Hidden and apparent twins in uranyl-oxide minerals agrinierite and rameauite: a demonstration of metric and reticular merohedry

Plášil, J.; Petříček, V.; Škoda, R.; Meisser, N.; Kasatkin, A.V.

doi:10.1107/S1600576721009663

research papers

JOURNAL OF
APPLIED
CRYSTALLOGRAPHY

ISSN: 1600-5767

Volume 54| Part 6| December 2021| Pages 1656-1663

https://doi.org/10.1107/S1600576721009663

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Hidden and apparent twins in uranyl-oxide minerals agrinierite and rameauite: a demonstration of metric and reticular merohedry

Jakub Plášil,^a ^* Václav Petříček,^a Radek Škoda,^b Nicolas Meisser ^c and Anatoly V. Kasatkin ^d

^aInstitute of Physics ASCR, v.v.i., Na Slovance 2, Prague 8, 18221, Czech Republic, ^bDepartment of Geological Sciences, Masaryk University, Kotlářská 2, Brno, 61137, Czech Republic, ^cMusée cantonal de géologie, Université de Lausanne, Anthropole, Dorigny CH-1015, Switzerland, and ^dFersman Mineralogical Museum of the Russian Academy of Sciences, Leninsky Prospekt 18-2, Moscow 119071, Russian Federation
^*Correspondence e-mail: plasil@fzu.cz

Edited by H. Brand, Australian Synchrotron, ANSTO, Australia (Received 17 May 2021; accepted 17 September 2021; online 2 November 2021)

In this work, the structures of chemically related uranyl-oxide minerals agrinierite and rameauite have been revisited and some corrections to the available structure data are provided. Both structures were found to be twinned. The two minerals are chemically similar, and though their structures differ considerably, their unit-cell metrics are similar. Agrinierite was found to be twinned by metric merohedry (diffraction type I), whereas the structure of rameauite is twinned by reticular merohedry (diffraction type II). The twinning of the monoclinic unit cells (true cells) leads to pseudo-orthorhombic or pseudo-tetragonal supercells in the single-crystal diffraction patterns of both minerals. According to the new data and refinement, agrinierite is monoclinic (space group Cm), with a = 14.069 (3), b = 14.220 (3), c = 13.967 (3) Å, β = 120.24 (12)° and V = 2414.2 (12) Å³ (Z = 2). The twinning can be expressed as a mirror in (101) (apart from the inversion twin), which leads to a supercell with a = 14.121, b = 14.276, c = 24.221 Å and V = 2 × 2441 Å³, which is F centered. The new structure refinement converged to R = 3.54% for 6545 unique observed reflections with I > 3σ(I) and GOF = 1.07. Rameauite is also monoclinic (space group Cc), with a = 13.947 (3), b = 14.300 (3), c = 13.888 (3) Å, β = 118.50 (3)° and V = 2434.3 (11) Å³ (Z = 2). The twinning can be expressed as a mirror in (101) (apart from the inversion twin), which leads to a supercell with a = 14.223, b = 14.300, c = 23.921 Å and V = 2 × 2434 Å³, which is C centered. The new structure refinement of rameauite converged to R = 4.23% for 2344 unique observed reflections with I > 3σ(I) and GOF = 1.48. The current investigation documented how peculiar twinning can be, not only for this group of minerals, and how care must be taken in handling the data biased by twinning.

Keywords: agrinierite; rameauite; twinning; merohedry; Jana2020.

CCDC references: 2110502; 2115477

1. Introduction

Uranyl-oxide hydroxy-hydrates (UOHs) represent a fascinating group of minerals and synthetic phases, closely connected with the hydration–oxidation of uranium dioxide, UO_2+x, as nuclear fuel or uraninite (Finch & Ewing, 1992 ; Wronkiewicz et al., 1996 ; Janeczek et al. 1996 ; Plášil, 2014 , 2018a ). They occur in nature as minerals and are among the first alteration products that form during weathering of uraninite (pitchblende) in oxidized zones of U deposits worldwide (Finch, Suksi et al., 1996 ; Finch, Cooper et al., 1996 ; Plášil, 2018a). Numerous studies focused on their structures, solubilities and thermodynamic stabilities were undertaken in the 1990s and at the beginning of the millennium (e.g. Casas et al., 1997 ; Finch & Murakami, 1999 ; Kubatko et al. 2006 ; Klingensmith et al., 2007 ; Gorman-Lewis et al., 2008 ) due to the general importance of UOHs in nuclear waste disposal and the environmental chemistry of uranium. Nevertheless, the results of recent scientific efforts have proven even greater complexity and variability of the entire group (Kirkegaard et al., 2019 ; Lu, Zhang, Wei et al., 2020 ; Lu, Zhang, Aughterson & Zheng, 2020 ; Olds et al., 2017 , 2018 ; Plášil, 2017 , 2018b ; Plášil et al., 2018 , 2020 ; Zhang et al., 2016 , 2018 , 2019 ).

Agrinierite and rameauite are interesting UOHs, having the same type locality, the Margnac mine (Compreignac, Haute-Vienne, Nouvelle-Aquitaine) in France (Cesbron et al., 1972 ). Agrinierite, K₂(Ca_0.65Sr_0.35)[(UO₂)₃O₃(OH)₂]₂·5H₂O (Cahill & Burns, 2000 ), has been so far the only naturally occurring UOH to contain an essential amount of Sr, reported by Cesbron et al. (1972). This is of interest due to the possible incorporation of ⁹⁰Sr into the alteration phases of spent nuclear fuel. The rameauite structure has been revealed relatively recently by Plášil et al. (2016 ). The ideal chemical formula of rameauite is K₂Ca[(UO₂)₃O₃(OH)₂]₂·6H₂O.

According to the structure studies by Cahill & Burns (2000), agrinierite is orthorhombic (space group F2mm, Z = 16) with a = 14.094 (2), b = 14.127 (2), c = 24.106 (4) Å and V = 4799.6 (1) Å³. Rameauite is reported (Plášil et al., 2016) to be monoclinic (space group Cc, Z = 4) with a = 13.9458 (19), b = 14.3105 (19), c = 13.8959 (18) Å, β = 118.477 (14)° and V = 2437.7 (6) Å³. The unit-cell volume of rameauite is approximately half that of agrinierite. The structure of agrinierite has been refined to R = 6.55% for 2710 unique observed reflections with I > 4σ(I) and GOF = 0.851 [SHELXTL (Sheldrick, 2008 ) software used]. The rameauite structure has been refined to R = 6.00% for 1696 unique observed reflections with I > 3σ(I) and GOF = 1.62 [Jana2006 (Petříček et al., 2014 ) software used].

While the UOH sheets in the structure of agrinierite are based on the α-U₃O₈ type, the sheets in rameauite, despite the overall chemical similarity, are based upon the β-U₃O₈ type (Fig. 1)

Figure 1
Topology of the UOH layers (red lines) and the distribution of interlayer constituents in (a) agrinierite and (b) rameauite. The agrinierite UOH sheet is based on the α-U₃O₈ type with rods of pentagons and rods of pentagons linked with triangles (oriented up and down). The sheet in rameauite is based on the β-U₃O₈ type with rods of pentagons linked with triangles (oriented up and down) and rectangles. Color scheme: Ca/Sr sites are pink, K sites are green, blue spheres are O of molecular H₂O, black dots within the sheets are OH groups.

The close chemical and structural similarities of the two UOHs prompted us to reinvestigate their structures. This revision led us to the conclusion that both structures are affected by twinning. Here we report the investigation of twinning in both minerals and provide a correct description of the agrinierite unit cell and improved structure models.

2. Methodology

2.1. Samples studied

The studied specimen of agrinierite originates from the type locality: the former Margnac U mine located about 3 km from Compreignac, Haute-Vienne, Nouvelle-Aquitaine, France (Cesbron et al., 1972). The studied sample (8 × 4 × 3 mm) is constituted of earthy and massive yellow or orange `gummite' crosscut by inframillimetre-sized veins covered with well shaped orange UOHs, including agrinierite and acicular uranophane-α crystals. In these veins, agrinierite occurs as small (up to 0.8 mm long) pumpkin-orange tabular crystals on {001} pseudo-hexagonal crystals. The sample is preserved in the collection of the Geological Museum of Lausanne, Switzerland (catalog No. MGL 093238). From the same centimetre-sized mineral association, other UOH minerals analyzed utilizing powder X-ray diffraction and energy-dispersive X-ray spectroscopy reflect the distribution of alkaline and alkaline-earth elements on a millimetre scale: compreignacite (K), becquerelite (Ca) and billietite (Ba) (samples MGL 094375–094378).

Rameauite has been studied by Plášil et al. (2016) using the specimen originating from Margnac, France.

2.2. Chemical composition of agrinierite

Even though agrinierite was discovered and described ca 50 years ago (Cesbron et al., 1972), its chemical composition remains poorly studied. In the original description, Cesbron et al. (1972) provided only one wet-chemical analysis and, for instance, reported a 2.05 wt% of SrO [∼0.40 Sr atoms per formula unit (apfu)]. Cahill & Burns (2000) did not provide any chemical data and only gave the composition from the refined structure. The official International Mineralogical Association list of minerals reports agrinierite as K₂Ca[(UO₂)₃O₃(OH)₂]₂·5H₂O, thus totally neglecting the Sr content in the mineral. In response, we decided to undertake new reliable quantitative chemistry determination by electron microprobe. Crystals of agrinierite were mounted on epoxy resin, polished and carbon-coated to determine their chemical compositions utilizing a CAMECA SX100 electron microprobe. The measurement was performed in wavelength-dispersive mode at 15 kV accelerating voltage, 2 nA beam current and 15 µm beam diameter using the following standards: synthetic UO₂ for U, synthetic SrSO₄ for Sr, wollastonite for Ca and sanidine for K. No other elements were above the detection limit. Regardless of the mild analytical conditions, a systematic decrease of K Kα X-ray intensity during the analysis was observed. Thus, K was analyzed at the beginning of each measurement; the integration time of K was divided into four periods and the concentration was calculated from the values of K Kα intensities extrapolated to time zero. The raw intensities were processed for matrix corrections using X-PHI matrix corrections (Merlet, 1994 ) involving a stoichiometric amount of H₂O. The empirical formula was calculated on the basis of 6 U and the amounts of O, OH and H₂O were derived from the structure and the rule of electroneutrality. Atomic proportions are shown in apfu (atoms per formula unit).

The agrinierite studied is chemically heterogeneous, particularly in the Ca (0.30–0.61 apfu; 0.83–1.69 wt% CaO) and Sr (0.48–0.67 apfu; 2.49–3.50 wt% SrO) contents. The K content is 1.23–1.38 apfu (2.87–3.23 wt% K₂O). Considering the average amounts of UO₃ (85.62 wt%) and H₂O (6.29 wt%), the average analytical sum is 99.16 wt%. The mean (n = 10) empirical formula of agrinierite is K_1.31(Sr_0.56Ca_0.47)[(UO₂)₃O_2.84(OH)₂]₂·5H₂O.

2.3. Single-crystal X-ray diffraction

Using single-crystal X-ray diffraction we studied a fragment of the tabular crystal of agrinierite from the Margnac deposit. The crystal of 0.122 × 0.072 × 0.020 mm dimensions was examined at room temperature using a Rigaku SuperNova single-crystal diffractometer. The diffraction experiment was carried out using Mo Kα radiation (λ = 0.71073 Å) from a micro-focus X-ray tube, collimated and monochromated by mirror optics and detected by an Atlas S2 CCD detector using binning of 2 × 2 pixels and a high-gain mode to register even very weak reflections with an acceptable resolution.

Rameauite was studied using the same instrument; details can be found in the paper by Plášil et al. (2016). Here, we reanalyzed the diffraction data and conducted a new crystal structure refinement. The experimental and refinement details are reported in Table 1.

Table 1
Details for the data collection and refinement for agrinierite and rameauite

	Agrinierite	Rameauite
Structural formula (sum)	K_3.758(Sr_1.32Ca_0.68)[(UO₂)₃O₃(OH)₂]₄(H₂O)₁₀	K₄Ca₂[(UO₂)₃O₃(OH)₂]₄(H₂O)₁₂
a, b, c (Å); β (°)	14.069 (3), 14.220 (3), 13.967 (3); 120.24 (12)	13.947 (3), 14.300 (3), 13.888 (3); 118.50 (3)
V (Å³)	2414.2 (12)	2434.3 (11)
Space group	Cm	Cc
Z	2	2
D_calc (g cm⁻³) for the above formula	5.500	5.442
Temperature (K)	296	296
Wavelength (Å)	Mo Kα, 0.71073	Mo Kα, 0.71073
Crystal dimensions (µm)	122 × 72 × 20	93 × 56 × 28
Limiting θ angles (°)	3.25–31.20	5.15–27.75
Limiting Miller indices	−19 ≤ h ≤ 20, −20 ≤ k ≤ 20, −19 ≤ l ≤ 19	−18 ≤ h ≤ 11, −18 ≤ k ≤ 18, −18 ≤ l ≤ 16
No. of measured reflections	24 870	7145
No. of unique reflections	7186	3280
No. of observed reflections (criterion)	6545 [I_obs > 3σ(I)]	2344 [I_obs > 3σ(I)]
Completeness, R_int	0.93, 0.045	0.93, 0.045
Absorption correction (mm^–1), T_min/T_max	42.05, 0.198/1	40.44, 0.417/1
F₀₀₀	3343	3336
Parameters refined, restraints, constraints	206, 0, 17	196, 0, 2
R, wR (obs)	0.0354, 0.0931	0.0423, 0.0843
R, wR (all)	0.0389, 0.0980	0.0596, 0.0912
GOF obs/all	1.07/1.07	1.48/1.34
Δρ_min, Δρ_max (e Å^–3)	−4.24, +4.58 (0.6 Å to U1)	−7.11, +5.41 (0.5 Å to U3)
Weighting scheme, weights	σ, w = 1/[σ²(I) + 0.003363I²]	σ, w = 1/[σ²(I) + 0.000485I²]
Twin fractions 1, 2, 3, 4	0.45 (2)/0.067 (13)/0.455 (13)/0.033 (13)	0.74 (4)/0.215 (4)/0.05 (4)
Twin matrices /1, 2, 3/	$[\left({\matrix{ {-1} & 0 & 0 \cr 0 & 1 & 0 \cr 0 & 0 & 1 \cr } } \right), \left({\matrix{ 1 & 0 & 0 \cr 0 & 1 & 0 \cr {-1} & 0 & {-1} \cr } } \right), \left({\matrix{ { - 1} & 0 & 0 \cr 0 & 1 & 0 \cr 0 & 0 & { - 1} \cr } } \right)]$	$[\left({\matrix{ 0 & 0 & 1 \cr 0 & 1 & 0 \cr 1 & 0 & 0 \cr } } \right), \left({\matrix{ { - 1} & 0 & 0 \cr 0 & { - 1} & 0 \cr 0 & 0 & { - 1} \cr } } \right)\hfill]$

3. Results

3.1. Twinning

The diffraction experiment revealed an F-centered orthorhombic unit cell similar to that reported by Cahill & Burns (2000). The initial refinements, using their structure model, led only to a fit with R ≃ 8% and a GOF > 2.5. The indexing procedure and unit-cell search in CrysAlis (Rigaku, 2019 $[Rigaku (2019). CrysAlis CCD and CrysAlis RED. Oxford Diffraction Ltd, Yarnton, Oxfordshire, UK.]$ ) did not return satisfactory unambiguous solutions. Therefore we undertook an indexing procedure implemented in Jana2006 (Tools → GrIndex, using the .tabbin reflection file from peakhunt; Petříček et al., 2014). This procedure revealed a monoclinic unit cell with a = 10.0400 (3), b = 24.2211 (8), c = 10.4020 (3) Å, β = 90.628 (3)° and V ≃ 2411.42 Å³, indexing about 90.4% of 21 813 reflections. The monoclinic angle close to 90° provides a warning of the possibility of metric merohedral twinning. The test quickly revealed the possibility of twin presence (represented by the mirror in [101]), leading to a supercell with a = 14.121, b = 14.276, c = 24.221 Å and V = 2 × 2441.42 Å³, which is F centered. The monoclinic I-centered cell, a = 13.9653 (2), b = 14.22243 (16), c = 13.9675 (2) Å, β = 119.515 (2)° (selected to be similar to that of rameauite) was later transformed during the space-group test procedure in Jana2006 to C2/m (14.0694 14.2203 13.9669 90 120.237 90; transformation matrix |1 0 1|0 1 0|1 0 0|). By averaging in C2/m we obtained 3501 reflections with an R_int of 5.12% (redundancy of 6.59). The structure solution in SHELXT (Sheldrick, 2015 ) returned a single solution in Cm (Flack 0.24 by SHELXT output), which we subsequently refined, with twinning by metric merohedry along with an inversion twin (this involves three symmetry elements to describe the twinning properly). Nevertheless, the refinement was not straightforward. The difficulties were mainly caused by the K sites; for instance, only two (K1 and K4) of the four independent K sites could be refined using a harmonic approach to the atomic displacement parameters. Only one of the K sites allowed the use of an anisotropic description for the atomic displacement parameters, and one of the K sites was found to have a lower occupancy than unity (K2; Table 2). Nevertheless, the refined occupancies and atomic displacement parameters are probably still greatly affected by the complete overlap of reflections as a result of twinning. For the final cycle of the refinement, the xyz coordinates of the U1 atom were fixed due to correlations. The final refinement (Table 1) for the agrinierite twinned crystal converged to R = 3.54% for 6545 unique observed reflections, with I > 3σ(I) and GOF = 1.07. The final atomic coordinates and displacement parameters for agrinierite are provided in Table 2, selected interatomic distances in Table 3 and a bond-valence analysis in Table 4. The bond-valence analysis was carried out following the procedure by Brown (2002 , 2009 ) using bond-valence parameters provided by Gagné & Hawthorne (2015 ).

Table 2
Atom coordinates, isotropic and equivalent displacement parameters (Å), and site-occupancies for agrinierite

Atom	x/a	y/b	z/c	U_iso*/U_eq
U1	0.371711	0.759536	0.616595	0.0129(5)
U2	0.1928 (3)	0.73988 (5)	0.25716 (7)	0.013 (6)
U3	0.49507 (17)	0.7501 (2)	0.4369 (2)	0.0132 (5)
U4	0.37008 (12)	0.27269 (11)	0.11730 (11)	0.0122 (5)
U5	0.48845 (17)	0.23312 (3)	0.9369 (2)	0.0124 (4)
U6	0.6896 (2)	0.77272 (13)	0.75662 (13)	0.0156 (6)
M1†	0.3431 (4)	0	0.2494 (5)	0.028 (2)
M2†	0.5324 (5)	0.5	0.6242 (5)	0.013 (2)
K1	0.2984 (7)	0	0.9361 (14)	0.033 (4)
K2†	0.5259 (7)	1	0.5946 (7)	0.023 (2)*
K3	0.3674 (6)	0.5	0.2524 (7)	0.0318 (18)*
K4	0.8533 (10)	0	0.9345 (11)	0.076 (6)
O1	0.8224 (19)	0.7678 (7)	0.937 (3)	0.027 (2)*
O2	0.4620 (15)	0.1083 (7)	0.935 (3)	0.0238 (19)*
O3	0.3304 (12)	0.7403 (13)	0.4431 (18)	0.017 (3)*
O4	0.3569 (13)	0.1534 (12)	0.1235 (13)	0.021 (4)*
O5	0.5224 (17)	0.631 (2)	0.4820 (17)	0.026 (6)*
O6	0.4730 (17)	0.875 (2)	0.3874 (16)	0.021 (5)*
O7	0.3965 (11)	0.3964 (11)	0.1223 (12)	0.014 (3)*
O8	0.4087 (15)	0.6352 (17)	0.6341 (14)	0.011 (4)*
O9	0.0252 (12)	0.7539 (12)	0.1116 (12)	0.014 (3)*
O10	0.8480 (12)	0.7338 (11)	0.7641 (11)	0.012 (3)*
O11	0.1689 (14)	0.6167 (15)	0.2818 (14)	0.025 (4)*
O12	0.3426 (15)	0.8801 (15)	0.5998 (14)	0.024 (4)*
O13	0.6892 (14)	0.7804 (12)	0.5586 (14)	0.015 (4)*
O14	0.053 (2)	0.6939 (18)	0.8100 (19)	0.022 (6)*
O15	0.210 (2)	0.862 (2)	0.2340 (18)	0.030 (6)*
O16	0.3597 (11)	0.6927 (10)	0.2751 (10)	0.013 (3)*
O17	0.6544 (11)	0.6446 (12)	0.7537 (12)	0.016 (3)*
O18	0.5188 (16)	0.3568 (7)	0.935 (3)	0.0229 (19)*
O19	0.5684 (14)	0.7034 (13)	0.3192 (14)	0.020 (4)*
O20	0.1810 (16)	0.7015 (15)	0.0650 (16)	0.011 (5)*
O21	0.7125 (14)	0.8993 (14)	0.7710 (13)	0.029 (5)*
O22	0.5240 (10)	0.7855 (9)	0.6074 (10)	0.006 (2)*
O23	0.3292 (18)	0.5	0.4734 (19)	0.036 (6)*
O24	0.671 (2)	1	0.541 (2)	0.054 (8)*
O25	0.5839 (19)	0.5	0.3128 (19)	0.037 (6)*
O26	0.185 (2)	0	0.059 (2)	0.029 (7)*
O27	0.5427 (19)	0.5	0.8131 (19)	0.026 (6)*
O28	0.675 (2)	0	1.055 (2)	0.062 (8)*
O29	0.482 (2)	0	0.179 (2)	0.051 (7)*
O30	0.503 (2)	0	0.774 (2)	0.051 (7)*
O31	0.8303 (18)	0.5	0.4306 (17)	0.024 (4)*
O32	0.7210 (18)	0.5	0.6618 (19)	0.034 (6)*

†Refined occupancies: M1 0.89 (3)Sr/0.11 (3)Ca; M2 0.43 (3)Sr/0.57 (3)Ca; K2 0.76 (2).

Table 3
Selected interatomic distances (Å) in the structure of agrinierite

U1–O8	1.83 (3)	U2—O11	1.845 (15)	U3—O5	1.78 (3)
U1—O12	1.748 (14)	U2—O15	1.80 (3)	U3—O6	1.88 (3)
U1—O3	2.21 (3)	U2—O3	2.33 (2)	U3—O3	2.37 (2)
U1—O10ⁱⁱ	2.247 (16)	U2—O9	2.214 (11)	U3—O13	2.418 (12)
U1—O13ⁱⁱ	2.343 (14)	U2—O16	2.335 (16)	U3—O16	2.249 (11)
U1—O14ⁱⁱⁱ	2.70 (2)	U2—O19ⁱⁱ	2.453 (17)	U3—O19	2.432 (17)
U1—O22	2.244 (16)	U2—O20	2.66 (3)	U3—O22	2.256 (15)
〈U1—O_Ur〉	1.79	〈U2—O_Ur〉	1.82	〈U3—O_Ur〉	1.83
〈U1—O_eq〉	2.35	〈U2—O_eq〉	2.40	〈U3—O_eq〉	2.35

U4—O4	1.720 (14)	U5—O2	1.811 (11)	U6—O17	1.879 (14)
U4—O7	1.785 (14)	U5—O18	1.814 (13)	U6—O21	1.819 (14)
U4—O1^vii	2.26 (4)	U5—O1^ix	2.39 (3)	U6—O1	2.26 (3)
U4—O9^viii	2.233 (16)	U5—O9^x	2.251 (15)	U6—O10	2.247 (16)
U4—O16ⁱ	2.329 (16)	U5—O10^ix	2.220 (11)	U6—O13	2.758 (16)
U4—O19ⁱ	2.812 (2)	U5—O14^viii	2.43 (3)	U6—O14ⁱⁱⁱ	2.43 (3)
U4—O20ⁱ	2.41 (3)	U5—O20^x	2.42 (2)	U6—O22	2.219 (10)
〈U4—O_Ur〉	1.75	〈U5—O_Ur〉	1.81	〈U6—O_Ur〉	1.85
〈U4—O_eq〉	2.35	〈U5—O_eq〉	2.34	〈U6—O_eq〉	2.38

M1—O4	2.861 (16)	M2—O5	2.67 (3)	K1—O2	2.78 (2)
M1—O4^xii	2.861 (16)	M2—O5ⁱ	2.67 (3)	K1—O2^xii	2.78 (2)
M1—O6^xiii	2.58 (2)	M2—O8	2.64 (3)	K1—O4^xv	3.182 (14)
M1—O6ⁱ	2.58 (2)	M2—O8ⁱ	2.64 (3)	K1—O4^xvi	3.182 (14)
M1—O15^xiii	2.65 (2)	M2—O17	2.710 (13)	K1—O17^x	3.105 (14)
M1—O15ⁱ	2.65 (2)	M2—O17ⁱ	2.710 (13)	K1—O17^xiv	3.105 (14)
M1—O26	2.46 (2)	M2—O23	2.56 (2)	K1—O26^xv	2.87 (4)
M1—O29	2.59 (4)	M2—O27	2.57 (3)	K1—O27^x	3.11 (3)
M1—O31^x	2.63 (3)	M2—O32	2.43 (3)	K1—O29^xv	3.06 (2)
〈M1—O〉	2.65	〈M2—O〉	2.62	K1—O32^x	3.41 (3)
				〈K1—O〉	3.19

K2—O6	3.15 (2)	K3—O5	3.39 (2)	K4—O1^xiii	3.334 (11)
K2—O6^xvii	3.15 (2)	K3—O5ⁱ	3.39 (2)	K4—O1ⁱ	3.334 (11)
K2—O12	3.12 (3)	K3—O7	2.531 (18)	K4—O7^xi	2.801 (19)
K2—O12^xvii	3.12 (3)	K3—O7ⁱ	2.531 (18)	K4—O7^xix	2.801 (19)
K2—O21	2.921 (13)	K3—O11	3.449 (18)	K4—O18^viii	3.09 (2)
K2—O21^xvii	2.921 (13)	K3—O11ⁱ	3.449 (18)	K4—O18^xx	3.09 (2)
K2—O22	3.056 (13)	K3—O16	2.771 (14)	K4—O21^xiii	2.571 (14)
K2—O22^xvii	3.056 (13)	K3—O16ⁱ	2.771 (14)	K4—O21ⁱ	2.571 (14)
K2—O24	2.50 (4)	K3—O23	3.39 (3)	K4—O27^ix	3.81 (4)
K2—O30^iv	2.68 (3)	K3—O25	2.72 (3)	K4—O28	3.66 (10)
K2—O31^v	2.54 (2)	K3—O28^vi	2.72 (2)	〈K4—O〉	3.11
〈K2—O〉	2.93	〈K3—O〉	2.99
Symmetry codes: (i) x, −y + 1, z; (ii) x − $[\textstyle {1\over2}]$ , −y + $[\textstyle {3\over2}]$ , z; (iii) x + $[\textstyle {1\over2}]$ , −y + $[\textstyle {3\over2}]$ , z; (iv) x − $[\textstyle {1\over2}]$ , y + $[\textstyle {1\over2}]$ , z; (v) x − $[\textstyle {1\over2}]$ , y + $[\textstyle {1\over2}]$ , z − 1; (vii) x − $[\textstyle {1\over2}]$ , y − $[\textstyle {1\over2}]$ , z − 1; (viii) x + $[\textstyle {1\over2}]$ , y − $[\textstyle {1\over2}]$ , z; (ix) x − $[\textstyle {1\over2}]$ , y − $[\textstyle {1\over2}]$ , z; (x) x + $[\textstyle {1\over2}]$ , y − $[\textstyle {1\over2}]$ , z + 1; (xi) x, −y, z; (xii) x, y − 1, z; (xiii) x − $[\textstyle {1\over2}]$ , −y + $[\textstyle {1\over2}]$ , z; (xiv) x, y, z + 1; (xv) x, −y, z + 1; (xvi) x, −y + 2, z; (xviii) x, y + 1, z; (xix) x + $[\textstyle {1\over2}]$ , −y + $[\textstyle {1\over2}]$ , z + 1; (xx) x + $[\textstyle {1\over2}]$ , −y + $[\textstyle {1\over2}]$ , z; (xxi) x + $[\textstyle {1\over2}]$ , y + $[\textstyle {1\over2}]$ , z + 1.

Table 4
Bond-valence analysis (all values given in valence units, vu) for agrinierite

The bond-valence parameters were taken from Gagné & Hawthorne (2015). H – including a contribution of donor–hydrogen bonds; nH – maximum number of possible weak H⋯acceptor bonds to a particular site. Idealized bond strengths were taken from Brown (2002). Donor–H (0.8 vu), H⋯acceptor (0.2 vu). Site occupancies considered.

	U1	U2	U3	U4	U5	U6	M1	M2	K1	K2	K3	K4	Sum	Sum^H	nH
O1				0.64	0.48	0.64			0.02			0.08	1.86	1.86	1
O2					1.64				0.32				1.96	1.96	0
O3	0.71	0.55	0.50										1.76	1.76	1
O4				1.99			0.29		0.12				2.20	2.20	0
O5			1.75					0.37			0.07		1.93	1.93	0
O6			1.42				0.53			0.10			1.72	1.72	1
O7				1.74							0.59	0.30	2.18	2.18	0
O8	1.58							0.40					1.78	1.78	1
O9		0.70		0.67	0.65								2.02	2.02	0
O10	0.65				0.69	0.65							2.00	2.00	0
O11		1.53									0.06		1.59	1.59	2
O12	1.88									0.10			1.93	1.93	0
O13	0.53		0.46			0.22							1.21	2.01	0
O14	0.25				0.44	0.44							1.14	1.94	0
O15		1.68					0.46						1.91	1.91	0
O16		0.54	0.65	0.55							0.32		1.91	1.91	0
O17						1.42		0.34	0.14				1.66	1.66	2
O18					1.63							0.15	1.71	1.71	1
O19		0.42	0.44	0.20									1.06	1.86	1
O20		0.27		0.46	0.45								1.19	1.99	0
O21						1.62				0.17		0.54	1.97	1.97	0
O22	0.66		0.64			0.69				0.12			2.05	2.05	0
O23								0.24			0.03		0.27	1.87	1
O24										0.24			0.24	2.04	0
O25											0.18		0.18	1.78	1
O26							0.34		0.13				0.47	2.07	0
O27								0.23	0.07			0.01	0.31	1.91	0
O28											0.18	0.02	0.20	1.80	1
O29							0.26		0.08				0.34	1.94	0
O30										0.15			0.15	1.75	1
O31							0.24			0.22			0.46	2.06	0
O32								0.32	0.03				0.35	1.95	0
Sum	6.26	5.70	5.87	6.25	6.00	5.69	2.11	1.90	0.90	1.11	1.45	1.09

Subsequently, the structure of rameauite was reinvestigated and tested for twinning presence, following the same procedure as for agrinierite. We used the same reflection file as used in the study by Plášil et al. (2016), but we reprocessed it with a newer version of the CrysAlis software (version 40.64.67a). We employed a new structure solution and refinement using this reflection file for consistency [we emphasize that by using the original reflection file from the study by Plášil et al. (2016) and a twin-handling procedure in the current version of the Jana software (Jana2020), several problems occur, which can simply be overcome by using newly processed reflection files from the original diffraction frames]. The unit cell of rameauite, a = 13.947 (3), b = 14.300 (3), c = 13.888 (3) Å, β = 118.50 (3)° with V = 2434.3 (11) Å³, aligns with previous work (Plášil et al., 2016). The structure was solved using SHELXT in the monoclinic space group Cc (Flack 0.42 by SHELXT output). The structure refinement involved an inversion twin due to merohedry and, in the final stages, also a reticular twin contribution, finally featuring eight twin elements (due to the group > subgroup relationship between tetragonal > monoclinic symmetry groups). As some of the twin-domain fractions returned slightly negative values they were fixed to 0; the rest of the refined twin fractions, mirror in (101) and inversion twin, returned meaningful values. The final refinement converged to R = 4.24% for 2344 unique observed reflections with I > 3σ(I) and GOF = 1.48. Statistical details for the refinement are given in Table 1. Final atom coordinates and displacement parameters for agrinierite are listed in Table 5, selected interatomic distances in Table 6 and a bond-valence analysis in Table 7. The bond-valence analysis was performed following the procedure by Brown (2002, 2009) using bond-valence parameters provided by Gagné & Hawthorne (2015).

