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The real crystal structure of the (NbSe4)10/3I charge density wave (CDW) compound is studied by simulation of the X-ray diffuse scattering. The average structure of the low-temperature twinned phase is determined and the phase transition is attributed to the formation of a CDW. The diffuse streaking, present in X-ray diffraction patterns above and below the transition at T = 282 K, is shown to be a projection of diffuse concentric rings perpendicular to the c* direction. The simulated patterns, based on a mismatch model between infinite NbSe4 chains, correlated by I atoms, are in good accordance with the experimental patterns. In addition to the experiments, the electronic properties of the high- and the low-temperature phases are calculated with the extended Hückel tight-binding method. The Fermi surfaces of the average structures above and below the phase transition appear very similar. Their shapes support a nesting instability and a CDW formation. The weak incommensurate CDW satellites, present below the phase transition, are at 100 K properly described by a modulation wavevector q = [0.06 (1), 0, 0.55 (1)].

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S2052519213010336/wf5106sup1.cif
Contains datablocks 300K, 100K

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S2052519213010336/wf5106300Ksup2.hkl
Contains datablock shelxl

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S2052519213010336/wf5106100Ksup3.hkl
Contains datablock shelxl

pdf

Portable Document Format (PDF) file https://doi.org/10.1107/S2052519213010336/wf5106sup4.pdf
Supplementary material contains additional figures of diffuse scattering and Nb chains in the superstructure cell

Computing details top

For both compounds, data collection: CrysAlis CCD, Oxford Diffraction Ltd., Version 1.171.32.29; cell refinement: CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.32.29; data reduction: CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.32.29; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008).

(300K) top
Crystal data top
Nb10Se40·3(I)F(000) = 3858
Mr = 4468.20Dx = 5.192 Mg m3
Tetragonal, P4/mccMo Kα radiation, λ = 0.71073 Å
Hall symbol: -P 4 2cµ = 29.03 mm1
a = 9.4644 (6) ÅT = 300 K
c = 31.9063 (19) ÅNeedle, black
V = 2858.0 (3) Å30.38 × 0.05 × 0.05 mm
Z = 2
Data collection top
Oxford Diffraction Diffractometer with Sapphire3 detector1307 independent reflections
Radiation source: fine-focus sealed tube931 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.067
Detector resolution: 16.0328 pixels mm-1θmax = 25.1°, θmin = 3.0°
ω – scanh = 1011
Absorption correction: multi-scan
CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.32.29 Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.
k = 1110
Tmin = 0.032, Tmax = 0.325l = 3238
16110 measured reflections
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.032 w = 1/[σ2(Fo2) + (0.0425P)2 + 5.1013P]
where P = (Fo2 + 2Fc2)/3
wR(F2) = 0.081(Δ/σ)max = 0.001
S = 1.03Δρmax = 2.59 e Å3
1307 reflectionsΔρmin = 0.93 e Å3
68 parametersExtinction correction: SHELXL, Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4
0 restraintsExtinction coefficient: 0.00012 (2)
Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
Nb10.00000.50000.25000.0243 (3)
Nb20.00000.50000.45059 (3)0.0256 (3)
Nb30.00000.50000.34927 (3)0.0260 (3)
Se10.12728 (8)0.31603 (8)0.40284 (2)0.0277 (2)
Se20.19141 (8)0.37854 (8)0.29652 (2)0.0283 (2)
Se30.03676 (8)0.72096 (8)0.30257 (2)0.0290 (2)
Se40.21663 (8)0.55007 (8)0.39673 (2)0.0287 (2)
Se50.10804 (12)0.69961 (11)0.50000.0307 (3)
Se60.22296 (11)0.48033 (12)0.50000.0294 (3)
I10.00000.00000.42070 (5)0.0593 (4)
I20.50000.50000.25000.0906 (9)
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Nb10.0159 (7)0.0154 (7)0.0415 (9)0.0000.0000.000
Nb20.0157 (5)0.0164 (5)0.0446 (7)0.0004 (3)0.0000.000
Nb30.0158 (5)0.0166 (5)0.0456 (6)0.0007 (4)0.0000.000
Se10.0197 (5)0.0180 (4)0.0455 (5)0.0018 (3)0.0001 (3)0.0003 (3)
Se20.0182 (5)0.0219 (5)0.0447 (5)0.0033 (3)0.0002 (3)0.0001 (3)
Se30.0230 (5)0.0178 (4)0.0462 (5)0.0024 (3)0.0008 (3)0.0003 (3)
Se40.0187 (4)0.0209 (4)0.0466 (5)0.0022 (3)0.0003 (3)0.0013 (3)
Se50.0258 (7)0.0184 (6)0.0480 (7)0.0044 (5)0.0000.000
Se60.0187 (6)0.0257 (7)0.0437 (7)0.0006 (5)0.0000.000
I10.0247 (4)0.0247 (4)0.1284 (12)0.0000.0000.000
I20.0249 (6)0.0249 (6)0.222 (3)0.0000.0000.000
Geometric parameters (Å, º) top
Nb1—Se2i2.6090 (8)Nb2—Se42.7170 (9)
Nb1—Se2ii2.6090 (7)Nb2—Nb2iv3.1529 (18)
Nb1—Se2iii2.6090 (7)Nb2—Nb33.2327 (12)
Nb1—Se22.6090 (8)Nb3—Se3i2.5913 (9)
Nb1—Se3iii2.7032 (8)Nb3—Se32.5913 (9)
Nb1—Se32.7032 (8)Nb3—Se4i2.5924 (10)
Nb1—Se3ii2.7032 (8)Nb3—Se42.5924 (10)
Nb1—Se3i2.7032 (8)Nb3—Se1i2.7210 (10)
Nb1—Nb3ii3.1674 (10)Nb3—Se12.7210 (10)
Nb1—Nb33.1674 (10)Nb3—Se22.7270 (10)
Nb2—Se12.6084 (9)Nb3—Se2i2.7270 (10)
Nb2—Se1i2.6084 (9)Se1—Se42.3789 (11)
Nb2—Se6iv2.6406 (10)Se2—Se3i2.3638 (11)
Nb2—Se62.6406 (10)Se3—Se2i2.3638 (11)
Nb2—Se52.6646 (10)Se5—Se62.3431 (16)
Nb2—Se5iv2.6646 (10)Se5—Nb2iv2.6646 (10)
Nb2—Se4i2.7170 (9)Se6—Nb2iv2.6406 (10)
Se2i—Nb1—Se2ii92.04 (3)Se5—Nb2—Nb2iv53.73 (2)
Se2i—Nb1—Se2iii127.71 (4)Se5iv—Nb2—Nb2iv53.73 (2)
Se2ii—Nb1—Se2iii110.65 (3)Se4i—Nb2—Nb2iv129.24 (2)
Se2i—Nb1—Se2110.65 (3)Se4—Nb2—Nb2iv129.24 (2)
Se2ii—Nb1—Se2127.71 (4)Se1—Nb2—Nb354.26 (2)
Se2iii—Nb1—Se292.04 (3)Se1i—Nb2—Nb354.26 (2)
Se2i—Nb1—Se3iii141.56 (2)Se6iv—Nb2—Nb3126.66 (2)
Se2ii—Nb1—Se3iii52.81 (2)Se6—Nb2—Nb3126.66 (2)
Se2iii—Nb1—Se3iii84.18 (3)Se5—Nb2—Nb3126.27 (2)
Se2—Nb1—Se3iii85.57 (2)Se5iv—Nb2—Nb3126.27 (2)
Se2i—Nb1—Se352.81 (2)Se4i—Nb2—Nb350.76 (2)
Se2ii—Nb1—Se3141.56 (2)Se4—Nb2—Nb350.76 (2)
Se2iii—Nb1—Se385.57 (2)Nb2iv—Nb2—Nb3180.0
Se2—Nb1—Se384.18 (3)Se3i—Nb3—Se3109.79 (5)
Se3iii—Nb1—Se3165.21 (3)Se3i—Nb3—Se4i94.71 (2)
Se2i—Nb1—Se3ii85.57 (2)Se3—Nb3—Se4i126.13 (3)
Se2ii—Nb1—Se3ii84.18 (3)Se3i—Nb3—Se4126.13 (3)
Se2iii—Nb1—Se3ii52.81 (2)Se3—Nb3—Se494.71 (2)
Se2—Nb1—Se3ii141.56 (2)Se4i—Nb3—Se4108.53 (5)
Se3iii—Nb1—Se3ii103.30 (3)Se3i—Nb3—Se1i144.90 (2)
Se3—Nb1—Se3ii78.64 (3)Se3—Nb3—Se1i84.51 (2)
Se2i—Nb1—Se3i84.18 (3)Se4i—Nb3—Se1i53.13 (3)
Se2ii—Nb1—Se3i85.57 (2)Se4—Nb3—Se1i82.32 (3)
Se2iii—Nb1—Se3i141.56 (2)Se3i—Nb3—Se184.51 (2)
Se2—Nb1—Se3i52.81 (2)Se3—Nb3—Se1144.90 (2)
Se3iii—Nb1—Se3i78.64 (3)Se4i—Nb3—Se182.32 (3)
Se3—Nb1—Se3i103.30 (3)Se4—Nb3—Se153.13 (3)
Se3ii—Nb1—Se3i165.21 (3)Se1i—Nb3—Se1102.18 (4)
Se2i—Nb1—Nb3ii124.675 (17)Se3i—Nb3—Se252.70 (3)
Se2ii—Nb1—Nb3ii55.325 (16)Se3—Nb3—Se284.03 (3)
Se2iii—Nb1—Nb3ii55.325 (16)Se4i—Nb3—Se2143.98 (2)
Se2—Nb1—Nb3ii124.675 (16)Se4—Nb3—Se284.96 (2)
Se3iii—Nb1—Nb3ii51.651 (16)Se1i—Nb3—Se2162.09 (2)
Se3—Nb1—Nb3ii128.349 (16)Se1—Nb3—Se279.85 (2)
Se3ii—Nb1—Nb3ii51.651 (16)Se3i—Nb3—Se2i84.03 (3)
Se3i—Nb1—Nb3ii128.349 (16)Se3—Nb3—Se2i52.70 (3)
Se2i—Nb1—Nb355.325 (17)Se4i—Nb3—Se2i84.96 (2)
Se2ii—Nb1—Nb3124.675 (16)Se4—Nb3—Se2i143.98 (2)
Se2iii—Nb1—Nb3124.675 (16)Se1i—Nb3—Se2i79.85 (2)
Se2—Nb1—Nb355.325 (16)Se1—Nb3—Se2i162.09 (2)
Se3iii—Nb1—Nb3128.349 (16)Se2—Nb3—Se2i103.77 (4)
Se3—Nb1—Nb351.651 (16)Se3i—Nb3—Nb154.89 (2)
Se3ii—Nb1—Nb3128.349 (16)Se3—Nb3—Nb154.89 (2)
Se3i—Nb1—Nb351.651 (16)Se4i—Nb3—Nb1125.74 (2)
Nb3ii—Nb1—Nb3180.0Se4—Nb3—Nb1125.74 (2)
Se1—Nb2—Se1i108.52 (5)Se1i—Nb3—Nb1128.91 (2)
Se1—Nb2—Se6iv139.89 (3)Se1—Nb3—Nb1128.91 (2)
Se1i—Nb2—Se6iv86.13 (2)Se2—Nb3—Nb151.89 (2)
Se1—Nb2—Se686.13 (2)Se2i—Nb3—Nb151.89 (2)
Se1i—Nb2—Se6139.89 (3)Se3i—Nb3—Nb2125.11 (2)
Se6iv—Nb2—Se6106.69 (4)Se3—Nb3—Nb2125.11 (2)
Se1—Nb2—Se5129.91 (3)Se4i—Nb3—Nb254.26 (2)
Se1i—Nb2—Se592.84 (3)Se4—Nb3—Nb254.26 (2)
Se6iv—Nb2—Se584.46 (4)Se1i—Nb3—Nb251.09 (2)
Se6—Nb2—Se552.42 (4)Se1—Nb3—Nb251.09 (2)
Se1—Nb2—Se5iv92.84 (3)Se2—Nb3—Nb2128.11 (2)
Se1i—Nb2—Se5iv129.91 (3)Se2i—Nb3—Nb2128.11 (2)
Se6iv—Nb2—Se5iv52.42 (4)Nb1—Nb3—Nb2180.0
Se6—Nb2—Se5iv84.46 (4)Se4—Se1—Nb265.83 (3)
Se5—Nb2—Se5iv107.45 (4)Se4—Se1—Nb360.66 (3)
Se1—Nb2—Se4i82.10 (3)Nb2—Se1—Nb374.65 (3)
Se1i—Nb2—Se4i53.02 (3)Se3i—Se2—Nb165.64 (3)
Se6iv—Nb2—Se4i77.70 (2)Se3i—Se2—Nb360.70 (3)
Se6—Nb2—Se4i165.55 (3)Nb1—Se2—Nb372.79 (3)
Se5—Nb2—Se4i141.95 (3)Se2i—Se3—Nb366.60 (3)
Se5iv—Nb2—Se4i87.76 (2)Se2i—Se3—Nb161.55 (3)
Se1—Nb2—Se453.02 (3)Nb3—Se3—Nb173.45 (3)
Se1i—Nb2—Se482.10 (3)Se1—Se4—Nb366.21 (3)
Se6iv—Nb2—Se4165.55 (3)Se1—Se4—Nb261.15 (2)
Se6—Nb2—Se477.70 (2)Nb3—Se4—Nb274.97 (3)
Se5—Nb2—Se487.76 (2)Se6—Se5—Nb263.26 (3)
Se5iv—Nb2—Se4141.95 (3)Se6—Se5—Nb2iv63.26 (3)
Se4i—Nb2—Se4101.52 (4)Nb2—Se5—Nb2iv72.55 (4)
Se1—Nb2—Nb2iv125.74 (2)Se5—Se6—Nb2iv64.32 (3)
