—C1174.66 (19)C28—Fe1—C26—C2737.89 (15)
C12—Fe2—C15—C1137.95 (14)C24—Fe1—C26—C27165.4 (2)
C20—Fe2—C15—C11159.66 (15)C29—Fe1—C26—C2781.42 (16)
C14—Fe2—C15—C11118.7 (2)C23—Fe1—C26—C2743.8 (5)
C18—Fe2—C15—C1140.4 (4)C30—C26—C27—C280.2 (3)
C19—Fe2—C15—C11165.3 (2)Fe1—C26—C27—C2859.73 (18)
C13—Fe2—C15—C1181.58 (15)C30—C26—C27—Fe159.96 (18)
C15—Fe2—C16—C17123.62 (17)C26—Fe1—C27—C28118.8 (2)
C11—Fe2—C16—C1780.06 (19)C22—Fe1—C27—C28116.19 (16)
C12—Fe2—C16—C1743.5 (3)C30—Fe1—C27—C2881.01 (17)
C20—Fe2—C16—C17119.0 (2)C25—Fe1—C27—C28163.0 (2)
C14—Fe2—C16—C17165.57 (16)C21—Fe1—C27—C28159.91 (14)
C18—Fe2—C16—C1737.51 (16)C24—Fe1—C27—C2837.8 (5)
C19—Fe2—C16—C1781.28 (17)C29—Fe1—C27—C2837.62 (15)
C13—Fe2—C16—C17157.9 (3)C23—Fe1—C27—C2874.52 (19)
C15—Fe2—C16—C20117.38 (17)C22—Fe1—C27—C26125.06 (16)
C17—Fe2—C16—C20119.0 (2)C30—Fe1—C27—C2637.74 (16)
C11—Fe2—C16—C20160.94 (15)C25—Fe1—C27—C2644.2 (3)
C12—Fe2—C16—C20162.5 (2)C21—Fe1—C27—C2681.33 (18)
C14—Fe2—C16—C2075.4 (2)C28—Fe1—C27—C26118.8 (2)
C18—Fe2—C16—C2081.49 (17)C24—Fe1—C27—C26156.5 (4)
C19—Fe2—C16—C2037.72 (16)C29—Fe1—C27—C2681.14 (17)
C13—Fe2—C16—C2038.9 (5)C23—Fe1—C27—C26166.72 (16)
C20—C16—C17—C180.1 (3)C26—C27—C28—C290.3 (3)
Fe2—C16—C17—C1859.76 (19)Fe1—C27—C28—C2959.68 (17)
C20—C16—C17—Fe259.89 (19)C26—C27—C28—Fe159.36 (18)
C15—Fe2—C17—C1676.5 (2)C26—Fe1—C28—C2980.86 (17)
C11—Fe2—C17—C16118.16 (17)C22—Fe1—C28—C29158.01 (15)
C12—Fe2—C17—C16161.03 (16)C27—Fe1—C28—C29118.9 (2)
C20—Fe2—C17—C1638.00 (17)C30—Fe1—C28—C2937.10 (16)
C14—Fe2—C17—C1644.6 (4)C25—Fe1—C28—C2937.9 (4)
C18—Fe2—C17—C16119.1 (2)C21—Fe1—C28—C29166.0 (2)
C19—Fe2—C17—C1681.59 (18)C24—Fe1—C28—C2973.34 (19)
C13—Fe2—C17—C16164.9 (2)C23—Fe1—C28—C29115.15 (16)
C16—Fe2—C17—C18119.1 (2)C26—Fe1—C28—C2738.04 (17)
C15—Fe2—C17—C18164.39 (15)C22—Fe1—C28—C2783.09 (19)
C11—Fe2—C17—C18122.74 (16)C30—Fe1—C28—C2781.80 (18)
C12—Fe2—C17—C1879.87 (18)C25—Fe1—C28—C27156.8 (3)
C20—Fe2—C17—C1881.10 (17)C21—Fe1—C28—C2747.1 (3)
C14—Fe2—C17—C18163.7 (3)C24—Fe1—C28—C27167.76 (17)
C19—Fe2—C17—C1837.51 (16)C29—Fe1—C28—C27118.9 (2)
C13—Fe2—C17—C1845.8 (3)C23—Fe1—C28—C27125.94 (17)