Table 5
Atom coordinates and isotropic and equivalent displacement parameters (Å) for rameauite

Atom	x/a	y/b	z/c	U_iso*/U_eq
U1	0.2214 (11)	0.50151 (9)	0.1010 (10)	0.0168 (6)
U2	0.0881 (11)	0.52239 (9)	0.2828 (10)	0.0196 (6)
U3	0.2102 (11)	0.00417 (9)	0.0935 (10)	0.0173 (5)
U4	0.4099 (11)	0.51689 (10)	0.4037 (10)	0.0173 (5)
U5	0.0692 (11)	−0.01326 (10)	0.2565 (10)	0.0170 (6)
U6	0.9025 (11)	0.51586 (10)	0.9074 (10)	0.0185 (6)
Ca1	0.0961 (13)	0.2526 (6)	0.1526 (12)	0.031 (3)
K1	0.2419 (13)	0.7507 (6)	0.2578 (12)	0.035 (3)
O1	0.200 (2)	0.3786 (16)	0.123 (2)	0.027 (6)*
O2	0.076 (2)	0.5070 (19)	0.429 (2)	0.026 (6)*
O3	0.092 (2)	0.6491 (13)	0.297 (2)	0.015 (4)*
K2	0.0953 (14)	0.7511 (7)	0.9147 (13)	0.037 (4)
O4	0.395 (2)	0.4876 (16)	0.2248 (19)	0.023 (6)*
O5	0.579 (2)	0.5040 (17)	0.9191 (19)	0.019 (5)*
O6	0.539 (2)	0.5270 (17)	0.584 (2)	0.018 (5)*
O7	0.038 (2)	0.5519 (17)	0.0945 (19)	0.024 (5)*
O8	0.238 (2)	0.5312 (18)	0.266 (2)	0.026 (6)*
O9	0.899 (2)	0.5389 (17)	0.236 (2)	0.024 (6)*
O10	0.028 (2)	0.747 (2)	0.084 (2)	0.033 (7)*
O11	0.283 (2)	0.5487 (17)	0.4747 (19)	0.031 (5)*
O12	0.240 (2)	0.623 (2)	0.082 (2)	0.037 (7)*
O13	0.892 (3)	0.396 (2)	0.942 (3)	0.052 (9)*
O14	0.419 (2)	0.8612 (14)	0.3798 (19)	0.015 (5)*
O15	0.735 (2)	0.518 (2)	0.763 (2)	0.038 (7)*
O16	0.081 (2)	0.3996 (17)	0.258 (2)	0.029 (7)*
O17	0.191 (2)	0.1289 (15)	0.110 (2)	0.022 (5)*
O18	0.073 (2)	0.1140 (14)	0.250 (2)	0.018 (5)*
O19	0.393 (3)	0.3907 (17)	0.420 (2)	0.031 (6)*
O20	0.253 (3)	0.2505 (17)	0.334 (3)	0.033 (6)*
O21	0.049 (3)	0.2527 (18)	−0.039 (2)	0.041 (8)*
O22	−0.111 (3)	0.7486 (18)	0.217 (3)	0.035 (7)*
O23	0.244 (2)	−0.1166 (19)	0.087 (2)	0.020 (6)*
O24	0.422 (2)	0.6448 (16)	0.391 (2)	0.031 (6)*
O25	0.073 (2)	−0.1438 (15)	0.2669 (18)	0.024 (6)*
O26	0.795 (2)	0.5542 (16)	0.9874 (19)	0.028 (5)*
O27	−0.231 (2)	0.7514 (19)	0.018 (2)	0.035 (7)*
O28	−0.086 (3)	0.254 (2)	0.127 (3)	0.055 (8)*

Table 6
Selected interatomic distances (Å) in the structure of rameauite

U1—O1	1.83 (3)	U2—O3	1.819 (15)	U3—O17	1.83 (3)
U1—O12	1.80 (3)	U2—O16	1.78 (3)	U3—O23	1.81 (3)
U1—O2ⁱ	2.28 (2)	U2—O7	2.41 (3)	U3—O5^vii	2.24 (2)
U1—O4	2.21 (2)	U2—O8	2.22 (4)	U3—O6^vi	2.36 (3)
U1—O7	2.61 (3)	U2—O9^iv	2.41 (3)	U3—O9^v	2.47 (2)
U1—O8	2.23 (3)	U2—O11	2.78 (2)	U3—O15^vi	2.22 (3)
U1—O11ⁱ	2.40 (4)	〈U2—O_Ur〉	1.80	U3—O26^vii	2.41 (4)
〈U1—O_Ur〉	1.81	〈U2—O_eq〉	2.39	〈U3—O_Ur〉	1.82
〈U1—O_eq〉	2.35			〈U3—O_eq〉	2.34

U4—O19	1.84 (3)	U5—O18	1.825 (15)	U6—O13	1.81 (3)
U4—O24	1.86 (3)	U5—O25	1.87 (3)	U6—O14^ix	1.839 (18)
U4—O4	2.43 (3)	U5—O4^v	2.25 (3)	U6—O2^x	2.32 (3)
U4—O5ⁱ	2.28 (3)	U5—O5^vi	2.19 (3)	U6—O7^xi	2.43 (2)
U4—O6	2.28 (2)	U5—O6^vi	2.24 (3)	U6—O9^xii	2.48 (3)
U4—O8	2.25 (2)	U5—O15^vi	2.28 (3)	U6—O15	2.23 (2)
U4—O11	2.45 (4)	〈U5—O_Ur〉	1.85	U6—O26	2.31 (4)
〈U4—O_Ur〉	1.85	〈U5—O_eq〉	2.24	〈U6—O_Ur〉	1.83
〈U4—O_eq〉	2.33			〈U6—O_eq〉	2.36

Ca1—O1	2.47 (3)	K1—O3	2.80 (3)	K2—O5^xvi	3.63 (3)
Ca1—O13ⁱⁱ	3.60 (3)	K1—O8	3.15 (3)	K2—O10^xvii	2.91 (4)
Ca1—O16	2.63 (3)	K1—O10	2.81 (2)	K2—O12^xvii	2.89 (3)
Ca1—O17	2.45 (3)	K1—O12	3.04 (3)	K2—O14^xviii	2.77 (3)
Ca1—O18	2.50 (3)	K1—O14	2.73 (2)	K2—O16^xii	3.01 (3)
Ca—O20	2.42 (3)	K1—O15^xiv	3.31 (3)	K2—O18^xii	2.90 (3)
Ca1—O21	2.42 (3)	K1—O23^xv	3.05 (3)	K2—O20^xii	2.91 (5)
Ca1—O28	2.39 (5)	K1—O24	2.75 (3)	K2—O23^xix	2.97 (3)
〈Ca1—O〉	2.61	K1—O25^xv	2.85 (3)	K2—O24^xviii	2.72 (3)
		K1—O27^ix	2.95 (3)	K2—O28^xii	3.57 (4)
		〈K1—O〉	2.97	K1—O33^ix	3.46 (3)
				〈K1—O〉	3.03
Symmetry codes: (i) x, −y + 1, z − $[\textstyle {1\over2}]$ ; (ii) x − 1, y, z − 1; (iv) x − 1, y, z; (v) x − $[\textstyle {1\over2}]$ , y − $[\textstyle {1\over2}]$ , z; (vi) x − $[\textstyle {1\over2}]$ , −y + $[\textstyle {1\over2}]$ , z − $[\textstyle {1\over2}]$ ; (vii) x − $[\textstyle {1\over2}]$ , y − $[\textstyle {1\over2}]$ , z − 1; (ix) x + $[\textstyle {1\over2}]$ , −y + $[\textstyle {3\over2}]$ , z + $[\textstyle {1\over2}]$ ; (x) x + 1, −y + 1, z + $[\textstyle {1\over2}]$ ; (xi) x + 1, y, z + 1; (xii) x, −y + 1, z + $[\textstyle {1\over2}]$ ; (xiv) x − $[\textstyle {1\over2}]$ , −y + $[\textstyle {3\over2}]$ , z − $[\textstyle {1\over2}]$ ; (xv) x, y + 1, z; (xvi) x − $[\textstyle {1\over2}]$ , y + $[\textstyle {1\over2}]$ , z; (xvii) x, y, z + 1; (xviii) x − $[\textstyle {1\over2}]$ , −y + $[\textstyle {3\over2}]$ , z + $[\textstyle {1\over2}]$ ; (xix) x, y + 1, z + 1.

Table 7
Bond-valence analysis (all values given in vu) for rameauite

The bond-valence parameters were taken from Gagné & Hawthorne (2015). H – including a contribution of donor–hydrogen bonds; nH – maximum number of possible weak H⋯acceptor bonds to the particular site. Idealized bond strengths were taken from Brown (2002) – donor–H (0.8 vu), H⋯acceptor (0.2 vu).

	U1	U2	U3	U4	U5	U6	Ca1	K1	K2	Sum	Sum^H	nH
O1	1.61						0.25			1.86	1.86	1
O2	0.61	0.86				0.56				2.03	2.03	0
O3		1.62						0.15		1.77	1.77	1
O4	0.71			0.44	0.65					1.80	1.80	1
O5			0.66	0.61	0.74				0.02	2.03	2.03	0
O6			0.51	0.61	0.66					1.79	1.79	1
O7	0.30	0.47				0.43				1.21	2.01	0
O8	0.68	0.69		0.65				0.06		2.08	2.08	0
O9		0.46	0.41			0.40				1.27	2.07	0
O10									0.11	0.11	1.71	1
O11	0.46	0.21		0.44						1.11	1.91	0
O12	1.68							0.15	0.12	1.95	1.95	0
O13						1.65	0.02			1.66	1.66	2
O14						1.55		0.08	0.16	1.79	1.79	1
O15			0.69		0.61	0.68		0.18		2.16	2.16	0
O16		1.75					0.17		0.09	2.01	2.01	0
O17			1.58				0.27			1.84	1.84	1
O18					1.60		0.23		0.12	1.95	1.95	0
O19				1.55						1.55	1.55	2
O20							0.29		0.11	0.40	2.00	0
O21							0.29			0.29	1.89	1
O22										0.00	1.60	2
O23			1.65					0.04	0.10	1.79	1.79	1
O24				1.48				0.08	0.18	1.75	1.75	1
O25					1.44			0.13		1.57	1.57	2
O26			0.46			0.57				1.04	1.84	1
O27								0.10		0.10	1.70	1
O28							0.31		0.02	0.33	1.93	0
Sum	6.05	6.06	5.97	5.78	5.70	5.84	1.82	0.98	1.04

Twin contributions for both minerals were evaluated also visually using the reciprocal layer reconstructions retrieved from the diffraction frames (the UNWARP tool within the CrysAlis software) and by computer methods using the program Jana2020 (Figs. 2). We have chosen the best representatives for twinning in both minerals to be displayed. Figs. 2(a) and 2(b) display the h1l layer of the reciprocal space in agrinierite, with apparently all reflections overlapping. This makes the recognition of the twin presence relatively difficult, at least more difficult than in the case of rameauite [Figs. 2(c) and 2(d)]. Although the diffraction intensities are vastly affected by the twin contributions, at least some of the observed reflections that are diagnostic (e.g. Petříček et al., 2016 ), i.e. warning us of twinning, are `visible' (i.e. are not completely overlapping as in the case of agrinierite).

Figure 2
Single-crystal diffraction patterns of agrinierite and rameauite. (a) Simulated h1l layer of the reciprocal space of agrinierite. Reflections from all domains overlap completely (i.e. `hidden twinning') due to twinning by metric merohedry and generate an F-centered (pseudo)orthorhombic pattern (the black array corresponds to the unit cell given by the previous structure determination). (b) Reciprocal space reconstruction (UNWARP tool) of the h1l layer from the experimental data for agrinierite. (c) Simulated h1l layer of the reciprocal space of rameauite. Reflections for the two main domains overlap only partially, due to twinning by reticular merohedry. The array corresponds to the supercell. (d) Reciprocal space reconstruction (UNWARP tool) of the h1l layer from the experimental data for rameauite.

For the evaluation of the twin type studied here, it is both necessary and useful to transform the C-centered unit cells into primitive ones. Otherwise, the results of the test for the higher-symmetry cell in Jana2020 will give correct results in terms of the searched cell, but the twin matrices will be applied to the conditions of the cell centering of our choice (and thus could be different from those without the applied conditions for centering and the systematic absences of reflections for the chosen space group). After C→P cell transformation the twin matrix of the mirror element for agrinierite is |1 0 0|0 1 0|1 0 1|, a mirror in (102), and for rameauite is |1/2 1/2 1/2|1/2 1/2 1/2|1 1 0|, a mirror in (111). Therefore, as the twin matrix for rameauite contains non-rational numbers, it appears to be twinned by reticular merohedry with apparent obliquity (diffraction type II). Agrinierite, with a matrix containing only rational numbers, thus appears to be twinned by metric merohedry [diffraction type I; see Petříček et al. (2016) for details]. To conclude, this is also the main reason for the distinct diffraction patterns of agrinierite [Figs. 2(a) and 2(b)] and rameauite [Figs. 2(c) and 2(d)]. In the case of agrinierite all reflections overlap (all displayed in red in the simulated pattern), whereas for agrinierite, they are separated (red and green) and form the pattern characteristic for this type of twin (we can call it an `hourglass'-like pattern; Petříček et al., 2016).

3.2. The refined structures of agrinierite and rameauite

The current structure model of agrinierite leaves the findings of Cahill & Burns (2000) about structure topology unchanged. Nevertheless, as the correct structure crystallizes in the monoclinic Cm space group, the single M²⁺-interlayer site in the model by Cahill & Burns (2000) is split into two symmetry non-equivalent sites. Moreover, Cahill & Burns (2000) restrained the occupation for Ca and Sr. The current model indicates that, while at one site (designated as M1) Sr is prevailing over Ca, at the second site (M2) Ca is slightly prevailing (Table 2). Therefore, we report the formula of agrinierite comprising two M²⁺ sites as K_3.758(Sr_0.89Ca_0.11)(Ca_0.57Sr_0.43)[(UO₂)₃O₃(OH)₂]₄·10H₂O, Z = 2. This formula is not electroneutral, having a 0.121 negative charge surplus; the scattering contribution of the K atoms, namely displacement parameters and occupation factors, is still probably vastly affected by twinning.

The same occurs for the structure model of rameauite, leaving the model proposed earlier by Plášil et al. (2016) unchanged in general. The fit to the data is better overall, as it can also be documented by the root-mean-squared deviation of the final bond-valence sums of the oxygen atoms within the structure (with the considered contribution of the D—H bonds, equal to 0.8 vu, for the H₂O and OH groups equally for both rameauite structure models). For the structure model given by Plášil et al. (2016), this is 0.25 vu, and for the currently presented model it is 0.14 vu. The formula of rameauite, based on refined occupancies and bond-valence calculations, is K₄Ca₂[(UO₂)₃O₃(OH)₂]₄·12H₂O, Z = 2. We report the formula based on the same Z as for agrinierite to obtain a better comparison.

4. Implications: the careful handling of structures with `hidden' twinning

The two uranyl-oxide hydroxy-hydrate minerals presented here demonstrate how careful one must be when handling diffraction data affected by twinning. Agrinierite is representative of a structure providing a single-crystal diffraction pattern with hidden twinning. From the symmetry and diffraction intensities, it is difficult in this particular case to discover the twinning at first glance. Nevertheless, there are some general guides (e.g. Petříček et al., 2016; Plášil et al., 2021 ) that are still valid:

(1) Awkward cell centering (systematic absences generated by the twinning) for the given symmetry of the structure affected by (unresolved) twinning. In the case of agrinierite it was an F-centered orthorhombic cell.

(2) Higher residuals. In the case of agrinierite R_obs > 6% along with the overestimated fit (S value from SHELX < 1 for the given weighting scheme).

Nevertheless, the handling of the twinned structures might not be as straightforward as for the untwinned structures. The second example, rameauite, is an illustrative case. The twinning features present in the structure (as documented in this study) were simply overlooked by one of the authors (JP). We emphasize that the tolerance limits (for maximal deviations for cell lengths and angles) had to be increased during the test for reticular twinning in Jana2020 for rameauite (up to 0.25 Å for cell lengths and 0.35° for angles). Then the procedure found the supercell of the higher symmetry unambiguously. We recommend doing so for cases of the worst diffraction data quality (and `worse' fitted unit-cell metrics, which could bias the algorithm). However, the presence has to be then verified every time by a reasonable and meaningful structure refinement. For complicated unusual cases, when ordinary indexing programs (like the algorithms in CrysAlis) for unit-cell search fail, we recommend using the Jana2020 built-in indexing feature, GrIndex. It is a powerful tool, not only for finding the unit cell even from biased data but also for various cell transformations and projections of data.

Supporting information

CCDC references: 2110502; 2115477

Crystal structure: contains datablocks general, agrinierite, rameauite. DOI: https://doi.org/10.1107/S1600576721009663/vb5019sup1.cif

Structure factors: contains datablock agrinierite. DOI: https://doi.org/10.1107/S1600576721009663/vb5019sup2.hkl

Structure factors: contains datablock rameauite. DOI: https://doi.org/10.1107/S1600576721009663/vb5019sup3.hkl

Computing details top

For both structures, data collection: CrysAlis PRO 1.171.39.46 (Rigaku OD, 2018); cell refinement: CrysAlis PRO 1.171.39.46 (Rigaku OD, 2018); data reduction: CrysAlis PRO 1.171.39.46 (Rigaku OD, 2018).

(agrinierite) top

Crystal data top

Ca_0.678K_3.758U₁₂O₅₄Sr_1.322	F(000) = 3343
M_r = 2005.1	D_x = 5.517 Mg m⁻³
Monoclinic, Cm	Mo Kα radiation, λ = 0.71073 Å
Hall symbol: C -2y	Cell parameters from 14868 reflections
a = 14.069 (3) Å	θ = 4.1–31°
b = 14.220 (3) Å	µ = 42.05 mm⁻¹
c = 13.967 (3) Å	T = 296 K
β = 120.24 (3)°	Tabular, orange
V = 2414.2 (12) Å³	0.12 × 0.07 × 0.02 mm
Z = 2

Data collection top

SuperNova, Dual, Cu at home/near, AtlasS2 diffractometer	7186 independent reflections
Radiation source: X-ray tube	6545 reflections with I > 3σ(I)
Mirror monochromator	R_int = 0.045
Detector resolution: 10.4054 pixels mm^-1	θ_max = 31.2°, θ_min = 3.3°
ω scans	h = −19→20
Absorption correction: multi-scan CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.	k = −20→20
T_min = 0.198, T_max = 1	l = −19→19
24870 measured reflections

Refinement top

Refinement on F²	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F² > 2σ(F²)] = 0.035	Weighting scheme based on measured s.u.'s w = 1/(σ²(I) + 0.003363I²)
wR(F²) = 0.098	(Δ/σ)_max = 0.049
S = 1.08	Δρ_max = 4.58 e Å⁻³
7186 reflections	Δρ_min = −4.24 e Å⁻³
206 parameters	Absolute structure: 3414 of Friedel pairs used in the refinement
0 restraints	Absolute structure parameter: 0.055 (13)
17 constraints

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å²) top

	x	y	z	U_iso*/U_eq	Occ. (<1)
U1	0.371711	0.759536	0.616595	0.0129 (5)
U2	0.1928 (3)	0.73988 (5)	0.25716 (7)	0.0131 (6)
U3	0.49507 (17)	0.7501 (2)	0.4369 (2)	0.0132 (5)
U4	0.37008 (12)	0.27269 (11)	0.11730 (11)	0.0122 (5)
U5	0.48845 (17)	0.23312 (3)	0.9369 (2)	0.0124 (4)
U6	0.6896 (2)	0.77272 (13)	0.75662 (13)	0.0156 (6)
Sr1	0.3431 (4)	0	0.2494 (5)	0.028 (2)	0.89 (3)
Sr1'	0.3431 (4)	0	0.2494 (5)	0.028 (2)	0.11 (3)
Sr2	0.5324 (5)	0.5	0.6242 (5)	0.013 (2)	0.43 (3)
Sr2'	0.5324 (5)	0.5	0.6242 (5)	0.013 (2)	0.57 (3)
K1	0.2984 (7)	0	0.9361 (14)	0.033 (4)
K2	0.5259 (7)	1	0.5946 (7)	0.023 (2)*	0.76 (2)
K3	0.3674 (6)	0.5	0.2524 (7)	0.0318 (18)*
K4	0.8533 (10)	0	0.9345 (11)	0.076 (6)
O1	0.8224 (19)	0.7678 (7)	0.937 (3)	0.027 (2)*
O2	0.4620 (15)	0.1083 (7)	0.935 (3)	0.0238 (19)*
O3	0.3304 (12)	0.7403 (13)	0.4431 (18)	0.017 (3)*
O4	0.3569 (13)	0.1534 (12)	0.1235 (13)	0.021 (4)*
O5	0.5224 (17)	0.631 (2)	0.4820 (17)	0.026 (6)*
O6	0.4730 (17)	0.875 (2)	0.3874 (16)	0.021 (5)*
O7	0.3965 (11)	0.3964 (11)	0.1223 (12)	0.014 (3)*
O8	0.4087 (15)	0.6352 (17)	0.6341 (14)	0.011 (4)*
O9	0.0252 (12)	0.7539 (12)	0.1116 (12)	0.014 (3)*
O10	0.8480 (12)	0.7338 (11)	0.7641 (11)	0.012 (3)*
O11	0.1689 (14)	0.6167 (15)	0.2818 (14)	0.025 (4)*
O12	0.3426 (15)	0.8801 (15)	0.5998 (14)	0.024 (4)*
O13	0.6892 (14)	0.7804 (12)	0.5586 (14)	0.015 (4)*
O14	0.053 (2)	0.6939 (18)	0.8100 (19)	0.022 (6)*
O15	0.210 (2)	0.862 (2)	0.2340 (18)	0.030 (6)*
O16	0.3597 (11)	0.6927 (10)	0.2751 (10)	0.013 (3)*
O17	0.6544 (11)	0.6446 (12)	0.7537 (12)	0.016 (3)*
O18	0.5188 (16)	0.3568 (7)	0.935 (3)	0.0229 (19)*
O19	0.5684 (14)	0.7034 (13)	0.3192 (14)	0.020 (4)*
O20	0.1810 (16)	0.7015 (15)	0.0650 (16)	0.011 (5)*
O21	0.7125 (14)	0.8993 (14)	0.7710 (13)	0.029 (5)*
O22	0.5240 (10)	0.7855 (9)	0.6074 (10)	0.006 (2)*
O23	0.3292 (18)	0.5	0.4734 (19)	0.036 (6)*
O24	0.671 (2)	1	0.541 (2)	0.054 (8)*
O25	0.5839 (19)	0.5	0.3128 (19)	0.037 (6)*
O26	0.185 (2)	0	0.059 (2)	0.029 (7)*
O27	0.5427 (19)	0.5	0.8131 (19)	0.026 (6)*
O28	0.675 (2)	0	1.055 (2)	0.062 (8)*
O29	0.482 (2)	0	0.179 (2)	0.051 (7)*
O30	0.503 (2)	0	0.774 (2)	0.051 (7)*
O31	0.8303 (18)	0.5	0.4306 (17)	0.024 (4)*
O32	0.7210 (18)	0.5	0.6618 (19)	0.034 (6)*

Atomic displacement parameters (Å²) top

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
U1	0.0082 (6)	0.0195 (9)	0.0082 (6)	0.0007 (8)	0.0021 (5)	0.0012 (7)
U2	0.0049 (6)	0.0151 (9)	0.0157 (7)	−0.0008 (8)	0.0026 (5)	0.0002 (7)
U3	0.0080 (7)	0.0196 (2)	0.0078 (2)	0.0010 (9)	0.0010 (7)	−0.0002 (2)
U4	0.0114 (6)	0.0115 (7)	0.0089 (6)	−0.0006 (7)	0.0017 (5)	0.0003 (8)
U5	0.0099 (7)	0.0160 (2)	0.0082 (2)	0.0000 (5)	0.0023 (7)	0.0004 (10)
U6	0.0029 (6)	0.0216 (9)	0.0185 (7)	0.0002 (6)	0.0026 (5)	−0.0022 (9)
Sr1	0.022 (2)	0.021 (4)	0.027 (2)	0	0.0031 (19)	0
Sr1'	0.022 (2)	0.021 (4)	0.027 (2)	0	0.0031 (19)	0
Sr2	0.011 (2)	0.010 (4)	0.011 (2)	0	0.0009 (18)	0
Sr2'	0.011 (2)	0.010 (4)	0.011 (2)	0	0.0009 (18)	0
K1	0.022 (5)	0.030 (3)	0.051 (3)	0	0.021 (5)	0
K4	0.157 (11)	0.023 (3)	0.0028 (17)	0	0.007 (8)	0

Geometric parameters (Å, º) top

U1—U3	3.704 (4)	O1—O9^xxii	2.67 (3)
U1—U5ⁱ	3.914 (4)	O1—O10	2.66 (5)
U1—U6	3.880 (4)	O1—O14ⁱⁱⁱ	3.32 (4)
U1—U6ⁱⁱ	3.955 (3)	O1—O17	3.01 (3)
U1—O3	2.21 (3)	O1—O18^xviii	3.06 (5)
U1—O5	3.92 (3)	O1—O20^xxiii	3.30 (6)
U1—O8	1.83 (3)	O1—O21	2.76 (3)
U1—O10ⁱⁱ	2.247 (16)	O2—O2^xii	3.080 (14)
U1—O12	1.748 (15)	O2—O4^xv	3.67 (4)
U1—O13ⁱⁱ	2.343 (14)	O2—O9^xi	3.00 (3)
U1—O14ⁱⁱⁱ	2.70 (2)	O2—O10^x	2.76 (3)
U1—O17	3.799 (13)	O2—O14^ix	2.90 (5)
U1—O22	2.244 (16)	O2—O17^x	3.796 (17)
U1—O30^iv	3.981 (10)	O2—O18	3.624 (17)
U2—U3	3.696 (5)	O2—O20^xi	2.98 (3)
U2—U4^v	3.964 (5)	O2—O28	3.02 (2)
U2—U4ⁱ	3.870 (4)	O2—O29^xv	3.62 (5)
U2—U5^vi	3.916 (4)	O2—O30	3.01 (5)
U2—O3	2.33 (2)	O2—O32^x	3.92 (3)
U2—O4ⁱ	3.930 (17)	O3—O5	2.92 (3)
U2—O6	3.91 (3)	O3—O6	3.15 (4)
U2—O9	2.214 (11)	O3—O8	2.76 (3)
U2—O11	1.845 (15)	O3—O11	2.849 (19)
U2—O15	1.80 (3)	O3—O12	2.90 (3)
U2—O16	2.335 (16)	O3—O13ⁱⁱ	3.14 (3)
U2—O19ⁱⁱ	2.453 (17)	O3—O15	3.07 (3)
U2—O20	2.66 (3)	O3—O16	2.67 (3)
U3—U4ⁱ	3.901 (4)	O3—O19ⁱⁱ	3.289 (18)
U3—U6	3.902 (4)	O3—O22	2.611 (17)
U3—O3	2.37 (2)	O3—O23	3.439 (15)
U3—O5	1.78 (3)	O3—O31^v	3.701 (14)
U3—O6	1.88 (3)	O4—O6ⁱ	3.21 (3)
U3—O8	3.88 (2)	O4—O7	3.50 (2)
U3—O13	2.418 (12)	O4—O9^ix	2.84 (2)
U3—O15	3.90 (2)	O4—O11^ix	3.827 (17)
U3—O16	2.249 (11)	O4—O15ⁱ	3.14 (4)
U3—O19	2.432 (17)	O4—O16ⁱ	3.03 (2)
U3—O22	2.256 (15)	O4—O19ⁱ	3.504 (17)
U4—U5^vii	3.696 (4)	O4—O20ⁱ	3.01 (3)
U4—K3	3.753 (6)	O4—O26	3.03 (2)
U4—O1^viii	2.26 (4)	O4—O29	2.66 (2)
U4—O4	1.720 (14)	O5—O5ⁱ	3.73 (4)
U4—O6ⁱ	3.90 (3)	O5—O6	3.65 (4)
U4—O7	1.785 (14)	O5—O8	3.23 (4)
U4—O9^ix	2.233 (16)	O5—O12ⁱⁱⁱ	3.95 (4)
U4—O15ⁱ	3.89 (3)	O5—O13	2.94 (3)
U4—O16ⁱ	2.329 (16)	O5—O16	2.77 (2)
U4—O19ⁱ	2.812 (10)	O5—O17	3.29 (3)
U4—O20ⁱ	2.41 (3)	O5—O19	2.85 (4)
U5—U6^x	3.697 (4)	O5—O22	2.80 (3)
U5—O1^x	2.39 (3)	O5—O23	3.24 (4)
U5—O2	1.811 (11)	O5—O25	3.45 (4)
U5—O9^xi	2.251 (15)	O5—O32	3.25 (3)
U5—O10^x	2.220 (11)	O6—O6^xvii	3.56 (4)
U5—O14^ix	2.43 (3)	O6—O11ⁱⁱⁱ	3.72 (4)
U5—O18	1.814 (13)	O6—O13	3.08 (3)
U5—O20^xi	2.42 (2)	O6—O15	3.21 (3)
U6—K2	3.953 (5)	O6—O16	3.03 (3)
U6—O1	2.26 (3)	O6—O19	3.15 (3)
U6—O5	3.90 (2)	O6—O22	3.06 (3)
U6—O8	3.943 (18)	O6—O24	3.08 (3)
U6—O10	2.247 (16)	O6—O29^iv	3.46 (4)
U6—O13	2.758 (16)	O6—O31^v	2.97 (4)
U6—O14ⁱⁱⁱ	2.43 (3)	O7—O7ⁱ	2.96 (2)
U6—O17	1.879 (14)	O7—O9^ix	2.77 (2)
U6—O21	1.819 (14)	O7—O15^ix	3.90 (3)
U6—O22	2.219 (10)	O7—O16ⁱ	2.74 (2)
Sr1—Sr1'	0	O7—O18^vii	3.83 (5)
Sr1—O4	2.861 (16)	O7—O19ⁱ	2.950 (16)
Sr1—O4^xii	2.861 (16)	O7—O20ⁱ	3.04 (3)
Sr1—O6^xiii	2.58 (2)	O7—O25	3.03 (2)
Sr1—O6ⁱ	2.58 (2)	O7—O28^vi	3.13 (3)
Sr1—O15^xiii	2.65 (3)	O8—O8ⁱ	3.84 (4)
Sr1—O15ⁱ	2.65 (3)	O8—O10ⁱⁱ	3.01 (3)
Sr1—O26	2.46 (2)	O8—O12	3.58 (3)
Sr1—O29	2.59 (3)	O8—O13ⁱⁱ	2.98 (2)
Sr1—O31^x	2.63 (3)	O8—O14ⁱⁱⁱ	3.32 (3)
Sr1'—O4	2.861 (16)	O8—O17	2.982 (18)
Sr1'—O4^xii	2.861 (16)	O8—O18ⁱ	3.68 (4)
Sr1'—O6^xiii	2.58 (2)	O8—O22	2.82 (3)
Sr1'—O6ⁱ	2.58 (2)	O8—O23	2.73 (3)
Sr1'—O15^xiii	2.65 (3)	O8—O24^x	3.49 (3)
Sr1'—O15ⁱ	2.65 (3)	O8—O27	2.96 (3)
Sr1'—O26	2.46 (2)	O9—O11	2.948 (17)
Sr1'—O29	2.59 (3)	O9—O15	2.75 (3)
Sr1'—O31^x	2.63 (3)	O9—O18^vi	2.84 (4)
Sr2—Sr2'	0	O9—O19ⁱⁱ	2.71 (2)
Sr2—O5	2.67 (3)	O9—O20	2.70 (4)
Sr2—O5ⁱ	2.67 (3)	O9—O29^v	3.855 (19)
Sr2—O8	2.64 (2)	O10—O12ⁱⁱⁱ	2.78 (2)
Sr2—O8ⁱ	2.64 (2)	O10—O13	2.679 (15)
Sr2—O17	2.710 (13)	O10—O14^xxiv	2.68 (3)
Sr2—O17ⁱ	2.710 (13)	O10—O17	2.95 (2)
Sr2—O23	2.56 (2)	O10—O18^xviii	2.96 (2)
Sr2—O27	2.57 (3)	O10—O21	3.05 (2)
Sr2—O32	2.43 (3)	O10—O30^xviii	3.94 (2)
Sr2'—O5	2.67 (3)	O10—O32	3.706 (16)
Sr2'—O5ⁱ	2.67 (3)	O11—O11ⁱ	3.33 (2)
Sr2'—O8	2.64 (2)	O11—O15	3.65 (3)
Sr2'—O8ⁱ	2.64 (2)	O11—O16	2.94 (2)
Sr2'—O17	2.710 (13)	O11—O19ⁱⁱ	3.09 (2)
Sr2'—O17ⁱ	2.710 (13)	O11—O20	3.34 (4)
Sr2'—O23	2.56 (2)	O11—O23	2.98 (2)
Sr2'—O27	2.57 (3)	O11—O24^x	3.97 (3)
Sr2'—O32	2.43 (3)	O11—O28^vi	3.62 (3)
K1—O1^x	3.822 (11)	O11—O29^v	2.82 (2)
K1—O1^xiv	3.822 (11)	O12—O12^xvii	3.41 (2)
K1—O2	2.78 (2)	O12—O13ⁱⁱ	2.99 (3)
K1—O2^xii	2.78 (2)	O12—O14ⁱⁱⁱ	3.12 (3)
K1—O4^xv	3.182 (17)	O12—O22	2.84 (3)
K1—O4^xvi	3.182 (17)	O12—O30^iv	2.89 (2)
K1—O17^x	3.105 (14)	O12—O31^v	2.84 (3)
K1—O17^xiv	3.105 (14)	O12—O32^v	2.85 (4)
K1—O26^xv	2.87 (4)	O13—O17	3.56 (2)
K1—O27^x	3.11 (3)	O13—O19	3.096 (18)
K1—O29^xv	3.06 (2)	O13—O21	3.28 (2)
K1—O32^x	3.41 (3)	O13—O22	2.72 (2)
K2—O6	3.15 (3)	O13—O24	3.139 (14)
K2—O6^xvii	3.15 (3)	O14—O17ⁱⁱ	3.00 (3)
K2—O12	3.12 (3)	O14—O18^v	3.08 (4)
K2—O12^xvii	3.12 (3)	O14—O20^xv	3.08 (3)
K2—O14^xviii	3.96 (3)	O14—O21ⁱⁱ	2.89 (4)
K2—O14ⁱⁱⁱ	3.96 (3)	O14—O22ⁱⁱ	2.67 (3)
K2—O21	2.921 (13)	O14—O30^v	2.83 (3)
K2—O21^xvii	2.921 (13)	O15—O15^xvii	3.92 (4)
K2—O22	3.056 (13)	O15—O16	3.06 (3)
K2—O22^xvii	3.056 (13)	O15—O18^vi	3.66 (4)
K2—O24	2.50 (4)	O15—O19ⁱⁱ	2.94 (4)
K2—O30^iv	2.68 (3)	O15—O20	3.16 (4)
K2—O31^v	2.54 (2)	O15—O25^v	3.19 (4)
K3—O5	3.39 (2)	O15—O26^iv	3.01 (4)
K3—O5ⁱ	3.39 (2)	O15—O31^v	3.10 (3)
K3—O7	2.531 (18)	O16—O19	2.67 (2)
K3—O7ⁱ	2.531 (18)	O16—O20	2.74 (2)
K3—O11	3.449 (18)	O16—O28^vi	3.962 (19)
K3—O11ⁱ	3.449 (18)	O17—O18ⁱ	3.85 (5)
K3—O16	2.771 (14)	O17—O21	3.69 (2)
K3—O16ⁱ	2.771 (14)	O17—O22	2.788 (17)
K3—O19	3.810 (15)	O17—O27	2.94 (3)
K3—O19ⁱ	3.810 (15)	O17—O32	2.83 (3)
K3—O20	3.87 (3)	O18—O20^xi	3.04 (3)
K3—O20ⁱ	3.87 (3)	O18—O21^x	3.77 (3)
K3—O23	3.39 (3)	O18—O26^xxi	2.92 (2)
K3—O25	2.72 (3)	O18—O27	2.78 (4)
K3—O28^vi	2.72 (2)	O19—O25	2.900 (15)
K4—O1^xiii	3.334 (11)	O20—O28^vi	2.86 (3)
K4—O1ⁱ	3.334 (11)	O21—O21^xvii	2.87 (2)
K4—O7^xi	2.801 (19)	O21—O22	2.964 (16)
K4—O7^xix	2.801 (19)	O21—O24	3.29 (3)
K4—O18^ix	3.09 (3)	O21—O30^iv	3.30 (3)
K4—O18^xx	3.09 (3)	O22—O30^iv	3.94 (2)
K4—O21^xiii	2.571 (14)	O23—O24^x	2.82 (5)
K4—O21ⁱ	2.571 (14)	O25—O31	2.99 (4)
K4—O27^ix	3.81 (4)	O26—O27^viii	2.98 (3)
K4—O28	3.66 (4)	O26—O29	3.64 (4)
O1—O2^xviii	3.01 (3)	O28—O29^xv	3.89 (5)
O1—O4^xxi	2.90 (4)	O28—O30	3.42 (3)
O1—O7^xxi	2.89 (3)	O30—O32^x	3.46 (4)