Se1i—Nb2—Nb2iv125.74 (2)Se5—Se6—Nb264.32 (3)
Se6iv—Nb2—Nb2iv53.34 (2)Nb2iv—Se6—Nb273.31 (4)
Se6—Nb2—Nb2iv53.34 (2)
Se2i—Nb1—Nb3—Se3i112.95 (3)Se4i—Nb2—Se1—Se4110.91 (4)
Se2ii—Nb1—Nb3—Se3i48.16 (3)Nb2iv—Nb2—Se1—Se4115.70 (2)
Se2iii—Nb1—Nb3—Se3i131.84 (3)Nb3—Nb2—Se1—Se464.30 (2)
Se2—Nb1—Nb3—Se3i67.05 (3)Se1i—Nb2—Se1—Nb30.0
Se3iii—Nb1—Nb3—Se3i18.89 (4)Se6iv—Nb2—Se1—Nb3106.70 (5)
Se3—Nb1—Nb3—Se3i180.0Se6—Nb2—Se1—Nb3141.80 (3)
Se3ii—Nb1—Nb3—Se3i161.11 (4)Se5—Nb2—Se1—Nb3110.39 (4)
Nb3ii—Nb1—Nb3—Se3i171 (7)Se5iv—Nb2—Se1—Nb3133.96 (3)
Se2i—Nb1—Nb3—Se367.05 (3)Se4i—Nb2—Se1—Nb346.61 (2)
Se2ii—Nb1—Nb3—Se3131.84 (3)Se4—Nb2—Se1—Nb364.30 (2)
Se2iii—Nb1—Nb3—Se348.16 (3)Nb2iv—Nb2—Se1—Nb3180.0
Se2—Nb1—Nb3—Se3112.95 (3)Se3i—Nb3—Se1—Se4144.34 (3)
Se3iii—Nb1—Nb3—Se3161.11 (4)Se3—Nb3—Se1—Se427.29 (6)
Se3ii—Nb1—Nb3—Se318.89 (4)Se4i—Nb3—Se1—Se4120.13 (4)
Se3i—Nb1—Nb3—Se3180.0Se1i—Nb3—Se1—Se470.56 (3)
Nb3ii—Nb1—Nb3—Se39 (7)Se2—Nb3—Se1—Se491.30 (3)
Se2i—Nb1—Nb3—Se4i45.41 (3)Se2i—Nb3—Se1—Se4165.24 (13)
Se2ii—Nb1—Nb3—Se4i19.38 (3)Nb1—Nb3—Se1—Se4109.44 (3)
Se2iii—Nb1—Nb3—Se4i160.62 (3)Nb2—Nb3—Se1—Se470.56 (3)
Se2—Nb1—Nb3—Se4i134.59 (3)Se3i—Nb3—Se1—Nb2145.10 (2)
Se3iii—Nb1—Nb3—Se4i86.43 (3)Se3—Nb3—Se1—Nb297.86 (6)
Se3—Nb1—Nb3—Se4i112.46 (3)Se4i—Nb3—Se1—Nb249.57 (2)
Se3ii—Nb1—Nb3—Se4i93.57 (3)Se4—Nb3—Se1—Nb270.56 (3)
Se3i—Nb1—Nb3—Se4i67.54 (3)Se1i—Nb3—Se1—Nb20.0
Nb3ii—Nb1—Nb3—Se4i103 (7)Se2—Nb3—Se1—Nb2161.86 (2)
Se2i—Nb1—Nb3—Se4134.59 (3)Se2i—Nb3—Se1—Nb294.68 (12)
Se2ii—Nb1—Nb3—Se4160.62 (3)Nb1—Nb3—Se1—Nb2180.0
Se2iii—Nb1—Nb3—Se419.38 (3)Se2i—Nb1—Se2—Se3i65.03 (2)
Se2—Nb1—Nb3—Se445.41 (3)Se2ii—Nb1—Se2—Se3i44.82 (2)
Se3iii—Nb1—Nb3—Se493.57 (3)Se2iii—Nb1—Se2—Se3i163.09 (3)
Se3—Nb1—Nb3—Se467.54 (3)Se3iii—Nb1—Se2—Se3i79.10 (4)
Se3ii—Nb1—Nb3—Se486.43 (3)Se3—Nb1—Se2—Se3i111.58 (3)
Se3i—Nb1—Nb3—Se4112.46 (3)Se3ii—Nb1—Se2—Se3i175.028 (16)
Nb3ii—Nb1—Nb3—Se477 (7)Nb3ii—Nb1—Se2—Se3i114.97 (2)
Se2i—Nb1—Nb3—Se1i22.92 (3)Nb3—Nb1—Se2—Se3i65.03 (2)
Se2ii—Nb1—Nb3—Se1i87.72 (3)Se2i—Nb1—Se2—Nb30.0
Se2iii—Nb1—Nb3—Se1i92.28 (3)Se2ii—Nb1—Se2—Nb3109.851 (17)
Se2—Nb1—Nb3—Se1i157.08 (3)Se2iii—Nb1—Se2—Nb3131.88 (3)
Se3iii—Nb1—Nb3—Se1i154.77 (3)Se3iii—Nb1—Se2—Nb3144.13 (2)
Se3—Nb1—Nb3—Se1i44.12 (3)Se3—Nb1—Se2—Nb346.54 (2)
Se3ii—Nb1—Nb3—Se1i25.23 (3)Se3ii—Nb1—Se2—Nb3110.00 (3)
Se3i—Nb1—Nb3—Se1i135.88 (3)Se3i—Nb1—Se2—Nb365.03 (2)
Nb3ii—Nb1—Nb3—Se1i35 (7)Nb3ii—Nb1—Se2—Nb3180.0
Se2i—Nb1—Nb3—Se1157.08 (3)Se3—Nb3—Se2—Se3i120.50 (4)
Se2ii—Nb1—Nb3—Se192.28 (3)Se4i—Nb3—Se2—Se3i29.30 (6)
Se2iii—Nb1—Nb3—Se187.72 (3)Se4—Nb3—Se2—Se3i144.21 (3)
Se2—Nb1—Nb3—Se122.92 (3)Se1i—Nb3—Se2—Se3i170.97 (12)
Se3iii—Nb1—Nb3—Se125.23 (3)Se1—Nb3—Se2—Se3i90.81 (3)
Se3—Nb1—Nb3—Se1135.88 (3)Se2i—Nb3—Se2—Se3i71.26 (3)
Se3ii—Nb1—Nb3—Se1154.77 (3)Nb1—Nb3—Se2—Se3i71.26 (3)
Se3i—Nb1—Nb3—Se144.12 (3)Nb2—Nb3—Se2—Se3i108.74 (3)
Nb3ii—Nb1—Nb3—Se1145 (38)Se3i—Nb3—Se2—Nb171.26 (3)
Se2i—Nb1—Nb3—Se2180.0Se3—Nb3—Se2—Nb149.24 (2)
Se2ii—Nb1—Nb3—Se2115.20 (4)Se4i—Nb3—Se2—Nb1100.56 (6)
Se2iii—Nb1—Nb3—Se264.80 (4)Se4—Nb3—Se2—Nb1144.53 (2)
Se3iii—Nb1—Nb3—Se248.16 (3)Se1i—Nb3—Se2—Nb199.71 (12)
Se3—Nb1—Nb3—Se2112.95 (3)Se1—Nb3—Se2—Nb1162.07 (2)
Se3ii—Nb1—Nb3—Se2131.84 (3)Se2i—Nb3—Se2—Nb10.0
Se3i—Nb1—Nb3—Se267.05 (3)Nb2—Nb3—Se2—Nb1180.0
Nb3ii—Nb1—Nb3—Se2122 (7)Se3i—Nb3—Se3—Se2i65.61 (2)
Se2ii—Nb1—Nb3—Se2i64.80 (4)Se4i—Nb3—Se3—Se2i46.15 (4)
Se2iii—Nb1—Nb3—Se2i115.20 (4)Se4—Nb3—Se3—Se2i163.22 (4)
Se2—Nb1—Nb3—Se2i180.0Se1i—Nb3—Se3—Se2i81.42 (3)
Se3iii—Nb1—Nb3—Se2i131.84 (3)Se1—Nb3—Se3—Se2i175.19 (7)
Se3—Nb1—Nb3—Se2i67.05 (3)Se2—Nb3—Se3—Se2i112.37 (4)
Se3ii—Nb1—Nb3—Se2i48.16 (3)Nb1—Nb3—Se3—Se2i65.61 (2)
Se3i—Nb1—Nb3—Se2i112.95 (3)Nb2—Nb3—Se3—Se2i114.39 (2)
Nb3ii—Nb1—Nb3—Se2i58 (7)Se3i—Nb3—Se3—Nb10.0
Se2i—Nb1—Nb3—Nb2122 (17)Se4i—Nb3—Se3—Nb1111.76 (4)
Se2ii—Nb1—Nb3—Nb258 (17)Se4—Nb3—Se3—Nb1131.18 (3)
Se2iii—Nb1—Nb3—Nb2122 (28)Se1i—Nb3—Se3—Nb1147.03 (2)
Se2—Nb1—Nb3—Nb258 (28)Se1—Nb3—Se3—Nb1109.58 (6)
Se3iii—Nb1—Nb3—Nb29 (17)Se2—Nb3—Se3—Nb146.76 (2)
Se3—Nb1—Nb3—Nb2171 (28)Se2i—Nb3—Se3—Nb165.61 (2)
Se3ii—Nb1—Nb3—Nb2171 (42)Nb2—Nb3—Se3—Nb1180.0
Se3i—Nb1—Nb3—Nb29 (17)Se2ii—Nb1—Se3—Se2i27.88 (6)
Nb3ii—Nb1—Nb3—Nb20 (24)Se2iii—Nb1—Se3—Se2i145.99 (3)
Se1—Nb2—Nb3—Se3i44.12 (3)Se2—Nb1—Se3—Se2i121.49 (3)
Se1i—Nb2—Nb3—Se3i135.88 (3)Se3iii—Nb1—Se3—Se2i167.82 (2)
Se6iv—Nb2—Nb3—Se3i85.60 (4)Se3ii—Nb1—Se3—Se2i93.07 (3)
Se6—Nb2—Nb3—Se3i94.40 (4)Se3i—Nb1—Se3—Se2i71.92 (3)
Se5—Nb2—Nb3—Se3i161.02 (4)Nb3ii—Nb1—Se3—Se2i108.08 (3)
Se5iv—Nb2—Nb3—Se3i18.98 (4)Nb3—Nb1—Se3—Se2i71.92 (3)
Se4i—Nb2—Nb3—Se3i67.54 (3)Se2i—Nb1—Se3—Nb371.92 (3)
Se4—Nb2—Nb3—Se3i112.46 (3)Se2ii—Nb1—Se3—Nb399.80 (3)
Nb2iv—Nb2—Nb3—Se3i171 (94)Se2iii—Nb1—Se3—Nb3142.09 (2)
Se1—Nb2—Nb3—Se3135.88 (3)Se2—Nb1—Se3—Nb349.57 (2)
Se1i—Nb2—Nb3—Se344.12 (3)Se3iii—Nb1—Se3—Nb395.89 (8)
Se6iv—Nb2—Nb3—Se394.40 (4)Se3ii—Nb1—Se3—Nb3164.99 (3)
Se6—Nb2—Nb3—Se385.60 (4)Se3i—Nb1—Se3—Nb30.0
Se5—Nb2—Nb3—Se318.98 (4)Nb3ii—Nb1—Se3—Nb3180.0
Se5iv—Nb2—Nb3—Se3161.02 (4)Nb2—Se1—Se4—Nb385.38 (3)
Se4i—Nb2—Nb3—Se3112.46 (3)Nb3—Se1—Se4—Nb285.38 (3)
Se4—Nb2—Nb3—Se367.54 (3)Se3i—Nb3—Se4—Se145.92 (4)
Nb2iv—Nb2—Nb3—Se39 (93)Se3—Nb3—Se4—Se1164.66 (3)
Se1—Nb2—Nb3—Se4i111.66 (3)Se4i—Nb3—Se4—Se164.68 (2)
Se1i—Nb2—Nb3—Se4i68.34 (3)Se1i—Nb3—Se4—Se1111.54 (4)
Se6iv—Nb2—Nb3—Se4i18.06 (4)Se2—Nb3—Se4—Se181.09 (3)
Se6—Nb2—Nb3—Se4i161.94 (4)Se2i—Nb3—Se4—Se1172.35 (7)
Se5—Nb2—Nb3—Se4i131.44 (4)Nb1—Nb3—Se4—Se1115.32 (2)
Se5iv—Nb2—Nb3—Se4i48.56 (4)Nb2—Nb3—Se4—Se164.68 (2)
Se4—Nb2—Nb3—Se4i180.0Se3i—Nb3—Se4—Nb2110.61 (4)
Nb2iv—Nb2—Nb3—Se4i103 (91)Se3—Nb3—Se4—Nb2130.66 (3)
Se1—Nb2—Nb3—Se468.34 (3)Se4i—Nb3—Se4—Nb20.0
Se1i—Nb2—Nb3—Se4111.66 (3)Se1i—Nb3—Se4—Nb246.86 (2)
Se6iv—Nb2—Nb3—Se4161.94 (4)Se1—Nb3—Se4—Nb264.68 (2)
Se6—Nb2—Nb3—Se418.06 (4)Se2—Nb3—Se4—Nb2145.77 (2)
Se5—Nb2—Nb3—Se448.56 (4)Se2i—Nb3—Se4—Nb2107.66 (6)
Se5iv—Nb2—Nb3—Se4131.44 (4)Nb1—Nb3—Se4—Nb2180.0
Se4i—Nb2—Nb3—Se4180.0Se1i—Nb2—Se4—Se1120.39 (4)
Nb2iv—Nb2—Nb3—Se477 (89)Se6iv—Nb2—Se4—Se1156.18 (14)
Se1—Nb2—Nb3—Se1i180.0Se6—Nb2—Se4—Se194.47 (3)
Se6iv—Nb2—Nb3—Se1i50.28 (4)Se5—Nb2—Se4—Se1146.43 (4)
Se6—Nb2—Nb3—Se1i129.72 (4)Se5iv—Nb2—Se4—Se130.51 (6)
Se5—Nb2—Nb3—Se1i63.10 (4)Se4i—Nb2—Se4—Se170.79 (3)
Se5iv—Nb2—Nb3—Se1i116.90 (4)Nb2iv—Nb2—Se4—Se1109.21 (3)
Se4i—Nb2—Nb3—Se1i68.34 (3)Nb3—Nb2—Se4—Se170.79 (3)
Se4—Nb2—Nb3—Se1i111.66 (3)Se1—Nb2—Se4—Nb370.79 (3)
Nb2iv—Nb2—Nb3—Se1i35 (87)Se1i—Nb2—Se4—Nb349.60 (2)
Se1i—Nb2—Nb3—Se1180.0Se6iv—Nb2—Se4—Nb385.39 (14)
Se6iv—Nb2—Nb3—Se1129.72 (4)Se6—Nb2—Se4—Nb3165.26 (3)
Se6—Nb2—Nb3—Se150.28 (4)Se5—Nb2—Se4—Nb3142.78 (3)
Se5—Nb2—Nb3—Se1116.90 (4)Se5iv—Nb2—Se4—Nb3101.30 (5)
Se5iv—Nb2—Nb3—Se163.10 (4)Se4i—Nb2—Se4—Nb30.0
Se4i—Nb2—Nb3—Se1111.66 (3)Nb2iv—Nb2—Se4—Nb3180.0
Se4—Nb2—Nb3—Se168.34 (3)Se1—Nb2—Se5—Se641.01 (4)
Nb2iv—Nb2—Nb3—Se1145 (94)Se1i—Nb2—Se5—Se6158.15 (3)
Se1—Nb2—Nb3—Se222.92 (3)Se6iv—Nb2—Se5—Se6116.02 (3)
Se1i—Nb2—Nb3—Se2157.08 (3)Se5iv—Nb2—Se5—Se668.31 (3)
Se6iv—Nb2—Nb3—Se2152.64 (4)Se4i—Nb2—Se5—Se6177.90 (6)
Se6—Nb2—Nb3—Se227.36 (4)Se4—Nb2—Se5—Se676.17 (3)
Se5—Nb2—Nb3—Se293.97 (4)Nb2iv—Nb2—Se5—Se668.31 (3)
Se5iv—Nb2—Nb3—Se286.03 (4)Nb3—Nb2—Se5—Se6111.69 (3)
Se4i—Nb2—Nb3—Se2134.59 (3)Se1—Nb2—Se5—Nb2iv109.31 (4)
Se4—Nb2—Nb3—Se245.41 (3)Se1i—Nb2—Se5—Nb2iv133.55 (3)
Nb2iv—Nb2—Nb3—Se2122 (92)Se6iv—Nb2—Se5—Nb2iv47.72 (3)
Se1—Nb2—Nb3—Se2i157.08 (3)Se6—Nb2—Se5—Nb2iv68.31 (3)
Se1i—Nb2—Nb3—Se2i22.92 (3)Se5iv—Nb2—Se5—Nb2iv0.0
Se6iv—Nb2—Nb3—Se2i27.36 (4)Se4i—Nb2—Se5—Nb2iv109.60 (5)
Se6—Nb2—Nb3—Se2i152.64 (4)Se4—Nb2—Se5—Nb2iv144.47 (3)
Se5—Nb2—Nb3—Se2i86.03 (4)Nb3—Nb2—Se5—Nb2iv180.0
Se5iv—Nb2—Nb3—Se2i93.97 (4)Nb2—Se5—Se6—Nb2iv82.97 (4)
Se4i—Nb2—Nb3—Se2i45.41 (3)Nb2iv—Se5—Se6—Nb282.97 (4)
Se4—Nb2—Nb3—Se2i134.59 (3)Se1—Nb2—Se6—Se5149.71 (3)
Nb2iv—Nb2—Nb3—Se2i58 (94)Se1i—Nb2—Se6—Se535.25 (5)
Se1—Nb2—Nb3—Nb135 (7)Se6iv—Nb2—Se6—Se569.03 (3)
Se1i—Nb2—Nb3—Nb1145 (38)Se5iv—Nb2—Se6—Se5117.06 (3)
Se6iv—Nb2—Nb3—Nb195 (7)Se4i—Nb2—Se6—Se5174.81 (14)
Se6—Nb2—Nb3—Nb185 (7)Se4—Nb2—Se6—Se596.75 (3)
Se5—Nb2—Nb3—Nb1152 (7)Nb2iv—Nb2—Se6—Se569.03 (3)
Se5iv—Nb2—Nb3—Nb128 (7)Nb3—Nb2—Se6—Se5110.97 (3)
Se4i—Nb2—Nb3—Nb177 (7)Se1—Nb2—Se6—Nb2iv141.26 (3)
Se4—Nb2—Nb3—Nb1103 (7)Se1i—Nb2—Se6—Nb2iv104.28 (5)
Nb2iv—Nb2—Nb3—Nb10 (22)Se6iv—Nb2—Se6—Nb2iv0.0
Se1i—Nb2—Se1—Se464.30 (2)Se5—Nb2—Se6—Nb2iv69.03 (3)
Se6iv—Nb2—Se1—Se4171.00 (6)Se5iv—Nb2—Se6—Nb2iv48.03 (3)
Se6—Nb2—Se1—Se477.50 (3)Se4i—Nb2—Se6—Nb2iv105.78 (14)
Se5—Nb2—Se1—Se446.09 (4)Se4—Nb2—Se6—Nb2iv165.78 (3)
Se5iv—Nb2—Se1—Se4161.75 (4)Nb3—Nb2—Se6—Nb2iv180.0
Symmetry codes: (i) x, y+1, z; (ii) x, y, z+1/2; (iii) x, y+1, z+1/2; (iv) x, y+1, z+1.