C16—C17—C18—C190.0 (3)C27—C28—C29—C300.3 (3)
Fe2—C17—C18—C1959.37 (18)Fe1—C28—C29—C3059.15 (17)
C16—C17—C18—Fe259.34 (19)C27—C28—C29—Fe159.43 (17)
C16—Fe2—C18—C1737.75 (18)C26—Fe1—C29—C3037.73 (17)
C15—Fe2—C18—C1745.0 (4)C22—Fe1—C29—C30169.9 (2)
C11—Fe2—C18—C1776.0 (2)C27—Fe1—C29—C3081.90 (18)
C12—Fe2—C18—C17117.35 (17)C25—Fe1—C29—C3073.58 (19)
C20—Fe2—C18—C1782.00 (19)C21—Fe1—C29—C3041.8 (4)
C14—Fe2—C18—C17168.9 (2)C28—Fe1—C29—C30119.8 (2)
C19—Fe2—C18—C17119.5 (2)C24—Fe1—C29—C30114.64 (17)
C13—Fe2—C18—C17159.30 (17)C23—Fe1—C29—C30156.75 (16)
C16—Fe2—C18—C1981.74 (18)C26—Fe1—C29—C2882.11 (18)
C15—Fe2—C18—C19164.5 (3)C22—Fe1—C29—C2850.0 (3)
C17—Fe2—C18—C19119.5 (2)C27—Fe1—C29—C2837.94 (17)
C11—Fe2—C18—C19164.50 (15)C30—Fe1—C29—C28119.8 (2)
C12—Fe2—C18—C19123.16 (16)C25—Fe1—C29—C28166.59 (15)
C20—Fe2—C18—C1937.50 (16)C21—Fe1—C29—C28161.7 (3)
C14—Fe2—C18—C1949.5 (3)C24—Fe1—C29—C28125.53 (16)
C13—Fe2—C18—C1981.21 (18)C23—Fe1—C29—C2883.41 (18)
C17—C18—C19—C200.1 (3)C28—C29—C30—C260.1 (3)
Fe2—C18—C19—C2059.37 (18)Fe1—C29—C30—C2659.39 (18)
C17—C18—C19—Fe259.29 (18)C28—C29—C30—Fe159.25 (17)
C16—Fe2—C19—C2038.20 (18)C27—C26—C30—C290.1 (3)
C15—Fe2—C19—C2048.8 (3)Fe1—C26—C30—C2959.81 (18)
C17—Fe2—C19—C2081.98 (19)C27—C26—C30—Fe159.87 (18)
C11—Fe2—C19—C20161.7 (3)C26—Fe1—C30—C29119.2 (2)
C12—Fe2—C19—C20165.65 (16)C22—Fe1—C30—C29164.8 (3)
C14—Fe2—C19—C2082.46 (19)C27—Fe1—C30—C2981.14 (17)
C18—Fe2—C19—C20119.3 (2)C25—Fe1—C30—C29124.51 (15)
C13—Fe2—C19—C20124.36 (17)C21—Fe1—C30—C29165.32 (14)
C16—Fe2—C19—C1881.08 (19)C28—Fe1—C30—C2937.22 (15)
C15—Fe2—C19—C18168.1 (3)C24—Fe1—C30—C2982.53 (17)
C17—Fe2—C19—C1837.30 (17)C23—Fe1—C30—C2950.5 (3)
C11—Fe2—C19—C1842.4 (4)C22—Fe1—C30—C2645.7 (4)
C12—Fe2—C19—C1875.07 (19)C27—Fe1—C30—C2638.02 (17)
C20—Fe2—C19—C18119.3 (2)C25—Fe1—C30—C26116.33 (17)
C14—Fe2—C19—C18158.26 (17)C21—Fe1—C30—C2675.51 (19)
C13—Fe2—C19—C18116.36 (17)C28—Fe1—C30—C2681.95 (18)
C18—C19—C20—C160.2 (3)C24—Fe1—C30—C26158.31 (16)
Fe2—C19—C20—C1659.26 (18)C29—Fe1—C30—C26119.2 (2)
C18—C19—C20—Fe259.41 (18)C23—Fe1—C30—C26169.7 (2)
C17—C16—C20—C190.2 (3)
 

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