U3—U1—U5ⁱ	134.86 (6)	O20—O9—O29^v	92.5 (9)
U3—U1—U6	61.87 (5)	U1ⁱⁱⁱ—O10—U5^xviii	122.4 (7)
U3—U1—U6ⁱⁱ	166.44 (5)	U1ⁱⁱⁱ—O10—U6	123.3 (5)
U3—U1—O3	37.5 (4)	U1ⁱⁱⁱ—O10—O1	167.3 (7)
U3—U1—O5	26.8 (4)	U1ⁱⁱⁱ—O10—O2^xviii	122.0 (10)
U3—U1—O8	81.6 (5)	U1ⁱⁱⁱ—O10—O8ⁱⁱⁱ	37.2 (5)
U3—U1—O10ⁱⁱ	163.5 (3)	U1ⁱⁱⁱ—O10—O12ⁱⁱⁱ	38.9 (5)
U3—U1—O12	95.8 (8)	U1ⁱⁱⁱ—O10—O13	56.0 (5)
U3—U1—O13ⁱⁱ	124.5 (4)	U1ⁱⁱⁱ—O10—O14^xxiv	65.8 (7)
U3—U1—O14ⁱⁱⁱ	99.1 (7)	U1ⁱⁱⁱ—O10—O17	122.4 (5)
U3—U1—O17	66.4 (2)	U1ⁱⁱⁱ—O10—O18^xviii	106.3 (10)
U3—U1—O22	34.7 (3)	U1ⁱⁱⁱ—O10—O21	112.3 (6)
U3—U1—O30^iv	99.2 (5)	U1ⁱⁱⁱ—O10—O30^xviii	74.5 (6)
U5ⁱ—U1—U6	73.09 (6)	U1ⁱⁱⁱ—O10—O32	87.1 (6)
U5ⁱ—U1—U6ⁱⁱ	56.04 (6)	U5^xviii—O10—U6	111.7 (7)
U5ⁱ—U1—O3	170.3 (4)	U5^xviii—O10—O1	57.8 (6)
U5ⁱ—U1—O5	122.9 (3)	U5^xviii—O10—O2^xviii	40.9 (4)
U5ⁱ—U1—O8	86.9 (4)	U5^xviii—O10—O8ⁱⁱⁱ	107.0 (6)
U5ⁱ—U1—O10ⁱⁱ	28.6 (3)	U5^xviii—O10—O12ⁱⁱⁱ	122.2 (7)
U5ⁱ—U1—O12	93.5 (5)	U5^xviii—O10—O13	166.0 (7)
U5ⁱ—U1—O13ⁱⁱ	98.9 (4)	U5^xviii—O10—O14^xxiv	58.5 (6)
U5ⁱ—U1—O14ⁱⁱⁱ	37.8 (7)	U5^xviii—O10—O17	110.2 (6)
U5ⁱ—U1—O17	72.8 (2)	U5^xviii—O10—O18^xviii	37.7 (5)
U5ⁱ—U1—O22	101.6 (3)	U5^xviii—O10—O21	101.3 (6)
U5ⁱ—U1—O30^iv	62.3 (4)	U5^xviii—O10—O30^xviii	77.5 (5)
U6—U1—U6ⁱⁱ	128.74 (4)	U5^xviii—O10—O32	113.9 (6)
U6—U1—O3	99.3 (4)	U6—O10—O1	53.9 (6)
U6—U1—O5	60.0 (3)	U6—O10—O2^xviii	109.2 (9)
U6—U1—O8	78.4 (4)	U6—O10—O8ⁱⁱⁱ	113.4 (6)
U6—U1—O10ⁱⁱ	101.6 (3)	U6—O10—O12ⁱⁱⁱ	119.5 (7)
U6—U1—O12	98.6 (8)	U6—O10—O13	67.4 (5)
U6—U1—O13ⁱⁱ	166.3 (3)	U6—O10—O14^xxiv	170.2 (8)
U6—U1—O14ⁱⁱⁱ	38.4 (7)	U6—O10—O17	39.6 (4)
U6—U1—O17	28.3 (2)	U6—O10—O18^xviii	106.1 (9)
U6—U1—O22	29.4 (3)	U6—O10—O21	36.3 (4)
U6—U1—O30^iv	65.4 (4)	U6—O10—O30^xviii	136.6 (7)
U6ⁱⁱ—U1—O3	130.4 (4)	U6—O10—O32	85.8 (6)
U6ⁱⁱ—U1—O5	145.5 (4)	O1—O10—O2^xviii	67.5 (9)
U6ⁱⁱ—U1—O8	92.1 (5)	O1—O10—O8ⁱⁱⁱ	130.3 (7)
U6ⁱⁱ—U1—O10ⁱⁱ	28.3 (3)	O1—O10—O12ⁱⁱⁱ	153.6 (8)
U6ⁱⁱ—U1—O12	90.9 (9)	O1—O10—O13	120.2 (8)
U6ⁱⁱ—U1—O13ⁱⁱ	43.1 (4)	O1—O10—O14^xxiv	116.3 (8)
U6ⁱⁱ—U1—O14ⁱⁱⁱ	93.1 (7)	O1—O10—O17	64.8 (6)
U6ⁱⁱ—U1—O17	118.2 (2)	O1—O10—O18^xviii	65.7 (10)
U6ⁱⁱ—U1—O22	157.6 (3)	O1—O10—O21	57.3 (5)
U6ⁱⁱ—U1—O30^iv	93.6 (5)	O1—O10—O30^xviii	116.5 (7)
O3—U1—O5	47.4 (5)	O1—O10—O32	104.5 (8)
O3—U1—O8	85.6 (6)	O2^xviii—O10—O8ⁱⁱⁱ	134.8 (8)
O3—U1—O10ⁱⁱ	158.7 (5)	O2^xviii—O10—O12ⁱⁱⁱ	95.6 (9)
O3—U1—O12	93.5 (6)	O2^xviii—O10—O13	153.1 (7)
O3—U1—O13ⁱⁱ	87.4 (5)	O2^xviii—O10—O14^xxiv	64.5 (9)
O3—U1—O14ⁱⁱⁱ	136.4 (8)	O2^xviii—O10—O17	83.3 (6)
O3—U1—O17	97.6 (4)	O2^xviii—O10—O18^xviii	78.6 (6)
O3—U1—O22	71.9 (5)	O2^xviii—O10—O21	124.8 (10)
O3—U1—O30^iv	120.5 (6)	O2^xviii—O10—O30^xviii	49.6 (9)
O5—U1—O8	54.8 (7)	O2^xviii—O10—O32	73.1 (5)
O5—U1—O10ⁱⁱ	145.5 (5)	O8ⁱⁱⁱ—O10—O12ⁱⁱⁱ	76.1 (7)
O5—U1—O12	122.5 (10)	O8ⁱⁱⁱ—O10—O13	62.8 (5)
O5—U1—O13ⁱⁱ	119.2 (5)	O8ⁱⁱⁱ—O10—O14^xxiv	71.2 (8)
O5—U1—O14ⁱⁱⁱ	97.4 (8)	O8ⁱⁱⁱ—O10—O17	140.8 (5)
O5—U1—O17	50.4 (4)	O8ⁱⁱⁱ—O10—O18^xviii	76.0 (9)
O5—U1—O22	44.4 (5)	O8ⁱⁱⁱ—O10—O21	85.1 (6)
O5—U1—O30^iv	117.0 (6)	O8ⁱⁱⁱ—O10—O30^xviii	102.9 (8)
O8—U1—O10ⁱⁱ	94.8 (6)	O8ⁱⁱⁱ—O10—O32	123.5 (8)
O8—U1—O12	176.7 (11)	O12ⁱⁱⁱ—O10—O13	66.5 (6)
O8—U1—O13ⁱⁱ	90.3 (6)	O12ⁱⁱⁱ—O10—O14^xxiv	69.6 (9)
O8—U1—O14ⁱⁱⁱ	92.3 (7)	O12ⁱⁱⁱ—O10—O17	94.1 (7)
O8—U1—O17	50.2 (5)	O12ⁱⁱⁱ—O10—O18^xviii	133.1 (11)
O8—U1—O22	87.1 (6)	O12ⁱⁱⁱ—O10—O21	135.8 (6)
O8—U1—O30^iv	137.4 (4)	O12ⁱⁱⁱ—O10—O30^xviii	47.2 (5)
O10ⁱⁱ—U1—O12	87.2 (8)	O12ⁱⁱⁱ—O10—O32	49.6 (7)
O10ⁱⁱ—U1—O13ⁱⁱ	71.4 (5)	O13—O10—O14^xxiv	121.8 (9)
O10ⁱⁱ—U1—O14ⁱⁱⁱ	64.8 (8)	O13—O10—O17	78.4 (5)
O10ⁱⁱ—U1—O17	98.9 (4)	O13—O10—O18^xviii	128.3 (8)
O10ⁱⁱ—U1—O22	129.4 (4)	O13—O10—O21	69.4 (5)
O10ⁱⁱ—U1—O30^iv	72.6 (6)	O13—O10—O30^xviii	113.2 (6)
O12—U1—O13ⁱⁱ	92.8 (9)	O13—O10—O32	80.0 (5)
O12—U1—O14ⁱⁱⁱ	86.1 (8)	O14^xxiv—O10—O17	141.2 (9)
O12—U1—O17	126.9 (8)	O14^xxiv—O10—O18^xviii	66.0 (9)
O12—U1—O22	89.7 (10)	O14^xxiv—O10—O21	140.1 (8)
O12—U1—O30^iv	40.9 (6)	O14^xxiv—O10—O30^xviii	45.8 (7)
O13ⁱⁱ—U1—O14ⁱⁱⁱ	136.2 (8)	O14^xxiv—O10—O32	98.9 (8)
O13ⁱⁱ—U1—O17	139.3 (4)	O17—O10—O18^xviii	130.5 (11)
O13ⁱⁱ—U1—O22	159.2 (5)	O17—O10—O21	75.8 (5)
O13ⁱⁱ—U1—O30^iv	121.3 (6)	O17—O10—O30^xviii	97.0 (6)
O14ⁱⁱⁱ—U1—O17	51.6 (7)	O17—O10—O32	48.7 (6)
O14ⁱⁱⁱ—U1—O22	64.6 (8)	O18^xviii—O10—O21	77.7 (6)
O14ⁱⁱⁱ—U1—O30^iv	45.2 (6)	O18^xviii—O10—O30^xviii	105.0 (6)
O17—U1—O22	46.7 (4)	O18^xviii—O10—O32	151.5 (6)
O17—U1—O30^iv	90.7 (4)	O21—O10—O30^xviii	172.0 (8)
O22—U1—O30^iv	72.6 (6)	O21—O10—O32	121.0 (6)
U3—U2—U4^v	166.12 (8)	O30^xviii—O10—O32	53.6 (5)
U3—U2—U4ⁱ	62.02 (9)	U2—O11—K3	101.5 (6)
U3—U2—U5^vi	135.14 (13)	U2—O11—O3	54.5 (5)
U3—U2—O3	38.6 (6)	U2—O11—O4^v	91.7 (5)
U3—U2—O4ⁱ	63.68 (17)	U2—O11—O6ⁱⁱ	106.6 (8)
U3—U2—O6	28.4 (4)	U2—O11—O9	48.6 (4)
U3—U2—O9	161.8 (5)	U2—O11—O11ⁱ	161.3 (9)
U3—U2—O11	99.5 (4)	U2—O11—O15	1.5 (6)
U3—U2—O15	82.6 (7)	U2—O11—O16	52.5 (5)
U3—U2—O16	35.5 (3)	U2—O11—O19ⁱⁱ	52.4 (5)
U3—U2—O19ⁱⁱ	122.1 (2)	U2—O11—O20	52.7 (6)
U3—U2—O20	99.2 (6)	U2—O11—O23	124.7 (6)
U4^v—U2—U4ⁱ	128.76 (4)	U2—O11—O24^x	130.5 (6)
U4^v—U2—U5^vi	55.94 (7)	U2—O11—O28^vi	100.6 (7)
U4^v—U2—O3	130.6 (6)	U2—O11—O29^v	132.4 (6)
U4^v—U2—O4ⁱ	121.44 (16)	K3—O11—O3	91.2 (5)
U4^v—U2—O6	143.8 (4)	K3—O11—O4^v	139.3 (4)
U4^v—U2—O9	27.1 (4)	K3—O11—O6ⁱⁱ	150.2 (6)
U4^v—U2—O11	86.1 (4)	K3—O11—O9	119.5 (6)
U4^v—U2—O15	91.3 (8)	K3—O11—O11ⁱ	61.2 (4)
U4^v—U2—O16	158.2 (3)	K3—O11—O15	103.1 (7)
U4^v—U2—O19ⁱⁱ	44.7 (2)	K3—O11—O16	50.6 (4)
U4^v—U2—O20	93.0 (5)	K3—O11—O19ⁱⁱ	152.4 (6)
U4ⁱ—U2—U5^vi	73.23 (7)	K3—O11—O20	69.5 (6)
U4ⁱ—U2—O3	100.3 (6)	K3—O11—O23	63.0 (7)
U4ⁱ—U2—O4ⁱ	25.5 (2)	K3—O11—O24^x	105.8 (5)
U4ⁱ—U2—O6	60.1 (5)	K3—O11—O28^vi	45.2 (4)
U4ⁱ—U2—O9	101.7 (4)	K3—O11—O29^v	104.9 (7)
U4ⁱ—U2—O11	106.0 (5)	O3—O11—O4^v	126.7 (6)
U4ⁱ—U2—O15	77.0 (11)	O3—O11—O6ⁱⁱ	97.0 (8)
U4ⁱ—U2—O16	33.9 (3)	O3—O11—O9	100.4 (6)
U4ⁱ—U2—O19ⁱⁱ	161.9 (3)	O3—O11—O11ⁱ	127.9 (5)
U4ⁱ—U2—O20	37.9 (6)	O3—O11—O15	54.7 (6)
U5^vi—U2—O3	173.5 (6)	O3—O11—O16	54.9 (7)
U5^vi—U2—O4ⁱ	74.78 (16)	O3—O11—O19ⁱⁱ	67.0 (5)
U5^vi—U2—O6	122.0 (4)	O3—O11—O20	96.5 (8)
U5^vi—U2—O9	29.0 (4)	O3—O11—O23	72.2 (5)
U5^vi—U2—O11	95.3 (3)	O3—O11—O24^x	84.3 (7)
U5^vi—U2—O15	84.6 (7)	O3—O11—O28^vi	127.9 (8)
U5^vi—U2—O16	103.6 (3)	O3—O11—O29^v	158.7 (11)
U5^vi—U2—O19ⁱⁱ	99.6 (3)	O4^v—O11—O6ⁱⁱ	50.2 (4)
U5^vi—U2—O20	37.5 (5)	O4^v—O11—O9	47.4 (4)
O3—U2—O4ⁱ	99.9 (6)	O4^v—O11—O11ⁱ	97.7 (4)
O3—U2—O6	53.6 (7)	O4^v—O11—O15	90.5 (5)
O3—U2—O9	157.5 (8)	O4^v—O11—O16	137.1 (5)
O3—U2—O11	85.3 (5)	O4^v—O11—O19ⁱⁱ	59.7 (4)
O3—U2—O15	95.1 (8)	O4^v—O11—O20	89.8 (5)
O3—U2—O16	69.9 (7)	O4^v—O11—O23	136.1 (8)
O3—U2—O19ⁱⁱ	86.9 (6)	O4^v—O11—O24^x	93.5 (6)
O3—U2—O20	136.1 (8)	O4^v—O11—O28^vi	94.7 (5)
O4ⁱ—U2—O6	48.2 (5)	O4^v—O11—O29^v	43.9 (4)
O4ⁱ—U2—O9	98.1 (5)	O6ⁱⁱ—O11—O9	87.3 (6)
O4ⁱ—U2—O11	131.4 (6)	O6ⁱⁱ—O11—O11ⁱ	91.8 (6)
O4ⁱ—U2—O15	51.6 (11)	O6ⁱⁱ—O11—O15	105.1 (8)
O4ⁱ—U2—O16	50.2 (4)	O6ⁱⁱ—O11—O16	150.7 (7)
O4ⁱ—U2—O19ⁱⁱ	137.2 (4)	O6ⁱⁱ—O11—O19ⁱⁱ	54.2 (6)
O4ⁱ—U2—O20	49.9 (6)	O6ⁱⁱ—O11—O20	137.1 (7)
O6—U2—O9	137.8 (5)	O6ⁱⁱ—O11—O23	92.3 (8)
O6—U2—O11	127.9 (5)	O6ⁱⁱ—O11—O24^x	47.2 (6)
O6—U2—O15	54.3 (8)	O6ⁱⁱ—O11—O28^vi	135.1 (6)
O6—U2—O16	50.6 (6)	O6ⁱⁱ—O11—O29^v	62.1 (8)
O6—U2—O19ⁱⁱ	114.0 (6)	O9—O11—O11ⁱ	131.4 (5)
O6—U2—O20	96.1 (8)	O9—O11—O15	47.9 (5)
O9—U2—O11	92.7 (5)	O9—O11—O16	90.0 (6)
O9—U2—O15	85.8 (7)	O9—O11—O19ⁱⁱ	53.2 (4)
O9—U2—O16	132.5 (5)	O9—O11—O20	50.3 (6)
O9—U2—O19ⁱⁱ	70.7 (5)	O9—O11—O23	172.5 (6)
O9—U2—O20	66.4 (7)	O9—O11—O24^x	134.2 (7)
O11—U2—O15	176.9 (12)	O9—O11—O28^vi	84.7 (5)
O11—U2—O16	88.7 (6)	O9—O11—O29^v	83.8 (5)
O11—U2—O19ⁱⁱ	91.0 (6)	O11ⁱ—O11—O15	162.7 (8)
O11—U2—O20	93.9 (8)	O11ⁱ—O11—O16	111.5 (6)
O15—U2—O16	94.3 (10)	O11ⁱ—O11—O19ⁱⁱ	145.8 (7)
O15—U2—O19ⁱⁱ	85.9 (11)	O11ⁱ—O11—O20	111.0 (7)
O15—U2—O20	88.0 (12)	O11ⁱ—O11—O23	56.1 (4)
O16—U2—O19ⁱⁱ	156.7 (4)	O11ⁱ—O11—O24^x	65.2 (4)
O16—U2—O20	66.2 (6)	O11ⁱ—O11—O28^vi	62.6 (4)
O19ⁱⁱ—U2—O20	137.0 (6)	O11ⁱ—O11—O29^v	53.8 (4)
U1—U3—U2	71.94 (8)	O15—O11—O16	54.0 (6)
U1—U3—U4ⁱ	133.10 (8)	O15—O11—O19ⁱⁱ	50.9 (6)
U1—U3—U6	61.28 (7)	O15—O11—O20	53.6 (7)
U1—U3—O3	34.5 (6)	O15—O11—O23	125.4 (6)
U1—U3—O5	83.3 (11)	O15—O11—O24^x	129.7 (6)
U1—U3—O6	99.8 (10)	O15—O11—O28^vi	101.7 (7)
U1—U3—O8	27.8 (4)	O15—O11—O29^v	131.5 (6)
U1—U3—O13	105.3 (4)	O16—O11—O19ⁱⁱ	101.9 (6)
U1—U3—O15	79.4 (5)	O16—O11—O20	51.3 (5)
U1—U3—O16	104.3 (4)	O16—O11—O23	86.8 (7)
U1—U3—O19	166.0 (4)	O16—O11—O24^x	126.6 (5)
U1—U3—O22	34.5 (4)	O16—O11—O28^vi	73.5 (6)
U2—U3—U4ⁱ	61.18 (7)	O16—O11—O29^v	146.4 (9)
U2—U3—U6	133.20 (12)	O19ⁱⁱ—O11—O20	95.3 (7)
U2—U3—O3	37.7 (6)	O19ⁱⁱ—O11—O23	121.0 (7)
U2—U3—O5	99.8 (8)	O19ⁱⁱ—O11—O24^x	89.3 (6)
U2—U3—O6	82.3 (7)	O19ⁱⁱ—O11—O28^vi	137.9 (5)
U2—U3—O8	78.57 (17)	O19ⁱⁱ—O11—O29^v	100.6 (7)
U2—U3—O13	171.8 (4)	O20—O11—O23	130.6 (10)
U2—U3—O15	27.3 (4)	O20—O11—O24^x	175.2 (8)
U2—U3—O16	37.1 (4)	O20—O11—O28^vi	48.3 (6)
U2—U3—O19	105.2 (3)	O20—O11—O29^v	102.0 (8)
U2—U3—O22	105.0 (4)	O23—O11—O24^x	45.2 (8)
U4ⁱ—U3—U6	165.61 (11)	O23—O11—O28^vi	100.8 (7)
U4ⁱ—U3—O3	98.7 (6)	O23—O11—O29^v	102.5 (6)
U4ⁱ—U3—O5	102.6 (9)	O24^x—O11—O28^vi	127.8 (5)
U4ⁱ—U3—O6	76.0 (8)	O24^x—O11—O29^v	78.1 (7)
U4ⁱ—U3—O8	130.9 (2)	O28^vi—O11—O29^v	73.1 (8)
U4ⁱ—U3—O13	121.3 (4)	U1—O12—K2	113.6 (12)
U4ⁱ—U3—O15	59.8 (5)	U1—O12—O3	49.4 (6)
U4ⁱ—U3—O16	32.2 (4)	U1—O12—O5ⁱⁱ	99.0 (10)
U4ⁱ—U3—O19	45.8 (2)	U1—O12—O8	1.7 (5)
U4ⁱ—U3—O22	164.1 (3)	U1—O12—O10ⁱⁱ	53.9 (6)
U6—U3—O3	95.7 (6)	U1—O12—O12^xvii	168.4 (12)
U6—U3—O5	76.8 (7)	U1—O12—O13ⁱⁱ	51.5 (6)
U6—U3—O6	103.7 (7)	U1—O12—O14ⁱⁱⁱ	59.9 (7)
U6—U3—O8	60.8 (2)	U1—O12—O22	52.3 (7)
U6—U3—O13	44.5 (4)	U1—O12—O30^iv	115.9 (8)
U6—U3—O15	132.1 (5)	U1—O12—O31^v	127.7 (11)
U6—U3—O16	158.6 (4)	U1—O12—O32^v	133.0 (13)
U6—U3—O19	120.4 (3)	K2—O12—O3	95.5 (9)
U6—U3—O22	29.1 (3)	K2—O12—O5ⁱⁱ	142.6 (6)
O3—U3—O5	88.1 (11)	K2—O12—O8	112.0 (8)
O3—U3—O6	95.1 (10)	K2—O12—O10ⁱⁱ	131.3 (7)
O3—U3—O8	44.6 (6)	K2—O12—O12^xvii	56.8 (6)
O3—U3—O13	139.7 (7)	K2—O12—O13ⁱⁱ	159.7 (9)
O3—U3—O15	51.9 (7)	K2—O12—O14ⁱⁱⁱ	78.7 (8)
O3—U3—O16	70.5 (7)	K2—O12—O22	61.5 (6)
O3—U3—O19	139.7 (6)	K2—O12—O30^iv	52.8 (8)
O3—U3—O22	68.7 (7)	K2—O12—O31^v	50.3 (6)
O5—U3—O6	176.7 (15)	K2—O12—O32^v	108.1 (6)
O5—U3—O8	55.6 (12)	O3—O12—O5ⁱⁱ	91.9 (7)
O5—U3—O13	87.4 (8)	O3—O12—O8	49.0 (5)
O5—U3—O15	127.1 (9)	O3—O12—O10ⁱⁱ	100.9 (7)
O5—U3—O16	86.2 (8)	O3—O12—O12^xvii	133.4 (8)
O5—U3—O19	83.7 (11)	O3—O12—O13ⁱⁱ	64.5 (6)
O5—U3—O22	86.9 (10)	O3—O12—O14ⁱⁱⁱ	98.6 (9)
O6—U3—O8	127.6 (11)	O3—O12—O22	54.2 (5)
O6—U3—O13	90.7 (8)	O3—O12—O30^iv	140.0 (12)
O6—U3—O15	55.0 (8)	O3—O12—O31^v	80.3 (7)
O6—U3—O16	94.0 (7)	O3—O12—O32^v	145.5 (9)
O6—U3—O19	93.3 (11)	O5ⁱⁱ—O12—O8	100.5 (7)
O6—U3—O22	95.1 (10)	O5ⁱⁱ—O12—O10ⁱⁱ	82.5 (8)
O8—U3—O13	102.6 (4)	O5ⁱⁱ—O12—O12^xvii	92.3 (8)
O8—U3—O15	96.5 (5)	O5ⁱⁱ—O12—O13ⁱⁱ	47.6 (6)
O8—U3—O16	98.8 (5)	O5ⁱⁱ—O12—O14ⁱⁱⁱ	136.2 (10)
O8—U3—O19	138.8 (5)	O5ⁱⁱ—O12—O22	144.3 (7)
O8—U3—O22	45.8 (5)	O5ⁱⁱ—O12—O30^iv	128.0 (10)
O13—U3—O15	145.4 (5)	O5ⁱⁱ—O12—O31^v	95.5 (8)
O13—U3—O16	148.8 (6)	O5ⁱⁱ—O12—O32^v	54.1 (7)
O13—U3—O19	79.4 (5)	O8—O12—O10ⁱⁱ	54.9 (5)
O13—U3—O22	71.2 (5)	O8—O12—O12^xvii	167.0 (9)
O15—U3—O16	51.5 (5)	O8—O12—O13ⁱⁱ	53.1 (4)
O15—U3—O19	104.5 (5)	O8—O12—O14ⁱⁱⁱ	59.1 (6)
O15—U3—O22	104.4 (6)	O8—O12—O22	50.6 (5)
O16—U3—O19	69.6 (5)	O8—O12—O30^iv	115.0 (6)
O16—U3—O22	138.8 (6)	O8—O12—O31^v	126.8 (9)
O19—U3—O22	149.4 (4)	O8—O12—O32^v	134.4 (9)
U2^ix—U4—U2ⁱ	127.97 (6)	O10ⁱⁱ—O12—O12^xvii	125.7 (8)
U2^ix—U4—U3ⁱ	71.45 (7)	O10ⁱⁱ—O12—O13ⁱⁱ	55.2 (5)
U2^ix—U4—U5^vii	61.37 (6)	O10ⁱⁱ—O12—O14ⁱⁱⁱ	53.7 (7)
U2^ix—U4—K3	98.78 (12)	O10ⁱⁱ—O12—O22	92.6 (6)
U2^ix—U4—O1^viii	99.9 (7)	O10ⁱⁱ—O12—O30^iv	88.0 (6)
U2^ix—U4—O4	89.1 (4)	O10ⁱⁱ—O12—O31^v	177.7 (13)
U2^ix—U4—O6ⁱ	71.6 (4)	O10ⁱⁱ—O12—O32^v	82.4 (9)
U2^ix—U4—O7	86.3 (4)	O12^xvii—O12—O13ⁱⁱ	139.5 (10)
U2^ix—U4—O9^ix	26.8 (3)	O12^xvii—O12—O14ⁱⁱⁱ	109.7 (7)
U2^ix—U4—O15ⁱ	119.8 (3)	O12^xvii—O12—O22	118.3 (10)
U2^ix—U4—O16ⁱ	99.1 (3)	O12^xvii—O12—O30^iv	53.9 (4)
U2^ix—U4—O19ⁱ	37.8 (3)	O12^xvii—O12—O31^v	53.1 (5)
U2^ix—U4—O20ⁱ	169.9 (7)	O12^xvii—O12—O32^v	53.2 (7)
U2ⁱ—U4—U3ⁱ	56.79 (6)	O13ⁱⁱ—O12—O14ⁱⁱⁱ	100.1 (7)
U2ⁱ—U4—U5^vii	164.38 (5)	O13ⁱⁱ—O12—O22	101.4 (6)
U2ⁱ—U4—K3	67.28 (15)	O13ⁱⁱ—O12—O30^iv	142.3 (9)
U2ⁱ—U4—O1^viii	130.9 (7)	O13ⁱⁱ—O12—O31^v	124.1 (6)
U2ⁱ—U4—O4	79.2 (6)	O13ⁱⁱ—O12—O32^v	91.4 (9)
U2ⁱ—U4—O6ⁱ	60.5 (5)	O14ⁱⁱⁱ—O12—O22	53.0 (8)
U2ⁱ—U4—O7	101.4 (6)	O14ⁱⁱⁱ—O12—O30^iv	56.0 (6)
U2ⁱ—U4—O9^ix	154.0 (3)	O14ⁱⁱⁱ—O12—O31^v	128.2 (12)
U2ⁱ—U4—O15ⁱ	26.9 (4)	O14ⁱⁱⁱ—O12—O32^v	110.3 (9)
U2ⁱ—U4—O16ⁱ	34.0 (3)	O22—O12—O30^iv	86.9 (9)
U2ⁱ—U4—O19ⁱ	93.7 (4)	O22—O12—O31^v	89.7 (10)
U2ⁱ—U4—O20ⁱ	42.7 (7)	O22—O12—O32^v	160.3 (7)
U3ⁱ—U4—U5^vii	132.00 (7)	O30^iv—O12—O31^v	92.3 (8)
U3ⁱ—U4—K3	66.99 (13)	O30^iv—O12—O32^v	74.0 (8)
U3ⁱ—U4—O1^viii	169.7 (6)	O31^v—O12—O32^v	95.5 (8)
U3ⁱ—U4—O4	81.6 (4)	U1ⁱⁱⁱ—O13—U3	148.6 (7)
U3ⁱ—U4—O6ⁱ	27.8 (4)	U1ⁱⁱⁱ—O13—U6	101.4 (4)
U3ⁱ—U4—O7	94.2 (4)	U1ⁱⁱⁱ—O13—O3ⁱⁱⁱ	44.5 (4)
U3ⁱ—U4—O9^ix	98.2 (3)	U1ⁱⁱⁱ—O13—O5	119.3 (8)
U3ⁱ—U4—O15ⁱ	60.1 (3)	U1ⁱⁱⁱ—O13—O6	148.7 (9)
U3ⁱ—U4—O16ⁱ	30.9 (3)	U1ⁱⁱⁱ—O13—O8ⁱⁱⁱ	37.9 (6)
U3ⁱ—U4—O19ⁱ	38.3 (3)	U1ⁱⁱⁱ—O13—O10	52.6 (4)
U3ⁱ—U4—O20ⁱ	98.8 (7)	U1ⁱⁱⁱ—O13—O12ⁱⁱⁱ	35.7 (5)
U5^vii—U4—K3	126.59 (16)	U1ⁱⁱⁱ—O13—O17	99.1 (4)
U5^vii—U4—O1^viii	38.7 (7)	U1ⁱⁱⁱ—O13—O19	101.4 (6)
U5^vii—U4—O4	89.1 (6)	U1ⁱⁱⁱ—O13—O21	102.6 (4)
U5^vii—U4—O6ⁱ	120.1 (5)	U1ⁱⁱⁱ—O13—O22	147.8 (6)
U5^vii—U4—O7	91.2 (6)	U1ⁱⁱⁱ—O13—O24	107.3 (7)
U5^vii—U4—O9^ix	34.6 (3)	U3—O13—U6	97.6 (6)
U5^vii—U4—O15ⁱ	140.0 (4)	U3—O13—O3ⁱⁱⁱ	113.7 (6)
U5^vii—U4—O16ⁱ	160.0 (3)	U3—O13—O5	37.3 (5)
U5^vii—U4—O19ⁱ	98.2 (4)	U3—O13—O6	37.5 (6)
U5^vii—U4—O20ⁱ	128.7 (7)	U3—O13—O8ⁱⁱⁱ	157.4 (7)
K3—U4—O1^viii	121.0 (3)	U3—O13—O10	138.5 (8)
K3—U4—O4	142.8 (6)	U3—O13—O12ⁱⁱⁱ	116.9 (6)
K3—U4—O6ⁱ	94.1 (4)	U3—O13—O17	84.4 (5)
K3—U4—O7	35.8 (6)	U3—O13—O19	50.5 (4)
K3—U4—O9^ix	112.1 (4)	U3—O13—O21	107.1 (6)
K3—U4—O15ⁱ	93.4 (5)	U3—O13—O22	51.7 (4)
K3—U4—O16ⁱ	47.4 (4)	U3—O13—O24	95.8 (6)
K3—U4—O19ⁱ	69.3 (3)	U6—O13—O3ⁱⁱⁱ	145.9 (5)
K3—U4—O20ⁱ	74.3 (7)	U6—O13—O5	86.4 (8)
O1^viii—U4—O4	92.9 (5)	U6—O13—O6	107.6 (8)
O1^viii—U4—O6ⁱ	144.9 (5)	U6—O13—O8ⁱⁱⁱ	100.6 (4)
O1^viii—U4—O7	90.7 (5)	U6—O13—O10	48.8 (4)
O1^viii—U4—O9^ix	73.1 (8)	U6—O13—O12ⁱⁱⁱ	98.2 (5)
O1^viii—U4—O15ⁱ	122.8 (7)	U6—O13—O17	31.4 (3)