(100K) top
Crystal data top
Nb10Se40·3(I)Z = 2
Mr = 4468.20F(000) = 3858
Monoclinic, P2/cDx = 5.236 Mg m3
Hall symbol: -P 2ycCu Kα radiation, λ = 1.54184 Å
a = 9.4415 (6) ŵ = 58.22 mm1
b = 9.4235 (7) ÅT = 100 K
c = 31.883 (3) ÅNeedle, black
β = 92.352 (8)°0.38 × 0.05 × 0.05 mm
V = 2834.3 (4) Å3
Data collection top
SuperNova, Dual, Cu at zero, Atlas
diffractometer
3316 independent reflections
Radiation source: SuperNova (Cu) X-ray Source2282 reflections with I > 2σ(I)
Mirror monochromatorRint = 0.113
Detector resolution: 10.3953 pixels mm-1θmax = 71.6°, θmin = 8.4°
ω scansh = 1111
Absorption correction: multi-scan
CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.32.29 Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.
k = 1111
Tmin = 0.017, Tmax = 0.159l = 3437
20280 measured reflections
Refinement top
Refinement on F20 restraints
Least-squares matrix: fullPrimary atom site location: structure-invariant direct methods
R[F2 > 2σ(F2)] = 0.058Secondary atom site location: difference Fourier map
wR(F2) = 0.153 w = 1/[σ2(Fo2) + (0.0443P)2 + 108.1739P]
where P = (Fo2 + 2Fc2)/3
S = 1.19(Δ/σ)max < 0.001
3316 reflectionsΔρmax = 1.88 e Å3
241 parametersΔρmin = 1.56 e Å3
Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
Nb1A0.00000.5009 (3)0.25000.0122 (5)
Nb1C0.50001.0013 (3)0.25000.0120 (5)
Nb2A0.00035 (16)0.5007 (2)0.45050 (4)0.0135 (4)
Nb2C0.49991 (16)1.0000 (2)0.45054 (4)0.0132 (4)
Nb3A0.00071 (16)0.50101 (19)0.34930 (4)0.0135 (4)
Nb3C0.49986 (16)1.0006 (2)0.34926 (4)0.0135 (4)
Se1A0.1277 (2)0.3155 (2)0.40105 (6)0.0141 (4)
Se1B0.1275 (2)0.6860 (2)0.40445 (5)0.0144 (4)
Se1C0.6845 (2)0.8729 (2)0.40468 (5)0.0147 (5)
Se1D0.3143 (2)1.1280 (2)0.40074 (6)0.0145 (5)
Se2A0.1913 (2)0.3793 (2)0.29447 (5)0.0146 (5)
Se2B0.1930 (2)0.6226 (2)0.20132 (5)0.0129 (4)
Se2C0.6222 (2)0.8090 (2)0.29792 (5)0.0147 (5)
Se2D0.3786 (2)1.1928 (2)0.29516 (5)0.0141 (4)
Se3A0.0359 (2)0.7231 (2)0.30215 (5)0.0140 (4)
Se3B0.0380 (2)0.2793 (3)0.19703 (5)0.0151 (5)
Se3C0.2779 (2)0.9644 (2)0.29976 (5)0.0139 (4)
Se3D0.7213 (2)1.0381 (2)0.30527 (5)0.0146 (5)
Se4A0.2170 (2)0.5516 (2)0.39409 (5)0.0151 (5)
Se4B0.2179 (2)0.4508 (2)0.39951 (5)0.0151 (5)
Se4C0.4493 (2)0.7828 (3)0.39618 (5)0.0154 (5)
Se4D0.5493 (2)1.2178 (2)0.39748 (5)0.0144 (4)
Se5A0.1088 (2)0.6997 (2)0.49905 (5)0.0152 (5)
Se5C0.3003 (2)0.8910 (2)0.49768 (6)0.0146 (4)
Se6A0.2234 (2)0.4791 (2)0.49719 (5)0.0135 (4)
Se6C0.5210 (2)0.7765 (2)0.50023 (6)0.0143 (4)
I10.99927 (16)1.00295 (19)0.42179 (4)0.0261 (3)
I20.50000.5047 (3)0.25000.0361 (5)
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Nb1A0.0084 (11)0.0122 (13)0.0159 (11)0.0000.0002 (6)0.000
Nb1C0.0086 (11)0.0104 (12)0.0169 (11)0.0000.0001 (6)0.000
Nb2A0.0088 (9)0.0116 (10)0.0200 (9)0.0005 (7)0.0001 (5)0.0012 (5)
Nb2C0.0074 (8)0.0117 (10)0.0204 (9)0.0002 (7)0.0000 (5)0.0015 (5)
Nb3A0.0088 (9)0.0116 (10)0.0201 (9)0.0002 (7)0.0005 (5)0.0042 (5)
Nb3C0.0079 (9)0.0120 (10)0.0206 (9)0.0017 (7)0.0014 (5)0.0035 (5)
Se1A0.0096 (11)0.0139 (12)0.0190 (11)0.0002 (9)0.0006 (6)0.0002 (6)
Se1B0.0111 (11)0.0139 (12)0.0183 (11)0.0011 (9)0.0010 (6)0.0003 (6)
Se1C0.0083 (11)0.0175 (13)0.0183 (11)0.0006 (9)0.0002 (6)0.0009 (6)
Se1D0.0087 (11)0.0147 (13)0.0199 (11)0.0011 (9)0.0007 (6)0.0004 (6)
Se2A0.0113 (11)0.0167 (13)0.0156 (11)0.0005 (9)0.0005 (6)0.0009 (6)
Se2B0.0093 (10)0.0102 (12)0.0190 (11)0.0020 (9)0.0005 (6)0.0008 (6)
Se2C0.0104 (11)0.0158 (13)0.0177 (11)0.0020 (9)0.0000 (6)0.0005 (6)
Se2D0.0098 (11)0.0143 (12)0.0181 (11)0.0006 (9)0.0004 (6)0.0003 (6)
Se3A0.0118 (11)0.0129 (12)0.0172 (11)0.0004 (9)0.0006 (6)0.0006 (6)
Se3B0.0120 (11)0.0148 (12)0.0186 (11)0.0018 (9)0.0014 (6)0.0023 (6)
Se3C0.0090 (10)0.0146 (13)0.0181 (10)0.0015 (9)0.0006 (6)0.0005 (6)
Se3D0.0103 (11)0.0151 (13)0.0183 (10)0.0009 (9)0.0019 (6)0.0012 (6)
Se4A0.0111 (11)0.0174 (13)0.0168 (10)0.0011 (9)0.0005 (6)0.0010 (6)
Se4B0.0105 (11)0.0165 (13)0.0185 (10)0.0026 (9)0.0013 (6)0.0005 (6)
Se4C0.0111 (11)0.0185 (13)0.0165 (11)0.0020 (9)0.0002 (6)0.0022 (6)
Se4D0.0114 (11)0.0132 (12)0.0185 (11)0.0014 (9)0.0002 (6)0.0004 (6)
Se5A0.0129 (11)0.0166 (13)0.0161 (11)0.0025 (9)0.0006 (6)0.0006 (6)
Se5C0.0094 (11)0.0155 (12)0.0188 (11)0.0004 (9)0.0012 (6)0.0002 (6)
Se6A0.0100 (11)0.0130 (12)0.0174 (10)0.0001 (9)0.0002 (6)0.0003 (6)
Se6C0.0115 (11)0.0140 (12)0.0173 (10)0.0015 (9)0.0001 (6)0.0006 (6)
I10.0120 (7)0.0165 (8)0.0497 (9)0.0005 (7)0.0005 (4)0.0006 (5)
I20.0137 (13)0.0179 (15)0.0765 (18)0.0000.0003 (8)0.000
Geometric parameters (Å, º) top
Nb1A—Se2Ai2.607 (2)Nb2C—Se4D2.712 (3)
Nb1A—Se2A2.607 (2)Nb2C—Nb2Civ3.154 (3)
Nb1A—Se2Bi2.610 (2)Nb2C—Nb3C3.2292 (19)
Nb1A—Se2B2.610 (2)Nb3A—Se3Bi2.591 (3)
Nb1A—Se3B2.701 (3)Nb3A—Se3A2.592 (3)
Nb1A—Se3Bi2.701 (3)Nb3A—Se4B2.593 (3)
Nb1A—Se3A2.704 (3)Nb3A—Se4A2.595 (3)
Nb1A—Se3Ai2.704 (3)Nb3A—Se1B2.719 (3)
Nb1A—Nb3A3.1656 (13)Nb3A—Se2A2.720 (3)
Nb1A—Nb3Ai3.1656 (13)Nb3A—Se1A2.722 (3)
Nb1C—Se2D2.604 (3)Nb3A—Se2Bi2.730 (3)
Nb1C—Se2Dii2.604 (3)Nb3C—Se3D2.590 (3)
Nb1C—Se2Cii2.609 (3)Nb3C—Se4D2.591 (3)
Nb1C—Se2C2.609 (3)Nb3C—Se3C2.593 (2)
Nb1C—Se3Dii2.700 (2)Nb3C—Se4C2.595 (3)
Nb1C—Se3D2.700 (2)Nb3C—Se1C2.712 (3)
Nb1C—Se3C2.703 (2)Nb3C—Se2D2.721 (3)
Nb1C—Se3Cii2.703 (2)Nb3C—Se2C2.726 (3)
Nb1C—Nb3Cii3.1648 (13)Nb3C—Se1D2.728 (3)
Nb1C—Nb3C3.1648 (13)Se1A—Se4A2.386 (3)
Nb2A—Se1B2.609 (3)Se1B—Se4B2.382 (3)
Nb2A—Se1A2.612 (3)Se1C—Se4C2.382 (3)
Nb2A—Se6A2.637 (3)Se1D—Se4D2.381 (3)
Nb2A—Se6Aiii2.644 (2)Se2A—Se3Bi2.367 (3)
Nb2A—Se5Aiii2.661 (3)Se2B—Se3Ai2.366 (3)
Nb2A—Se5A2.663 (3)Se2B—Nb3Ai2.730 (3)
Nb2A—Se4A2.710 (2)Se2C—Se3D2.361 (3)
Nb2A—Se4B2.718 (3)Se2D—Se3C2.360 (3)
Nb2A—Nb2Aiii3.156 (3)Se3A—Se2Bi2.366 (3)
Nb2A—Nb3A3.2272 (19)Se3B—Se2Ai2.367 (3)
Nb2C—Se1C2.611 (3)Se3B—Nb3Ai2.591 (3)
Nb2C—Se1D2.612 (3)Se5A—Se6A2.344 (3)
Nb2C—Se6C2.638 (3)Se5A—Nb2Aiii2.661 (3)
Nb2C—Se6Civ2.639 (3)Se5C—Se6C2.345 (3)
Nb2C—Se5Civ2.661 (2)Se5C—Nb2Civ2.661 (2)
Nb2C—Se5C2.664 (3)Se6A—Nb2Aiii2.644 (2)
Nb2C—Se4C2.712 (3)Se6C—Nb2Civ2.639 (3)
Se2Ai—Nb1A—Se2A127.84 (14)Se6C—Nb2C—Nb2Civ53.31 (6)
Se2Ai—Nb1A—Se2Bi91.96 (6)Se6Civ—Nb2C—Nb2Civ53.29 (7)
Se2A—Nb1A—Se2Bi110.62 (6)Se5Civ—Nb2C—Nb2Civ53.73 (6)
Se2Ai—Nb1A—Se2B110.62 (6)Se5C—Nb2C—Nb2Civ53.64 (6)
Se2A—Nb1A—Se2B91.96 (6)Se4C—Nb2C—Nb2Civ129.20 (10)
Se2Bi—Nb1A—Se2B127.85 (14)Se4D—Nb2C—Nb2Civ129.10 (10)
Se2Ai—Nb1A—Se3B52.94 (7)Se1C—Nb2C—Nb3C54.10 (6)
Se2A—Nb1A—Se3B85.57 (9)Se1D—Nb2C—Nb3C54.45 (6)
Se2Bi—Nb1A—Se3B141.58 (8)Se6C—Nb2C—Nb3C126.78 (8)
Se2B—Nb1A—Se3B84.05 (7)Se6Civ—Nb2C—Nb3C126.62 (8)
Se2Ai—Nb1A—Se3Bi85.57 (9)Se5Civ—Nb2C—Nb3C126.21 (7)
Se2A—Nb1A—Se3Bi52.94 (7)Se5C—Nb2C—Nb3C126.42 (7)
Se2Bi—Nb1A—Se3Bi84.05 (7)Se4C—Nb2C—Nb3C50.90 (6)
Se2B—Nb1A—Se3Bi141.58 (8)Se4D—Nb2C—Nb3C50.79 (6)
Se3B—Nb1A—Se3Bi78.69 (11)Nb2Civ—Nb2C—Nb3C179.90 (11)
Se2Ai—Nb1A—Se3A141.45 (9)Se3Bi—Nb3A—Se3A109.80 (8)
Se2A—Nb1A—Se3A84.20 (7)Se3Bi—Nb3A—Se4B94.71 (9)