O1^viii—U4—O16ⁱ	159.3 (7)	U6—O13—O19	142.5 (6)
O1^viii—U4—O19ⁱ	135.3 (8)	U6—O13—O21	33.7 (3)
O1^viii—U4—O20ⁱ	90.1 (10)	U6—O13—O22	47.8 (4)
O4—U4—O6ⁱ	54.0 (6)	U6—O13—O24	94.4 (7)
O4—U4—O7	174.6 (5)	O3ⁱⁱⁱ—O13—O5	110.0 (8)
O4—U4—O9^ix	91.0 (6)	O3ⁱⁱⁱ—O13—O6	105.6 (8)
O4—U4—O15ⁱ	52.3 (7)	O3ⁱⁱⁱ—O13—O8ⁱⁱⁱ	53.4 (5)
O4—U4—O16ⁱ	95.5 (6)	O3ⁱⁱⁱ—O13—O10	97.2 (6)
O4—U4—O19ⁱ	98.4 (4)	O3ⁱⁱⁱ—O13—O12ⁱⁱⁱ	56.3 (6)
O4—U4—O20ⁱ	92.2 (8)	O3ⁱⁱⁱ—O13—O17	135.3 (6)
O6ⁱ—U4—O7	121.6 (6)	O3ⁱⁱⁱ—O13—O19	63.6 (5)
O6ⁱ—U4—O9^ix	94.2 (6)	O3ⁱⁱⁱ—O13—O21	135.1 (6)
O6ⁱ—U4—O15ⁱ	48.8 (5)	O3ⁱⁱⁱ—O13—O22	165.3 (6)
O6ⁱ—U4—O16ⁱ	50.9 (6)	O3ⁱⁱⁱ—O13—O24	95.5 (8)
O6ⁱ—U4—O19ⁱ	53.1 (5)	O5—O13—O6	74.8 (7)
O6ⁱ—U4—O20ⁱ	101.1 (8)	O5—O13—O8ⁱⁱⁱ	156.9 (10)
O7—U4—O9^ix	86.2 (6)	O5—O13—O10	107.4 (7)
O7—U4—O15ⁱ	128.3 (7)	O5—O13—O12ⁱⁱⁱ	83.7 (8)
O7—U4—O16ⁱ	82.4 (6)	O5—O13—O17	59.9 (6)
O7—U4—O19ⁱ	76.2 (4)	O5—O13—O19	56.4 (7)
O7—U4—O20ⁱ	91.9 (8)	O5—O13—O21	113.8 (9)
O9^ix—U4—O15ⁱ	137.5 (5)	O5—O13—O22	59.1 (8)
O9^ix—U4—O16ⁱ	125.6 (4)	O5—O13—O24	132.3 (8)
O9^ix—U4—O19ⁱ	63.7 (5)	O6—O13—O8ⁱⁱⁱ	122.6 (9)
O9^ix—U4—O20ⁱ	163.0 (7)	O6—O13—O10	154.9 (9)
O15ⁱ—U4—O16ⁱ	51.8 (5)	O6—O13—O12ⁱⁱⁱ	144.9 (7)
O15ⁱ—U4—O19ⁱ	97.5 (5)	O6—O13—O17	111.8 (8)
O15ⁱ—U4—O20ⁱ	54.4 (8)	O6—O13—O19	61.4 (6)
O16ⁱ—U4—O19ⁱ	61.8 (5)	O6—O13—O21	95.2 (7)
O16ⁱ—U4—O20ⁱ	70.7 (7)	O6—O13—O22	63.3 (7)
O19ⁱ—U4—O20ⁱ	132.1 (7)	O6—O13—O24	59.5 (7)
U1ⁱ—U5—U2^xi	161.62 (11)	O8ⁱⁱⁱ—O13—O10	64.1 (5)
U1ⁱ—U5—U4^xv	134.54 (7)	O8ⁱⁱⁱ—O13—O12ⁱⁱⁱ	73.6 (7)
U1ⁱ—U5—U6^x	62.54 (6)	O8ⁱⁱⁱ—O13—O17	118.0 (5)
U1ⁱ—U5—O1^x	98.5 (9)	O8ⁱⁱⁱ—O13—O19	115.6 (7)
U1ⁱ—U5—O2	92.6 (12)	O8ⁱⁱⁱ—O13—O21	81.8 (5)
U1ⁱ—U5—O9^xi	166.7 (4)	O8ⁱⁱⁱ—O13—O22	140.0 (7)
U1ⁱ—U5—O10^x	29.0 (4)	O8ⁱⁱⁱ—O13—O24	69.6 (8)
U1ⁱ—U5—O14^ix	42.9 (5)	O10—O13—O12ⁱⁱⁱ	58.4 (5)
U1ⁱ—U5—O18	85.6 (12)	O10—O13—O17	54.1 (5)
U1ⁱ—U5—O20^xi	121.2 (8)	O10—O13—O19	141.1 (7)
U2^xi—U5—U4^xv	62.70 (8)	O10—O13—O21	60.6 (5)
U2^xi—U5—U6^x	134.70 (12)	O10—O13—O22	95.8 (7)
U2^xi—U5—O1^x	98.6 (9)	O10—O13—O24	108.6 (6)
U2^xi—U5—O2	93.9 (10)	O12ⁱⁱⁱ—O13—O17	79.0 (6)
U2^xi—U5—O9^xi	28.5 (3)	O12ⁱⁱⁱ—O13—O19	83.6 (5)
U2^xi—U5—O10^x	169.0 (5)	O12ⁱⁱⁱ—O13—O21	119.0 (5)
U2^xi—U5—O14^ix	120.6 (5)	O12ⁱⁱⁱ—O13—O22	126.9 (8)
U2^xi—U5—O18	87.1 (10)	O12ⁱⁱⁱ—O13—O24	142.6 (9)
U2^xi—U5—O20^xi	41.9 (8)	O17—O13—O19	115.1 (5)
U4^xv—U5—U6^x	72.13 (7)	O17—O13—O21	65.1 (5)
U4^xv—U5—O1^x	36.1 (9)	O17—O13—O22	50.5 (4)
U4^xv—U5—O2	90.0 (13)	O17—O13—O24	124.2 (8)
U4^xv—U5—O9^xi	34.3 (3)	O19—O13—O21	155.7 (6)
U4^xv—U5—O10^x	106.3 (5)	O19—O13—O22	101.8 (5)
U4^xv—U5—O14^ix	174.2 (6)	O19—O13—O24	106.7 (6)
U4^xv—U5—O18	93.1 (14)	O21—O13—O22	58.4 (5)
U4^xv—U5—O20^xi	104.2 (8)	O21—O13—O24	61.6 (7)
U6^x—U5—O1^x	36.1 (9)	O22—O13—O24	86.9 (8)
U6^x—U5—O2	89.1 (4)	U1ⁱⁱ—O14—U5^v	99.3 (10)
U6^x—U5—O9^xi	106.2 (4)	U1ⁱⁱ—O14—U6ⁱⁱ	98.0 (10)
U6^x—U5—O10^x	34.4 (4)	U1ⁱⁱ—O14—K2^x	74.3 (6)
U6^x—U5—O14^ix	104.6 (5)	U1ⁱⁱ—O14—O1ⁱⁱ	138.0 (13)
U6^x—U5—O18	92.3 (7)	U1ⁱⁱ—O14—O2^v	102.9 (10)
U6^x—U5—O20^xi	175.6 (8)	U1ⁱⁱ—O14—O8ⁱⁱ	33.3 (5)
O1^x—U5—O2	90.5 (8)	U1ⁱⁱ—O14—O10^xxvi	49.3 (5)
O1^x—U5—O9^xi	70.2 (9)	U1ⁱⁱ—O14—O12ⁱⁱ	34.0 (4)
O1^x—U5—O10^x	70.4 (10)	U1ⁱⁱ—O14—O17ⁱⁱ	83.4 (8)
O1^x—U5—O14^ix	140.6 (10)	U1ⁱⁱ—O14—O18^v	92.6 (9)
O1^x—U5—O18	92.3 (11)	U1ⁱⁱ—O14—O20^xv	148.9 (14)
O1^x—U5—O20^xi	140.3 (12)	U1ⁱⁱ—O14—O21ⁱⁱ	110.9 (10)
O2—U5—O9^xi	94.5 (14)	U1ⁱⁱ—O14—O22ⁱⁱ	49.4 (5)
O2—U5—O10^x	85.8 (9)	U1ⁱⁱ—O14—O30^v	92.0 (8)
O2—U5—O14^ix	85.1 (15)	U5^v—O14—U6ⁱⁱ	145.4 (11)
O2—U5—O18	176.9 (18)	U5^v—O14—K2^x	141.9 (11)
O2—U5—O20^xi	88.3 (8)	U5^v—O14—O1ⁱⁱ	108.5 (10)
O9^xi—U5—O10^x	140.6 (6)	U5^v—O14—O2^v	38.4 (6)
O9^xi—U5—O14^ix	149.1 (6)	U5^v—O14—O8ⁱⁱ	93.4 (9)
O9^xi—U5—O18	87.8 (14)	U5^v—O14—O10^xxvi	51.2 (7)
O9^xi—U5—O20^xi	70.3 (8)	U5^v—O14—O12ⁱⁱ	103.8 (11)
O10^x—U5—O14^ix	70.3 (7)	U5^v—O14—O17ⁱⁱ	114.6 (11)
O10^x—U5—O18	93.8 (10)	U5^v—O14—O18^v	36.1 (8)
O10^x—U5—O20^xi	148.9 (9)	U5^v—O14—O20^xv	50.5 (8)
O14^ix—U5—O18	91.9 (16)	U5^v—O14—O21ⁱⁱ	148.8 (10)
O14^ix—U5—O20^xi	78.8 (9)	U5^v—O14—O22ⁱⁱ	146.8 (11)
O18—U5—O20^xi	90.5 (10)	U5^v—O14—O30^v	101.7 (13)
U1—U6—U1ⁱⁱⁱ	127.92 (4)	U6ⁱⁱ—O14—K2^x	72.0 (8)
U1—U6—U3	56.85 (6)	U6ⁱⁱ—O14—O1ⁱⁱ	42.9 (9)
U1—U6—U5^xviii	164.30 (7)	U6ⁱⁱ—O14—O2^v	157.2 (10)
U1—U6—K2	63.86 (13)	U6ⁱⁱ—O14—O8ⁱⁱ	85.0 (9)
U1—U6—O1	130.9 (10)	U6ⁱⁱ—O14—O10^xxvi	143.7 (11)
U1—U6—O5	60.5 (5)	U6ⁱⁱ—O14—O12ⁱⁱ	107.3 (11)
U1—U6—O8	27.0 (4)	U6ⁱⁱ—O14—O17ⁱⁱ	38.7 (6)
U1—U6—O10	151.2 (3)	U6ⁱⁱ—O14—O18^v	113.6 (11)
U1—U6—O13	94.3 (3)	U6ⁱⁱ—O14—O20^xv	104.8 (9)
U1—U6—O14ⁱⁱⁱ	43.6 (5)	U6ⁱⁱ—O14—O21ⁱⁱ	38.8 (6)
U1—U6—O17	73.5 (4)	U6ⁱⁱ—O14—O22ⁱⁱ	51.3 (7)
U1—U6—O21	101.6 (4)	U6ⁱⁱ—O14—O30^v	107.4 (13)
U1—U6—O22	29.8 (4)	K2^x—O14—O1ⁱⁱ	99.7 (10)
U1ⁱⁱⁱ—U6—U3	71.35 (7)	K2^x—O14—O2^v	105.2 (9)
U1ⁱⁱⁱ—U6—U5^xviii	61.42 (7)	K2^x—O14—O8ⁱⁱ	99.1 (7)
U1ⁱⁱⁱ—U6—K2	98.49 (18)	K2^x—O14—O10^xxvi	106.6 (7)
U1ⁱⁱⁱ—U6—O1	99.9 (10)	K2^x—O14—O12ⁱⁱ	50.7 (6)
U1ⁱⁱⁱ—U6—O5	71.1 (5)	K2^x—O14—O17ⁱⁱ	102.2 (9)
U1ⁱⁱⁱ—U6—O8	118.9 (3)	K2^x—O14—O18^v	166.6 (8)
U1ⁱⁱⁱ—U6—O10	28.3 (3)	K2^x—O14—O20^xv	132.7 (10)
U1ⁱⁱⁱ—U6—O13	35.5 (3)	K2^x—O14—O21ⁱⁱ	47.4 (5)
U1ⁱⁱⁱ—U6—O14ⁱⁱⁱ	169.3 (5)	K2^x—O14—O22ⁱⁱ	50.5 (6)
U1ⁱⁱⁱ—U6—O17	96.4 (5)	K2^x—O14—O30^v	42.7 (8)
U1ⁱⁱⁱ—U6—O21	92.5 (5)	O1ⁱⁱ—O14—O2^v	118.5 (11)
U1ⁱⁱⁱ—U6—O22	100.3 (4)	O1ⁱⁱ—O14—O8ⁱⁱ	112.5 (10)
U3—U6—U5^xviii	131.96 (10)	O1ⁱⁱ—O14—O10^xxvi	153.3 (12)
U3—U6—K2	62.71 (12)	O1ⁱⁱ—O14—O12ⁱⁱ	147.6 (14)
U3—U6—O1	169.7 (8)	O1ⁱⁱ—O14—O17ⁱⁱ	56.7 (7)
U3—U6—O5	26.4 (4)	O1ⁱⁱ—O14—O18^v	92.0 (9)
U3—U6—O8	59.4 (2)	O1ⁱⁱ—O14—O20^xv	62.0 (10)
U3—U6—O10	98.1 (3)	O1ⁱⁱ—O14—O21ⁱⁱ	52.3 (8)
U3—U6—O13	37.9 (3)	O1ⁱⁱ—O14—O22ⁱⁱ	94.2 (12)
U3—U6—O14ⁱⁱⁱ	99.2 (5)	O1ⁱⁱ—O14—O30^v	111.7 (10)
U3—U6—O17	82.6 (4)	O2^v—O14—O8ⁱⁱ	117.6 (10)
U3—U6—O21	101.0 (4)	O2^v—O14—O10^xxvi	59.1 (8)
U3—U6—O22	29.6 (4)	O2^v—O14—O12ⁱⁱ	85.9 (10)
U5^xviii—U6—K2	130.49 (13)	O2^v—O14—O17ⁱⁱ	152.6 (12)
U5^xviii—U6—O1	38.6 (10)	O2^v—O14—O18^v	74.5 (11)
U5^xviii—U6—O5	120.5 (4)	O2^v—O14—O20^xv	59.7 (9)
U5^xviii—U6—O8	140.1 (4)	O2^v—O14—O21ⁱⁱ	122.9 (10)
U5^xviii—U6—O10	33.9 (3)	O2^v—O14—O22ⁱⁱ	143.8 (11)
U5^xviii—U6—O13	96.7 (3)	O2^v—O14—O30^v	63.4 (10)
U5^xviii—U6—O14ⁱⁱⁱ	128.6 (5)	O8ⁱⁱ—O14—O10^xxvi	59.1 (6)
U5^xviii—U6—O17	93.8 (4)	O8ⁱⁱ—O14—O12ⁱⁱ	67.4 (6)
U5^xviii—U6—O21	89.7 (4)	O8ⁱⁱ—O14—O17ⁱⁱ	56.0 (6)
U5^xviii—U6—O22	161.5 (5)	O8ⁱⁱ—O14—O18^v	70.0 (9)
K2—U6—O1	125.4 (3)	O8ⁱⁱ—O14—O20^xv	128.0 (11)
K2—U6—O5	88.3 (4)	O8ⁱⁱ—O14—O21ⁱⁱ	116.0 (11)
K2—U6—O8	89.4 (4)	O8ⁱⁱ—O14—O22ⁱⁱ	54.8 (6)
K2—U6—O10	120.3 (4)	O8ⁱⁱ—O14—O30^v	125.3 (9)
K2—U6—O13	71.9 (3)	O10^xxvi—O14—O12ⁱⁱ	56.7 (7)
K2—U6—O14ⁱⁱⁱ	72.2 (7)	O10^xxvi—O14—O17ⁱⁱ	111.7 (10)
K2—U6—O17	134.9 (3)	O10^xxvi—O14—O18^v	61.4 (8)
K2—U6—O21	43.7 (3)	O10^xxvi—O14—O20^xv	101.7 (12)
K2—U6—O22	50.3 (3)	O10^xxvi—O14—O21ⁱⁱ	153.9 (10)
O1—U6—O5	146.3 (5)	O10^xxvi—O14—O22ⁱⁱ	98.7 (8)
O1—U6—O8	123.5 (9)	O10^xxvi—O14—O30^v	91.3 (10)
O1—U6—O10	72.5 (10)	O12ⁱⁱ—O14—O17ⁱⁱ	111.2 (9)
O1—U6—O13	134.7 (11)	O12ⁱⁱ—O14—O18^v	116.3 (10)
O1—U6—O14ⁱⁱⁱ	89.9 (11)	O12ⁱⁱ—O14—O20^xv	145.6 (14)
O1—U6—O17	93.1 (5)	O12ⁱⁱ—O14—O21ⁱⁱ	97.3 (10)
O1—U6—O21	84.6 (4)	O12ⁱⁱ—O14—O22ⁱⁱ	58.1 (7)
O1—U6—O22	159.8 (11)	O12ⁱⁱ—O14—O30^v	58.0 (7)
O5—U6—O8	48.6 (6)	O17ⁱⁱ—O14—O18^v	78.6 (10)
O5—U6—O10	90.8 (6)	O17ⁱⁱ—O14—O20^xv	101.5 (9)
O5—U6—O13	48.7 (6)	O17ⁱⁱ—O14—O21ⁱⁱ	77.5 (9)
O5—U6—O14ⁱⁱⁱ	102.8 (7)	O17ⁱⁱ—O14—O22ⁱⁱ	58.6 (7)
O5—U6—O17	57.2 (6)	O17ⁱⁱ—O14—O30^v	143.7 (15)
O5—U6—O21	127.2 (6)	O18^v—O14—O20^xv	59.1 (9)
O5—U6—O22	44.6 (5)	O18^v—O14—O21ⁱⁱ	144.0 (10)
O8—U6—O10	130.6 (5)	O18^v—O14—O22ⁱⁱ	122.4 (12)
O8—U6—O13	95.0 (3)	O18^v—O14—O30^v	137.6 (15)
O8—U6—O14ⁱⁱⁱ	57.1 (7)	O20^xv—O14—O21ⁱⁱ	100.1 (9)
O8—U6—O17	46.6 (5)	O20^xv—O14—O22ⁱⁱ	155.9 (13)
O8—U6—O21	128.6 (6)	O20^xv—O14—O30^v	100.7 (11)
O8—U6—O22	44.3 (5)	O21ⁱⁱ—O14—O22ⁱⁱ	64.3 (8)
O10—U6—O13	63.8 (4)	O21ⁱⁱ—O14—O30^v	70.6 (10)
O10—U6—O14ⁱⁱⁱ	162.2 (6)	O22ⁱⁱ—O14—O30^v	91.5 (11)
O10—U6—O17	90.7 (6)	U2—O15—U3	70.1 (7)
O10—U6—O21	96.7 (6)	U2—O15—U4ⁱ	76.1 (10)
O10—U6—O22	127.6 (5)	U2—O15—Sr1^iv	148.5 (13)
O13—U6—O14ⁱⁱⁱ	134.0 (6)	U2—O15—Sr1'^iv	148.5 (13)
O13—U6—O17	98.7 (6)	U2—O15—O3	49.1 (6)
O13—U6—O21	89.0 (6)	U2—O15—O4ⁱ	101.7 (13)
O13—U6—O22	65.3 (5)	U2—O15—O6	98.6 (10)
O14ⁱⁱⁱ—U6—O17	87.1 (8)	U2—O15—O7^v	87.9 (10)
O14ⁱⁱⁱ—U6—O21	84.3 (9)	U2—O15—O9	53.4 (7)
O14ⁱⁱⁱ—U6—O22	69.9 (7)	U2—O15—O11	1.6 (6)
O17—U6—O21	171.1 (8)	U2—O15—O15^xvii	164.2 (16)
O17—U6—O22	85.3 (5)	U2—O15—O16	49.6 (8)
O21—U6—O22	93.9 (5)	U2—O15—O18^vi	95.6 (9)
Sr1'—Sr1—O4	0	U2—O15—O19ⁱⁱ	56.3 (9)
Sr1'—Sr1—O4^xii	0	U2—O15—O20	57.2 (9)
Sr1'—Sr1—O6^xiii	0	U2—O15—O25^v	112.4 (15)
Sr1'—Sr1—O6ⁱ	0	U2—O15—O26^iv	143.2 (13)
Sr1'—Sr1—O15^xiii	0	U2—O15—O31^v	120.8 (12)
Sr1'—Sr1—O15ⁱ	0	U3—O15—U4ⁱ	60.1 (4)
Sr1'—Sr1—O26	0	U3—O15—Sr1^iv	79.4 (6)
Sr1'—Sr1—O29	0	U3—O15—Sr1'^iv	79.4 (6)
Sr1'—Sr1—O31^x	0	U3—O15—O3	37.5 (5)
O4—Sr1—O4^xii	99.0 (5)	U3—O15—O4ⁱ	68.8 (6)
O4—Sr1—O6^xiii	137.6 (8)	U3—O15—O6	28.6 (5)
O4—Sr1—O6ⁱ	72.0 (7)	U3—O15—O7^v	152.2 (9)
O4—Sr1—O15^xiii	141.1 (5)	U3—O15—O9	121.9 (9)
O4—Sr1—O15ⁱ	69.5 (8)	U3—O15—O11	71.1 (5)
O4—Sr1—O26	69.0 (5)	U3—O15—O15^xvii	114.1 (7)
O4—Sr1—O29	58.1 (4)	U3—O15—O16	35.1 (3)
O4—Sr1—O31^x	130.5 (3)	U3—O15—O18^vi	135.8 (10)
O4^xii—Sr1—O6^xiii	72.0 (7)	U3—O15—O19ⁱⁱ	103.8 (8)
O4^xii—Sr1—O6ⁱ	137.6 (8)	U3—O15—O20	86.9 (8)
O4^xii—Sr1—O15^xiii	69.5 (8)	U3—O15—O25^v	123.2 (8)
O4^xii—Sr1—O15ⁱ	141.1 (5)	U3—O15—O26^iv	120.8 (11)
O4^xii—Sr1—O26	69.0 (5)	U3—O15—O31^v	73.3 (5)
O4^xii—Sr1—O29	58.1 (4)	U4ⁱ—O15—Sr1^iv	82.2 (8)
O4^xii—Sr1—O31^x	130.5 (3)	U4ⁱ—O15—Sr1'^iv	82.2 (8)
O6^xiii—Sr1—O6ⁱ	87.1 (8)	U4ⁱ—O15—O3	87.9 (8)
O6^xiii—Sr1—O15^xiii	75.9 (8)	U4ⁱ—O15—O4ⁱ	25.6 (4)
O6^xiii—Sr1—O15ⁱ	141.1 (10)	U4ⁱ—O15—O6	65.8 (8)
O6^xiii—Sr1—O26	136.1 (6)	U4ⁱ—O15—O7^v	132.2 (7)
O6^xiii—Sr1—O29	84.0 (8)	U4ⁱ—O15—O9	91.9 (8)
O6^xiii—Sr1—O31^x	69.5 (8)	U4ⁱ—O15—O11	77.6 (6)
O6ⁱ—Sr1—O15^xiii	141.1 (10)	U4ⁱ—O15—O15^xvii	119.5 (10)
O6ⁱ—Sr1—O15ⁱ	75.9 (8)	U4ⁱ—O15—O16	36.8 (5)
O6ⁱ—Sr1—O26	136.1 (6)	U4ⁱ—O15—O18^vi	76.0 (8)
O6ⁱ—Sr1—O29	84.0 (8)	U4ⁱ—O15—O19ⁱⁱ	132.0 (9)
O6ⁱ—Sr1—O31^x	69.5 (8)	U4ⁱ—O15—O20	38.2 (6)
O15^xiii—Sr1—O15ⁱ	95.8 (9)	U4ⁱ—O15—O25^v	171.4 (11)
O15^xiii—Sr1—O26	72.2 (7)	U4ⁱ—O15—O26^iv	80.6 (9)
O15^xiii—Sr1—O29	127.4 (7)	U4ⁱ—O15—O31^v	120.9 (10)
O15^xiii—Sr1—O31^x	71.8 (7)	Sr1^iv—O15—Sr1'^iv	0
O15ⁱ—Sr1—O26	72.2 (7)	Sr1^iv—O15—O3	108.3 (7)
O15ⁱ—Sr1—O29	127.4 (7)	Sr1^iv—O15—O4ⁱ	58.5 (7)
O15ⁱ—Sr1—O31^x	71.8 (7)	Sr1^iv—O15—O6	51.1 (7)
O26—Sr1—O29	91.9 (9)	Sr1^iv—O15—O7^v	123.5 (9)
O26—Sr1—O31^x	125.2 (10)	Sr1^iv—O15—O9	151.0 (11)
O29—Sr1—O31^x	142.8 (7)	Sr1^iv—O15—O11	149.8 (9)
Sr1—Sr1'—O4	0	Sr1^iv—O15—O15^xvii	42.1 (6)
Sr1—Sr1'—O4^xii	0	Sr1^iv—O15—O16	100.0 (10)
Sr1—Sr1'—O6^xiii	0	Sr1^iv—O15—O18^vi	101.0 (10)
Sr1—Sr1'—O6ⁱ	0	Sr1^iv—O15—O19ⁱⁱ	142.9 (12)
Sr1—Sr1'—O15^xiii	0	Sr1^iv—O15—O20	114.7 (13)
Sr1—Sr1'—O15ⁱ	0	Sr1^iv—O15—O25^v	90.5 (9)
Sr1—Sr1'—O26	0	Sr1^iv—O15—O26^iv	51.1 (7)
Sr1—Sr1'—O29	0	Sr1^iv—O15—O31^v	53.9 (7)
Sr1—Sr1'—O31^x	0	Sr1'^iv—O15—O3	108.3 (7)
O4—Sr1'—O4^xii	99.0 (5)	Sr1'^iv—O15—O4ⁱ	58.5 (7)
O4—Sr1'—O6^xiii	137.6 (8)	Sr1'^iv—O15—O6	51.1 (7)
O4—Sr1'—O6ⁱ	72.0 (7)	Sr1'^iv—O15—O7^v	123.5 (9)
O4—Sr1'—O15^xiii	141.1 (5)	Sr1'^iv—O15—O9	151.0 (11)
O4—Sr1'—O15ⁱ	69.5 (8)	Sr1'^iv—O15—O11	149.8 (9)
O4—Sr1'—O26	69.0 (5)	Sr1'^iv—O15—O15^xvii	42.1 (6)
O4—Sr1'—O29	58.1 (4)	Sr1'^iv—O15—O16	100.0 (10)
O4—Sr1'—O31^x	130.5 (3)	Sr1'^iv—O15—O18^vi	101.0 (10)
O4^xii—Sr1'—O6^xiii	72.0 (7)	Sr1'^iv—O15—O19ⁱⁱ	142.9 (12)
O4^xii—Sr1'—O6ⁱ	137.6 (8)	Sr1'^iv—O15—O20	114.7 (13)
O4^xii—Sr1'—O15^xiii	69.5 (8)	Sr1'^iv—O15—O25^v	90.5 (9)
O4^xii—Sr1'—O15ⁱ	141.1 (5)	Sr1'^iv—O15—O26^iv	51.1 (7)
O4^xii—Sr1'—O26	69.0 (5)	Sr1'^iv—O15—O31^v	53.9 (7)
O4^xii—Sr1'—O29	58.1 (4)	O3—O15—O4ⁱ	104.1 (9)
O4^xii—Sr1'—O31^x	130.5 (3)	O3—O15—O6	60.2 (7)
O6^xiii—Sr1'—O6ⁱ	87.1 (8)	O3—O15—O7^v	114.9 (10)
O6^xiii—Sr1'—O15^xiii	75.9 (8)	O3—O15—O9	99.7 (10)
O6^xiii—Sr1'—O15ⁱ	141.1 (10)	O3—O15—O11	49.3 (5)
O6^xiii—Sr1'—O26	136.1 (6)	O3—O15—O15^xvii	124.4 (9)
O6^xiii—Sr1'—O29	84.0 (8)	O3—O15—O16	51.7 (7)
O6^xiii—Sr1'—O31^x	69.5 (8)	O3—O15—O18^vi	144.2 (10)
O6ⁱ—Sr1'—O15^xiii	141.1 (10)	O3—O15—O19ⁱⁱ	66.3 (8)
O6ⁱ—Sr1'—O15ⁱ	75.9 (8)	O3—O15—O20	95.9 (10)
O6ⁱ—Sr1'—O26	136.1 (6)	O3—O15—O25^v	98.9 (11)
O6ⁱ—Sr1'—O29	84.0 (8)	O3—O15—O26^iv	157.4 (12)
O6ⁱ—Sr1'—O31^x	69.5 (8)	O3—O15—O31^v	73.8 (7)
O15^xiii—Sr1'—O15ⁱ	95.8 (9)	O4ⁱ—O15—O6	60.6 (8)
O15^xiii—Sr1'—O26	72.2 (7)	O4ⁱ—O15—O7^v	134.7 (8)
O15^xiii—Sr1'—O29	127.4 (7)	O4ⁱ—O15—O9	108.0 (10)
O15^xiii—Sr1'—O31^x	71.8 (7)	O4ⁱ—O15—O11	103.2 (9)
O15ⁱ—Sr1'—O26	72.2 (7)	O4ⁱ—O15—O15^xvii	93.9 (9)
O15ⁱ—Sr1'—O29	127.4 (7)	O4ⁱ—O15—O16	58.4 (7)
O15ⁱ—Sr1'—O31^x	71.8 (7)	O4ⁱ—O15—O18^vi	74.1 (9)
O26—Sr1'—O29	91.9 (9)	O4ⁱ—O15—O19ⁱⁱ	157.5 (11)
O26—Sr1'—O31^x	125.2 (10)	O4ⁱ—O15—O20	57.0 (8)
O29—Sr1'—O31^x	142.8 (7)	O4ⁱ—O15—O25^v	145.8 (11)
Sr2'—Sr2—O5	0	O4ⁱ—O15—O26^iv	59.0 (9)
Sr2'—Sr2—O5ⁱ	0	O4ⁱ—O15—O31^v	106.2 (10)
Sr2'—Sr2—O8	0	O6—O15—O7^v	162.0 (11)
Sr2'—Sr2—O8ⁱ	0	O6—O15—O9	149.0 (12)
Sr2'—Sr2—O17	0	O6—O15—O11	99.7 (8)
Sr2'—Sr2—O17ⁱ	0	O6—O15—O15^xvii	86.7 (9)
Sr2'—Sr2—O23	0	O6—O15—O16	57.7 (7)
Sr2'—Sr2—O27	0	O6—O15—O18^vi	134.3 (13)
Sr2'—Sr2—O32	0	O6—O15—O19ⁱⁱ	122.6 (10)
O5—Sr2—O5ⁱ	88.4 (9)	O6—O15—O20	102.1 (11)
O5—Sr2—O8	74.9 (8)	O6—O15—O25^v	112.9 (10)
O5—Sr2—O8ⁱ	139.0 (6)	O6—O15—O26^iv	97.3 (11)
O5—Sr2—O17	75.3 (6)	O6—O15—O31^v	56.1 (8)
O5—Sr2—O17ⁱ	143.8 (8)	O7^v—O15—O9	45.1 (5)
O5—Sr2—O23	76.5 (7)	O7^v—O15—O11	86.6 (7)
O5—Sr2—O27	135.8 (6)	O7^v—O15—O15^xvii	82.9 (7)
O5—Sr2—O32	78.9 (8)	O7^v—O15—O16	135.1 (9)
O5ⁱ—Sr2—O8	139.0 (6)	O7^v—O15—O18^vi	60.8 (7)
O5ⁱ—Sr2—O8ⁱ	74.9 (8)	O7^v—O15—O19ⁱⁱ	48.6 (5)
O5ⁱ—Sr2—O17	143.8 (8)	O7^v—O15—O20	95.5 (7)
O5ⁱ—Sr2—O17ⁱ	75.3 (6)	O7^v—O15—O25^v	49.4 (6)
O5ⁱ—Sr2—O23	76.5 (7)	O7^v—O15—O26^iv	87.0 (8)
O5ⁱ—Sr2—O27	135.8 (6)	O7^v—O15—O31^v	106.1 (10)
O5ⁱ—Sr2—O32	78.9 (8)	O9—O15—O11	52.6 (6)
O8—Sr2—O8ⁱ	93.4 (7)	O9—O15—O15^xvii	123.9 (9)
O8—Sr2—O17	67.8 (5)	O9—O15—O16	91.5 (9)
O8—Sr2—O17ⁱ	136.8 (6)	O9—O15—O18^vi	50.2 (6)
O8—Sr2—O23	63.4 (5)	O9—O15—O19ⁱⁱ	56.7 (7)
O8—Sr2—O27	69.2 (5)	O9—O15—O20	53.7 (8)
O8—Sr2—O32	131.6 (5)	O9—O15—O25^v	92.3 (10)
O8ⁱ—Sr2—O17	136.8 (6)	O9—O15—O26^iv	100.0 (8)
O8ⁱ—Sr2—O17ⁱ	67.8 (5)	O9—O15—O31^v	145.7 (15)
O8ⁱ—Sr2—O23	63.4 (5)	O11—O15—O15^xvii	162.7 (12)
O8ⁱ—Sr2—O27	69.2 (5)	O11—O15—O16	51.2 (6)
O8ⁱ—Sr2—O32	131.6 (5)	O11—O15—O18^vi	95.6 (6)
O17—Sr2—O17ⁱ	99.1 (4)	O11—O15—O19ⁱⁱ	54.8 (6)
O17—Sr2—O23	128.2 (4)	O11—O15—O20	58.2 (8)
O17—Sr2—O27	67.8 (5)	O11—O15—O25^v	110.9 (10)
O17—Sr2—O32	66.6 (5)	O11—O15—O26^iv	143.7 (9)
O17ⁱ—Sr2—O23	128.2 (4)	O11—O15—O31^v	120.5 (9)
O17ⁱ—Sr2—O27	67.8 (5)	O15^xvii—O15—O16	141.8 (10)
O17ⁱ—Sr2—O32	66.6 (5)	O15^xvii—O15—O18^vi	91.2 (7)
O23—Sr2—O27	108.1 (10)	O15^xvii—O15—O19ⁱⁱ	108.3 (11)
O23—Sr2—O32	145.4 (10)	O15^xvii—O15—O20	136.4 (11)
O27—Sr2—O32	106.5 (9)	O15^xvii—O15—O25^v	52.0 (8)
Sr2—Sr2'—O5	0	O15^xvii—O15—O26^iv	49.4 (7)
Sr2—Sr2'—O5ⁱ	0	O15^xvii—O15—O31^v	50.7 (6)
Sr2—Sr2'—O8	0	O16—O15—O18^vi	103.8 (9)
Sr2—Sr2'—O8ⁱ	0	O16—O15—O19ⁱⁱ	102.9 (10)
Sr2—Sr2'—O17	0	O16—O15—O20	52.3 (7)
Sr2—Sr2'—O17ⁱ	0	O16—O15—O25^v	150.5 (11)
Sr2—Sr2'—O23	0	O16—O15—O26^iv	116.8 (13)
Sr2—Sr2'—O27	0	O16—O15—O31^v	108.4 (7)
Sr2—Sr2'—O32	0	O18^vi—O15—O19ⁱⁱ	101.4 (9)
O5—Sr2'—O5ⁱ	88.4 (9)	O18^vi—O15—O20	52.3 (6)
O5—Sr2'—O8	74.9 (8)	O18^vi—O15—O25^v	101.0 (9)
O5—Sr2'—O8ⁱ	139.0 (6)	O18^vi—O15—O26^iv	50.8 (6)
O5—Sr2'—O17	75.3 (6)	O18^vi—O15—O31^v	141.8 (9)
O5—Sr2'—O17ⁱ	143.8 (8)	O19ⁱⁱ—O15—O20	102.4 (10)
O5—Sr2'—O23	76.5 (7)	O19ⁱⁱ—O15—O25^v	56.3 (8)
O5—Sr2'—O27	135.8 (6)	O19ⁱⁱ—O15—O26^iv	135.0 (11)
O5—Sr2'—O32	78.9 (8)	O19ⁱⁱ—O15—O31^v	91.0 (11)
O5ⁱ—Sr2'—O8	139.0 (6)	O20—O15—O25^v	144.9 (10)
O5ⁱ—Sr2'—O8ⁱ	74.9 (8)	O20—O15—O26^iv	87.0 (10)
O5ⁱ—Sr2'—O17	143.8 (8)	O20—O15—O31^v	158.3 (12)
O5ⁱ—Sr2'—O17ⁱ	75.3 (6)	O25^v—O15—O26^iv	91.2 (10)
O5ⁱ—Sr2'—O23	76.5 (7)	O25^v—O15—O31^v	56.8 (8)
O5ⁱ—Sr2'—O27	135.8 (6)	O26^iv—O15—O31^v	95.5 (9)
O5ⁱ—Sr2'—O32	78.9 (8)	U2—O16—U3	107.5 (6)
O8—Sr2'—O8ⁱ	93.4 (7)	U2—O16—U4ⁱ	112.2 (4)
O8—Sr2'—O17	67.8 (5)	U2—O16—K3	111.4 (6)
O8—Sr2'—O17ⁱ	136.8 (6)	U2—O16—O3	54.9 (4)
O8—Sr2'—O23	63.4 (5)	U2—O16—O4ⁱ	93.4 (5)
O8—Sr2'—O27	69.2 (5)	U2—O16—O5	117.2 (9)
O8—Sr2'—O32	131.6 (5)	U2—O16—O6	92.8 (7)
O8ⁱ—Sr2'—O17	136.8 (6)	U2—O16—O7ⁱ	128.3 (5)
O8ⁱ—Sr2'—O17ⁱ	67.8 (5)	U2—O16—O11	38.8 (4)
O8ⁱ—Sr2'—O23	63.4 (5)	U2—O16—O15	36.1 (6)
O8ⁱ—Sr2'—O27	69.2 (5)	U2—O16—O19	159.5 (7)
O8ⁱ—Sr2'—O32	131.6 (5)	U2—O16—O20	62.7 (8)
O17—Sr2'—O17ⁱ	99.1 (4)	U2—O16—O28^vi	83.2 (5)
O17—Sr2'—O23	128.2 (4)	U3—O16—U4ⁱ	116.9 (7)
O17—Sr2'—O27	67.8 (5)	U3—O16—K3	114.3 (5)
O17—Sr2'—O32	66.6 (5)	U3—O16—O3	56.9 (4)
O17ⁱ—Sr2'—O23	128.2 (4)	U3—O16—O4ⁱ	98.5 (5)
O17ⁱ—Sr2'—O27	67.8 (5)	U3—O16—O5	39.8 (6)
O17ⁱ—Sr2'—O32	66.6 (5)	U3—O16—O6	38.2 (5)
O23—Sr2'—O27	108.1 (10)	U3—O16—O7ⁱ	123.8 (7)
O23—Sr2'—O32	145.4 (10)	U3—O16—O11	115.0 (7)
O27—Sr2'—O32	106.5 (9)	U3—O16—O15	93.4 (6)
O1^x—K1—O1^xiv	170.2 (8)	U3—O16—O19	58.4 (4)
O1^x—K1—O2	51.4 (6)	U3—O16—O20	156.4 (9)
O1^x—K1—O2^xii	118.8 (7)	U3—O16—O28^vi	157.3 (6)
O1^x—K1—O4^xv	47.9 (7)	U4ⁱ—O16—K3	94.4 (6)
O1^x—K1—O4^xvi	133.8 (7)	U4ⁱ—O16—O3	153.0 (7)
O1^x—K1—O17^x	50.3 (5)	U4ⁱ—O16—O4ⁱ	34.5 (4)
O1^x—K1—O17^xiv	133.2 (6)	U4ⁱ—O16—O5	130.0 (9)
O1^x—K1—O26^xv	94.1 (7)	U4ⁱ—O16—O6	92.5 (8)
O1^x—K1—O27^x	94.4 (4)	U4ⁱ—O16—O7ⁱ	40.2 (4)
O1^x—K1—O29^xv	88.4 (5)	U4ⁱ—O16—O11	126.9 (5)
O1^x—K1—O32^x	89.0 (6)	U4ⁱ—O16—O15	91.3 (7)
O1^xiv—K1—O2	118.8 (7)	U4ⁱ—O16—O19	68.0 (5)
O1^xiv—K1—O2^xii	51.4 (6)	U4ⁱ—O16—O20	56.0 (8)
O1^xiv—K1—O4^xv	133.8 (7)	U4ⁱ—O16—O28^vi	75.0 (5)
O1^xiv—K1—O4^xvi	47.9 (7)	K3—O16—O3	112.3 (7)
O1^xiv—K1—O17^x	133.2 (6)	K3—O16—O4ⁱ	128.7 (7)
O1^xiv—K1—O17^xiv	50.3 (5)	K3—O16—O5	75.3 (7)
O1^xiv—K1—O26^xv	94.1 (7)	K3—O16—O6	149.9 (6)
O1^xiv—K1—O27^x	94.4 (4)	K3—O16—O7ⁱ	54.7 (5)
O1^xiv—K1—O29^xv	88.4 (5)	K3—O16—O11	74.2 (5)
O1^xiv—K1—O32^x	89.0 (6)	K3—O16—O15	145.0 (7)
O2—K1—O2^xii	67.4 (6)	K3—O16—O19	88.8 (6)
O2—K1—O4^xv	75.8 (8)	K3—O16—O20	89.2 (7)
O2—K1—O4^xvi	120.8 (6)	K3—O16—O28^vi	43.4 (3)
O2—K1—O17^x	80.2 (5)	O3—O16—O4ⁱ	118.6 (7)
O2—K1—O17^xiv	124.5 (10)	O3—O16—O5	64.8 (8)
O2—K1—O26^xv	135.6 (8)	O3—O16—O6	66.8 (8)
O2—K1—O27^x	136.8 (6)	O3—O16—O7ⁱ	166.8 (7)
O2—K1—O29^xv	76.5 (9)	O3—O16—O11	60.8 (5)
O2—K1—O32^x	78.0 (9)	O3—O16—O15	64.4 (7)
O2^xii—K1—O4^xv	120.8 (6)	O3—O16—O19	115.1 (5)
O2^xii—K1—O4^xvi	75.8 (8)	O3—O16—O20	117.6 (9)
O2^xii—K1—O17^x	124.5 (10)	O3—O16—O28^vi	121.5 (7)
O2^xii—K1—O17^xiv	80.2 (5)	O4ⁱ—O16—O5	132.2 (8)
O2^xii—K1—O26^xv	135.6 (8)	O4ⁱ—O16—O6	64.0 (6)
O2^xii—K1—O27^x	136.8 (6)	O4ⁱ—O16—O7ⁱ	74.6 (6)
O2^xii—K1—O29^xv	76.5 (9)	O4ⁱ—O16—O11	126.6 (5)
O2^xii—K1—O32^x	78.0 (9)	O4ⁱ—O16—O15	62.2 (7)
O4^xv—K1—O4^xvi	86.3 (5)	O4ⁱ—O16—O19	75.6 (6)
O4^xv—K1—O17^x	90.7 (4)	O4ⁱ—O16—O20	62.7 (7)
O4^xv—K1—O17^xiv	157.0 (6)	O4ⁱ—O16—O28^vi	100.8 (5)
O4^xv—K1—O26^xv	59.9 (5)	O5—O16—O6	77.9 (8)
O4^xv—K1—O27^x	101.7 (6)	O5—O16—O7ⁱ	106.8 (9)
O4^xv—K1—O29^xv	50.3 (4)	O5—O16—O11	97.7 (8)
O4^xv—K1—O32^x	136.8 (3)	O5—O16—O15	124.9 (9)
O4^xvi—K1—O17^x	157.0 (6)	O5—O16—O19	63.1 (8)
O4^xvi—K1—O17^xiv	90.7 (4)	O5—O16—O20	163.4 (10)
O4^xvi—K1—O26^xv	59.9 (5)	O5—O16—O28^vi	117.5 (7)
O4^xvi—K1—O27^x	101.7 (6)	O6—O16—O7ⁱ	122.8 (9)
O4^xvi—K1—O29^xv	50.3 (4)	O6—O16—O11	123.2 (9)
O4^xvi—K1—O32^x	136.8 (3)	O6—O16—O15	63.8 (7)
O17^x—K1—O17^xiv	83.2 (4)	O6—O16—O19	66.8 (7)
O17^x—K1—O26^xv	99.1 (5)	O6—O16—O20	118.5 (9)
O17^x—K1—O27^x	56.6 (5)	O6—O16—O28^vi	164.1 (7)
O17^x—K1—O29^xv	138.3 (3)	O7ⁱ—O16—O11	112.7 (6)
O17^x—K1—O32^x	51.2 (4)	O7ⁱ—O16—O15	126.7 (7)
O17^xiv—K1—O26^xv	99.1 (5)	O7ⁱ—O16—O19	66.0 (6)
O17^xiv—K1—O27^x	56.6 (5)	O7ⁱ—O16—O20	67.4 (8)
O17^xiv—K1—O29^xv	138.3 (3)	O7ⁱ—O16—O28^vi	51.9 (6)
O17^xiv—K1—O32^x	51.2 (4)	O11—O16—O15	74.9 (7)
O26^xv—K1—O27^x	59.6 (7)	O11—O16—O19	157.5 (7)
O26^xv—K1—O29^xv	75.5 (8)	O11—O16—O20	71.9 (8)
O26^xv—K1—O32^x	135.3 (7)	O11—O16—O28^vi	61.1 (6)
O27^x—K1—O29^xv	135.1 (10)	O15—O16—O19	125.0 (8)
O27^x—K1—O32^x	75.7 (8)	O15—O16—O20	65.9 (8)
O29^xv—K1—O32^x	149.2 (9)	O15—O16—O28^vi	106.1 (6)
U6—K2—U6^xvii	109.72 (17)	O19—O16—O20	123.6 (10)
U6—K2—O6	82.2 (5)	O19—O16—O28^vi	115.5 (7)
U6—K2—O6^xvii	141.9 (7)	O20—O16—O28^vi	46.2 (7)
U6—K2—O12	77.8 (3)	U1—O17—U6	78.2 (4)
U6—K2—O12^xvii	133.1 (5)	U1—O17—Sr2	80.9 (3)
U6—K2—O14^xviii	109.2 (4)	U1—O17—Sr2'	80.9 (3)
U6—K2—O14ⁱⁱⁱ	35.8 (5)	U1—O17—K1^xviii	141.7 (6)
U6—K2—O21	25.5 (3)	U1—O17—O1	110.7 (6)
U6—K2—O21^xvii	84.3 (3)	U1—O17—O2^xviii	161.4 (5)
U6—K2—O22	34.0 (2)	U1—O17—O5	66.7 (6)
U6—K2—O22^xvii	143.4 (3)	U1—O17—O8	28.1 (6)
U6—K2—O24	81.0 (3)	U1—O17—O10	123.2 (5)
U6—K2—O30^iv	77.0 (3)	U1—O17—O13	84.0 (3)
U6—K2—O31^v	124.71 (13)	U1—O17—O14ⁱⁱⁱ	44.9 (4)
U6^xvii—K2—O6	141.9 (7)	U1—O17—O18ⁱ	66.3 (4)
U6^xvii—K2—O6^xvii	82.2 (5)	U1—O17—O21	75.9 (3)
U6^xvii—K2—O12	133.1 (5)	U1—O17—O22	35.8 (4)
U6^xvii—K2—O12^xvii	77.8 (3)	U1—O17—O27	82.8 (5)
U6^xvii—K2—O14^xviii	35.8 (5)	U1—O17—O32	125.8 (5)
U6^xvii—K2—O14ⁱⁱⁱ	109.2 (4)	U6—O17—Sr2	145.1 (6)
U6^xvii—K2—O21	84.3 (3)	U6—O17—Sr2'	145.1 (6)
U6^xvii—K2—O21^xvii	25.5 (3)	U6—O17—K1^xviii	124.6 (5)
U6^xvii—K2—O22	143.4 (3)	U6—O17—O1	48.4 (5)
U6^xvii—K2—O22^xvii	34.0 (2)	U6—O17—O2^xviii	85.2 (4)
U6^xvii—K2—O24	81.0 (3)	U6—O17—O5	94.1 (7)
U6^xvii—K2—O30^iv	77.0 (3)	U6—O17—O8	106.2 (8)
U6^xvii—K2—O31^v	124.71 (13)	U6—O17—O10	49.7 (5)
O6—K2—O6^xvii	68.6 (8)	U6—O17—O13	49.9 (4)
O6—K2—O12	84.2 (7)	U6—O17—O14ⁱⁱⁱ	54.1 (7)
O6—K2—O12^xvii	121.0 (6)	U6—O17—O18ⁱ	102.0 (6)
O6—K2—O14^xviii	168.5 (6)	U6—O17—O21	4.4 (4)
O6—K2—O14ⁱⁱⁱ	101.2 (7)	U6—O17—O22	52.5 (4)
O6—K2—O21	101.2 (6)	U6—O17—O27	147.7 (9)
O6—K2—O21^xvii	138.4 (7)	U6—O17—O32	124.5 (9)
O6—K2—O22	59.0 (6)	Sr2—O17—Sr2'	0
O6—K2—O22^xvii	127.6 (6)	Sr2—O17—K1^xviii	88.6 (4)
O6—K2—O24	64.9 (7)	Sr2—O17—O1	165.8 (6)
O6—K2—O30^iv	140.8 (7)	Sr2—O17—O2^xviii	117.7 (5)
O6—K2—O31^v	61.8 (8)	Sr2—O17—O5	51.8 (6)
O6^xvii—K2—O12	121.0 (6)	Sr2—O17—O8	55.0 (6)
O6^xvii—K2—O12^xvii	84.2 (7)	Sr2—O17—O10	128.0 (7)
O6^xvii—K2—O14^xviii	101.2 (7)	Sr2—O17—O13	100.5 (5)
O6^xvii—K2—O14ⁱⁱⁱ	168.5 (6)	Sr2—O17—O14ⁱⁱⁱ	122.2 (7)
O6^xvii—K2—O21	138.4 (7)	Sr2—O17—O18ⁱ	94.6 (5)
O6^xvii—K2—O21^xvii	101.2 (6)	Sr2—O17—O21	146.6 (4)
O6^xvii—K2—O22	127.6 (6)	Sr2—O17—O22	95.4 (4)
O6^xvii—K2—O22^xvii	59.0 (6)	Sr2—O17—O27	53.8 (6)
O6^xvii—K2—O24	64.9 (7)	Sr2—O17—O32	52.0 (6)
O6^xvii—K2—O30^iv	140.8 (7)	Sr2'—O17—K1^xviii	88.6 (4)
O6^xvii—K2—O31^v	61.8 (8)	Sr2'—O17—O1	165.8 (6)
O12—K2—O12^xvii	66.3 (6)	Sr2'—O17—O2^xviii	117.7 (5)
O12—K2—O14^xviii	97.3 (6)	Sr2'—O17—O5	51.8 (6)
O12—K2—O14ⁱⁱⁱ	50.6 (4)	Sr2'—O17—O8	55.0 (6)
O12—K2—O21	96.6 (5)	Sr2'—O17—O10	128.0 (7)
O12—K2—O21^xvii	130.7 (5)	Sr2'—O17—O13	100.5 (5)
O12—K2—O22	54.7 (5)	Sr2'—O17—O14ⁱⁱⁱ	122.2 (7)
O12—K2—O22^xvii	120.9 (6)	Sr2'—O17—O18ⁱ	94.6 (5)
O12—K2—O24	144.5 (4)	Sr2'—O17—O21	146.6 (4)
O12—K2—O30^iv	59.3 (5)	Sr2'—O17—O22	95.4 (4)
O12—K2—O31^v	59.2 (7)	Sr2'—O17—O27	53.8 (6)
O12^xvii—K2—O14^xviii	50.6 (4)	Sr2'—O17—O32	52.0 (6)
O12^xvii—K2—O14ⁱⁱⁱ	97.3 (6)	K1^xviii—O17—O1	77.3 (4)
O12^xvii—K2—O21	130.7 (5)	K1^xviii—O17—O2^xviii	46.1 (5)
O12^xvii—K2—O21^xvii	96.6 (5)	K1^xviii—O17—O5	131.4 (7)
O12^xvii—K2—O22	120.9 (6)	K1^xviii—O17—O8	121.5 (7)
O12^xvii—K2—O22^xvii	54.7 (5)	K1^xviii—O17—O10	92.2 (4)
O12^xvii—K2—O24	144.5 (4)	K1^xviii—O17—O13	134.3 (6)
O12^xvii—K2—O30^iv	59.3 (5)	K1^xviii—O17—O14ⁱⁱⁱ	119.6 (7)
O12^xvii—K2—O31^v	59.2 (7)	K1^xviii—O17—O18ⁱ	78.1 (5)
O14^xviii—K2—O14ⁱⁱⁱ	88.4 (6)	K1^xviii—O17—O21	124.4 (4)
O14^xviii—K2—O21	90.0 (5)	K1^xviii—O17—O22	174.4 (7)
O14^xviii—K2—O21^xvii	46.8 (5)	K1^xviii—O17—O27	61.7 (5)
O14^xviii—K2—O22	130.8 (6)	K1^xviii—O17—O32	70.0 (6)
O14^xviii—K2—O22^xvii	42.4 (5)	O1—O17—O2^xviii	51.0 (6)
O14^xviii—K2—O24	116.5 (6)	O1—O17—O5	139.5 (10)
O14^xviii—K2—O30^iv	45.6 (5)	O1—O17—O8	134.0 (9)
O14^xviii—K2—O31^v	109.2 (7)	O1—O17—O10	53.1 (9)
O14ⁱⁱⁱ—K2—O21	46.8 (5)	O1—O17—O13	89.1 (8)
O14ⁱⁱⁱ—K2—O21^xvii	90.0 (5)	O1—O17—O14ⁱⁱⁱ	67.0 (7)
O14ⁱⁱⁱ—K2—O22	42.4 (5)	O1—O17—O18ⁱ	83.3 (9)
O14ⁱⁱⁱ—K2—O22^xvii	130.8 (6)	O1—O17—O21	47.4 (5)
O14ⁱⁱⁱ—K2—O24	116.5 (6)	O1—O17—O22	98.8 (6)
O14ⁱⁱⁱ—K2—O30^iv	45.6 (5)	O1—O17—O27	117.9 (10)
O14ⁱⁱⁱ—K2—O31^v	109.2 (7)	O1—O17—O32	120.6 (9)
O21—K2—O21^xvii	58.9 (4)	O2^xviii—O17—O5	123.5 (10)
O21—K2—O22	59.4 (3)	O2^xviii—O17—O8	167.6 (8)
O21—K2—O22^xvii	118.2 (4)	O2^xviii—O17—O10	46.2 (5)
O21—K2—O24	74.2 (6)	O2^xviii—O17—O13	91.9 (7)
O21—K2—O30^iv	72.1 (6)	O2^xviii—O17—O14ⁱⁱⁱ	117.6 (7)
O21—K2—O31^v	150.0 (3)	O2^xviii—O17—O18ⁱ	109.7 (8)
O21^xvii—K2—O22	118.2 (4)	O2^xviii—O17—O21	87.0 (4)
O21^xvii—K2—O22^xvii	59.4 (3)	O2^xviii—O17—O22	134.0 (7)
O21^xvii—K2—O24	74.2 (6)	O2^xviii—O17—O27	107.8 (7)
O21^xvii—K2—O30^iv	72.1 (6)	O2^xviii—O17—O32	70.9 (7)
O21^xvii—K2—O31^v	150.0 (3)	O5—O17—O8	61.8 (7)
O22—K2—O22^xvii	172.9 (6)	O5—O17—O10	93.0 (7)
O22—K2—O24	92.8 (4)	O5—O17—O13	50.6 (6)
O22—K2—O30^iv	86.5 (4)	O5—O17—O14ⁱⁱⁱ	106.3 (7)
O22—K2—O31^v	90.8 (2)	O5—O17—O18ⁱ	125.4 (7)
O22^xvii—K2—O24	92.8 (4)	O5—O17—O21	96.4 (6)
O22^xvii—K2—O30^iv	86.5 (4)	O5—O17—O22	54.1 (6)
O22^xvii—K2—O31^v	90.8 (2)	O5—O17—O27	102.1 (8)
O24—K2—O30^iv	141.2 (7)	O5—O17—O32	63.6 (7)
O24—K2—O31^v	114.1 (10)	O8—O17—O10	145.9 (7)
O30^iv—K2—O31^v	104.7 (10)	O8—O17—O13	99.3 (5)
U4—K3—U4ⁱ	118.9 (3)	O8—O17—O14ⁱⁱⁱ	67.5 (7)
U4—K3—O5	141.8 (5)	O8—O17—O18ⁱ	63.6 (6)
U4—K3—O5ⁱ	80.7 (5)	O8—O17—O21	104.0 (7)
U4—K3—O7	24.4 (3)	O8—O17—O22	58.4 (6)
U4—K3—O7ⁱ	95.5 (4)	O8—O17—O27	59.9 (7)
U4—K3—O11	133.6 (3)	O8—O17—O32	105.4 (7)
U4—K3—O11ⁱ	81.9 (3)	O10—O17—O13	47.4 (4)
U4—K3—O16	157.1 (5)	O10—O17—O14ⁱⁱⁱ	102.1 (8)
U4—K3—O16ⁱ	38.2 (3)	O10—O17—O18ⁱ	136.3 (6)
U4—K3—O19	125.6 (4)	O10—O17—O21	53.4 (4)
U4—K3—O19ⁱ	43.65 (18)	O10—O17—O22	88.6 (6)
U4—K3—O20	118.1 (5)	O10—O17—O27	153.7 (6)
U4—K3—O20ⁱ	36.8 (5)	O10—O17—O32	79.8 (7)
U4—K3—O23	120.28 (15)	O13—O17—O14ⁱⁱⁱ	93.1 (7)
U4—K3—O25	82.1 (4)	O13—O17—O18ⁱ	144.0 (5)
U4—K3—O28^vi	75.4 (4)	O13—O17—O21	53.7 (4)
U4ⁱ—K3—O5	80.7 (5)	O13—O17—O22	48.9 (5)
U4ⁱ—K3—O5ⁱ	141.8 (5)	O13—O17—O27	152.7 (6)
U4ⁱ—K3—O7	95.5 (4)	O13—O17—O32	80.8 (7)
U4ⁱ—K3—O7ⁱ	24.4 (3)	O14ⁱⁱⁱ—O17—O18ⁱ	51.6 (7)
U4ⁱ—K3—O11	81.9 (3)	O14ⁱⁱⁱ—O17—O21	49.9 (7)
U4ⁱ—K3—O11ⁱ	133.6 (3)	O14ⁱⁱⁱ—O17—O22	54.8 (6)
U4ⁱ—K3—O16	38.2 (3)	O14ⁱⁱⁱ—O17—O27	94.2 (9)
U4ⁱ—K3—O16ⁱ	157.1 (5)	O14ⁱⁱⁱ—O17—O32	169.9 (7)
U4ⁱ—K3—O19	43.65 (18)	O18ⁱ—O17—O21	97.7 (5)
U4ⁱ—K3—O19ⁱ	125.6 (4)	O18ⁱ—O17—O22	97.5 (6)
U4ⁱ—K3—O20	36.8 (5)	O18ⁱ—O17—O27	46.0 (6)
U4ⁱ—K3—O20ⁱ	118.1 (5)	O18ⁱ—O17—O32	132.9 (7)
U4ⁱ—K3—O23	120.28 (15)	O21—O17—O22	52.3 (4)
U4ⁱ—K3—O25	82.1 (4)	O21—O17—O27	143.3 (8)
U4ⁱ—K3—O28^vi	75.4 (4)	O21—O17—O32	128.8 (8)
O5—K3—O5ⁱ	66.8 (7)	O22—O17—O27	117.7 (7)
O5—K3—O7	138.1 (7)	O22—O17—O32	115.6 (7)
O5—K3—O7ⁱ	95.8 (6)	O27—O17—O32	87.8 (8)
O5—K3—O11	78.1 (6)	U5—O18—K4^v	117.0 (15)
O5—K3—O11ⁱ	108.9 (7)	U5—O18—O1^x	51.4 (9)
O5—K3—O16	52.4 (5)	U5—O18—O2	1.6 (9)
O5—K3—O16ⁱ	118.7 (6)	U5—O18—O7^xv	86.5 (15)
O5—K3—O19	46.2 (6)	U5—O18—O8ⁱ	94.7 (13)
O5—K3—O19ⁱ	98.2 (5)	U5—O18—O9^xi	52.5 (10)
O5—K3—O20	97.3 (6)	U5—O18—O10^x	48.5 (6)
O5—K3—O20ⁱ	160.1 (8)	U5—O18—O14^ix	52.0 (10)
O5—K3—O23	57.2 (7)	U5—O18—O15^xi	92.7 (12)
O5—K3—O25	67.7 (7)	U5—O18—O17ⁱ	101.7 (14)
O5—K3—O28^vi	142.8 (6)	U5—O18—O20^xi	52.9 (7)
O5ⁱ—K3—O7	95.8 (6)	U5—O18—O21^x	87.5 (9)
O5ⁱ—K3—O7ⁱ	138.1 (7)	U5—O18—O26^xxi	142.4 (12)
O5ⁱ—K3—O11	108.9 (7)	U5—O18—O27	145 (2)
O5ⁱ—K3—O11ⁱ	78.1 (6)	K4^v—O18—O1^x	65.6 (8)
O5ⁱ—K3—O16	118.7 (6)	K4^v—O18—O2	118.4 (11)
O5ⁱ—K3—O16ⁱ	52.4 (5)	K4^v—O18—O7^xv	46.2 (7)
O5ⁱ—K3—O19	98.2 (5)	K4^v—O18—O8ⁱ	95.3 (7)
O5ⁱ—K3—O19ⁱ	46.2 (6)	K4^v—O18—O9^xi	92.0 (13)
O5ⁱ—K3—O20	160.1 (8)	K4^v—O18—O10^x	94.6 (7)
O5ⁱ—K3—O20ⁱ	97.3 (6)	K4^v—O18—O14^ix	145.6 (10)
O5ⁱ—K3—O23	57.2 (7)	K4^v—O18—O15^xi	96.4 (11)
O5ⁱ—K3—O25	67.7 (7)	K4^v—O18—O17ⁱ	128.5 (9)
O5ⁱ—K3—O28^vi	142.8 (6)	K4^v—O18—O20^xi	145.1 (17)
O7—K3—O7ⁱ	71.5 (6)	K4^v—O18—O21^x	42.6 (4)
O7—K3—O11	143.1 (4)	K4^v—O18—O26^xxi	85.4 (7)
O7—K3—O11ⁱ	103.6 (4)	K4^v—O18—O27	80.8 (7)
O7—K3—O16	133.6 (6)	O1^x—O18—O2	52.8 (6)
O7—K3—O16ⁱ	62.1 (5)	O1^x—O18—O7^xv	48.1 (9)
O7—K3—O19	104.6 (5)	O1^x—O18—O8ⁱ	99.3 (10)
O7—K3—O19ⁱ	50.7 (3)	O1^x—O18—O9^xi	53.7 (9)
O7—K3—O20	104.1 (6)	O1^x—O18—O10^x	52.5 (8)
O7—K3—O20ⁱ	51.8 (6)	O1^x—O18—O14^ix	95.4 (9)
O7—K3—O23	144.2 (4)	O1^x—O18—O15^xi	98.4 (14)
O7—K3—O25	70.4 (6)	O1^x—O18—O17ⁱ	138.7 (11)
O7—K3—O28^vi	73.1 (7)	O1^x—O18—O20^xi	95.9 (10)
O7ⁱ—K3—O11	103.6 (4)	O1^x—O18—O21^x	46.3 (6)
O7ⁱ—K3—O11ⁱ	143.1 (4)	O1^x—O18—O26^xxi	137.8 (18)
O7ⁱ—K3—O16	62.1 (5)	O1^x—O18—O27	134.3 (10)