Se2Bi—Nb1A—Se3A52.85 (7)Se3A—Nb3A—Se4B126.06 (10)
Se2B—Nb1A—Se3A85.59 (9)Se3Bi—Nb3A—Se4A126.24 (10)
Se3B—Nb1A—Se3A165.17 (6)Se3A—Nb3A—Se4A94.65 (9)
Se3Bi—Nb1A—Se3A103.37 (6)Se4B—Nb3A—Se4A108.54 (8)
Se2Ai—Nb1A—Se3Ai84.20 (7)Se3Bi—Nb3A—Se1B145.00 (9)
Se2A—Nb1A—Se3Ai141.45 (9)Se3A—Nb3A—Se1B84.38 (8)
Se2Bi—Nb1A—Se3Ai85.59 (9)Se4B—Nb3A—Se1B53.23 (7)
Se2B—Nb1A—Se3Ai52.85 (7)Se4A—Nb3A—Se1B82.18 (8)
Se3B—Nb1A—Se3Ai103.37 (6)Se3Bi—Nb3A—Se2A52.86 (7)
Se3Bi—Nb1A—Se3Ai165.17 (6)Se3A—Nb3A—Se2A84.16 (8)
Se3A—Nb1A—Se3Ai78.48 (11)Se4B—Nb3A—Se2A144.03 (10)
Se2Ai—Nb1A—Nb3A124.82 (7)Se4A—Nb3A—Se2A84.78 (8)
Se2A—Nb1A—Nb3A55.21 (5)Se1B—Nb3A—Se2A161.86 (10)
Se2Bi—Nb1A—Nb3A55.42 (5)Se3Bi—Nb3A—Se1A84.38 (8)
Se2B—Nb1A—Nb3A124.56 (7)Se3A—Nb3A—Se1A144.88 (9)
Se3B—Nb1A—Nb3A128.35 (10)Se4B—Nb3A—Se1A82.48 (8)
Se3Bi—Nb1A—Nb3A51.69 (6)Se4A—Nb3A—Se1A53.26 (7)
Se3A—Nb1A—Nb3A51.68 (6)Se1B—Nb3A—Se1A102.40 (7)
Se3Ai—Nb1A—Nb3A128.28 (9)Se2A—Nb3A—Se1A79.47 (8)
Se2Ai—Nb1A—Nb3Ai55.21 (5)Se3Bi—Nb3A—Se2Bi83.82 (8)
Se2A—Nb1A—Nb3Ai124.82 (7)Se3A—Nb3A—Se2Bi52.72 (7)
Se2Bi—Nb1A—Nb3Ai124.56 (7)Se4B—Nb3A—Se2Bi85.02 (8)
Se2B—Nb1A—Nb3Ai55.42 (5)Se4A—Nb3A—Se2Bi144.02 (10)
Se3B—Nb1A—Nb3Ai51.69 (6)Se1B—Nb3A—Se2Bi80.06 (8)
Se3Bi—Nb1A—Nb3Ai128.35 (10)Se2A—Nb3A—Se2Bi103.83 (7)
Se3A—Nb1A—Nb3Ai128.28 (9)Se1A—Nb3A—Se2Bi162.03 (10)
Se3Ai—Nb1A—Nb3Ai51.68 (6)Se3Bi—Nb3A—Nb1A54.86 (7)
Nb3A—Nb1A—Nb3Ai179.96 (11)Se3A—Nb3A—Nb1A54.93 (7)
Se2D—Nb1C—Se2Dii92.24 (13)Se4B—Nb3A—Nb1A125.91 (7)
Se2D—Nb1C—Se2Cii127.69 (7)Se4A—Nb3A—Nb1A125.54 (7)
Se2Dii—Nb1C—Se2Cii110.59 (6)Se1B—Nb3A—Nb1A129.04 (8)
Se2D—Nb1C—Se2C110.59 (6)Se2A—Nb3A—Nb1A51.91 (5)
Se2Dii—Nb1C—Se2C127.69 (7)Se1A—Nb3A—Nb1A128.55 (8)
Se2Cii—Nb1C—Se2C91.98 (12)Se2Bi—Nb3A—Nb1A51.91 (5)
Se2D—Nb1C—Se3Dii85.73 (7)Se3Bi—Nb3A—Nb2A125.12 (8)
Se2Dii—Nb1C—Se3Dii84.06 (7)Se3A—Nb3A—Nb2A125.08 (8)
Se2Cii—Nb1C—Se3Dii52.79 (7)Se4B—Nb3A—Nb2A54.36 (6)
Se2C—Nb1C—Se3Dii141.56 (11)Se4A—Nb3A—Nb2A54.18 (6)
Se2D—Nb1C—Se3D84.06 (7)Se1B—Nb3A—Nb2A51.18 (6)
Se2Dii—Nb1C—Se3D85.73 (7)Se2A—Nb3A—Nb2A127.80 (7)
Se2Cii—Nb1C—Se3D141.56 (11)Se1A—Nb3A—Nb2A51.22 (6)
Se2C—Nb1C—Se3D52.79 (7)Se2Bi—Nb3A—Nb2A128.37 (7)
Se3Dii—Nb1C—Se3D165.24 (15)Nb1A—Nb3A—Nb2A179.69 (7)
Se2D—Nb1C—Se3C52.78 (7)Se3D—Nb3C—Se4D94.81 (9)
Se2Dii—Nb1C—Se3C141.58 (11)Se3D—Nb3C—Se3C109.80 (7)
Se2Cii—Nb1C—Se3C85.37 (7)Se4D—Nb3C—Se3C125.91 (10)
Se2C—Nb1C—Se3C84.36 (7)Se3D—Nb3C—Se4C126.29 (10)
Se3Dii—Nb1C—Se3C78.55 (6)Se4D—Nb3C—Se4C108.39 (8)
Se3D—Nb1C—Se3C103.39 (6)Se3C—Nb3C—Se4C94.79 (9)
Se2D—Nb1C—Se3Cii141.58 (11)Se3D—Nb3C—Se1C84.36 (8)
Se2Dii—Nb1C—Se3Cii52.78 (7)Se4D—Nb3C—Se1C82.46 (8)
Se2Cii—Nb1C—Se3Cii84.36 (7)Se3C—Nb3C—Se1C145.04 (10)
Se2C—Nb1C—Se3Cii85.37 (7)Se4C—Nb3C—Se1C53.28 (7)
Se3Dii—Nb1C—Se3Cii103.39 (6)Se3D—Nb3C—Se2D83.91 (8)
Se3D—Nb1C—Se3Cii78.55 (6)Se4D—Nb3C—Se2D84.90 (8)
Se3C—Nb1C—Se3Cii165.20 (14)Se3C—Nb3C—Se2D52.67 (7)
Se2D—Nb1C—Nb3Cii124.94 (8)Se4C—Nb3C—Se2D144.01 (9)
Se2Dii—Nb1C—Nb3Cii55.26 (5)Se1C—Nb3C—Se2D161.95 (10)
Se2Cii—Nb1C—Nb3Cii55.33 (6)Se3D—Nb3C—Se2C52.68 (7)
Se2C—Nb1C—Nb3Cii124.46 (8)Se4D—Nb3C—Se2C144.04 (9)
Se3Dii—Nb1C—Nb3Cii51.66 (5)Se3C—Nb3C—Se2C84.20 (7)
Se3D—Nb1C—Nb3Cii128.38 (5)Se4C—Nb3C—Se2C85.11 (8)
Se3C—Nb1C—Nb3Cii128.23 (5)Se1C—Nb3C—Se2C79.66 (7)
Se3Cii—Nb1C—Nb3Cii51.73 (5)Se2D—Nb3C—Se2C103.76 (7)
Se2D—Nb1C—Nb3C55.26 (5)Se3D—Nb3C—Se1D144.96 (10)
Se2Dii—Nb1C—Nb3C124.94 (8)Se4D—Nb3C—Se1D53.11 (7)
Se2Cii—Nb1C—Nb3C124.46 (8)Se3C—Nb3C—Se1D84.33 (8)
Se2C—Nb1C—Nb3C55.33 (6)Se4C—Nb3C—Se1D82.14 (8)
Se3Dii—Nb1C—Nb3C128.38 (5)Se1C—Nb3C—Se1D102.41 (7)
Se3D—Nb1C—Nb3C51.66 (5)Se2D—Nb3C—Se1D79.89 (8)
Se3C—Nb1C—Nb3C51.73 (5)Se2C—Nb3C—Se1D162.05 (10)
Se3Cii—Nb1C—Nb3C128.23 (5)Se3D—Nb3C—Nb1C54.88 (5)
Nb3Cii—Nb1C—Nb3C179.76 (11)Se4D—Nb3C—Nb1C125.76 (9)
Se1B—Nb2A—Se1A108.64 (8)Se3C—Nb3C—Nb1C54.92 (5)
Se1B—Nb2A—Se6A140.20 (10)Se4C—Nb3C—Nb1C125.85 (9)
Se1A—Nb2A—Se6A86.02 (8)Se1C—Nb3C—Nb1C128.74 (7)
Se1B—Nb2A—Se6Aiii86.02 (8)Se2D—Nb3C—Nb1C51.84 (6)
Se1A—Nb2A—Se6Aiii139.90 (10)Se2C—Nb3C—Nb1C51.92 (6)
Se6A—Nb2A—Se6Aiii106.60 (7)Se1D—Nb3C—Nb1C128.86 (7)
Se1B—Nb2A—Se5Aiii129.68 (9)Se3D—Nb3C—Nb2C125.09 (7)
Se1A—Nb2A—Se5Aiii92.74 (9)Se4D—Nb3C—Nb2C54.22 (6)
Se6A—Nb2A—Se5Aiii84.40 (8)Se3C—Nb3C—Nb2C125.12 (7)
Se6Aiii—Nb2A—Se5Aiii52.43 (7)Se4C—Nb3C—Nb2C54.18 (6)
Se1B—Nb2A—Se5A93.07 (9)Se1C—Nb3C—Nb2C51.25 (5)
Se1A—Nb2A—Se5A130.02 (9)Se2D—Nb3C—Nb2C128.16 (8)
Se6A—Nb2A—Se5A52.49 (7)Se2C—Nb3C—Nb2C128.08 (8)
Se6Aiii—Nb2A—Se5A84.21 (8)Se1D—Nb3C—Nb2C51.16 (5)
Se5Aiii—Nb2A—Se5A107.29 (7)Nb1C—Nb3C—Nb2C179.96 (9)
Se1B—Nb2A—Se4A82.09 (8)Se4A—Se1A—Nb2A65.51 (8)
Se1A—Nb2A—Se4A53.23 (7)Se4A—Se1A—Nb3A60.63 (8)
Se6A—Nb2A—Se4A77.86 (7)Nb2A—Se1A—Nb3A74.43 (8)
Se6Aiii—Nb2A—Se4A165.35 (11)Se4B—Se1B—Nb2A65.80 (8)
Se5Aiii—Nb2A—Se4A142.15 (10)Se4B—Se1B—Nb3A60.68 (8)
Se5A—Nb2A—Se4A87.91 (8)Nb2A—Se1B—Nb3A74.53 (7)
Se1B—Nb2A—Se4B53.09 (7)Se4C—Se1C—Nb2C65.59 (8)
Se1A—Nb2A—Se4B82.23 (8)Se4C—Se1C—Nb3C60.84 (8)
Se6A—Nb2A—Se4B165.32 (11)Nb2C—Se1C—Nb3C74.66 (7)
Se6Aiii—Nb2A—Se4B77.52 (7)Se4D—Se1D—Nb2C65.62 (8)
Se5Aiii—Nb2A—Se4B87.39 (8)Se4D—Se1D—Nb3C60.48 (8)
Se5A—Nb2A—Se4B142.06 (10)Nb2C—Se1D—Nb3C74.39 (7)
Se4A—Nb2A—Se4B101.76 (7)Se3Bi—Se2A—Nb1A65.56 (8)
Se1B—Nb2A—Nb2Aiii125.71 (10)Se3Bi—Se2A—Nb3A60.77 (8)
Se1A—Nb2A—Nb2Aiii125.65 (10)Nb1A—Se2A—Nb3A72.88 (7)
Se6A—Nb2A—Nb2Aiii53.41 (6)Se3Ai—Se2B—Nb1A65.61 (8)
Se6Aiii—Nb2A—Nb2Aiii53.18 (6)Se3Ai—Se2B—Nb3Ai60.64 (8)
Se5Aiii—Nb2A—Nb2Aiii53.67 (6)Nb1A—Se2B—Nb3Ai72.67 (7)
Se5A—Nb2A—Nb2Aiii53.62 (6)Se3D—Se2C—Nb1C65.60 (8)
Se4A—Nb2A—Nb2Aiii129.41 (9)Se3D—Se2C—Nb3C60.70 (8)
Se4B—Nb2A—Nb2Aiii128.83 (9)Nb1C—Se2C—Nb3C72.75 (7)
Se1B—Nb2A—Nb3A54.29 (6)Se3C—Se2D—Nb1C65.78 (9)
Se1A—Nb2A—Nb3A54.35 (6)Se3C—Se2D—Nb3C60.89 (8)
Se6A—Nb2A—Nb3A126.87 (7)Nb1C—Se2D—Nb3C72.90 (7)
Se6Aiii—Nb2A—Nb3A126.54 (7)Se2Bi—Se3A—Nb3A66.65 (8)
Se5Aiii—Nb2A—Nb3A126.01 (8)Se2Bi—Se3A—Nb1A61.54 (7)
Se5A—Nb2A—Nb3A126.70 (8)Nb3A—Se3A—Nb1A73.38 (8)
Se4A—Nb2A—Nb3A50.92 (5)Se2Ai—Se3B—Nb3Ai66.36 (8)
Se4B—Nb2A—Nb3A50.84 (5)Se2Ai—Se3B—Nb1A61.50 (7)
Nb2Aiii—Nb2A—Nb3A179.64 (10)Nb3Ai—Se3B—Nb1A73.45 (8)
Se1C—Nb2C—Se1D108.55 (8)Se2D—Se3C—Nb3C66.44 (8)
Se1C—Nb2C—Se6C86.23 (8)Se2D—Se3C—Nb1C61.45 (9)
Se1D—Nb2C—Se6C140.00 (9)Nb3C—Se3C—Nb1C73.35 (6)
Se1C—Nb2C—Se6Civ140.10 (9)Se2C—Se3D—Nb3C66.62 (8)
Se1D—Nb2C—Se6Civ85.89 (8)Se2C—Se3D—Nb1C61.61 (9)
Se6C—Nb2C—Se6Civ106.60 (7)Nb3C—Se3D—Nb1C73.46 (6)
Se1C—Nb2C—Se5Civ93.00 (8)Se1A—Se4A—Nb3A66.11 (8)
Se1D—Nb2C—Se5Civ129.77 (10)Se1A—Se4A—Nb2A61.26 (8)
Se6C—Nb2C—Se5Civ84.36 (8)Nb3A—Se4A—Nb2A74.90 (7)
Se6Civ—Nb2C—Se5Civ52.51 (7)Se1B—Se4B—Nb3A66.09 (8)
Se1C—Nb2C—Se5C129.99 (10)Se1B—Se4B—Nb2A61.11 (8)
Se1D—Nb2C—Se5C92.78 (8)Nb3A—Se4B—Nb2A74.80 (7)
Se6C—Nb2C—Se5C52.49 (7)Se1C—Se4C—Nb3C65.88 (8)
Se6Civ—Nb2C—Se5C84.28 (8)Se1C—Se4C—Nb2C61.28 (8)
Se5Civ—Nb2C—Se5C107.37 (7)Nb3C—Se4C—Nb2C74.92 (8)
Se1C—Nb2C—Se4C53.13 (7)Se1D—Se4D—Nb3C66.41 (8)
Se1D—Nb2C—Se4C82.16 (8)Se1D—Se4D—Nb2C61.29 (8)