O7ⁱ—K3—O16ⁱ	133.6 (6)	O2—O18—O7^xv	88.0 (10)
O7ⁱ—K3—O19	50.7 (3)	O2—O18—O8ⁱ	93.7 (10)
O7ⁱ—K3—O19ⁱ	104.6 (5)	O2—O18—O9^xi	53.6 (8)
O7ⁱ—K3—O20	51.8 (6)	O2—O18—O10^x	48.3 (5)
O7ⁱ—K3—O20ⁱ	104.1 (6)	O2—O18—O14^ix	50.5 (9)
O7ⁱ—K3—O23	144.2 (4)	O2—O18—O15^xi	93.2 (9)
O7ⁱ—K3—O25	70.4 (6)	O2—O18—O17ⁱ	100.1 (10)
O7ⁱ—K3—O28^vi	73.1 (7)	O2—O18—O20^xi	52.3 (6)
O11—K3—O11ⁱ	57.7 (4)	O2—O18—O21^x	88.3 (6)
O11—K3—O16	55.2 (4)	O2—O18—O26^xxi	142.3 (9)
O11—K3—O16ⁱ	112.7 (5)	O2—O18—O27	144.0 (16)
O11—K3—O19	98.6 (3)	O7^xv—O18—O8ⁱ	134.4 (7)
O11—K3—O19ⁱ	151.8 (4)	O7^xv—O18—O9^xi	46.1 (7)
O11—K3—O20	53.9 (6)	O7^xv—O18—O10^x	100.0 (10)
O11—K3—O20ⁱ	97.1 (5)	O7^xv—O18—O14^ix	138.5 (10)
O11—K3—O23	51.8 (4)	O7^xv—O18—O15^xi	62.8 (9)
O11—K3—O25	144.1 (4)	O7^xv—O18—O17ⁱ	171.8 (4)
O11—K3—O28^vi	70.7 (7)	O7^xv—O18—O20^xi	99.2 (12)
O11ⁱ—K3—O16	112.7 (5)	O7^xv—O18—O21^x	67.8 (7)
O11ⁱ—K3—O16ⁱ	55.2 (4)	O7^xv—O18—O26^xxi	89.7 (11)
O11ⁱ—K3—O19	151.8 (4)	O7^xv—O18—O27	123.1 (9)
O11ⁱ—K3—O19ⁱ	98.6 (3)	O8ⁱ—O18—O9^xi	145.4 (7)
O11ⁱ—K3—O20	97.1 (5)	O8ⁱ—O18—O10^x	52.6 (7)
O11ⁱ—K3—O20ⁱ	53.9 (6)	O8ⁱ—O18—O14^ix	58.1 (9)
O11ⁱ—K3—O23	51.8 (4)	O8ⁱ—O18—O15^xi	161.7 (12)
O11ⁱ—K3—O25	144.1 (4)	O8ⁱ—O18—O17ⁱ	46.6 (6)
O11ⁱ—K3—O28^vi	70.7 (7)	O8ⁱ—O18—O20^xi	117.6 (12)
O16—K3—O16ⁱ	164.3 (7)	O8ⁱ—O18—O21^x	66.8 (6)
O16—K3—O19	44.6 (4)	O8ⁱ—O18—O26^xxi	114.0 (12)
O16—K3—O19ⁱ	142.0 (4)	O8ⁱ—O18—O27	52.3 (9)
O16—K3—O20	45.1 (4)	O9^xi—O18—O10^x	93.1 (8)
O16—K3—O20ⁱ	139.2 (5)	O9^xi—O18—O14^ix	99.3 (7)
O16—K3—O23	82.2 (4)	O9^xi—O18—O15^xi	48.1 (8)
O16—K3—O25	93.7 (3)	O9^xi—O18—O17ⁱ	139.5 (8)
O16—K3—O28^vi	92.3 (3)	O9^xi—O18—O20^xi	54.5 (8)
O16ⁱ—K3—O19	142.0 (4)	O9^xi—O18—O21^x	97.8 (10)
O16ⁱ—K3—O19ⁱ	44.6 (4)	O9^xi—O18—O26^xxi	100.3 (12)
O16ⁱ—K3—O20	139.2 (5)	O9^xi—O18—O27	162.0 (11)
O16ⁱ—K3—O20ⁱ	45.1 (4)	O10^x—O18—O14^ix	52.7 (7)
O16ⁱ—K3—O23	82.2 (4)	O10^x—O18—O15^xi	139.9 (10)
O16ⁱ—K3—O25	93.7 (3)	O10^x—O18—O17ⁱ	86.3 (10)
O16ⁱ—K3—O28^vi	92.3 (3)	O10^x—O18—O20^xi	96.5 (6)
O19—K3—O19ⁱ	98.5 (3)	O10^x—O18—O21^x	52.3 (5)
O19—K3—O20	76.8 (4)	O10^x—O18—O26^xxi	166.6 (16)
O19—K3—O20ⁱ	153.0 (6)	O10^x—O18—O27	103.7 (12)
O19—K3—O23	102.5 (4)	O14^ix—O18—O15^xi	115.4 (8)
O19—K3—O25	49.3 (2)	O14^ix—O18—O17ⁱ	49.8 (9)
O19—K3—O28^vi	118.9 (4)	O14^ix—O18—O20^xi	60.4 (8)
O19ⁱ—K3—O20	153.0 (6)	O14^ix—O18—O21^x	103.4 (8)
O19ⁱ—K3—O20ⁱ	76.8 (4)	O14^ix—O18—O26^xxi	123.7 (14)
O19ⁱ—K3—O23	102.5 (4)	O14^ix—O18—O27	95.8 (15)
O19ⁱ—K3—O25	49.3 (2)	O15^xi—O18—O17ⁱ	115.3 (9)
O19ⁱ—K3—O28^vi	118.9 (4)	O15^xi—O18—O20^xi	55.5 (8)
O20—K3—O20ⁱ	95.2 (5)	O15^xi—O18—O21^x	130.4 (13)
O20—K3—O23	104.5 (6)	O15^xi—O18—O26^xxi	53.1 (8)
O20—K3—O25	118.8 (6)	O15^xi—O18—O27	116.0 (8)
O20—K3—O28^vi	47.6 (4)	O17ⁱ—O18—O20^xi	85.3 (10)
O20ⁱ—K3—O23	104.5 (6)	O17ⁱ—O18—O21^x	113.1 (9)
O20ⁱ—K3—O25	118.8 (6)	O17ⁱ—O18—O26^xxi	83.2 (11)
O20ⁱ—K3—O28^vi	47.6 (4)	O17ⁱ—O18—O27	49.5 (9)
O23—K3—O25	112.6 (7)	O20^xi—O18—O21^x	139.7 (9)
O23—K3—O28^vi	112.9 (9)	O20^xi—O18—O26^xxi	91.1 (8)
O25—K3—O28^vi	134.6 (10)	O20^xi—O18—O27	127.9 (15)
O1^xiii—K4—O1ⁱ	164.2 (10)	O21^x—O18—O26^xxi	125.2 (7)
O1^xiii—K4—O7^xi	55.5 (8)	O21^x—O18—O27	88.0 (8)
O1^xiii—K4—O7^xix	118.6 (9)	O26^xxi—O18—O27	63.0 (7)
O1^xiii—K4—O18^ix	56.7 (8)	U2ⁱⁱⁱ—O19—U3	140.2 (6)
O1^xiii—K4—O18^xx	139.0 (9)	U2ⁱⁱⁱ—O19—U4ⁱ	97.5 (5)
O1^xiii—K4—O21^xiii	53.9 (6)	U2ⁱⁱⁱ—O19—K3	137.6 (6)
O1^xiii—K4—O21ⁱ	121.2 (6)	U2ⁱⁱⁱ—O19—O3ⁱⁱⁱ	45.0 (5)
O1^xiii—K4—O27^ix	97.5 (8)	U2ⁱⁱⁱ—O19—O4ⁱ	90.5 (5)
O1^xiii—K4—O28	82.5 (8)	U2ⁱⁱⁱ—O19—O5	152.9 (6)
O1ⁱ—K4—O7^xi	118.6 (9)	U2ⁱⁱⁱ—O19—O6	109.7 (8)
O1ⁱ—K4—O7^xix	55.5 (8)	U2ⁱⁱⁱ—O19—O7ⁱ	103.1 (6)
O1ⁱ—K4—O18^ix	139.0 (9)	U2ⁱⁱⁱ—O19—O9ⁱⁱⁱ	50.5 (4)
O1ⁱ—K4—O18^xx	56.7 (8)	U2ⁱⁱⁱ—O19—O11ⁱⁱⁱ	36.6 (4)
O1ⁱ—K4—O21^xiii	121.2 (6)	U2ⁱⁱⁱ—O19—O13	99.4 (5)
O1ⁱ—K4—O21ⁱ	53.9 (6)	U2ⁱⁱⁱ—O19—O15ⁱⁱⁱ	37.8 (6)
O1ⁱ—K4—O27^ix	97.5 (8)	U2ⁱⁱⁱ—O19—O16	146.2 (6)
O1ⁱ—K4—O28	82.5 (8)	U2ⁱⁱⁱ—O19—O25	103.9 (9)
O7^xi—K4—O7^xix	63.7 (5)	U3—O19—U4ⁱ	95.9 (5)
O7^xi—K4—O18^ix	80.9 (8)	U3—O19—K3	82.0 (4)
O7^xi—K4—O18^xx	122.5 (7)	U3—O19—O3ⁱⁱⁱ	108.6 (6)
O7^xi—K4—O21^xiii	104.0 (5)	U3—O19—O4ⁱ	83.4 (5)
O7^xi—K4—O21ⁱ	146.4 (8)	U3—O19—O5	38.3 (6)
O7^xi—K4—O27^ix	123.1 (5)	U3—O19—O6	36.4 (6)
O7^xi—K4—O28	56.1 (5)	U3—O19—O7ⁱ	109.6 (6)
O7^xix—K4—O18^ix	122.5 (7)	U3—O19—O9ⁱⁱⁱ	135.8 (6)
O7^xix—K4—O18^xx	80.9 (8)	U3—O19—O11ⁱⁱⁱ	105.7 (6)
O7^xix—K4—O21^xiii	146.4 (8)	U3—O19—O13	50.1 (4)
O7^xix—K4—O21ⁱ	104.0 (5)	U3—O19—O15ⁱⁱⁱ	164.6 (6)
O7^xix—K4—O27^ix	123.1 (5)	U3—O19—O16	52.0 (4)
O7^xix—K4—O28	56.1 (5)	U3—O19—O25	111.0 (9)
O18^ix—K4—O18^xx	82.3 (7)	U4ⁱ—O19—K3	67.1 (3)
O18^ix—K4—O21^xiii	82.9 (6)	U4ⁱ—O19—O3ⁱⁱⁱ	141.2 (7)
O18^ix—K4—O21ⁱ	127.7 (10)	U4ⁱ—O19—O4ⁱ	29.0 (2)
O18^ix—K4—O27^ix	46.1 (7)	U4ⁱ—O19—O5	109.6 (7)
O18^ix—K4—O28	133.5 (7)	U4ⁱ—O19—O6	81.4 (5)
O18^xx—K4—O21^xiii	127.7 (10)	U4ⁱ—O19—O7ⁱ	36.0 (3)
O18^xx—K4—O21ⁱ	82.9 (6)	U4ⁱ—O19—O9ⁱⁱⁱ	47.7 (3)
O18^xx—K4—O27^ix	46.1 (7)	U4ⁱ—O19—O11ⁱⁱⁱ	92.1 (4)
O18^xx—K4—O28	133.5 (7)	U4ⁱ—O19—O13	140.2 (6)
O21^xiii—K4—O21ⁱ	67.9 (5)	U4ⁱ—O19—O15ⁱⁱⁱ	99.5 (6)
O21^xiii—K4—O27^ix	90.2 (6)	U4ⁱ—O19—O16	50.2 (4)
O21^xiii—K4—O28	90.7 (6)	U4ⁱ—O19—O25	98.4 (5)
O21ⁱ—K4—O27^ix	90.2 (6)	K3—O19—O3ⁱⁱⁱ	144.2 (5)
O21ⁱ—K4—O28	90.7 (6)	K3—O19—O4ⁱ	91.1 (3)
O27^ix—K4—O28	179.0 (5)	K3—O19—O5	59.0 (6)
U4^xxi—O1—U5^xviii	105.3 (9)	K3—O19—O6	106.7 (7)
U4^xxi—O1—U6	149.3 (17)	K3—O19—O7ⁱ	41.6 (4)
U4^xxi—O1—K1^xviii	90.7 (8)	K3—O19—O9ⁱⁱⁱ	99.8 (4)
U4^xxi—O1—K4^iv	90.9 (7)	K3—O19—O11ⁱⁱⁱ	158.7 (4)
U4^xxi—O1—O2^xviii	101.7 (10)	K3—O19—O13	117.9 (6)
U4^xxi—O1—O4^xxi	36.3 (6)	K3—O19—O15ⁱⁱⁱ	103.5 (7)
U4^xxi—O1—O7^xxi	38.1 (6)	K3—O19—O16	46.6 (4)
U4^xxi—O1—O9^xxii	53.1 (7)	K3—O19—O25	45.4 (6)
U4^xxi—O1—O10	156.5 (11)	O3ⁱⁱⁱ—O19—O4ⁱ	123.5 (6)
U4^xxi—O1—O14ⁱⁱⁱ	102.2 (14)	O3ⁱⁱⁱ—O19—O5	108.2 (7)
U4^xxi—O1—O17	129.1 (13)	O3ⁱⁱⁱ—O19—O6	100.5 (7)
U4^xxi—O1—O18^xviii	103.5 (10)	O3ⁱⁱⁱ—O19—O7ⁱ	141.7 (8)
U4^xxi—O1—O20^xxiii	46.8 (9)	O3ⁱⁱⁱ—O19—O9ⁱⁱⁱ	95.5 (7)
U4^xxi—O1—O21	130.1 (11)	O3ⁱⁱⁱ—O19—O11ⁱⁱⁱ	52.9 (4)
U5^xviii—O1—U6	105.3 (17)	O3ⁱⁱⁱ—O19—O13	58.9 (6)
U5^xviii—O1—K1^xviii	83.0 (5)	O3ⁱⁱⁱ—O19—O15ⁱⁱⁱ	58.7 (7)
U5^xviii—O1—K4^iv	94.0 (8)	O3ⁱⁱⁱ—O19—O16	160.2 (8)
U5^xviii—O1—O2^xviii	36.9 (5)	O3ⁱⁱⁱ—O19—O25	100.2 (7)
U5^xviii—O1—O4^xxi	99.3 (7)	O4ⁱ—O19—O5	112.7 (7)
U5^xviii—O1—O7^xxi	102.6 (8)	O4ⁱ—O19—O6	57.3 (5)
U5^xviii—O1—O9^xxii	52.4 (6)	O4ⁱ—O19—O7ⁱ	65.0 (4)
U5^xviii—O1—O10	51.8 (9)	O4ⁱ—O19—O9ⁱⁱⁱ	52.6 (5)
U5^xviii—O1—O14ⁱⁱⁱ	152.4 (17)	O4ⁱ—O19—O11ⁱⁱⁱ	70.6 (4)
U5^xviii—O1—O17	103.3 (12)	O4ⁱ—O19—O13	115.1 (6)
U5^xviii—O1—O18^xviii	36.3 (6)	O4ⁱ—O19—O15ⁱⁱⁱ	110.6 (7)
U5^xviii—O1—O20^xxiii	152.0 (13)	O4ⁱ—O19—O16	56.8 (5)
U5^xviii—O1—O21	105.6 (15)	O4ⁱ—O19—O25	127.4 (6)
U6—O1—K1^xviii	90.3 (5)	O5—O19—O6	74.8 (9)
U6—O1—K4^iv	89.7 (7)	O5—O19—O7ⁱ	99.4 (7)
U6—O1—O2^xviii	100.9 (14)	O5—O19—O9ⁱⁱⁱ	156.1 (7)
U6—O1—O4^xxi	133.8 (10)	O5—O19—O11ⁱⁱⁱ	137.6 (8)
U6—O1—O7^xxi	134.5 (7)	O5—O19—O13	59.0 (6)
U6—O1—O9^xxii	158 (2)	O5—O19—O15ⁱⁱⁱ	133.1 (9)
U6—O1—O10	53.6 (9)	O5—O19—O16	60.2 (6)
U6—O1—O14ⁱⁱⁱ	47.2 (7)	O5—O19—O25	73.6 (9)
U6—O1—O17	38.5 (4)	O6—O19—O7ⁱ	112.2 (6)
U6—O1—O18^xviii	102.7 (16)	O6—O19—O9ⁱⁱⁱ	104.2 (7)
U6—O1—O20^xxiii	102.5 (10)	O6—O19—O11ⁱⁱⁱ	73.1 (7)
U6—O1—O21	41.0 (5)	O6—O19—O13	59.0 (5)
K1^xviii—O1—K4^iv	176.9 (13)	O6—O19—O15ⁱⁱⁱ	147.4 (10)
K1^xviii—O1—O2^xviii	46.1 (4)	O6—O19—O16	62.0 (7)
K1^xviii—O1—O4^xxi	54.4 (4)	O6—O19—O25	146.2 (11)
K1^xviii—O1—O7^xxi	128.5 (12)	O7ⁱ—O19—O9ⁱⁱⁱ	58.3 (5)
K1^xviii—O1—O9^xxii	88.9 (5)	O7ⁱ—O19—O11ⁱⁱⁱ	118.0 (6)
K1^xviii—O1—O10	82.4 (7)	O7ⁱ—O19—O13	157.5 (8)
K1^xviii—O1—O14ⁱⁱⁱ	95.0 (7)	O7ⁱ—O19—O15ⁱⁱⁱ	83.0 (7)
K1^xviii—O1—O17	52.4 (3)	O7ⁱ—O19—O16	58.1 (5)
K1^xviii—O1—O18^xviii	119.3 (9)	O7ⁱ—O19—O25	62.4 (5)
K1^xviii—O1—O20^xxiii	93.5 (9)	O9ⁱⁱⁱ—O19—O11ⁱⁱⁱ	60.6 (5)
K1^xviii—O1—O21	131.3 (9)	O9ⁱⁱⁱ—O19—O13	141.4 (7)
K4^iv—O1—O2^xviii	130.9 (12)	O9ⁱⁱⁱ—O19—O15ⁱⁱⁱ	58.1 (6)
K4^iv—O1—O4^xxi	127.2 (12)	O9ⁱⁱⁱ—O19—O16	97.8 (5)
K4^iv—O1—O7^xxi	52.9 (4)	O9ⁱⁱⁱ—O19—O25	99.9 (8)
K4^iv—O1—O9^xxii	89.9 (6)	O11ⁱⁱⁱ—O19—O13	80.8 (5)
K4^iv—O1—O10	95.1 (11)	O11ⁱⁱⁱ—O19—O15ⁱⁱⁱ	74.3 (7)
K4^iv—O1—O14ⁱⁱⁱ	87.3 (7)	O11ⁱⁱⁱ—O19—O16	123.2 (6)
K4^iv—O1—O17	127.9 (9)	O11ⁱⁱⁱ—O19—O25	140.3 (9)
K4^iv—O1—O18^xviii	57.7 (6)	O13—O19—O15ⁱⁱⁱ	115.7 (6)
K4^iv—O1—O20^xxiii	89.5 (9)	O13—O19—O16	102.1 (7)
K4^iv—O1—O21	48.8 (4)	O13—O19—O25	112.0 (7)
O2^xviii—O1—O4^xxi	76.7 (9)	O15ⁱⁱⁱ—O19—O16	141.1 (7)
O2^xviii—O1—O7^xxi	122.7 (10)	O15ⁱⁱⁱ—O19—O25	66.2 (9)
O2^xviii—O1—O9^xxii	63.3 (7)	O16—O19—O25	91.9 (8)
O2^xviii—O1—O10	57.8 (11)	U2—O20—U4ⁱ	99.4 (7)
O2^xviii—O1—O14ⁱⁱⁱ	133.9 (9)	U2—O20—U5^vi	100.6 (12)
O2^xviii—O1—O17	78.1 (7)	U2—O20—K3	78.2 (6)
O2^xviii—O1—O18^xviii	73.3 (9)	U2—O20—O1^xxvii	140.2 (10)
O2^xviii—O1—O20^xxiii	132.8 (13)	U2—O20—O2^vi	103.1 (13)
O2^xviii—O1—O21	126.2 (18)	U2—O20—O4ⁱ	87.5 (7)
O4^xxi—O1—O7^xxi	74.3 (10)	U2—O20—O7ⁱ	106.3 (7)
O4^xxi—O1—O9^xxii	61.1 (8)	U2—O20—O9	48.8 (6)
O4^xxi—O1—O10	132.5 (7)	U2—O20—O11	33.4 (4)
O4^xxi—O1—O14ⁱⁱⁱ	101.8 (12)	U2—O20—O14^vii	151.2 (12)
O4^xxi—O1—O17	98.2 (7)	U2—O20—O15	34.8 (7)
O4^xxi—O1—O18^xviii	119.8 (10)	U2—O20—O16	51.2 (6)
O4^xxi—O1—O20^xxiii	57.6 (10)	U2—O20—O18^vi	95.6 (12)
O4^xxi—O1—O21	154.9 (15)	U2—O20—O28^vi	104.0 (12)
O7^xxi—O1—O9^xxii	59.4 (7)	U4ⁱ—O20—U5^vi	148.1 (14)
O7^xxi—O1—O10	140.5 (11)	U4ⁱ—O20—K3	68.9 (6)
O7^xxi—O1—O14ⁱⁱⁱ	100.1 (11)	U4ⁱ—O20—O1^xxvii	43.1 (7)
O7^xxi—O1—O17	153.9 (15)	U4ⁱ—O20—O2^vi	154.0 (15)
O7^xxi—O1—O18^xviii	80.1 (9)	U4ⁱ—O20—O4ⁱ	34.8 (5)
O7^xxi—O1—O20^xxiii	58.4 (9)	U4ⁱ—O20—O7ⁱ	35.9 (5)
O7^xxi—O1—O21	97.0 (5)	U4ⁱ—O20—O9	142.5 (11)
O9^xxii—O1—O10	104.2 (12)	U4ⁱ—O20—O11	109.5 (7)
O9^xxii—O1—O14ⁱⁱⁱ	155.1 (18)	U4ⁱ—O20—O14^vii	105.6 (13)
O9^xxii—O1—O17	138.9 (7)	U4ⁱ—O20—O15	87.3 (9)
O9^xxii—O1—O18^xviii	58.9 (9)	U4ⁱ—O20—O16	53.3 (5)
O9^xxii—O1—O20^xxiii	99.9 (13)	U4ⁱ—O20—O18^vi	116.7 (12)
O9^xxii—O1—O21	134.7 (9)	U4ⁱ—O20—O28^vi	99.8 (11)
O10—O1—O14ⁱⁱⁱ	100.7 (11)	U5^vi—O20—K3	139.8 (11)
O10—O1—O17	62.2 (8)	U5^vi—O20—O1^xxvii	109.2 (10)
O10—O1—O18^xviii	61.8 (11)	U5^vi—O20—O2^vi	37.4 (4)
O10—O1—O20^xxiii	155.5 (10)	U5^vi—O20—O4ⁱ	122.1 (11)
O10—O1—O21	68.4 (10)	U5^vi—O20—O7ⁱ	150.9 (12)
O14ⁱⁱⁱ—O1—O17	56.3 (7)	U5^vi—O20—O9	51.8 (6)
O14ⁱⁱⁱ—O1—O18^xviii	136.2 (11)	U5^vi—O20—O11	100.9 (11)
O14ⁱⁱⁱ—O1—O20^xxiii	55.4 (8)	U5^vi—O20—O14^vii	50.7 (7)
O14ⁱⁱⁱ—O1—O21	55.9 (7)	U5^vi—O20—O15	95.2 (10)
O17—O1—O18^xviii	124.0 (17)	U5^vi—O20—O16	151.8 (15)
O17—O1—O20^xxiii	96.2 (10)	U5^vi—O20—O18^vi	36.7 (5)
O17—O1—O21	79.2 (8)	U5^vi—O20—O28^vi	99.1 (9)
O18^xviii—O1—O20^xxiii	138.0 (11)	K3—O20—O1^xxvii	94.5 (8)
O18^xviii—O1—O21	80.5 (10)	K3—O20—O2^vi	103.0 (8)
O20^xxiii—O1—O21	97.6 (9)	K3—O20—O4ⁱ	98.1 (6)
U5—O2—K1	135.1 (11)	K3—O20—O7ⁱ	40.8 (5)
U5—O2—O1^x	52.6 (7)	K3—O20—O9	113.5 (10)
U5—O2—O2^xii	168.6 (12)	K3—O20—O11	56.6 (5)
U5—O2—O4^xv	88.5 (12)	K3—O20—O14^vii	124.1 (10)
U5—O2—O9^xi	48.5 (8)	K3—O20—O15	103.9 (7)
U5—O2—O10^x	53.4 (7)	K3—O20—O16	45.7 (5)
U5—O2—O14^ix	56.5 (11)	K3—O20—O18^vi	172.5 (14)
U5—O2—O17^x	91.8 (5)	K3—O20—O28^vi	44.7 (5)
U5—O2—O18	1.6 (9)	O1^xxvii—O20—O2^vi	116.6 (12)
U5—O2—O20^xi	54.3 (6)	O1^xxvii—O20—O4ⁱ	54.5 (7)
U5—O2—O28	110.7 (6)	O1^xxvii—O20—O7ⁱ	54.1 (7)
U5—O2—O29^xv	119.0 (16)	O1^xxvii—O20—O9	151.5 (11)
U5—O2—O30	113.4 (17)	O1^xxvii—O20—O11	149.1 (9)
U5—O2—O32^x	118.0 (11)	O1^xxvii—O20—O14^vii	62.5 (9)
K1—O2—O1^x	82.5 (9)	O1^xxvii—O20—O15	114.8 (11)
K1—O2—O2^xii	56.3 (6)	O1^xxvii—O20—O16	96.1 (10)
K1—O2—O4^xv	57.1 (8)	O1^xxvii—O20—O18^vi	93.0 (12)
K1—O2—O9^xi	106.3 (13)	O1^xxvii—O20—O28^vi	96.8 (12)
K1—O2—O10^x	104.0 (5)	O2^vi—O20—O4ⁱ	157.9 (11)
K1—O2—O14^ix	148.7 (13)	O2^vi—O20—O7ⁱ	123.0 (11)
K1—O2—O17^x	53.7 (3)	O2^vi—O20—O9	63.5 (9)
K1—O2—O18	136.5 (9)	O2^vi—O20—O11	83.4 (11)
K1—O2—O20^xi	147.9 (16)	O2^vi—O20—O14^vii	57.2 (10)
K1—O2—O28	108.0 (8)	O2^vi—O20—O15	118.7 (13)
K1—O2—O29^xv	55.3 (8)	O2^vi—O20—O16	138.0 (14)
K1—O2—O30	101.0 (7)	O2^vi—O20—O18^vi	74.0 (7)
K1—O2—O32^x	58.3 (6)	O2^vi—O20—O28^vi	62.1 (7)
O1^x—O2—O2^xii	138.8 (11)	O4ⁱ—O20—O7ⁱ	70.7 (7)
O1^x—O2—O4^xv	50.3 (10)	O4ⁱ—O20—O9	113.5 (11)
O1^x—O2—O9^xi	52.8 (7)	O4ⁱ—O20—O11	114.1 (8)
O1^x—O2—O10^x	54.7 (9)	O4ⁱ—O20—O14^vii	105.1 (11)
O1^x—O2—O14^ix	100.2 (11)	O4ⁱ—O20—O15	61.2 (8)
O1^x—O2—O17^x	51.0 (5)	O4ⁱ—O20—O16	63.3 (6)
O1^x—O2—O18	54.0 (8)	O4ⁱ—O20—O18^vi	85.8 (9)
O1^x—O2—O20^xi	98.1 (8)	O4ⁱ—O20—O28^vi	134.6 (12)
O1^x—O2—O28	148.2 (13)	O7ⁱ—O20—O9	152.5 (11)
O1^x—O2—O29^xv	93.0 (13)	O7ⁱ—O20—O11	95.6 (7)
O1^x—O2—O30	139.8 (14)	O7ⁱ—O20—O14^vii	102.3 (11)
O1^x—O2—O32^x	93.2 (7)	O7ⁱ—O20—O15	113.3 (8)
O2^xii—O2—O4^xv	100.0 (12)	O7ⁱ—O20—O16	56.3 (6)
O2^xii—O2—O9^xi	133.7 (15)	O7ⁱ—O20—O18^vi	146.6 (14)
O2^xii—O2—O10^x	130.4 (12)	O7ⁱ—O20—O28^vi	64.0 (9)
O2^xii—O2—O14^ix	114.8 (14)	O9—O20—O11	57.3 (7)
O2^xii—O2—O17^x	97.9 (4)	O9—O20—O14^vii	102.5 (9)
O2^xii—O2—O18	167.2 (11)	O9—O20—O15	55.3 (8)
O2^xii—O2—O20^xi	116.2 (7)	O9—O20—O16	100.0 (11)
O2^xii—O2—O28	59.3 (4)	O9—O20—O18^vi	58.9 (10)
O2^xii—O2—O29^xv	64.8 (10)	O9—O20—O28^vi	106.5 (13)
O2^xii—O2—O30	59.2 (9)	O11—O20—O14^vii	140.4 (11)
O2^xii—O2—O32^x	66.9 (6)	O11—O20—O15	68.2 (9)
O4^xv—O2—O9^xi	49.2 (7)	O11—O20—O16	56.9 (7)
O4^xv—O2—O10^x	104.0 (7)	O11—O20—O18^vi	115.9 (13)
O4^xv—O2—O14^ix	145.0 (8)	O11—O20—O28^vi	70.9 (9)
O4^xv—O2—O17^x	73.6 (5)	O14^vii—O20—O15	131.8 (11)
O4^xv—O2—O18	90.0 (9)	O14^vii—O20—O16	157.4 (15)
O4^xv—O2—O20^xi	98.8 (11)	O14^vii—O20—O18^vi	60.4 (10)
O4^xv—O2—O28	109.6 (12)	O14^vii—O20—O28^vi	85.7 (10)
O4^xv—O2—O29^xv	42.7 (6)	O15—O20—O16	61.8 (7)
O4^xv—O2—O30	157.4 (7)	O15—O20—O18^vi	72.2 (10)
O4^xv—O2—O32^x	107.6 (7)	O15—O20—O28^vi	138.5 (13)
O9^xi—O2—O10^x	93.9 (5)	O16—O20—O18^vi	132.7 (12)
O9^xi—O2—O14^ix	99.7 (7)	O16—O20—O28^vi	90.0 (9)
O9^xi—O2—O17^x	102.6 (7)	O18^vi—O20—O28^vi	134.8 (9)
O9^xi—O2—O18	49.6 (7)	U6—O21—K2	110.9 (5)
O9^xi—O2—O20^xi	53.6 (8)	U6—O21—K4^iv	131.7 (6)
O9^xi—O2—O28	95.5 (8)	U6—O21—O1	54.5 (5)
O9^xi—O2—O29^xv	70.6 (9)	U6—O21—O10	47.0 (5)
O9^xi—O2—O30	151.8 (9)	U6—O21—O13	57.3 (5)
O9^xi—O2—O32^x	145.6 (7)	U6—O21—O14ⁱⁱⁱ	56.9 (7)
O10^x—O2—O14^ix	56.5 (9)	U6—O21—O17	4.5 (4)
O10^x—O2—O17^x	50.5 (4)	U6—O21—O18^xviii	89.9 (5)
O10^x—O2—O18	53.2 (6)	U6—O21—O21^xvii	170.9 (6)