Se6C—Nb2C—Se4C77.78 (8)Nb3C—Se4D—Nb2C74.99 (8)
Se6Civ—Nb2C—Se4C165.24 (9)Se6A—Se5A—Nb2Aiii63.41 (8)
Se5Civ—Nb2C—Se4C142.16 (9)Se6A—Se5A—Nb2A63.17 (8)
Se5C—Nb2C—Se4C87.67 (8)Nb2Aiii—Se5A—Nb2A72.71 (7)
Se1C—Nb2C—Se4D82.08 (8)Se6C—Se5C—Nb2Civ63.26 (8)
Se1D—Nb2C—Se4D53.09 (7)Se6C—Se5C—Nb2C63.19 (8)
Se6C—Nb2C—Se4D165.48 (9)Nb2Civ—Se5C—Nb2C72.63 (7)
Se6Civ—Nb2C—Se4D77.64 (8)Se5A—Se6A—Nb2A64.33 (8)
Se5Civ—Nb2C—Se4D87.67 (8)Se5A—Se6A—Nb2Aiii64.15 (8)
Se5C—Nb2C—Se4D141.93 (9)Nb2A—Se6A—Nb2Aiii73.40 (7)
Se4C—Nb2C—Se4D101.69 (7)Se5C—Se6C—Nb2C64.33 (8)
Se1C—Nb2C—Nb2Civ125.94 (9)Se5C—Se6C—Nb2Civ64.23 (8)
Se1D—Nb2C—Nb2Civ125.51 (9)Nb2C—Se6C—Nb2Civ73.40 (7)
Se2Ai—Nb1A—Nb3A—Se3Bi47.99 (12)Se2C—Nb3C—Se1D—Nb2C94.8 (3)
Se2A—Nb1A—Nb3A—Se3Bi67.27 (9)Nb1C—Nb3C—Se1D—Nb2C179.96 (10)
Se2Bi—Nb1A—Nb3A—Se3Bi112.60 (9)Se2Ai—Nb1A—Se2A—Se3Bi44.82 (6)
Se2B—Nb1A—Nb3A—Se3Bi131.93 (12)Se2Bi—Nb1A—Se2A—Se3Bi64.98 (10)
Se3B—Nb1A—Nb3A—Se3Bi19.31 (13)Se2B—Nb1A—Se2A—Se3Bi163.05 (10)
Se3A—Nb1A—Nb3A—Se3Bi179.63 (9)Se3B—Nb1A—Se2A—Se3Bi79.17 (11)
Se3Ai—Nb1A—Nb3A—Se3Bi161.06 (8)Se3A—Nb1A—Se2A—Se3Bi111.59 (8)
Nb3Ai—Nb1A—Nb3A—Se3Bi170 (100)Se3Ai—Nb1A—Se2A—Se3Bi174.87 (14)
Se2Ai—Nb1A—Nb3A—Se3A131.64 (13)Nb3A—Nb1A—Se2A—Se3Bi65.09 (7)
Se2A—Nb1A—Nb3A—Se3A113.09 (9)Nb3Ai—Nb1A—Se2A—Se3Bi114.95 (12)
Se2Bi—Nb1A—Nb3A—Se3A67.04 (9)Se2Ai—Nb1A—Se2A—Nb3A109.91 (6)
Se2B—Nb1A—Nb3A—Se3A48.44 (12)Se2Bi—Nb1A—Se2A—Nb3A0.11 (10)
Se3B—Nb1A—Nb3A—Se3A161.05 (8)Se2B—Nb1A—Se2A—Nb3A131.86 (9)
Se3Bi—Nb1A—Nb3A—Se3A179.63 (9)Se3B—Nb1A—Se2A—Nb3A144.26 (8)
Se3Ai—Nb1A—Nb3A—Se3A18.57 (13)Se3Bi—Nb1A—Se2A—Nb3A65.09 (7)
Nb3Ai—Nb1A—Nb3A—Se3A9 (100)Se3A—Nb1A—Se2A—Nb3A46.50 (7)
Se2Ai—Nb1A—Nb3A—Se4B19.33 (18)Se3Ai—Nb1A—Se2A—Nb3A109.78 (14)
Se2A—Nb1A—Nb3A—Se4B134.59 (13)Nb3Ai—Nb1A—Se2A—Nb3A179.96 (12)
Se2Bi—Nb1A—Nb3A—Se4B45.28 (12)Se3A—Nb3A—Se2A—Se3Bi120.30 (9)
Se2B—Nb1A—Nb3A—Se4B160.75 (12)Se4B—Nb3A—Se2A—Se3Bi29.78 (15)
Se3B—Nb1A—Nb3A—Se4B86.63 (12)Se4A—Nb3A—Se2A—Se3Bi144.47 (10)
Se3Bi—Nb1A—Nb3A—Se4B67.32 (12)Se1B—Nb3A—Se2A—Se3Bi171.4 (3)
Se3A—Nb1A—Nb3A—Se4B112.32 (12)Se1A—Nb3A—Se2A—Se3Bi90.91 (9)
Se3Ai—Nb1A—Nb3A—Se4B93.75 (13)Se2Bi—Nb3A—Se2A—Se3Bi71.01 (9)
Nb3Ai—Nb1A—Nb3A—Se4B103 (100)Nb1A—Nb3A—Se2A—Se3Bi71.11 (9)
Se2Ai—Nb1A—Nb3A—Se4A160.67 (12)Nb2A—Nb3A—Se2A—Se3Bi109.02 (11)
Se2A—Nb1A—Nb3A—Se4A45.41 (12)Se3Bi—Nb3A—Se2A—Nb1A71.11 (9)
Se2Bi—Nb1A—Nb3A—Se4A134.72 (13)Se3A—Nb3A—Se2A—Nb1A49.19 (8)
Se2B—Nb1A—Nb3A—Se4A19.25 (17)Se4B—Nb3A—Se2A—Nb1A100.89 (15)
Se3B—Nb1A—Nb3A—Se4A93.37 (12)Se4A—Nb3A—Se2A—Nb1A144.42 (9)
Se3Bi—Nb1A—Nb3A—Se4A112.68 (12)Se1B—Nb3A—Se2A—Nb1A100.3 (3)
Se3A—Nb1A—Nb3A—Se4A67.68 (12)Se1A—Nb3A—Se2A—Nb1A162.02 (9)
Se3Ai—Nb1A—Nb3A—Se4A86.25 (11)Se2Bi—Nb3A—Se2A—Nb1A0.10 (9)
Nb3Ai—Nb1A—Nb3A—Se4A77 (100)Nb2A—Nb3A—Se2A—Nb1A179.87 (10)
Se2Ai—Nb1A—Nb3A—Se1B87.97 (16)Se2Ai—Nb1A—Se2B—Se3Ai65.12 (10)
Se2A—Nb1A—Nb3A—Se1B156.77 (12)Se2A—Nb1A—Se2B—Se3Ai162.90 (10)
Se2Bi—Nb1A—Nb3A—Se1B23.36 (11)Se2Bi—Nb1A—Se2B—Se3Ai44.68 (6)
Se2B—Nb1A—Nb3A—Se1B92.11 (12)Se3B—Nb1A—Se2B—Se3Ai111.75 (8)
Se3B—Nb1A—Nb3A—Se1B155.27 (10)Se3Bi—Nb1A—Se2B—Se3Ai175.11 (14)
Se3Bi—Nb1A—Nb3A—Se1B135.96 (12)Se3A—Nb1A—Se2B—Se3Ai78.88 (11)
Se3A—Nb1A—Nb3A—Se1B43.67 (10)Nb3A—Nb1A—Se2B—Se3Ai114.95 (12)
Se3Ai—Nb1A—Nb3A—Se1B25.10 (13)Nb3Ai—Nb1A—Se2B—Se3Ai65.01 (7)
Nb3Ai—Nb1A—Nb3A—Se1B34 (100)Se2Ai—Nb1A—Se2B—Nb3Ai0.11 (10)
Se2Ai—Nb1A—Nb3A—Se2A115.26 (17)Se2A—Nb1A—Se2B—Nb3Ai132.09 (9)
Se2Bi—Nb1A—Nb3A—Se2A179.87 (11)Se2Bi—Nb1A—Se2B—Nb3Ai109.69 (6)
Se2B—Nb1A—Nb3A—Se2A64.66 (11)Se3B—Nb1A—Se2B—Nb3Ai46.75 (7)
Se3B—Nb1A—Nb3A—Se2A47.96 (9)Se3Bi—Nb1A—Se2B—Nb3Ai110.10 (14)
Se3Bi—Nb1A—Nb3A—Se2A67.27 (9)Se3A—Nb1A—Se2B—Nb3Ai143.89 (8)
Se3A—Nb1A—Nb3A—Se2A113.09 (9)Se3Ai—Nb1A—Se2B—Nb3Ai65.01 (7)
Se3Ai—Nb1A—Nb3A—Se2A131.66 (10)Nb3A—Nb1A—Se2B—Nb3Ai179.96 (12)
Nb3Ai—Nb1A—Nb3A—Se2A122 (100)Se2D—Nb1C—Se2C—Se3D64.90 (10)
Se2Ai—Nb1A—Nb3A—Se1A92.43 (13)Se2Dii—Nb1C—Se2C—Se3D45.17 (12)
Se2A—Nb1A—Nb3A—Se1A22.83 (11)Se2Cii—Nb1C—Se2C—Se3D163.30 (9)
Se2Bi—Nb1A—Nb3A—Se1A157.04 (12)Se3Dii—Nb1C—Se2C—Se3D175.10 (6)
Se2B—Nb1A—Nb3A—Se1A87.49 (15)Se3C—Nb1C—Se2C—Se3D111.55 (9)
Se3B—Nb1A—Nb3A—Se1A25.13 (13)Se3Cii—Nb1C—Se2C—Se3D79.13 (8)
Se3Bi—Nb1A—Nb3A—Se1A44.44 (10)Nb3Cii—Nb1C—Se2C—Se3D115.11 (9)
Se3A—Nb1A—Nb3A—Se1A135.93 (12)Nb3C—Nb1C—Se2C—Se3D65.05 (8)
Se3Ai—Nb1A—Nb3A—Se1A154.50 (10)Se2D—Nb1C—Se2C—Nb3C0.15 (9)
Nb3Ai—Nb1A—Nb3A—Se1A145 (100)Se2Dii—Nb1C—Se2C—Nb3C110.22 (11)
Se2Ai—Nb1A—Nb3A—Se2Bi64.61 (11)Se2Cii—Nb1C—Se2C—Nb3C131.65 (8)
Se2A—Nb1A—Nb3A—Se2Bi179.87 (11)Se3Dii—Nb1C—Se2C—Nb3C110.05 (10)
Se2B—Nb1A—Nb3A—Se2Bi115.47 (17)Se3D—Nb1C—Se2C—Nb3C65.05 (8)
Se3B—Nb1A—Nb3A—Se2Bi131.91 (10)Se3C—Nb1C—Se2C—Nb3C46.50 (7)
Se3Bi—Nb1A—Nb3A—Se2Bi112.60 (9)Se3Cii—Nb1C—Se2C—Nb3C144.18 (8)
Se3A—Nb1A—Nb3A—Se2Bi67.04 (9)Nb3Cii—Nb1C—Se2C—Nb3C179.84 (7)
Se3Ai—Nb1A—Nb3A—Se2Bi48.47 (9)Se4D—Nb3C—Se2C—Se3D29.39 (16)
Nb3Ai—Nb1A—Nb3A—Se2Bi58 (100)Se3C—Nb3C—Se2C—Se3D120.36 (9)
Se2Ai—Nb1A—Nb3A—Nb2A135 (16)Se4C—Nb3C—Se2C—Se3D144.31 (9)
Se2A—Nb1A—Nb3A—Nb2A19 (16)Se1C—Nb3C—Se2C—Se3D90.78 (8)
Se2Bi—Nb1A—Nb3A—Nb2A161 (16)Se2D—Nb3C—Se2C—Se3D71.09 (9)
Se2B—Nb1A—Nb3A—Nb2A45 (16)Se1D—Nb3C—Se2C—Se3D170.9 (3)
Se3B—Nb1A—Nb3A—Nb2A67 (16)Nb1C—Nb3C—Se2C—Se3D71.23 (8)
Se3Bi—Nb1A—Nb3A—Nb2A87 (16)Nb2C—Nb3C—Se2C—Se3D108.72 (10)
Se3A—Nb1A—Nb3A—Nb2A94 (16)Se3D—Nb3C—Se2C—Nb1C71.23 (8)
Se3Ai—Nb1A—Nb3A—Nb2A112 (16)Se4D—Nb3C—Se2C—Nb1C100.61 (15)
Nb3Ai—Nb1A—Nb3A—Nb2A103 (100)Se3C—Nb3C—Se2C—Nb1C49.14 (7)
Se1B—Nb2A—Nb3A—Se3Bi136.01 (11)Se4C—Nb3C—Se2C—Nb1C144.46 (8)
Se1A—Nb2A—Nb3A—Se3Bi44.06 (11)Se1C—Nb3C—Se2C—Nb1C162.01 (8)
Se6A—Nb2A—Nb3A—Se3Bi93.93 (13)Se2D—Nb3C—Se2C—Nb1C0.14 (8)
Se6Aiii—Nb2A—Nb3A—Se3Bi85.74 (13)Se1D—Nb3C—Se2C—Nb1C99.6 (3)
Se5Aiii—Nb2A—Nb3A—Se3Bi19.28 (14)Nb2C—Nb3C—Se2C—Nb1C179.95 (9)
Se5A—Nb2A—Nb3A—Se3Bi160.96 (11)Se2Dii—Nb1C—Se2D—Se3C162.72 (9)
Se4A—Nb2A—Nb3A—Se3Bi112.56 (12)Se2Cii—Nb1C—Se2D—Se3C44.36 (12)
Se4B—Nb2A—Nb3A—Se3Bi67.63 (11)Se2C—Nb1C—Se2D—Se3C65.33 (9)
Nb2Aiii—Nb2A—Nb3A—Se3Bi47 (18)Se3Dii—Nb1C—Se2D—Se3C78.86 (8)
Se1B—Nb2A—Nb3A—Se3A44.06 (11)Se3D—Nb1C—Se2D—Se3C111.81 (8)
Se1A—Nb2A—Nb3A—Se3A135.88 (11)Se3Cii—Nb1C—Se2D—Se3C174.91 (6)
Se6A—Nb2A—Nb3A—Se3A86.01 (13)Nb3Cii—Nb1C—Se2D—Se3C114.66 (9)
Se6Aiii—Nb2A—Nb3A—Se3A94.33 (13)Nb3C—Nb1C—Se2D—Se3C65.18 (7)
Se5Aiii—Nb2A—Nb3A—Se3A160.78 (10)Se2Dii—Nb1C—Se2D—Nb3C132.09 (8)
Se5A—Nb2A—Nb3A—Se3A18.98 (14)Se2Cii—Nb1C—Se2D—Nb3C109.54 (11)
Se4A—Nb2A—Nb3A—Se3A67.37 (11)Se2C—Nb1C—Se2D—Nb3C0.15 (9)
Se4B—Nb2A—Nb3A—Se3A112.43 (12)Se3Dii—Nb1C—Se2D—Nb3C144.04 (8)
Nb2Aiii—Nb2A—Nb3A—Se3A133 (18)Se3D—Nb1C—Se2D—Nb3C46.63 (7)
Se1B—Nb2A—Nb3A—Se4B68.38 (9)Se3C—Nb1C—Se2D—Nb3C65.18 (7)
Se1A—Nb2A—Nb3A—Se4B111.69 (10)Se3Cii—Nb1C—Se2D—Nb3C109.73 (10)
Se6A—Nb2A—Nb3A—Se4B161.56 (13)Nb3Cii—Nb1C—Se2D—Nb3C179.84 (7)
Se6Aiii—Nb2A—Nb3A—Se4B18.11 (11)Se3D—Nb3C—Se2D—Se3C120.64 (9)
Se5Aiii—Nb2A—Nb3A—Se4B48.34 (11)Se4D—Nb3C—Se2D—Se3C143.95 (9)
Se5A—Nb2A—Nb3A—Se4B131.41 (12)Se4C—Nb3C—Se2D—Se3C29.36 (15)
Se4A—Nb2A—Nb3A—Se4B179.81 (12)Se1C—Nb3C—Se2D—Se3C170.4 (3)
Nb2Aiii—Nb2A—Nb3A—Se4B21 (18)Se2C—Nb3C—Se2D—Se3C71.48 (9)
Se1B—Nb2A—Nb3A—Se4A111.43 (10)Se1D—Nb3C—Se2D—Se3C90.56 (9)
Se1A—Nb2A—Nb3A—Se4A68.50 (9)Nb1C—Nb3C—Se2D—Se3C71.34 (8)
Se6A—Nb2A—Nb3A—Se4A18.64 (11)Nb2C—Nb3C—Se2D—Se3C108.71 (10)
Se6Aiii—Nb2A—Nb3A—Se4A161.70 (13)Se3D—Nb3C—Se2D—Nb1C49.31 (7)
Se5Aiii—Nb2A—Nb3A—Se4A131.85 (12)Se4D—Nb3C—Se2D—Nb1C144.71 (8)
Se5A—Nb2A—Nb3A—Se4A48.40 (11)Se3C—Nb3C—Se2D—Nb1C71.34 (8)
Se4B—Nb2A—Nb3A—Se4A179.81 (12)Se4C—Nb3C—Se2D—Nb1C100.70 (14)
Nb2Aiii—Nb2A—Nb3A—Se4A159 (18)Se1C—Nb3C—Se2D—Nb1C99.1 (3)
Se1A—Nb2A—Nb3A—Se1B179.93 (10)Se2C—Nb3C—Se2D—Nb1C0.14 (8)
Se6A—Nb2A—Nb3A—Se1B130.06 (13)Se1D—Nb3C—Se2D—Nb1C161.89 (8)
Se6Aiii—Nb2A—Nb3A—Se1B50.27 (11)Nb2C—Nb3C—Se2D—Nb1C179.95 (9)
Se5Aiii—Nb2A—Nb3A—Se1B116.72 (11)Se3Bi—Nb3A—Se3A—Se2Bi65.30 (10)
Se5A—Nb2A—Nb3A—Se1B63.03 (11)Se4B—Nb3A—Se3A—Se2Bi46.43 (11)
Se4A—Nb2A—Nb3A—Se1B111.43 (10)Se4A—Nb3A—Se3A—Se2Bi163.43 (9)
Se4B—Nb2A—Nb3A—Se1B68.38 (9)Se1B—Nb3A—Se3A—Se2Bi81.77 (8)
Nb2Aiii—Nb2A—Nb3A—Se1B89 (18)Se2A—Nb3A—Se3A—Se2Bi112.32 (8)
Se1B—Nb2A—Nb3A—Se2A156.86 (12)Se1A—Nb3A—Se3A—Se2Bi174.62 (16)
Se1A—Nb2A—Nb3A—Se2A23.08 (11)Nb1A—Nb3A—Se3A—Se2Bi65.62 (6)
Se6A—Nb2A—Nb3A—Se2A26.79 (16)Nb2A—Nb3A—Se3A—Se2Bi114.75 (10)
Se6Aiii—Nb2A—Nb3A—Se2A152.87 (11)Se3Bi—Nb3A—Se3A—Nb1A0.32 (8)
Se5Aiii—Nb2A—Nb3A—Se2A86.42 (13)Se4B—Nb3A—Se3A—Nb1A112.05 (10)
Se5A—Nb2A—Nb3A—Se2A93.82 (13)Se4A—Nb3A—Se3A—Nb1A130.96 (7)
Se4A—Nb2A—Nb3A—Se2A45.43 (11)Se1B—Nb3A—Se3A—Nb1A147.39 (7)
Se4B—Nb2A—Nb3A—Se2A134.77 (13)Se2A—Nb3A—Se3A—Nb1A46.70 (6)
Nb2Aiii—Nb2A—Nb3A—Se2A114 (18)Se1A—Nb3A—Se3A—Nb1A109.01 (15)
Se1B—Nb2A—Nb3A—Se1A179.93 (10)Se2Bi—Nb3A—Se3A—Nb1A65.62 (6)
Se6A—Nb2A—Nb3A—Se1A49.87 (11)Nb2A—Nb3A—Se3A—Nb1A179.63 (8)
Se6Aiii—Nb2A—Nb3A—Se1A129.80 (13)Se2Ai—Nb1A—Se3A—Se2Bi28.12 (14)
Se5Aiii—Nb2A—Nb3A—Se1A63.34 (11)Se2A—Nb1A—Se3A—Se2Bi121.41 (9)
Se5A—Nb2A—Nb3A—Se1A116.90 (12)Se2B—Nb1A—Se3A—Se2Bi146.16 (9)
Se4A—Nb2A—Nb3A—Se1A68.50 (9)Se3B—Nb1A—Se3A—Se2Bi168.0 (4)
Se4B—Nb2A—Nb3A—Se1A111.69 (10)Se3Bi—Nb1A—Se3A—Se2Bi71.72 (8)
Nb2Aiii—Nb2A—Nb3A—Se1A91 (18)Se3Ai—Nb1A—Se3A—Se2Bi93.21 (9)
Se1B—Nb2A—Nb3A—Se2Bi23.11 (11)Nb3A—Nb1A—Se3A—Se2Bi72.01 (8)
Se1A—Nb2A—Nb3A—Se2Bi156.95 (12)Nb3Ai—Nb1A—Se3A—Se2Bi107.98 (8)
Se6A—Nb2A—Nb3A—Se2Bi153.18 (11)Se2Ai—Nb1A—Se3A—Nb3A100.14 (13)
Se6Aiii—Nb2A—Nb3A—Se2Bi27.16 (16)Se2A—Nb1A—Se3A—Nb3A49.40 (7)
Se5Aiii—Nb2A—Nb3A—Se2Bi93.61 (13)Se2Bi—Nb1A—Se3A—Nb3A72.01 (8)
Se5A—Nb2A—Nb3A—Se2Bi86.15 (13)Se2B—Nb1A—Se3A—Nb3A141.83 (8)
Se4A—Nb2A—Nb3A—Se2Bi134.54 (13)Se3B—Nb1A—Se3A—Nb3A96.0 (4)
Se4B—Nb2A—Nb3A—Se2Bi45.26 (11)Se3Bi—Nb1A—Se3A—Nb3A0.30 (8)
Nb2Aiii—Nb2A—Nb3A—Se2Bi66 (18)Se3Ai—Nb1A—Se3A—Nb3A165.22 (10)
Se1B—Nb2A—Nb3A—Nb1A137 (16)Nb3Ai—Nb1A—Se3A—Nb3A179.99 (2)
Se1A—Nb2A—Nb3A—Nb1A42 (16)Se2A—Nb1A—Se3B—Se2Ai146.06 (9)
Se6A—Nb2A—Nb3A—Nb1A7 (16)Se2Bi—Nb1A—Se3B—Se2Ai27.97 (14)
Se6Aiii—Nb2A—Nb3A—Nb1A172 (100)Se2B—Nb1A—Se3B—Se2Ai121.50 (9)
Se5Aiii—Nb2A—Nb3A—Nb1A106 (16)Se3Bi—Nb1A—Se3B—Se2Ai93.00 (9)
Se5A—Nb2A—Nb3A—Nb1A74 (16)Se3A—Nb1A—Se3B—Se2Ai167.4 (4)
Se4A—Nb2A—Nb3A—Nb1A26 (16)Se3Ai—Nb1A—Se3B—Se2Ai71.96 (8)
Se4B—Nb2A—Nb3A—Nb1A154 (16)Nb3A—Nb1A—Se3B—Se2Ai108.35 (9)
Nb2Aiii—Nb2A—Nb3A—Nb1A133 (19)Nb3Ai—Nb1A—Se3B—Se2Ai71.66 (8)
Se2D—Nb1C—Nb3C—Se3D112.81 (11)Se2Ai—Nb1A—Se3B—Nb3Ai71.66 (8)
Se2Dii—Nb1C—Nb3C—Se3D48.05 (10)Se2A—Nb1A—Se3B—Nb3Ai142.28 (8)
Se2Cii—Nb1C—Nb3C—Se3D131.94 (12)Se2Bi—Nb1A—Se3B—Nb3Ai99.63 (14)
Se2C—Nb1C—Nb3C—Se3D67.02 (9)Se2B—Nb1A—Se3B—Nb3Ai49.84 (7)
Se3Dii—Nb1C—Nb3C—Se3D161.15 (19)Se3Bi—Nb1A—Se3B—Nb3Ai164.66 (10)
Se3C—Nb1C—Nb3C—Se3D179.82 (12)Se3A—Nb1A—Se3B—Nb3Ai95.8 (4)
Se3Cii—Nb1C—Nb3C—Se3D19.06 (12)Se3Ai—Nb1A—Se3B—Nb3Ai0.29 (8)
Nb3Cii—Nb1C—Nb3C—Se3D99.52 (19)Nb3A—Nb1A—Se3B—Nb3Ai179.99 (2)
Se2D—Nb1C—Nb3C—Se4D45.16 (10)Nb1C—Se2D—Se3C—Nb3C83.19 (6)
Se2Dii—Nb1C—Nb3C—Se4D19.60 (13)Nb3C—Se2D—Se3C—Nb1C83.19 (6)
Se2Cii—Nb1C—Nb3C—Se4D160.41 (11)Se3D—Nb3C—Se3C—Se2D65.40 (10)
Se2C—Nb1C—Nb3C—Se4D134.67 (12)Se4D—Nb3C—Se3C—Se2D46.35 (11)
Se3Dii—Nb1C—Nb3C—Se4D93.49 (15)Se4C—Nb3C—Se3C—Se2D163.20 (9)
Se3D—Nb1C—Nb3C—Se4D67.65 (11)Se1C—Nb3C—Se3C—Se2D174.82 (14)
Se3C—Nb1C—Nb3C—Se4D112.17 (12)Se2C—Nb3C—Se3C—Se2D112.23 (9)
Se3Cii—Nb1C—Nb3C—Se4D86.71 (16)Se1D—Nb3C—Se3C—Se2D81.60 (9)
Nb3Cii—Nb1C—Nb3C—Se4D167.17 (15)Nb1C—Nb3C—Se3C—Se2D65.55 (9)
Se2D—Nb1C—Nb3C—Se3C67.01 (9)Nb2C—Nb3C—Se3C—Se2D114.43 (10)
Se2Dii—Nb1C—Nb3C—Se3C131.77 (12)Se3D—Nb3C—Se3C—Nb1C0.15 (10)
Se2Cii—Nb1C—Nb3C—Se3C48.24 (10)Se4D—Nb3C—Se3C—Nb1C111.91 (11)
Se2C—Nb1C—Nb3C—Se3C113.16 (11)Se4C—Nb3C—Se3C—Nb1C131.25 (9)
Se3Dii—Nb1C—Nb3C—Se3C18.68 (13)Se1C—Nb3C—Se3C—Nb1C109.27 (15)
Se3D—Nb1C—Nb3C—Se3C179.82 (12)Se2D—Nb3C—Se3C—Nb1C65.55 (9)
Se3Cii—Nb1C—Nb3C—Se3C161.12 (18)Se2C—Nb3C—Se3C—Nb1C46.67 (8)
Nb3Cii—Nb1C—Nb3C—Se3C80.66 (15)Se1D—Nb3C—Se3C—Nb1C147.15 (9)
Se2D—Nb1C—Nb3C—Se4C134.57 (12)Nb2C—Nb3C—Se3C—Nb1C179.98 (10)
Se2Dii—Nb1C—Nb3C—Se4C160.66 (11)Se2Dii—Nb1C—Se3C—Se2D28.52 (15)
Se2Cii—Nb1C—Nb3C—Se4C19.33 (13)Se2Cii—Nb1C—Se3C—Se2D146.29 (9)
Se2C—Nb1C—Nb3C—Se4C45.60 (10)Se2C—Nb1C—Se3C—Se2D121.26 (8)
Se3Dii—Nb1C—Nb3C—Se4C86.24 (16)Se3Dii—Nb1C—Se3C—Se2D93.35 (9)
Se3D—Nb1C—Nb3C—Se4C112.61 (12)Se3D—Nb1C—Se3C—Se2D71.67 (10)
Se3C—Nb1C—Nb3C—Se4C67.56 (11)Se3Cii—Nb1C—Se3C—Se2D167.53 (6)
Se3Cii—Nb1C—Nb3C—Se4C93.56 (14)Nb3Cii—Nb1C—Se3C—Se2D108.50 (13)
Nb3Cii—Nb1C—Nb3C—Se4C13.09 (18)Nb3C—Nb1C—Se3C—Se2D71.81 (8)
Se2D—Nb1C—Nb3C—Se1C156.90 (13)Se2D—Nb1C—Se3C—Nb3C71.81 (8)
Se2Dii—Nb1C—Nb3C—Se1C92.14 (14)Se2Dii—Nb1C—Se3C—Nb3C100.33 (11)
Se2Cii—Nb1C—Nb3C—Se1C87.85 (12)Se2Cii—Nb1C—Se3C—Nb3C141.90 (9)
Se2C—Nb1C—Nb3C—Se1C22.93 (11)Se2C—Nb1C—Se3C—Nb3C49.45 (8)
Se3Dii—Nb1C—Nb3C—Se1C154.77 (13)Se3Dii—Nb1C—Se3C—Nb3C165.16 (10)
Se3D—Nb1C—Nb3C—Se1C44.08 (12)Se3D—Nb1C—Se3C—Nb3C0.14 (10)
Se3C—Nb1C—Nb3C—Se1C136.09 (13)Se3Cii—Nb1C—Se3C—Nb3C95.73 (6)
Se3Cii—Nb1C—Nb3C—Se1C25.03 (19)Nb3Cii—Nb1C—Se3C—Nb3C179.70 (14)
Nb3Cii—Nb1C—Nb3C—Se1C55.4 (2)Nb1C—Se2C—Se3D—Nb3C83.17 (6)
Se2Dii—Nb1C—Nb3C—Se2D64.76 (14)Nb3C—Se2C—Se3D—Nb1C83.17 (6)
Se2Cii—Nb1C—Nb3C—Se2D115.25 (9)Se4D—Nb3C—Se3D—Se2C163.19 (9)
Se2C—Nb1C—Nb3C—Se2D179.83 (10)Se3C—Nb3C—Se3D—Se2C65.83 (10)
Se3Dii—Nb1C—Nb3C—Se2D48.33 (13)Se4C—Nb3C—Se3D—Se2C46.15 (11)
Se3D—Nb1C—Nb3C—Se2D112.81 (11)Se1C—Nb3C—Se3D—Se2C81.28 (9)
Se3C—Nb1C—Nb3C—Se2D67.01 (9)Se2D—Nb3C—Se3D—Se2C112.47 (8)
Se3Cii—Nb1C—Nb3C—Se2D131.87 (15)Se1D—Nb3C—Se3D—Se2C175.11 (14)
Nb3Cii—Nb1C—Nb3C—Se2D147.67 (13)Nb1C—Nb3C—Se3D—Se2C65.67 (9)
Se2D—Nb1C—Nb3C—Se2C179.83 (10)Nb2C—Nb3C—Se3D—Se2C114.34 (10)
Se2Dii—Nb1C—Nb3C—Se2C115.07 (10)Se4D—Nb3C—Se3D—Nb1C131.13 (9)
Se2Cii—Nb1C—Nb3C—Se2C64.92 (14)Se3C—Nb3C—Se3D—Nb1C0.15 (10)
Se3Dii—Nb1C—Nb3C—Se2C131.84 (15)Se4C—Nb3C—Se3D—Nb1C111.83 (11)
Se3D—Nb1C—Nb3C—Se2C67.02 (9)Se1C—Nb3C—Se3D—Nb1C146.95 (9)
Se3C—Nb1C—Nb3C—Se2C113.16 (11)Se2D—Nb3C—Se3D—Nb1C46.80 (8)
Se3Cii—Nb1C—Nb3C—Se2C47.96 (13)Se2C—Nb3C—Se3D—Nb1C65.67 (9)