O10^x—O2—O20^xi	102.3 (8)	U6—O21—O22	48.3 (4)
O10^x—O2—O28	142.5 (15)	U6—O21—O24	112.9 (6)
O10^x—O2—O29^xv	145.7 (11)	U6—O21—O30^iv	108.5 (7)
O10^x—O2—O30	86.1 (12)	K2—O21—K4^iv	115.8 (5)
O10^x—O2—O32^x	64.6 (6)	K2—O21—O1	157.5 (9)
O14^ix—O2—O17^x	104.1 (9)	K2—O21—O10	131.5 (6)
O14^ix—O2—O18	55.0 (10)	K2—O21—O13	81.5 (4)
O14^ix—O2—O20^xi	63.1 (8)	K2—O21—O14ⁱⁱⁱ	85.8 (6)
O14^ix—O2—O28	86.1 (10)	K2—O21—O17	110.4 (4)
O14^ix—O2—O29^xv	153.7 (7)	K2—O21—O18^xviii	149.2 (8)
O14^ix—O2—O30	57.1 (10)	K2—O21—O21^xvii	60.5 (3)
O14^ix—O2—O32^x	90.4 (11)	K2—O21—O22	62.6 (3)
O17^x—O2—O18	92.5 (5)	K2—O21—O24	47.1 (6)
O17^x—O2—O20^xi	145.9 (7)	K2—O21—O30^iv	50.6 (5)
O17^x—O2—O28	157.2 (5)	K4^iv—O21—O1	77.3 (5)
O17^x—O2—O29^xv	101.9 (9)	K4^iv—O21—O10	104.3 (5)
O17^x—O2—O30	99.0 (9)	K4^iv—O21—O13	140.6 (7)
O17^x—O2—O32^x	43.0 (5)	K4^iv—O21—O14ⁱⁱⁱ	114.3 (8)
O18—O2—O20^xi	53.7 (6)	K4^iv—O21—O17	130.7 (5)
O18—O2—O28	109.9 (6)	K4^iv—O21—O18^xviii	54.5 (5)
O18—O2—O29^xv	120.2 (12)	K4^iv—O21—O21^xvii	56.0 (4)
O18—O2—O30	111.9 (13)	K4^iv—O21—O22	167.8 (9)
O18—O2—O32^x	117.8 (9)	K4^iv—O21—O24	107.6 (6)
O20^xi—O2—O28	57.0 (6)	K4^iv—O21—O30^iv	92.1 (6)
O20^xi—O2—O29^xv	92.8 (10)	O1—O21—O10	54.3 (9)
O20^xi—O2—O30	98.8 (11)	O1—O21—O13	99.8 (9)
O20^xi—O2—O32^x	152.6 (16)	O1—O21—O14ⁱⁱⁱ	71.8 (9)
O28—O2—O29^xv	71.0 (9)	O1—O21—O17	53.4 (5)
O28—O2—O30	69.1 (8)	O1—O21—O18^xviii	53.2 (8)
O28—O2—O32^x	118.0 (8)	O1—O21—O21^xvii	132.5 (7)
O29^xv—O2—O30	122.2 (5)	O1—O21—O22	100.6 (6)
O29^xv—O2—O32^x	111.6 (6)	O1—O21—O24	149.9 (11)
O30—O2—O32^x	58.0 (8)	O1—O21—O30^iv	113.9 (11)
U1—O3—U2	146.9 (9)	O10—O21—O13	49.9 (4)
U1—O3—U3	108.0 (5)	O10—O21—O14ⁱⁱⁱ	102.2 (8)
U1—O3—O5	98.8 (7)	O10—O21—O17	50.8 (4)
U1—O3—O6	110.3 (7)	O10—O21—O18^xviii	50.1 (4)
U1—O3—O8	41.4 (7)	O10—O21—O21^xvii	140.3 (7)
U1—O3—O11	127.6 (10)	O10—O21—O22	83.5 (5)
U1—O3—O12	37.0 (4)	O10—O21—O24	96.5 (7)
U1—O3—O13ⁱⁱ	48.1 (6)	O10—O21—O30^iv	155.5 (6)
U1—O3—O15	133.5 (9)	O13—O21—O14ⁱⁱⁱ	101.4 (7)
U1—O3—O16	157.7 (6)	O13—O21—O17	61.2 (4)
U1—O3—O19ⁱⁱ	98.9 (8)	O13—O21—O18^xviii	91.9 (7)
U1—O3—O22	54.7 (6)	O13—O21—O21^xvii	121.1 (6)
U1—O3—O23	90.4 (8)	O13—O21—O22	51.4 (5)
U1—O3—O31^v	85.3 (7)	O13—O21—O24	57.1 (4)
U2—O3—U3	103.7 (11)	O13—O21—O30^iv	123.4 (5)
U2—O3—O5	112.2 (11)	O14ⁱⁱⁱ—O21—O17	52.6 (7)
U2—O3—O6	89.9 (9)	O14ⁱⁱⁱ—O21—O18^xviii	124.9 (8)
U2—O3—O8	141.5 (8)	O14ⁱⁱⁱ—O21—O21^xvii	117.2 (9)
U2—O3—O11	40.2 (4)	O14ⁱⁱⁱ—O21—O22	54.2 (6)
U2—O3—O12	123.0 (6)	O14ⁱⁱⁱ—O21—O24	127.6 (7)
U2—O3—O13ⁱⁱ	101.0 (5)	O14ⁱⁱⁱ—O21—O30^iv	53.8 (7)
U2—O3—O15	35.9 (6)	O17—O21—O18^xviii	92.0 (4)
U2—O3—O16	55.2 (6)	O17—O21—O21^xvii	168.4 (6)
U2—O3—O19ⁱⁱ	48.1 (4)	O17—O21—O22	48.1 (3)
U2—O3—O22	153.1 (12)	O17—O21—O24	116.2 (5)
U2—O3—O23	94.8 (6)	O17—O21—O30^iv	104.6 (5)
U2—O3—O31^v	88.2 (6)	O18^xviii—O21—O21^xvii	99.2 (4)
U3—O3—O5	37.6 (7)	O18^xviii—O21—O22	133.5 (6)
U3—O3—O6	36.4 (6)	O18^xviii—O21—O24	104.6 (9)
U3—O3—O8	98.2 (5)	O18^xviii—O21—O30^iv	144.7 (8)
U3—O3—O11	114.4 (10)	O21^xvii—O21—O22	123.0 (5)
U3—O3—O12	107.2 (7)	O21^xvii—O21—O24	64.1 (5)
U3—O3—O13ⁱⁱ	155.2 (9)	O21^xvii—O21—O30^iv	64.2 (5)
U3—O3—O15	90.6 (10)	O22—O21—O24	80.4 (5)
U3—O3—O16	52.6 (6)	O22—O21—O30^iv	77.7 (5)
U3—O3—O19ⁱⁱ	145.6 (10)	O24—O21—O30^iv	95.8 (7)
U3—O3—O22	53.6 (5)	U1—O22—U3	110.8 (4)
U3—O3—O23	97.4 (7)	U1—O22—U6	120.8 (7)
U3—O3—O31^v	85.2 (7)	U1—O22—K2	101.7 (5)
O5—O3—O6	73.9 (9)	U1—O22—O3	53.4 (7)
O5—O3—O8	69.3 (8)	U1—O22—O5	101.4 (8)
O5—O3—O11	96.6 (8)	U1—O22—O6	112.4 (6)
O5—O3—O12	121.6 (8)	U1—O22—O8	40.3 (5)
O5—O3—O13ⁱⁱ	128.4 (10)	U1—O22—O12	38.0 (4)
O5—O3—O15	119.5 (13)	U1—O22—O13	165.5 (6)
O5—O3—O16	59.3 (7)	U1—O22—O14ⁱⁱⁱ	66.1 (7)
O5—O3—O19ⁱⁱ	156.4 (9)	U1—O22—O17	97.5 (6)
O5—O3—O22	60.5 (6)	U1—O22—O21	123.7 (7)
O5—O3—O23	60.7 (8)	U1—O22—O30^iv	74.5 (6)
O5—O3—O31^v	121.2 (9)	U3—O22—U6	121.3 (7)
O6—O3—O8	125.0 (6)	U3—O22—K2	99.5 (5)
O6—O3—O11	122.1 (11)	U3—O22—O3	57.8 (7)
O6—O3—O12	88.0 (8)	U3—O22—O5	39.4 (6)
O6—O3—O13ⁱⁱ	146.2 (9)	U3—O22—O6	37.7 (6)
O6—O3—O15	62.2 (8)	U3—O22—O8	99.2 (5)
O6—O3—O16	62.0 (8)	U3—O22—O12	112.8 (5)
O6—O3—O19ⁱⁱ	113.9 (7)	U3—O22—O13	57.2 (5)
O6—O3—O22	63.3 (6)	U3—O22—O14ⁱⁱⁱ	173.2 (9)
O6—O3—O23	132.6 (10)	U3—O22—O17	108.6 (6)
O6—O3—O31^v	50.6 (8)	U3—O22—O21	123.4 (7)
O8—O3—O11	101.8 (7)	U3—O22—O30^iv	140.2 (6)
O8—O3—O12	78.4 (9)	U6—O22—K2	95.8 (4)
O8—O3—O13ⁱⁱ	60.2 (7)	U6—O22—O3	160.7 (7)
O8—O3—O15	171.0 (11)	U6—O22—O5	101.5 (7)
O8—O3—O16	123.4 (8)	U6—O22—O6	125.7 (8)
O8—O3—O19ⁱⁱ	116.2 (9)	U6—O22—O8	102.3 (5)
O8—O3—O22	63.3 (7)	U6—O22—O12	124.7 (6)
O8—O3—O23	50.9 (7)	U6—O22—O13	66.9 (4)
O8—O3—O31^v	125.2 (10)	U6—O22—O14ⁱⁱⁱ	58.8 (6)
O11—O3—O12	137.8 (9)	U6—O22—O17	42.2 (3)
O11—O3—O13ⁱⁱ	83.9 (6)	U6—O22—O21	37.7 (3)
O11—O3—O15	76.0 (7)	U6—O22—O30^iv	82.1 (5)
O11—O3—O16	64.4 (7)	K2—O22—O3	103.5 (5)
O11—O3—O19ⁱⁱ	60.1 (4)	K2—O22—O5	138.3 (9)
O11—O3—O22	155.4 (7)	K2—O22—O6	62.1 (6)
O11—O3—O23	55.7 (5)	K2—O22—O8	141.9 (8)
O11—O3—O31^v	126.6 (6)	K2—O22—O12	63.8 (5)
O12—O3—O13ⁱⁱ	59.2 (8)	K2—O22—O13	89.0 (6)
O12—O3—O15	97.3 (7)	K2—O22—O14ⁱⁱⁱ	87.1 (7)
O12—O3—O16	149.2 (9)	K2—O22—O17	137.4 (5)
O12—O3—O19ⁱⁱ	81.7 (7)	K2—O22—O21	58.0 (4)
O12—O3—O22	61.7 (7)	K2—O22—O30^iv	42.8 (5)
O12—O3—O23	126.3 (11)	O3—O22—O5	65.2 (7)
O12—O3—O31^v	49.2 (6)	O3—O22—O6	67.0 (8)
O13ⁱⁱ—O3—O15	110.7 (8)	O3—O22—O8	60.8 (6)
O13ⁱⁱ—O3—O16	148.3 (6)	O3—O22—O12	64.1 (6)
O13ⁱⁱ—O3—O19ⁱⁱ	57.5 (5)	O3—O22—O13	114.9 (8)
O13ⁱⁱ—O3—O22	102.9 (10)	O3—O22—O14ⁱⁱⁱ	119.5 (10)
O13ⁱⁱ—O3—O23	78.8 (8)	O3—O22—O17	118.5 (6)
O13ⁱⁱ—O3—O31^v	97.4 (8)	O3—O22—O21	161.3 (6)
O15—O3—O16	63.9 (9)	O3—O22—O30^iv	110.7 (7)
O15—O3—O19ⁱⁱ	55.0 (7)	O5—O22—O6	77.1 (9)
O15—O3—O22	121.7 (8)	O5—O22—O8	70.2 (8)
O15—O3—O23	130.0 (9)	O5—O22—O12	128.6 (7)
O15—O3—O31^v	53.5 (7)	O5—O22—O13	64.3 (8)
O16—O3—O19ⁱⁱ	103.3 (7)	O5—O22—O14ⁱⁱⁱ	134.2 (10)
O16—O3—O22	106.0 (8)	O5—O22—O17	72.1 (6)
O16—O3—O23	82.6 (8)	O5—O22—O21	129.3 (8)
O16—O3—O31^v	101.9 (9)	O5—O22—O30^iv	175.7 (8)
O19ⁱⁱ—O3—O22	143.1 (9)	O6—O22—O8	126.1 (6)
O19ⁱⁱ—O3—O23	103.7 (6)	O6—O22—O12	90.9 (7)
O19ⁱⁱ—O3—O31^v	75.8 (5)	O6—O22—O13	64.0 (7)
O22—O3—O23	101.9 (6)	O6—O22—O14ⁱⁱⁱ	148.7 (10)
O22—O3—O31^v	76.6 (5)	O6—O22—O17	140.6 (9)
O23—O3—O31^v	175.5 (12)	O6—O22—O21	102.4 (7)
U2ⁱ—O4—U4	75.3 (5)	O6—O22—O30^iv	102.9 (7)
U2ⁱ—O4—Sr1	76.5 (4)	O8—O22—O12	78.4 (7)
U2ⁱ—O4—Sr1'	76.5 (4)	O8—O22—O13	129.0 (7)
U2ⁱ—O4—K1^vii	133.3 (4)	O8—O22—O14ⁱⁱⁱ	74.5 (8)
U2ⁱ—O4—O1^viii	109.5 (7)	O8—O22—O17	64.2 (5)
U2ⁱ—O4—O2^vii	162.3 (5)	O8—O22—O21	131.4 (6)
U2ⁱ—O4—O6ⁱ	65.6 (6)	O8—O22—O30^iv	106.8 (8)
U2ⁱ—O4—O7	75.7 (4)	O12—O22—O13	150.1 (7)
U2ⁱ—O4—O9^ix	122.5 (5)	O12—O22—O14ⁱⁱⁱ	68.9 (7)
U2ⁱ—O4—O11^ix	123.8 (4)	O12—O22—O17	127.6 (8)
U2ⁱ—O4—O15ⁱ	26.7 (5)	O12—O22—O21	102.1 (6)
U2ⁱ—O4—O16ⁱ	36.4 (3)	O12—O22—O30^iv	47.2 (5)
U2ⁱ—O4—O19ⁱ	82.8 (4)	O13—O22—O14ⁱⁱⁱ	124.9 (7)
U2ⁱ—O4—O20ⁱ	42.6 (6)	O13—O22—O17	80.6 (6)
U2ⁱ—O4—O26	81.3 (7)	O13—O22—O21	70.2 (5)
U2ⁱ—O4—O29	129.9 (9)	O13—O22—O30^iv	119.7 (6)
U4—O4—Sr1	145.9 (8)	O14ⁱⁱⁱ—O22—O17	66.6 (7)
U4—O4—Sr1'	145.9 (8)	O14ⁱⁱⁱ—O22—O21	61.4 (7)
U4—O4—K1^vii	128.5 (7)	O14ⁱⁱⁱ—O22—O30^iv	45.9 (7)
U4—O4—O1^viii	50.9 (6)	O17—O22—O21	79.7 (4)
U4—O4—O2^vii	92.3 (7)	O17—O22—O30^iv	109.6 (6)
U4—O4—O6ⁱ	100.3 (7)	O21—O22—O30^iv	55.0 (5)
U4—O4—O7	2.7 (2)	Sr2—O23—Sr2'	0
U4—O4—O9^ix	51.8 (5)	Sr2—O23—K3	97.3 (10)
U4—O4—O11^ix	92.3 (5)	Sr2—O23—O3	91.7 (4)
U4—O4—O15ⁱ	102.0 (9)	Sr2—O23—O3ⁱ	91.7 (4)
U4—O4—O16ⁱ	50.0 (5)	Sr2—O23—O5	53.3 (6)
U4—O4—O19ⁱ	52.5 (4)	Sr2—O23—O5ⁱ	53.3 (6)
U4—O4—O20ⁱ	53.0 (7)	Sr2—O23—O8	59.7 (5)
U4—O4—O26	141.7 (7)	Sr2—O23—O8ⁱ	59.7 (5)
U4—O4—O29	138.8 (9)	Sr2—O23—O11	139.8 (8)
Sr1—O4—Sr1'	0	Sr2—O23—O11ⁱ	139.8 (8)
Sr1—O4—K1^vii	85.2 (4)	Sr2—O23—O24^x	117.7 (11)
Sr1—O4—O1^viii	160.9 (6)	Sr2'—O23—K3	97.3 (10)
Sr1—O4—O2^vii	119.0 (5)	Sr2'—O23—O3	91.7 (4)
Sr1—O4—O6ⁱ	49.9 (6)	Sr2'—O23—O3ⁱ	91.7 (4)
Sr1—O4—O7	144.6 (6)	Sr2'—O23—O5	53.3 (6)
Sr1—O4—O9^ix	137.4 (5)	Sr2'—O23—O5ⁱ	53.3 (6)
Sr1—O4—O11^ix	87.6 (4)	Sr2'—O23—O8	59.7 (5)
Sr1—O4—O15ⁱ	52.0 (6)	Sr2'—O23—O8ⁱ	59.7 (5)
Sr1—O4—O16ⁱ	96.0 (6)	Sr2'—O23—O11	139.8 (8)
Sr1—O4—O19ⁱ	105.1 (4)	Sr2'—O23—O11ⁱ	139.8 (8)
Sr1—O4—O20ⁱ	113.1 (8)	Sr2'—O23—O24^x	117.7 (11)
Sr1—O4—O26	49.3 (5)	K3—O23—O3	82.9 (7)
Sr1—O4—O29	55.9 (8)	K3—O23—O3ⁱ	82.9 (7)
Sr1'—O4—K1^vii	85.2 (4)	K3—O23—O5	61.4 (8)
Sr1'—O4—O1^viii	160.9 (6)	K3—O23—O5ⁱ	61.4 (8)
Sr1'—O4—O2^vii	119.0 (5)	K3—O23—O8	124.1 (9)
Sr1'—O4—O6ⁱ	49.9 (6)	K3—O23—O8ⁱ	124.1 (9)
Sr1'—O4—O7	144.6 (6)	K3—O23—O11	65.2 (6)
Sr1'—O4—O9^ix	137.4 (5)	K3—O23—O11ⁱ	65.2 (6)
Sr1'—O4—O11^ix	87.6 (4)	K3—O23—O24^x	145.1 (8)
Sr1'—O4—O15ⁱ	52.0 (6)	O3—O23—O3ⁱ	165.8 (12)
Sr1'—O4—O16ⁱ	96.0 (6)	O3—O23—O5	51.7 (6)
Sr1'—O4—O19ⁱ	105.1 (4)	O3—O23—O5ⁱ	121.3 (11)
Sr1'—O4—O20ⁱ	113.1 (8)	O3—O23—O8	51.5 (6)
Sr1'—O4—O26	49.3 (5)	O3—O23—O8ⁱ	140.6 (9)
Sr1'—O4—O29	55.9 (8)	O3—O23—O11	52.1 (4)
K1^vii—O4—O1^viii	77.7 (6)	O3—O23—O11ⁱ	119.5 (7)
K1^vii—O4—O2^vii	47.1 (4)	O3—O23—O24^x	95.3 (7)
K1^vii—O4—O6ⁱ	129.2 (7)	O3ⁱ—O23—O5	121.3 (11)
K1^vii—O4—O7	130.1 (6)	O3ⁱ—O23—O5ⁱ	51.7 (6)
K1^vii—O4—O9^ix	100.0 (6)	O3ⁱ—O23—O8	140.6 (9)
K1^vii—O4—O11^ix	97.5 (5)	O3ⁱ—O23—O8ⁱ	51.5 (6)
K1^vii—O4—O15ⁱ	113.3 (7)	O3ⁱ—O23—O11	119.5 (7)
K1^vii—O4—O16ⁱ	167.6 (5)	O3ⁱ—O23—O11ⁱ	52.1 (4)
K1^vii—O4—O19ⁱ	143.8 (6)	O3ⁱ—O23—O24^x	95.3 (7)
K1^vii—O4—O20ⁱ	114.2 (6)	O5—O23—O5ⁱ	70.1 (10)
K1^vii—O4—O26	55.0 (7)	O5—O23—O8	64.8 (7)
K1^vii—O4—O29	62.4 (6)	O5—O23—O8ⁱ	112.5 (9)
O1^viii—O4—O2^vii	53.0 (7)	O5—O23—O11	87.4 (7)
O1^viii—O4—O6ⁱ	149.1 (8)	O5—O23—O11ⁱ	126.5 (12)
O1^viii—O4—O7	52.7 (6)	O5—O23—O24^x	140.6 (8)
O1^viii—O4—O9^ix	55.4 (6)	O5ⁱ—O23—O8	112.5 (9)
O1^viii—O4—O11^ix	102.7 (7)	O5ⁱ—O23—O8ⁱ	64.8 (7)
O1^viii—O4—O15ⁱ	128.5 (9)	O5ⁱ—O23—O11	126.5 (12)
O1^viii—O4—O16ⁱ	99.0 (7)	O5ⁱ—O23—O11ⁱ	87.4 (7)
O1^viii—O4—O19ⁱ	93.7 (6)	O5ⁱ—O23—O24^x	140.6 (8)
O1^viii—O4—O20ⁱ	67.8 (9)	O8—O23—O8ⁱ	89.3 (10)
O1^viii—O4—O26	112.7 (7)	O8—O23—O11	99.0 (5)
O1^viii—O4—O29	120.5 (11)	O8—O23—O11ⁱ	160.1 (11)
O2^vii—O4—O6ⁱ	130.2 (7)	O8—O23—O24^x	77.9 (9)
O2^vii—O4—O7	92.5 (5)	O8ⁱ—O23—O11	160.1 (11)
O2^vii—O4—O9^ix	52.9 (4)	O8ⁱ—O23—O11ⁱ	99.0 (5)
O2^vii—O4—O11^ix	68.4 (5)	O8ⁱ—O23—O24^x	77.9 (9)
O2^vii—O4—O15ⁱ	160.3 (6)	O11—O23—O11ⁱ	67.8 (6)
O2^vii—O4—O16ⁱ	139.2 (6)	O11—O23—O24^x	86.2 (8)
O2^vii—O4—O19ⁱ	99.8 (5)	O11ⁱ—O23—O24^x	86.2 (8)
O2^vii—O4—O20ⁱ	119.7 (8)	K2—O24—O6	67.8 (9)
O2^vii—O4—O26	102.1 (7)	K2—O24—O6^xvii	67.8 (9)
O2^vii—O4—O29	67.6 (8)	K2—O24—O8^xviii	131.5 (8)
O6ⁱ—O4—O7	98.1 (6)	K2—O24—O8ⁱⁱⁱ	131.5 (8)
O6ⁱ—O4—O9^ix	99.9 (7)	K2—O24—O11^xviii	129.8 (6)
O6ⁱ—O4—O11^ix	63.2 (6)	K2—O24—O11ⁱⁱⁱ	129.8 (6)
O6ⁱ—O4—O15ⁱ	60.8 (7)	K2—O24—O13	91.2 (7)
O6ⁱ—O4—O16ⁱ	58.1 (6)	K2—O24—O13^xvii	91.2 (7)
O6ⁱ—O4—O19ⁱ	55.9 (6)	K2—O24—O21	58.7 (7)
O6ⁱ—O4—O20ⁱ	105.9 (9)	K2—O24—O21^xvii	58.7 (7)
O6ⁱ—O4—O26	97.1 (8)	K2—O24—O23^xviii	178.1 (10)
O6ⁱ—O4—O29	71.7 (8)	O6—O24—O6^xvii	70.4 (8)
O7—O4—O9^ix	50.4 (5)	O6—O24—O8^xviii	159.4 (13)
O7—O4—O11^ix	89.9 (4)	O6—O24—O8ⁱⁱⁱ	107.6 (7)
O7—O4—O15ⁱ	102.4 (7)	O6—O24—O11^xviii	91.0 (8)
O7—O4—O16ⁱ	49.0 (4)	O6—O24—O11ⁱⁱⁱ	62.2 (8)
O7—O4—O19ⁱ	49.8 (3)	O6—O24—O13	59.3 (5)
O7—O4—O20ⁱ	55.1 (6)	O6—O24—O13^xvii	129.7 (8)
O7—O4—O26	144.1 (6)	O6—O24—O21	94.8 (8)
O7—O4—O29	136.6 (7)	O6—O24—O21^xvii	126.0 (13)
O9^ix—O4—O11^ix	49.8 (4)	O6—O24—O23^xviii	110.7 (11)
O9^ix—O4—O15ⁱ	146.6 (8)	O6^xvii—O24—O8^xviii	107.6 (7)
O9^ix—O4—O16ⁱ	87.4 (6)	O6^xvii—O24—O8ⁱⁱⁱ	159.4 (13)
O9^ix—O4—O19ⁱ	49.2 (4)	O6^xvii—O24—O11^xviii	62.2 (8)
O9^ix—O4—O20ⁱ	103.2 (8)	O6^xvii—O24—O11ⁱⁱⁱ	91.0 (8)
O9^ix—O4—O26	155.1 (9)	O6^xvii—O24—O13	129.7 (8)
O9^ix—O4—O29	89.0 (8)	O6^xvii—O24—O13^xvii	59.3 (5)
O11^ix—O4—O15ⁱ	123.7 (6)	O6^xvii—O24—O21	126.0 (13)
O11^ix—O4—O16ⁱ	94.9 (4)	O6^xvii—O24—O21^xvii	94.8 (8)
O11^ix—O4—O19ⁱ	49.7 (4)	O6^xvii—O24—O23^xviii	110.7 (11)
O11^ix—O4—O20ⁱ	142.8 (7)	O8^xviii—O24—O8ⁱⁱⁱ	66.7 (7)
O11^ix—O4—O26	126.0 (6)	O8^xviii—O24—O11^xviii	71.0 (6)
O11^ix—O4—O29	47.4 (5)	O8^xviii—O24—O11ⁱⁱⁱ	97.7 (9)
O15ⁱ—O4—O16ⁱ	59.3 (7)	O8^xviii—O24—O13	119.6 (8)
O15ⁱ—O4—O19ⁱ	99.7 (6)	O8^xviii—O24—O13^xvii	53.1 (5)
O15ⁱ—O4—O20ⁱ	61.8 (8)	O8^xviii—O24—O21	102.1 (6)
O15ⁱ—O4—O26	58.4 (8)	O8^xviii—O24—O21^xvii	74.3 (5)
O15ⁱ—O4—O29	107.8 (10)	O8^xviii—O24—O23^xviii	49.9 (6)
O16ⁱ—O4—O19ⁱ	47.7 (4)	O8ⁱⁱⁱ—O24—O11^xviii	97.7 (9)
O16ⁱ—O4—O20ⁱ	54.0 (6)	O8ⁱⁱⁱ—O24—O11ⁱⁱⁱ	71.0 (6)
O16ⁱ—O4—O26	117.2 (8)	O8ⁱⁱⁱ—O24—O13	53.1 (5)
O16ⁱ—O4—O29	128.1 (7)	O8ⁱⁱⁱ—O24—O13^xvii	119.6 (8)
O19ⁱ—O4—O20ⁱ	93.9 (6)	O8ⁱⁱⁱ—O24—O21	74.3 (5)
O19ⁱ—O4—O26	152.6 (8)	O8ⁱⁱⁱ—O24—O21^xvii	102.1 (6)
O19ⁱ—O4—O29	94.3 (5)	O8ⁱⁱⁱ—O24—O23^xviii	49.9 (6)
O20ⁱ—O4—O26	89.5 (7)	O11^xviii—O24—O11ⁱⁱⁱ	49.6 (5)
O20ⁱ—O4—O29	167.8 (10)	O11^xviii—O24—O13	117.0 (9)
O26—O4—O29	79.1 (7)	O11^xviii—O24—O13^xvii	67.6 (5)
U1—O5—U3	69.9 (10)	O11^xviii—O24—O21	171.3 (9)
U1—O5—U6	59.5 (4)	O11^xviii—O24—O21^xvii	128.5 (4)
U1—O5—Sr2	79.0 (8)	O11^xviii—O24—O23^xviii	48.6 (6)
U1—O5—Sr2'	79.0 (8)	O11ⁱⁱⁱ—O24—O13	67.6 (5)
U1—O5—K3	117.8 (7)	O11ⁱⁱⁱ—O24—O13^xvii	117.0 (9)
U1—O5—O3	33.8 (6)	O11ⁱⁱⁱ—O24—O21	128.5 (4)
U1—O5—O5ⁱ	117.8 (10)	O11ⁱⁱⁱ—O24—O21^xvii	171.3 (9)
U1—O5—O6	71.5 (8)	O11ⁱⁱⁱ—O24—O23^xviii	48.6 (6)
U1—O5—O8	27.5 (6)	O13—O24—O13^xvii	170.8 (8)
U1—O5—O12ⁱⁱⁱ	126.7 (7)	O13—O24—O21	61.2 (5)
U1—O5—O13	90.8 (8)	O13—O24—O21^xvii	112.9 (8)
U1—O5—O16	89.6 (8)	O13—O24—O23^xviii	88.9 (7)
U1—O5—O17	62.9 (6)	O13^xvii—O24—O21	112.9 (8)
U1—O5—O19	127.6 (9)	O13^xvii—O24—O21^xvii	61.2 (5)
U1—O5—O22	34.1 (5)	O13^xvii—O24—O23^xviii	88.9 (7)
U1—O5—O23	69.1 (8)	O21—O24—O21^xvii	51.8 (6)
U1—O5—O25	164.7 (8)	O21—O24—O23^xviii	123.0 (8)
U1—O5—O32	111.1 (10)	O21^xvii—O24—O23^xviii	123.0 (8)
U3—O5—U6	76.8 (8)	K3—O25—O5	65.4 (8)
U3—O5—Sr2	148.0 (17)	K3—O25—O5ⁱ	65.4 (8)
U3—O5—Sr2'	148.0 (17)	K3—O25—O7	51.8 (5)
U3—O5—K3	105.5 (9)	K3—O25—O7ⁱ	51.8 (5)
U3—O5—O3	54.3 (9)	K3—O25—O15^ix	128.5 (7)
U3—O5—O5ⁱ	162.1 (11)	K3—O25—O15ⁱⁱⁱ	128.5 (7)
U3—O5—O6	1.7 (8)	K3—O25—O19	85.3 (6)
U3—O5—O8	97.4 (14)	K3—O25—O19ⁱ	85.3 (6)
U3—O5—O12ⁱⁱⁱ	100.4 (11)	K3—O25—O31	167.2 (13)
U3—O5—O13	55.3 (8)	O5—O25—O5ⁱ	65.4 (9)
U3—O5—O16	54.0 (6)	O5—O25—O7	117.2 (10)
U3—O5—O17	104.3 (11)	O5—O25—O7ⁱ	86.0 (7)
U3—O5—O19	57.9 (9)	O5—O25—O15^ix	161.0 (8)
U3—O5—O22	53.6 (8)	O5—O25—O15ⁱⁱⁱ	106.3 (8)
U3—O5—O23	120.5 (12)	O5—O25—O19	52.6 (7)