Nb3Cii—Nb1C—Nb3C—Se2C32.50 (18)Se1D—Nb3C—Se3D—Nb1C109.44 (15)
Se2D—Nb1C—Nb3C—Se1D23.13 (11)Nb2C—Nb3C—Se3D—Nb1C179.98 (10)
Se2Dii—Nb1C—Nb3C—Se1D87.90 (11)Se2D—Nb1C—Se3D—Se2C121.54 (8)
Se2Cii—Nb1C—Nb3C—Se1D92.11 (14)Se2Dii—Nb1C—Se3D—Se2C145.75 (9)
Se2C—Nb1C—Nb3C—Se1D157.04 (13)Se2Cii—Nb1C—Se3D—Se2C27.51 (16)
Se3Dii—Nb1C—Nb3C—Se1D25.20 (19)Se3Dii—Nb1C—Se3D—Se2C167.97 (7)
Se3D—Nb1C—Nb3C—Se1D135.95 (13)Se3C—Nb1C—Se3D—Se2C72.08 (10)
Se3C—Nb1C—Nb3C—Se1D43.88 (12)Se3Cii—Nb1C—Se3D—Se2C92.89 (9)
Se3Cii—Nb1C—Nb3C—Se1D155.00 (12)Nb3Cii—Nb1C—Se3D—Se2C107.76 (13)
Nb3Cii—Nb1C—Nb3C—Se1D124.53 (18)Nb3C—Nb1C—Se3D—Se2C71.94 (8)
Se2D—Nb1C—Nb3C—Nb2C92 (100)Se2D—Nb1C—Se3D—Nb3C49.60 (8)
Se2Dii—Nb1C—Nb3C—Nb2C27 (100)Se2Dii—Nb1C—Se3D—Nb3C142.31 (9)
Se2Cii—Nb1C—Nb3C—Nb2C153 (100)Se2Cii—Nb1C—Se3D—Nb3C99.45 (11)
Se2C—Nb1C—Nb3C—Nb2C88 (100)Se2C—Nb1C—Se3D—Nb3C71.94 (8)
Se3Dii—Nb1C—Nb3C—Nb2C140 (100)Se3Dii—Nb1C—Se3D—Nb3C96.04 (6)
Se3D—Nb1C—Nb3C—Nb2C21 (100)Se3C—Nb1C—Se3D—Nb3C0.14 (10)
Se3C—Nb1C—Nb3C—Nb2C159 (100)Se3Cii—Nb1C—Se3D—Nb3C164.83 (10)
Se3Cii—Nb1C—Nb3C—Nb2C40 (100)Nb3Cii—Nb1C—Se3D—Nb3C179.70 (14)
Nb3Cii—Nb1C—Nb3C—Nb2C120 (100)Nb2A—Se1A—Se4A—Nb3A85.29 (7)
Se1C—Nb2C—Nb3C—Se3D44.12 (11)Nb3A—Se1A—Se4A—Nb2A85.29 (7)
Se1D—Nb2C—Nb3C—Se3D135.97 (13)Se3Bi—Nb3A—Se4A—Se1A45.69 (11)
Se6C—Nb2C—Nb3C—Se3D94.14 (13)Se3A—Nb3A—Se4A—Se1A164.43 (9)
Se6Civ—Nb2C—Nb3C—Se3D85.81 (13)Se4B—Nb3A—Se4A—Se1A65.00 (10)
Se5Civ—Nb2C—Nb3C—Se3D19.13 (15)Se1B—Nb3A—Se4A—Se1A111.90 (8)
Se5C—Nb2C—Nb3C—Se3D160.98 (11)Se2A—Nb3A—Se4A—Se1A80.74 (8)
Se4C—Nb2C—Nb3C—Se3D112.64 (12)Se2Bi—Nb3A—Se4A—Se1A172.84 (14)
Se4D—Nb2C—Nb3C—Se3D67.66 (11)Nb1A—Nb3A—Se4A—Se1A114.99 (11)
Nb2Civ—Nb2C—Nb3C—Se3D69 (59)Nb2A—Nb3A—Se4A—Se1A64.84 (8)
Se1C—Nb2C—Nb3C—Se4D111.78 (10)Se3Bi—Nb3A—Se4A—Nb2A110.53 (10)
Se1D—Nb2C—Nb3C—Se4D68.31 (9)Se3A—Nb3A—Se4A—Nb2A130.73 (8)
Se6C—Nb2C—Nb3C—Se4D161.80 (12)Se4B—Nb3A—Se4A—Nb2A0.17 (10)
Se6Civ—Nb2C—Nb3C—Se4D18.15 (10)Se1B—Nb3A—Se4A—Nb2A47.06 (7)
Se5Civ—Nb2C—Nb3C—Se4D48.53 (11)Se2A—Nb3A—Se4A—Nb2A145.58 (8)
Se5C—Nb2C—Nb3C—Se4D131.36 (12)Se1A—Nb3A—Se4A—Nb2A64.84 (8)
Se4C—Nb2C—Nb3C—Se4D179.70 (10)Se2Bi—Nb3A—Se4A—Nb2A108.00 (14)
Nb2Civ—Nb2C—Nb3C—Se4D1 (59)Nb1A—Nb3A—Se4A—Nb2A179.83 (10)
Se1C—Nb2C—Nb3C—Se3C136.07 (13)Se1B—Nb2A—Se4A—Se1A120.44 (9)
Se1D—Nb2C—Nb3C—Se3C43.84 (11)Se6A—Nb2A—Se4A—Se1A94.14 (9)
Se6C—Nb2C—Nb3C—Se3C86.05 (13)Se6Aiii—Nb2A—Se4A—Se1A156.5 (3)
Se6Civ—Nb2C—Nb3C—Se3C93.99 (13)Se5Aiii—Nb2A—Se4A—Se1A30.21 (14)
Se5Civ—Nb2C—Nb3C—Se3C160.67 (11)Se5A—Nb2A—Se4A—Se1A146.16 (9)
Se5C—Nb2C—Nb3C—Se3C19.21 (16)Se4B—Nb2A—Se4A—Se1A70.86 (9)
Se4C—Nb2C—Nb3C—Se3C67.55 (11)Nb2Aiii—Nb2A—Se4A—Se1A109.13 (14)
Se4D—Nb2C—Nb3C—Se3C112.14 (12)Nb3A—Nb2A—Se4A—Se1A70.71 (8)
Nb2Civ—Nb2C—Nb3C—Se3C111 (59)Se1B—Nb2A—Se4A—Nb3A49.74 (8)
Se1C—Nb2C—Nb3C—Se4C68.52 (10)Se1A—Nb2A—Se4A—Nb3A70.71 (8)
Se1D—Nb2C—Nb3C—Se4C111.39 (10)Se6A—Nb2A—Se4A—Nb3A164.84 (9)
Se6C—Nb2C—Nb3C—Se4C18.50 (10)Se6Aiii—Nb2A—Se4A—Nb3A85.8 (3)
Se6Civ—Nb2C—Nb3C—Se4C161.54 (11)Se5Aiii—Nb2A—Se4A—Nb3A100.92 (14)
Se5Civ—Nb2C—Nb3C—Se4C131.77 (12)Se5A—Nb2A—Se4A—Nb3A143.13 (9)
Se5C—Nb2C—Nb3C—Se4C48.34 (11)Se4B—Nb2A—Se4A—Nb3A0.15 (9)
Se4D—Nb2C—Nb3C—Se4C179.70 (10)Nb2Aiii—Nb2A—Se4A—Nb3A179.84 (13)
Nb2Civ—Nb2C—Nb3C—Se4C179 (100)Nb2A—Se1B—Se4B—Nb3A85.24 (7)
Se1D—Nb2C—Nb3C—Se1C179.91 (11)Nb3A—Se1B—Se4B—Nb2A85.24 (7)
Se6C—Nb2C—Nb3C—Se1C50.02 (11)Se3Bi—Nb3A—Se4B—Se1B164.66 (9)
Se6Civ—Nb2C—Nb3C—Se1C129.94 (12)Se3A—Nb3A—Se4B—Se1B45.94 (11)
Se5Civ—Nb2C—Nb3C—Se1C63.26 (11)Se4A—Nb3A—Se4B—Se1B64.55 (10)
Se5C—Nb2C—Nb3C—Se1C116.86 (13)Se2A—Nb3A—Se4B—Se1B171.94 (14)
Se4C—Nb2C—Nb3C—Se1C68.52 (10)Se1A—Nb3A—Se4B—Se1B111.66 (8)
Se4D—Nb2C—Nb3C—Se1C111.78 (10)Se2Bi—Nb3A—Se4B—Se1B81.30 (9)
Nb2Civ—Nb2C—Nb3C—Se1C113 (59)Nb1A—Nb3A—Se4B—Se1B115.45 (11)
Se1C—Nb2C—Nb3C—Se2D156.90 (12)Nb2A—Nb3A—Se4B—Se1B64.72 (8)
Se1D—Nb2C—Nb3C—Se2D23.19 (11)Se3Bi—Nb3A—Se4B—Nb2A130.63 (8)
Se6C—Nb2C—Nb3C—Se2D153.09 (10)Se3A—Nb3A—Se4B—Nb2A110.66 (10)
Se6Civ—Nb2C—Nb3C—Se2D26.96 (14)Se4A—Nb3A—Se4B—Nb2A0.16 (10)
Se5Civ—Nb2C—Nb3C—Se2D93.64 (13)Se1B—Nb3A—Se4B—Nb2A64.72 (8)
Se5C—Nb2C—Nb3C—Se2D86.24 (14)Se2A—Nb3A—Se4B—Nb2A107.22 (14)
Se4C—Nb2C—Nb3C—Se2D134.58 (12)Se1A—Nb3A—Se4B—Nb2A46.94 (7)
Se4D—Nb2C—Nb3C—Se2D45.11 (11)Se2Bi—Nb3A—Se4B—Nb2A146.01 (8)
Nb2Civ—Nb2C—Nb3C—Se2D44 (59)Nb1A—Nb3A—Se4B—Nb2A179.84 (10)
Se1C—Nb2C—Nb3C—Se2C22.87 (11)Se1A—Nb2A—Se4B—Se1B120.39 (9)
Se1D—Nb2C—Nb3C—Se2C157.04 (12)Se6A—Nb2A—Se4B—Se1B157.6 (3)
Se6C—Nb2C—Nb3C—Se2C27.15 (14)Se6Aiii—Nb2A—Se4B—Se1B94.44 (9)
Se6Civ—Nb2C—Nb3C—Se2C152.81 (11)Se5Aiii—Nb2A—Se4B—Se1B146.48 (9)
Se5Civ—Nb2C—Nb3C—Se2C86.13 (13)Se5A—Nb2A—Se4B—Se1B31.31 (14)
Se5C—Nb2C—Nb3C—Se2C93.99 (13)Se4A—Nb2A—Se4B—Se1B70.59 (9)
Se4C—Nb2C—Nb3C—Se2C45.65 (11)Nb2Aiii—Nb2A—Se4B—Se1B109.42 (14)
Se4D—Nb2C—Nb3C—Se2C134.66 (12)Nb3A—Nb2A—Se4B—Se1B70.75 (8)
Nb2Civ—Nb2C—Nb3C—Se2C136 (59)Se1B—Nb2A—Se4B—Nb3A70.75 (8)
Se1C—Nb2C—Nb3C—Se1D179.91 (11)Se1A—Nb2A—Se4B—Nb3A49.65 (8)
Se6C—Nb2C—Nb3C—Se1D129.89 (12)Se6A—Nb2A—Se4B—Nb3A86.8 (3)
Se6Civ—Nb2C—Nb3C—Se1D50.15 (11)Se6Aiii—Nb2A—Se4B—Nb3A165.18 (9)
Se5Civ—Nb2C—Nb3C—Se1D116.83 (12)Se5Aiii—Nb2A—Se4B—Nb3A142.77 (9)
Se5C—Nb2C—Nb3C—Se1D63.05 (11)Se5A—Nb2A—Se4B—Nb3A102.06 (13)
Se4C—Nb2C—Nb3C—Se1D111.39 (10)Se4A—Nb2A—Se4B—Nb3A0.15 (9)
Se4D—Nb2C—Nb3C—Se1D68.31 (9)Nb2Aiii—Nb2A—Se4B—Nb3A179.84 (13)
Nb2Civ—Nb2C—Nb3C—Se1D67 (59)Nb2C—Se1C—Se4C—Nb3C85.44 (8)
Se1C—Nb2C—Nb3C—Nb1C65 (100)Nb3C—Se1C—Se4C—Nb2C85.44 (8)
Se1D—Nb2C—Nb3C—Nb1C115 (100)Se3D—Nb3C—Se4C—Se1C45.59 (11)
Se6C—Nb2C—Nb3C—Nb1C115 (100)Se4D—Nb3C—Se4C—Se1C65.13 (10)
Se6Civ—Nb2C—Nb3C—Nb1C65 (100)Se3C—Nb3C—Se4C—Se1C164.48 (9)
Se5Civ—Nb2C—Nb3C—Nb1C2 (100)Se2D—Nb3C—Se4C—Se1C172.49 (15)
Se5C—Nb2C—Nb3C—Nb1C178 (100)Se2C—Nb3C—Se4C—Se1C80.73 (8)
Se4C—Nb2C—Nb3C—Nb1C133 (100)Se1D—Nb3C—Se4C—Se1C111.93 (8)
Se4D—Nb2C—Nb3C—Nb1C47 (100)Nb1C—Nb3C—Se4C—Se1C115.10 (9)
Nb2Civ—Nb2C—Nb3C—Nb1C48 (100)Nb2C—Nb3C—Se4C—Se1C64.87 (7)
Se1B—Nb2A—Se1A—Se4A64.31 (9)Se3D—Nb3C—Se4C—Nb2C110.46 (10)
Se6A—Nb2A—Se1A—Se4A77.81 (8)Se4D—Nb3C—Se4C—Nb2C0.26 (9)
Se6Aiii—Nb2A—Se1A—Se4A170.98 (13)Se3C—Nb3C—Se4C—Nb2C130.65 (8)
Se5Aiii—Nb2A—Se1A—Se4A161.99 (9)Se1C—Nb3C—Se4C—Nb2C64.87 (7)
Se5A—Nb2A—Se1A—Se4A46.61 (12)Se2D—Nb3C—Se4C—Nb2C107.62 (14)
Se4B—Nb2A—Se1A—Se4A111.02 (8)Se2C—Nb3C—Se4C—Nb2C145.60 (8)
Nb2Aiii—Nb2A—Se1A—Se4A116.07 (12)Se1D—Nb3C—Se4C—Nb2C47.06 (7)
Nb3A—Nb2A—Se1A—Se4A64.37 (7)Nb1C—Nb3C—Se4C—Nb2C179.97 (8)
Se1B—Nb2A—Se1A—Nb3A0.06 (9)Se1D—Nb2C—Se4C—Se1C120.31 (9)
Se6A—Nb2A—Se1A—Nb3A142.18 (8)Se6C—Nb2C—Se4C—Se1C94.50 (9)
Se6Aiii—Nb2A—Se1A—Nb3A106.60 (13)Se6Civ—Nb2C—Se4C—Se1C156.5 (3)
Se5Aiii—Nb2A—Se1A—Nb3A133.64 (8)Se5Civ—Nb2C—Se4C—Se1C30.79 (15)
Se5A—Nb2A—Se1A—Nb3A110.98 (11)Se5C—Nb2C—Se4C—Se1C146.57 (9)
Se4A—Nb2A—Se1A—Nb3A64.37 (7)Se4D—Nb2C—Se4C—Se1C70.66 (9)
Se4B—Nb2A—Se1A—Nb3A46.65 (7)Nb2Civ—Nb2C—Se4C—Se1C109.58 (13)
Nb2Aiii—Nb2A—Se1A—Nb3A179.56 (11)Nb3C—Nb2C—Se4C—Se1C70.42 (8)
Se3Bi—Nb3A—Se1A—Se4A144.56 (9)Se1C—Nb2C—Se4C—Nb3C70.42 (8)
Se3A—Nb3A—Se1A—Se4A27.71 (16)Se1D—Nb2C—Se4C—Nb3C49.88 (7)
Se4B—Nb3A—Se1A—Se4A119.92 (9)Se6C—Nb2C—Se4C—Nb3C164.93 (8)
Se1B—Nb3A—Se1A—Se4A70.25 (9)Se6Civ—Nb2C—Se4C—Nb3C86.1 (3)
Se2A—Nb3A—Se1A—Se4A91.34 (8)Se5Civ—Nb2C—Se4C—Nb3C101.22 (14)
Se2Bi—Nb3A—Se1A—Se4A166.3 (3)Se5C—Nb2C—Se4C—Nb3C143.01 (8)
Nb1A—Nb3A—Se1A—Se4A109.43 (10)Se4D—Nb2C—Se4C—Nb3C0.24 (8)
Nb2A—Nb3A—Se1A—Se4A70.30 (8)Nb2Civ—Nb2C—Se4C—Nb3C180.00 (11)
Se3Bi—Nb3A—Se1A—Nb2A145.14 (8)Nb2C—Se1D—Se4D—Nb3C85.24 (8)
Se3A—Nb3A—Se1A—Nb2A98.01 (15)Nb3C—Se1D—Se4D—Nb2C85.24 (8)
Se4B—Nb3A—Se1A—Nb2A49.62 (7)Se3D—Nb3C—Se4D—Se1D164.61 (9)
Se4A—Nb3A—Se1A—Nb2A70.30 (8)Se3C—Nb3C—Se4D—Se1D45.89 (11)
Se1B—Nb3A—Se1A—Nb2A0.05 (8)Se4C—Nb3C—Se4D—Se1D64.55 (10)
Se2A—Nb3A—Se1A—Nb2A161.64 (8)Se1C—Nb3C—Se4D—Se1D111.74 (9)
Se2Bi—Nb3A—Se1A—Nb2A96.0 (3)Se2D—Nb3C—Se4D—Se1D81.18 (8)
Nb1A—Nb3A—Se1A—Nb2A179.74 (9)Se2C—Nb3C—Se4D—Se1D172.33 (15)
Se1A—Nb2A—Se1B—Se4B64.42 (9)Nb1C—Nb3C—Se4D—Se1D115.22 (9)
Se6A—Nb2A—Se1B—Se4B171.30 (12)Nb2C—Nb3C—Se4D—Se1D64.81 (7)
Se6Aiii—Nb2A—Se1B—Se4B77.37 (8)Se3D—Nb3C—Se4D—Nb2C130.58 (8)
Se5Aiii—Nb2A—Se1B—Se4B45.79 (12)Se3C—Nb3C—Se4D—Nb2C110.70 (10)
Se5A—Nb2A—Se1B—Se4B161.34 (9)Se4C—Nb3C—Se4D—Nb2C0.26 (9)
Se4A—Nb2A—Se1B—Se4B111.21 (8)Se1C—Nb3C—Se4D—Nb2C46.93 (7)
Nb2Aiii—Nb2A—Se1B—Se4B115.20 (12)Se2D—Nb3C—Se4D—Nb2C145.99 (8)
Nb3A—Nb2A—Se1B—Se4B64.36 (7)Se2C—Nb3C—Se4D—Nb2C107.52 (15)
Se1A—Nb2A—Se1B—Nb3A0.06 (9)Se1D—Nb3C—Se4D—Nb2C64.81 (7)
Se6A—Nb2A—Se1B—Nb3A106.94 (12)Nb1C—Nb3C—Se4D—Nb2C179.97 (8)
Se6Aiii—Nb2A—Se1B—Nb3A141.73 (8)Se1C—Nb2C—Se4D—Se1D120.41 (9)
Se5Aiii—Nb2A—Se1B—Nb3A110.15 (11)Se6C—Nb2C—Se4D—Se1D157.1 (4)
Se5A—Nb2A—Se1B—Nb3A134.30 (8)Se6Civ—Nb2C—Se4D—Se1D94.17 (9)
Se4A—Nb2A—Se1B—Nb3A46.85 (7)Se5Civ—Nb2C—Se4D—Se1D146.24 (9)
Se4B—Nb2A—Se1B—Nb3A64.36 (7)Se5C—Nb2C—Se4D—Se1D30.60 (14)
Nb2Aiii—Nb2A—Se1B—Nb3A179.56 (11)Se4C—Nb2C—Se4D—Se1D70.76 (9)
Se3Bi—Nb3A—Se1B—Se4B27.37 (16)Nb2Civ—Nb2C—Se4D—Se1D109.00 (13)
Se3A—Nb3A—Se1B—Se4B144.29 (9)Nb3C—Nb2C—Se4D—Se1D71.00 (8)
Se4A—Nb3A—Se1B—Se4B120.22 (9)Se1C—Nb2C—Se4D—Nb3C49.41 (7)
Se2A—Nb3A—Se1B—Se4B164.7 (3)Se1D—Nb2C—Se4D—Nb3C71.00 (8)
Se1A—Nb3A—Se1B—Se4B70.64 (9)Se6C—Nb2C—Se4D—Nb3C86.1 (4)
Se2Bi—Nb3A—Se1B—Se4B91.21 (9)Se6Civ—Nb2C—Se4D—Nb3C165.17 (8)
Nb1A—Nb3A—Se1B—Se4B109.68 (11)Se5Civ—Nb2C—Se4D—Nb3C142.76 (8)
Nb2A—Nb3A—Se1B—Se4B70.58 (8)Se5C—Nb2C—Se4D—Nb3C101.60 (14)
Se3Bi—Nb3A—Se1B—Nb2A97.95 (15)Se4C—Nb2C—Se4D—Nb3C0.24 (8)
Se3A—Nb3A—Se1B—Nb2A145.13 (8)Nb2Civ—Nb2C—Se4D—Nb3C180.00 (11)
Se4B—Nb3A—Se1B—Nb2A70.58 (8)Se1B—Nb2A—Se5A—Se6A158.23 (9)
Se4A—Nb3A—Se1B—Nb2A49.63 (7)Se1A—Nb2A—Se5A—Se6A40.65 (12)
Se2A—Nb3A—Se1B—Nb2A94.1 (3)Se6Aiii—Nb2A—Se5A—Se6A116.09 (8)
Se1A—Nb3A—Se1B—Nb2A0.05 (8)Se5Aiii—Nb2A—Se5A—Se6A68.42 (8)
Se2Bi—Nb3A—Se1B—Nb2A161.79 (8)Se4A—Nb2A—Se5A—Se6A76.28 (8)
Nb1A—Nb3A—Se1B—Nb2A179.73 (9)Se4B—Nb2A—Se5A—Se6A177.18 (13)
Se1D—Nb2C—Se1C—Se4C64.44 (10)Nb2Aiii—Nb2A—Se5A—Se6A68.42 (8)
Se6C—Nb2C—Se1C—Se4C77.53 (9)Nb3A—Nb2A—Se5A—Se6A111.79 (10)
Se6Civ—Nb2C—Se1C—Se4C170.90 (13)Se1B—Nb2A—Se5A—Nb2Aiii133.35 (9)
Se5Civ—Nb2C—Se1C—Se4C161.67 (9)Se1A—Nb2A—Se5A—Nb2Aiii109.07 (12)
Se5C—Nb2C—Se1C—Se4C45.94 (11)Se6A—Nb2A—Se5A—Nb2Aiii68.42 (8)
Se4D—Nb2C—Se1C—Se4C111.11 (8)Se6Aiii—Nb2A—Se5A—Nb2Aiii47.67 (6)
Nb2Civ—Nb2C—Se1C—Se4C115.60 (13)Se5Aiii—Nb2A—Se5A—Nb2Aiii0.0
Nb3C—Nb2C—Se1C—Se4C64.51 (8)Se4A—Nb2A—Se5A—Nb2Aiii144.70 (10)
Se1D—Nb2C—Se1C—Nb3C0.08 (10)Se4B—Nb2A—Se5A—Nb2Aiii108.76 (14)
Se6C—Nb2C—Se1C—Nb3C142.05 (8)Nb3A—Nb2A—Se5A—Nb2Aiii179.79 (11)
Se6Civ—Nb2C—Se1C—Nb3C106.38 (13)Se1C—Nb2C—Se5C—Se6C41.23 (11)
Se5Civ—Nb2C—Se1C—Nb3C133.82 (8)Se1D—Nb2C—Se5C—Se6C158.38 (10)
Se5C—Nb2C—Se1C—Nb3C110.45 (10)Se6Civ—Nb2C—Se5C—Se6C116.03 (8)
Se4C—Nb2C—Se1C—Nb3C64.51 (8)Se5Civ—Nb2C—Se5C—Se6C68.28 (8)
Se4D—Nb2C—Se1C—Nb3C46.59 (7)Se4C—Nb2C—Se5C—Se6C76.35 (9)
Nb2Civ—Nb2C—Se1C—Nb3C179.88 (12)Se4D—Nb2C—Se5C—Se6C177.57 (14)
Se3D—Nb3C—Se1C—Se4C144.65 (10)Nb2Civ—Nb2C—Se5C—Se6C68.28 (8)
Se4D—Nb3C—Se1C—Se4C119.72 (9)Nb3C—Nb2C—Se5C—Se6C111.82 (11)
Se3C—Nb3C—Se1C—Se4C27.74 (15)Se1C—Nb2C—Se5C—Nb2Civ109.51 (11)
Se2D—Nb3C—Se1C—Se4C165.7 (3)Se1D—Nb2C—Se5C—Nb2Civ133.34 (10)
Se2C—Nb3C—Se1C—Se4C91.61 (9)Se6C—Nb2C—Se5C—Nb2Civ68.28 (8)
Se1D—Nb3C—Se1C—Se4C70.20 (9)Se6Civ—Nb2C—Se5C—Nb2Civ47.76 (7)
Nb1C—Nb3C—Se1C—Se4C109.77 (12)Se5Civ—Nb2C—Se5C—Nb2Civ0.0
Nb2C—Nb3C—Se1C—Se4C70.27 (8)Se4C—Nb2C—Se5C—Nb2Civ144.63 (10)
Se3D—Nb3C—Se1C—Nb2C145.08 (9)Se4D—Nb2C—Se5C—Nb2Civ109.29 (15)
Se4D—Nb3C—Se1C—Nb2C49.45 (8)Nb3C—Nb2C—Se5C—Nb2Civ179.90 (12)
Se3C—Nb3C—Se1C—Nb2C98.01 (15)Nb2Aiii—Se5A—Se6A—Nb2A83.15 (7)
Se4C—Nb3C—Se1C—Nb2C70.27 (8)Nb2A—Se5A—Se6A—Nb2Aiii83.15 (7)
Se2D—Nb3C—Se1C—Nb2C95.4 (3)Se1B—Nb2A—Se6A—Se5A35.34 (13)
Se2C—Nb3C—Se1C—Nb2C161.88 (9)Se1A—Nb2A—Se6A—Se5A149.99 (9)
Se1D—Nb3C—Se1C—Nb2C0.07 (9)Se6Aiii—Nb2A—Se6A—Se5A68.81 (8)
Nb1C—Nb3C—Se1C—Nb2C179.96 (10)Se5Aiii—Nb2A—Se6A—Se5A116.86 (8)
Se1C—Nb2C—Se1D—Se4D64.29 (10)Se4A—Nb2A—Se6A—Se5A96.77 (9)
Se6C—Nb2C—Se1D—Se4D171.28 (14)Se4B—Nb2A—Se6A—Se5A173.1 (3)
Se6Civ—Nb2C—Se1D—Se4D77.63 (9)Nb2Aiii—Nb2A—Se6A—Se5A68.81 (8)
Se5Civ—Nb2C—Se1D—Se4D46.26 (11)Nb3A—Nb2A—Se6A—Se5A111.47 (11)
Se5C—Nb2C—Se1D—Se4D161.68 (9)Se1B—Nb2A—Se6A—Nb2Aiii104.15 (14)
Se4C—Nb2C—Se1D—Se4D111.05 (8)Se1A—Nb2A—Se6A—Nb2Aiii141.20 (10)
Nb2Civ—Nb2C—Se1D—Se4D115.67 (13)Se6Aiii—Nb2A—Se6A—Nb2Aiii0.0
Nb3C—Nb2C—Se1D—Se4D64.22 (8)Se5Aiii—Nb2A—Se6A—Nb2Aiii48.05 (7)
Se1C—Nb2C—Se1D—Nb3C0.08 (9)Se5A—Nb2A—Se6A—Nb2Aiii68.81 (8)
Se6C—Nb2C—Se1D—Nb3C107.06 (13)Se4A—Nb2A—Se6A—Nb2Aiii165.58 (11)
Se6Civ—Nb2C—Se1D—Nb3C141.84 (8)Se4B—Nb2A—Se6A—Nb2Aiii104.3 (3)
Se5Civ—Nb2C—Se1D—Nb3C110.47 (10)Nb3A—Nb2A—Se6A—Nb2Aiii179.72 (13)
Se5C—Nb2C—Se1D—Nb3C134.10 (8)Nb2Civ—Se5C—Se6C—Nb2C83.11 (7)
Se4C—Nb2C—Se1D—Nb3C46.83 (7)Nb2C—Se5C—Se6C—Nb2Civ83.11 (7)
Se4D—Nb2C—Se1D—Nb3C64.22 (8)Se1C—Nb2C—Se6C—Se5C149.60 (9)
Nb2Civ—Nb2C—Se1D—Nb3C179.88 (12)Se1D—Nb2C—Se6C—Se5C34.92 (14)
Se3D—Nb3C—Se1D—Se4D27.42 (15)Se6Civ—Nb2C—Se6C—Se5C68.90 (8)
Se3C—Nb3C—Se1D—Se4D144.24 (10)Se5Civ—Nb2C—Se6C—Se5C117.01 (8)
Se4C—Nb3C—Se1D—Se4D120.12 (9)Se4C—Nb2C—Se6C—Se5C96.54 (9)
Se1C—Nb3C—Se1D—Se4D70.54 (9)Se4D—Nb2C—Se6C—Se5C174.0 (4)
Se2D—Nb3C—Se1D—Se4D91.20 (9)Nb2Civ—Nb2C—Se6C—Se5C68.90 (8)
Se2C—Nb3C—Se1D—Se4D165.3 (3)Nb3C—Nb2C—Se6C—Se5C111.14 (10)
Nb1C—Nb3C—Se1D—Se4D109.49 (12)Se1C—Nb2C—Se6C—Nb2Civ141.50 (9)
Nb2C—Nb3C—Se1D—Se4D70.47 (8)Se1D—Nb2C—Se6C—Nb2Civ103.82 (14)
Se3D—Nb3C—Se1D—Nb2C97.89 (14)Se6Civ—Nb2C—Se6C—Nb2Civ0.0
Se4D—Nb3C—Se1D—Nb2C70.47 (8)Se5Civ—Nb2C—Se6C—Nb2Civ48.11 (6)
Se3C—Nb3C—Se1D—Nb2C145.30 (9)Se5C—Nb2C—Se6C—Nb2Civ68.90 (8)
Se4C—Nb3C—Se1D—Nb2C49.65 (7)Se4C—Nb2C—Se6C—Nb2Civ165.44 (9)
Se1C—Nb3C—Se1D—Nb2C0.07 (9)Se4D—Nb2C—Se6C—Nb2Civ105.1 (4)
Se2D—Nb3C—Se1D—Nb2C161.67 (9)Nb3C—Nb2C—Se6C—Nb2Civ179.96 (11)
Symmetry codes: (i) x, y, z+1/2; (ii) x+1, y, z+1/2; (iii) x, y+1, z+1; (iv) x+1, y+2, z+1.
 

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