U3—O5—O25	110.7 (14)	O5—O25—O19ⁱ	117.9 (11)
U3—O5—O32	140.1 (11)	O5—O25—O31	104.1 (8)
U6—O5—Sr2	81.4 (6)	O5ⁱ—O25—O7	86.0 (7)
U6—O5—Sr2'	81.4 (6)	O5ⁱ—O25—O7ⁱ	117.2 (10)
U6—O5—K3	175.8 (11)	O5ⁱ—O25—O15^ix	106.3 (8)
U6—O5—O3	87.3 (8)	O5ⁱ—O25—O15ⁱⁱⁱ	161.0 (8)
U6—O5—O5ⁱ	121.1 (7)	O5ⁱ—O25—O19	117.9 (11)
U6—O5—O6	77.1 (6)	O5ⁱ—O25—O19ⁱ	52.6 (7)
U6—O5—O8	66.3 (6)	O5ⁱ—O25—O31	104.1 (8)
U6—O5—O12ⁱⁱⁱ	67.2 (4)	O7—O25—O7ⁱ	58.4 (5)
U6—O5—O13	44.9 (4)	O7—O25—O15^ix	77.7 (7)
U6—O5—O16	129.3 (10)	O7—O25—O15ⁱⁱⁱ	112.7 (10)
U6—O5—O17	28.7 (3)	O7—O25—O19	117.7 (7)
U6—O5—O19	109.4 (8)	O7—O25—O19ⁱ	59.6 (4)
U6—O5—O22	33.9 (3)	O7—O25—O31	137.7 (10)
U6—O5—O23	114.5 (10)	O7ⁱ—O25—O15^ix	112.7 (10)
U6—O5—O25	135.8 (9)	O7ⁱ—O25—O15ⁱⁱⁱ	77.7 (7)
U6—O5—O32	71.1 (5)	O7ⁱ—O25—O19	59.6 (4)
Sr2—O5—Sr2'	0	O7ⁱ—O25—O19ⁱ	117.7 (7)
Sr2—O5—K3	95.1 (8)	O7ⁱ—O25—O31	137.7 (10)
Sr2—O5—O3	102.0 (12)	O15^ix—O25—O15ⁱⁱⁱ	75.9 (11)
Sr2—O5—O5ⁱ	45.8 (7)	O15^ix—O25—O19	133.4 (12)
Sr2—O5—O6	149.5 (13)	O15^ix—O25—O19ⁱ	57.5 (7)
Sr2—O5—O8	52.0 (8)	O15^ix—O25—O31	60.0 (8)
Sr2—O5—O12ⁱⁱⁱ	92.2 (6)	O15ⁱⁱⁱ—O25—O19	57.5 (7)
Sr2—O5—O13	119.8 (8)	O15ⁱⁱⁱ—O25—O19ⁱ	133.4 (12)
Sr2—O5—O16	134.8 (11)	O15ⁱⁱⁱ—O25—O31	60.0 (8)
Sr2—O5—O17	52.8 (5)	O19—O25—O19ⁱ	169.0 (14)
Sr2—O5—O19	153.4 (13)	O19—O25—O31	94.0 (5)
Sr2—O5—O22	96.0 (10)	O19ⁱ—O25—O31	94.0 (5)
Sr2—O5—O23	50.2 (6)	Sr1—O26—Sr1'	0
Sr2—O5—O25	101.2 (9)	Sr1—O26—K1^vii	100.0 (10)
Sr2—O5—O32	47.3 (7)	Sr1—O26—O4	61.7 (5)
Sr2'—O5—K3	95.1 (8)	Sr1—O26—O4^xii	61.7 (5)
Sr2'—O5—O3	102.0 (12)	Sr1—O26—O15^xiii	56.7 (6)
Sr2'—O5—O5ⁱ	45.8 (7)	Sr1—O26—O15ⁱ	56.7 (6)
Sr2'—O5—O6	149.5 (13)	Sr1—O26—O18^viii	131.2 (8)
Sr2'—O5—O8	52.0 (8)	Sr1—O26—O18^xxviii	131.2 (8)
Sr2'—O5—O12ⁱⁱⁱ	92.2 (6)	Sr1—O26—O27^viii	164.1 (16)
Sr2'—O5—O13	119.8 (8)	Sr1—O26—O29	45.5 (7)
Sr2'—O5—O16	134.8 (11)	Sr1'—O26—K1^vii	100.0 (10)
Sr2'—O5—O17	52.8 (5)	Sr1'—O26—O4	61.7 (5)
Sr2'—O5—O19	153.4 (13)	Sr1'—O26—O4^xii	61.7 (5)
Sr2'—O5—O22	96.0 (10)	Sr1'—O26—O15^xiii	56.7 (6)
Sr2'—O5—O23	50.2 (6)	Sr1'—O26—O15ⁱ	56.7 (6)
Sr2'—O5—O25	101.2 (9)	Sr1'—O26—O18^viii	131.2 (8)
Sr2'—O5—O32	47.3 (7)	Sr1'—O26—O18^xxviii	131.2 (8)
K3—O5—O3	91.3 (7)	Sr1'—O26—O27^viii	164.1 (16)
K3—O5—O5ⁱ	56.6 (5)	Sr1'—O26—O29	45.5 (7)
K3—O5—O6	105.4 (7)	K1^vii—O26—O4	65.1 (7)
K3—O5—O8	109.8 (9)	K1^vii—O26—O4^xii	65.1 (7)
K3—O5—O12ⁱⁱⁱ	115.3 (9)	K1^vii—O26—O15^xiii	127.7 (9)
K3—O5—O13	139.3 (12)	K1^vii—O26—O15ⁱ	127.7 (9)
K3—O5—O16	52.3 (5)	K1^vii—O26—O18^viii	99.5 (11)
K3—O5—O17	147.9 (10)	K1^vii—O26—O18^xxviii	99.5 (11)
K3—O5—O19	74.8 (7)	K1^vii—O26—O27^viii	64.1 (9)
K3—O5—O22	145.4 (9)	K1^vii—O26—O29	54.6 (7)
K3—O5—O23	61.4 (7)	O4—O26—O4^xii	91.7 (8)
K3—O5—O25	46.9 (6)	O4—O26—O15^xiii	118.3 (8)
K3—O5—O32	108.1 (9)	O4—O26—O15ⁱ	62.6 (7)
O3—O5—O5ⁱ	122.1 (10)	O4—O26—O18^viii	163.1 (15)
O3—O5—O6	56.0 (8)	O4—O26—O18^xxviii	87.5 (5)
O3—O5—O8	53.0 (9)	O4—O26—O27^viii	108.4 (9)
O3—O5—O12ⁱⁱⁱ	148.7 (9)	O4—O26—O29	45.9 (4)
O3—O5—O13	100.4 (9)	O4^xii—O26—O15^xiii	62.6 (7)
O3—O5—O16	55.9 (8)	O4^xii—O26—O15ⁱ	118.3 (8)
O3—O5—O17	96.6 (11)	O4^xii—O26—O18^viii	87.5 (5)
O3—O5—O19	102.8 (10)	O4^xii—O26—O18^xxviii	163.1 (15)
O3—O5—O22	54.3 (7)	O4^xii—O26—O27^viii	108.4 (9)
O3—O5—O23	67.6 (8)	O4^xii—O26—O29	45.9 (4)
O3—O5—O25	133.6 (9)	O15^xiii—O26—O15ⁱ	81.3 (11)
O3—O5—O32	143.7 (14)	O15^xiii—O26—O18^viii	76.0 (9)
O5ⁱ—O5—O6	161.7 (9)	O15^xiii—O26—O18^xxviii	131.8 (16)
O5ⁱ—O5—O8	91.0 (10)	O15^xiii—O26—O27^viii	132.2 (7)
O5ⁱ—O5—O12ⁱⁱⁱ	87.7 (7)	O15^xiii—O26—O29	89.3 (8)
O5ⁱ—O5—O13	136.2 (10)	O15ⁱ—O26—O18^viii	131.8 (16)
O5ⁱ—O5—O16	108.5 (8)	O15ⁱ—O26—O18^xxviii	76.0 (9)
O5ⁱ—O5—O17	93.5 (8)	O15ⁱ—O26—O27^viii	132.2 (7)
O5ⁱ—O5—O19	111.0 (11)	O15ⁱ—O26—O29	89.3 (8)
O5ⁱ—O5—O22	141.8 (12)	O18^viii—O26—O18^xxviii	88.4 (7)
O5ⁱ—O5—O23	54.9 (7)	O18^viii—O26—O27^viii	56.3 (9)
O5ⁱ—O5—O25	57.3 (7)	O18^viii—O26—O29	131.6 (8)
O5ⁱ—O5—O32	55.0 (6)	O18^xxviii—O26—O27^viii	56.3 (9)
O6—O5—O8	99.0 (11)	O18^xxviii—O26—O29	131.6 (8)
O6—O5—O12ⁱⁱⁱ	99.0 (8)	O27^viii—O26—O29	118.6 (13)
O6—O5—O13	54.4 (6)	Sr2—O27—Sr2'	0
O6—O5—O16	54.1 (6)	Sr2—O27—K1^xviii	91.2 (10)
O6—O5—O17	104.8 (9)	Sr2—O27—K4^v	139.9 (8)
O6—O5—O19	56.4 (8)	Sr2—O27—O8	56.5 (6)
O6—O5—O22	54.7 (7)	Sr2—O27—O8ⁱ	56.5 (6)
O6—O5—O23	122.0 (9)	Sr2—O27—O17	58.4 (7)
O6—O5—O25	109.3 (10)	Sr2—O27—O17ⁱ	58.4 (7)
O6—O5—O32	139.2 (9)	Sr2—O27—O18	131.9 (8)
O8—O5—O12ⁱⁱⁱ	124.3 (7)	Sr2—O27—O18ⁱ	131.9 (8)
O8—O5—O13	108.3 (10)	Sr2—O27—O26^xxi	147.5 (13)
O8—O5—O16	105.1 (10)	Sr2'—O27—K1^xviii	91.2 (10)
O8—O5—O17	54.4 (6)	Sr2'—O27—K4^v	139.9 (8)
O8—O5—O19	154.5 (11)	Sr2'—O27—O8	56.5 (6)
O8—O5—O22	55.2 (8)	Sr2'—O27—O8ⁱ	56.5 (6)
O8—O5—O23	49.9 (8)	Sr2'—O27—O17	58.4 (7)
O8—O5—O25	146.9 (11)	Sr2'—O27—O17ⁱ	58.4 (7)
O8—O5—O32	91.1 (10)	Sr2'—O27—O18	131.9 (8)
O12ⁱⁱⁱ—O5—O13	48.8 (5)	Sr2'—O27—O18ⁱ	131.9 (8)
O12ⁱⁱⁱ—O5—O16	127.8 (12)	Sr2'—O27—O26^xxi	147.5 (13)
O12ⁱⁱⁱ—O5—O17	70.1 (5)	K1^xviii—O27—K4^v	128.9 (8)
O12ⁱⁱⁱ—O5—O19	71.1 (7)	K1^xviii—O27—O8	122.4 (9)
O12ⁱⁱⁱ—O5—O22	96.9 (7)	K1^xviii—O27—O8ⁱ	122.4 (9)
O12ⁱⁱⁱ—O5—O23	138.7 (9)	K1^xviii—O27—O17	61.7 (6)
O12ⁱⁱⁱ—O5—O25	68.5 (7)	K1^xviii—O27—O17ⁱ	61.7 (6)
O12ⁱⁱⁱ—O5—O32	45.3 (6)	K1^xviii—O27—O18	97.2 (7)
O13—O5—O16	103.8 (10)	K1^xviii—O27—O18ⁱ	97.2 (7)
O13—O5—O17	69.6 (6)	K1^xviii—O27—O26^xxi	56.3 (8)
O13—O5—O19	64.7 (8)	K4^v—O27—O8	94.8 (8)
O13—O5—O22	56.6 (7)	K4^v—O27—O8ⁱ	94.8 (8)
O13—O5—O23	158.2 (13)	K4^v—O27—O17	135.5 (6)
O13—O5—O25	102.1 (11)	K4^v—O27—O17ⁱ	135.5 (6)
O13—O5—O32	84.9 (7)	K4^v—O27—O18	53.2 (9)
O16—O5—O17	151.0 (12)	K4^v—O27—O18ⁱ	53.2 (9)
O16—O5—O19	56.7 (7)	K4^v—O27—O26^xxi	72.6 (9)
O16—O5—O22	98.4 (9)	O8—O27—O8ⁱ	81.0 (8)
O16—O5—O23	84.8 (8)	O8—O27—O17	60.7 (6)
O16—O5—O25	79.4 (8)	O8—O27—O17ⁱ	114.9 (11)
O16—O5—O32	157.7 (13)	O8—O27—O18	140.4 (12)
O17—O5—O19	132.6 (9)	O8—O27—O18ⁱ	79.6 (8)
O17—O5—O22	53.8 (6)	O8—O27—O26^xxi	138.3 (6)
O17—O5—O23	93.1 (10)	O8ⁱ—O27—O17	114.9 (11)
O17—O5—O25	129.3 (9)	O8ⁱ—O27—O17ⁱ	60.7 (6)
O17—O5—O32	51.3 (6)	O8ⁱ—O27—O18	79.6 (8)
O19—O5—O22	106.3 (10)	O8ⁱ—O27—O18ⁱ	140.4 (12)
O19—O5—O23	134.2 (9)	O8ⁱ—O27—O26^xxi	138.3 (6)
O19—O5—O25	53.8 (7)	O17—O27—O17ⁱ	88.9 (10)
O19—O5—O32	111.7 (12)	O17—O27—O18	158.3 (9)
O22—O5—O23	102.7 (12)	O17—O27—O18ⁱ	84.5 (8)
O22—O5—O25	157.7 (12)	O17—O27—O26^xxi	100.4 (7)
O22—O5—O32	103.5 (8)	O17ⁱ—O27—O18	84.5 (8)
O23—O5—O25	99.1 (9)	O17ⁱ—O27—O18ⁱ	158.3 (9)
O23—O5—O32	94.5 (9)	O17ⁱ—O27—O26^xxi	100.4 (7)
O25—O5—O32	78.6 (9)	O18—O27—O18ⁱ	94.1 (14)
U2—O6—U3	69.3 (8)	O18—O27—O26^xxi	60.8 (8)
U2—O6—U4ⁱ	59.4 (3)	O18ⁱ—O27—O26^xxi	60.8 (8)
U2—O6—Sr1^iv	79.8 (6)	K3^xi—O28—K4	84.5 (8)
U2—O6—Sr1'^iv	79.8 (6)	K3^xi—O28—O2	139.9 (10)
U2—O6—K2	114.8 (10)	K3^xi—O28—O2^xii	139.9 (10)
U2—O6—O3	36.5 (5)	K3^xi—O28—O7^xi	50.6 (5)
U2—O6—O4ⁱ	66.1 (5)	K3^xi—O28—O7^xix	50.6 (5)
U2—O6—O5	70.4 (6)	K3^xi—O28—O11^xi	64.1 (6)
U2—O6—O6^xvii	119.4 (8)	K3^xi—O28—O11^xix	64.1 (6)
U2—O6—O11ⁱⁱⁱ	127.3 (8)	K3^xi—O28—O16^xi	44.3 (3)
U2—O6—O13	120.9 (9)	K3^xi—O28—O16^xix	44.3 (3)
U2—O6—O15	27.1 (6)	K3^xi—O28—O20^xi	87.7 (6)
U2—O6—O16	36.6 (4)	K3^xi—O28—O20^xix	87.7 (6)
U2—O6—O19	87.7 (6)	K3^xi—O28—O29^xv	96.3 (9)
U2—O6—O22	86.2 (8)	K3^xi—O28—O30	158.5 (14)
U2—O6—O24	162.0 (13)	K4—O28—O2	117.6 (11)
U2—O6—O29^iv	108.5 (6)	K4—O28—O2^xii	117.6 (11)
U2—O6—O31^v	76.1 (7)	K4—O28—O7^xi	48.0 (6)
U3—O6—U4ⁱ	76.1 (8)	K4—O28—O7^xix	48.0 (6)
U3—O6—Sr1^iv	148.4 (12)	K4—O28—O11^xi	136.7 (6)
U3—O6—Sr1'^iv	148.4 (12)	K4—O28—O11^xix	136.7 (6)
U3—O6—K2	105.9 (11)	K4—O28—O16^xi	91.3 (6)
U3—O6—O3	48.6 (8)	K4—O28—O16^xix	91.3 (6)
U3—O6—O4ⁱ	101.6 (11)	K4—O28—O20^xi	90.7 (10)
U3—O6—O5	1.6 (7)	K4—O28—O20^xix	90.7 (10)
U3—O6—O6^xvii	161.2 (12)	K4—O28—O29^xv	179.1 (7)
U3—O6—O11ⁱⁱⁱ	99.1 (12)	K4—O28—O30	73.9 (8)
U3—O6—O13	51.7 (6)	O2—O28—O2^xii	61.4 (5)
U3—O6—O15	96.5 (11)	O2—O28—O7^xi	165.1 (14)
U3—O6—O16	47.8 (6)	O2—O28—O7^xix	119.0 (5)
U3—O6—O19	50.3 (8)	O2—O28—O11^xi	78.3 (10)
U3—O6—O22	47.3 (7)	O2—O28—O11^xix	105.5 (12)
U3—O6—O24	111.4 (9)	O2—O28—O16^xi	99.1 (5)
U3—O6—O29^iv	136.8 (15)	O2—O28—O16^xix	149.9 (12)
U3—O6—O31^v	119.5 (15)	O2—O28—O20^xi	60.9 (6)
U4ⁱ—O6—Sr1^iv	82.7 (6)	O2—O28—O20^xix	122.3 (9)
U4ⁱ—O6—Sr1'^iv	82.7 (6)	O2—O28—O29^xv	61.7 (10)
U4ⁱ—O6—K2	173.0 (9)	O2—O28—O30	55.4 (9)
U4ⁱ—O6—O3	86.5 (7)	O2^xii—O28—O7^xi	119.0 (5)
U4ⁱ—O6—O4ⁱ	25.7 (3)	O2^xii—O28—O7^xix	165.1 (14)
U4ⁱ—O6—O5	75.5 (7)	O2^xii—O28—O11^xi	105.5 (12)
U4ⁱ—O6—O6^xvii	122.6 (8)	O2^xii—O28—O11^xix	78.3 (10)
U4ⁱ—O6—O11ⁱⁱⁱ	67.9 (6)	O2^xii—O28—O16^xi	149.9 (12)
U4ⁱ—O6—O13	104.9 (9)	O2^xii—O28—O16^xix	99.1 (5)
U4ⁱ—O6—O15	65.4 (7)	O2^xii—O28—O20^xi	122.3 (9)
U4ⁱ—O6—O16	36.6 (4)	O2^xii—O28—O20^xix	60.9 (6)
U4ⁱ—O6—O19	45.5 (4)	O2^xii—O28—O29^xv	61.7 (10)
U4ⁱ—O6—O22	122.1 (9)	O2^xii—O28—O30	55.4 (9)
U4ⁱ—O6—O24	138.6 (12)	O7^xi—O28—O7^xix	56.4 (6)
U4ⁱ—O6—O29^iv	67.6 (6)	O7^xi—O28—O11^xi	114.4 (7)
U4ⁱ—O6—O31^v	124.1 (7)	O7^xi—O28—O11^xix	88.8 (5)
Sr1^iv—O6—Sr1'^iv	0	O7^xi—O28—O16^xi	86.0 (6)
Sr1^iv—O6—K2	92.7 (9)	O7^xi—O28—O16^xix	43.5 (4)
Sr1^iv—O6—O3	107.7 (9)	O7^xi—O28—O20^xi	117.2 (10)
Sr1^iv—O6—O4ⁱ	58.1 (5)	O7^xi—O28—O20^xix	60.9 (7)
Sr1^iv—O6—O5	149.1 (9)	O7^xi—O28—O29^xv	132.7 (8)
Sr1^iv—O6—O6^xvii	46.4 (6)	O7^xi—O28—O30	111.4 (10)
Sr1^iv—O6—O11ⁱⁱⁱ	94.2 (9)	O7^xix—O28—O11^xi	88.8 (5)
Sr1^iv—O6—O13	159.1 (12)	O7^xix—O28—O11^xix	114.4 (7)
Sr1^iv—O6—O15	53.0 (7)	O7^xix—O28—O16^xi	43.5 (4)
Sr1^iv—O6—O16	102.3 (7)	O7^xix—O28—O16^xix	86.0 (6)
Sr1^iv—O6—O19	124.0 (10)	O7^xix—O28—O20^xi	60.9 (7)
Sr1^iv—O6—O22	139.0 (13)	O7^xix—O28—O20^xix	117.2 (10)
Sr1^iv—O6—O24	100.1 (9)	O7^xix—O28—O29^xv	132.7 (8)
Sr1^iv—O6—O29^iv	48.1 (7)	O7^xix—O28—O30	111.4 (10)
Sr1^iv—O6—O31^v	56.1 (7)	O11^xi—O28—O11^xix	54.7 (6)
Sr1'^iv—O6—K2	92.7 (9)	O11^xi—O28—O16^xi	45.4 (4)
Sr1'^iv—O6—O3	107.7 (9)	O11^xi—O28—O16^xix	86.3 (6)
Sr1'^iv—O6—O4ⁱ	58.1 (5)	O11^xi—O28—O20^xi	60.7 (8)
Sr1'^iv—O6—O5	149.1 (9)	O11^xi—O28—O20^xix	115.4 (11)
Sr1'^iv—O6—O6^xvii	46.4 (6)	O11^xi—O28—O29^xv	43.9 (5)
Sr1'^iv—O6—O11ⁱⁱⁱ	94.2 (9)	O11^xi—O28—O30	133.6 (8)
Sr1'^iv—O6—O13	159.1 (12)	O11^xix—O28—O16^xi	86.3 (6)
Sr1'^iv—O6—O15	53.0 (7)	O11^xix—O28—O16^xix	45.4 (4)
Sr1'^iv—O6—O16	102.3 (7)	O11^xix—O28—O20^xi	115.4 (11)
Sr1'^iv—O6—O19	124.0 (10)	O11^xix—O28—O20^xix	60.7 (8)
Sr1'^iv—O6—O22	139.0 (13)	O11^xix—O28—O29^xv	43.9 (5)
Sr1'^iv—O6—O24	100.1 (9)	O11^xix—O28—O30	133.6 (8)
Sr1'^iv—O6—O29^iv	48.1 (7)	O16^xi—O28—O16^xix	87.7 (5)
Sr1'^iv—O6—O31^v	56.1 (7)	O16^xi—O28—O20^xi	43.8 (5)
K2—O6—O3	90.0 (10)	O16^xi—O28—O20^xix	131.5 (8)
K2—O6—O4ⁱ	150.7 (10)	O16^xi—O28—O29^xv	89.3 (7)
K2—O6—O5	106.7 (9)	O16^xi—O28—O30	134.3 (4)
K2—O6—O6^xvii	55.7 (7)	O16^xix—O28—O20^xi	131.5 (8)
K2—O6—O11ⁱⁱⁱ	117.8 (8)	O16^xix—O28—O20^xix	43.8 (5)
K2—O6—O13	81.2 (6)	O16^xix—O28—O29^xv	89.3 (7)
K2—O6—O15	107.7 (11)	O16^xix—O28—O30	134.3 (4)
K2—O6—O16	140.9 (12)	O20^xi—O28—O20^xix	175.1 (11)
K2—O6—O19	140.7 (7)	O20^xi—O28—O29^xv	89.3 (10)
K2—O6—O22	58.9 (6)	O20^xi—O28—O30	92.4 (6)
K2—O6—O24	47.3 (7)	O20^xix—O28—O29^xv	89.3 (10)
K2—O6—O29^iv	113.0 (9)	O20^xix—O28—O30	92.4 (6)
K2—O6—O31^v	49.0 (6)	O29^xv—O28—O30	105.2 (9)
O3—O6—O4ⁱ	100.9 (8)	Sr1—O29—Sr1'	0
O3—O6—O5	50.1 (7)	Sr1—O29—K1^vii	92.5 (8)
O3—O6—O6^xvii	127.5 (12)	Sr1—O29—O2^vii	129.9 (7)
O3—O6—O11ⁱⁱⁱ	144.0 (10)	Sr1—O29—O2^xxix	129.9 (7)
O3—O6—O13	92.4 (8)	Sr1—O29—O4	66.0 (8)
O3—O6—O15	57.6 (8)	Sr1—O29—O4^xii	66.0 (8)
O3—O6—O16	51.2 (7)	Sr1—O29—O6^xiii	47.8 (7)
O3—O6—O19	91.3 (9)	Sr1—O29—O6ⁱ	47.8 (7)
O3—O6—O22	49.7 (7)	Sr1—O29—O9^ix	109.4 (5)
O3—O6—O24	130.0 (12)	Sr1—O29—O9^xx	109.4 (5)
O3—O6—O29^iv	145.0 (8)	Sr1—O29—O11^ix	119.6 (9)
O3—O6—O31^v	74.3 (9)	Sr1—O29—O11^xx	119.6 (9)
O4ⁱ—O6—O5	101.1 (9)	Sr1—O29—O26	42.6 (6)
O4ⁱ—O6—O6^xvii	97.1 (8)	Sr1—O29—O28^vii	176.5 (8)
O4ⁱ—O6—O11ⁱⁱⁱ	66.6 (7)	Sr1'—O29—K1^vii	92.5 (8)
O4ⁱ—O6—O13	124.9 (11)	Sr1'—O29—O2^vii	129.9 (7)
O4ⁱ—O6—O15	58.6 (7)	Sr1'—O29—O2^xxix	129.9 (7)
O4ⁱ—O6—O16	58.0 (6)	Sr1'—O29—O4	66.0 (8)
O4ⁱ—O6—O19	66.9 (7)	Sr1'—O29—O4^xii	66.0 (8)
O4ⁱ—O6—O22	145.7 (10)	Sr1'—O29—O6^xiii	47.8 (7)
O4ⁱ—O6—O24	129.1 (13)	Sr1'—O29—O6ⁱ	47.8 (7)
O4ⁱ—O6—O29^iv	46.8 (5)	Sr1'—O29—O9^ix	109.4 (5)
O4ⁱ—O6—O31^v	107.7 (8)	Sr1'—O29—O9^xx	109.4 (5)
O5—O6—O6^xvii	161.7 (9)	Sr1'—O29—O11^ix	119.6 (9)
O5—O6—O11ⁱⁱⁱ	97.5 (9)	Sr1'—O29—O11^xx	119.6 (9)
O5—O6—O13	50.8 (6)	Sr1'—O29—O26	42.6 (6)
O5—O6—O15	97.5 (10)	Sr1'—O29—O28^vii	176.5 (8)
O5—O6—O16	47.9 (6)	K1^vii—O29—O2^vii	48.2 (5)
O5—O6—O19	48.9 (7)	K1^vii—O29—O2^xxix	48.2 (5)
O5—O6—O22	48.3 (7)	K1^vii—O29—O4	67.2 (5)
O5—O6—O24	110.8 (7)	K1^vii—O29—O4^xii	67.2 (5)
O5—O6—O29^iv	135.4 (11)	K1^vii—O29—O6^xiii	124.3 (8)
O5—O6—O31^v	121.1 (12)	K1^vii—O29—O6ⁱ	124.3 (8)
O6^xvii—O6—O11ⁱⁱⁱ	88.2 (9)	K1^vii—O29—O9^ix	83.0 (4)
O6^xvii—O6—O13	116.0 (8)	K1^vii—O29—O9^xx	83.0 (4)
O6^xvii—O6—O15	93.3 (9)	K1^vii—O29—O11^ix	128.0 (9)
O6^xvii—O6—O16	148.7 (8)	K1^vii—O29—O11^xx	128.0 (9)
O6^xvii—O6—O19	140.8 (13)	K1^vii—O29—O26	49.9 (6)
O6^xvii—O6—O22	114.6 (10)	K1^vii—O29—O28^vii	84.0 (8)
O6^xvii—O6—O24	54.8 (6)	O2^vii—O29—O2^xxix	50.4 (6)
O6^xvii—O6—O29^iv	59.1 (7)	O2^vii—O29—O4	69.7 (6)
O6^xvii—O6—O31^v	53.3 (8)	O2^vii—O29—O4^xii	110.5 (8)
O11ⁱⁱⁱ—O6—O13	71.6 (7)	O2^vii—O29—O6^xiii	172.0 (7)
O11ⁱⁱⁱ—O6—O15	125.0 (10)	O2^vii—O29—O6ⁱ	123.6 (6)
O11ⁱⁱⁱ—O6—O16	97.1 (9)	O2^vii—O29—O9^ix	47.2 (4)
O11ⁱⁱⁱ—O6—O19	52.7 (6)	O2^vii—O29—O9^xx	96.7 (8)
O11ⁱⁱⁱ—O6—O22	124.3 (8)	O2^vii—O29—O11^ix	80.8 (7)
O11ⁱⁱⁱ—O6—O24	70.7 (9)	O2^vii—O29—O11^xx	110.0 (11)
O11ⁱⁱⁱ—O6—O29^iv	46.0 (6)	O2^vii—O29—O26	92.3 (6)
O11ⁱⁱⁱ—O6—O31^v	141.0 (11)	O2^vii—O29—O28^vii	47.2 (5)
O13—O6—O15	147.9 (12)	O2^xxix—O29—O4	110.5 (8)
O13—O6—O16	94.8 (8)	O2^xxix—O29—O4^xii	69.7 (6)
O13—O6—O19	59.6 (6)	O2^xxix—O29—O6^xiii	123.6 (6)
O13—O6—O22	52.7 (6)	O2^xxix—O29—O6ⁱ	172.0 (7)
O13—O6—O24	61.2 (5)	O2^xxix—O29—O9^ix	96.7 (8)
O13—O6—O29^iv	116.2 (11)	O2^xxix—O29—O9^xx	47.2 (4)
O13—O6—O31^v	127.3 (11)	O2^xxix—O29—O11^ix	110.0 (11)
O15—O6—O16	58.5 (7)	O2^xxix—O29—O11^xx	80.8 (7)
O15—O6—O19	106.0 (9)	O2^xxix—O29—O26	92.3 (6)
O15—O6—O22	104.7 (11)	O2^xxix—O29—O28^vii	47.2 (5)
O15—O6—O24	146.1 (12)	O4—O29—O4^xii	110.0 (10)
O15—O6—O29^iv	89.3 (9)	O4—O29—O6^xiii	111.4 (12)
O15—O6—O31^v	59.9 (8)	O4—O29—O6ⁱ	61.5 (7)
O16—O6—O19	51.2 (6)	O4—O29—O9^ix	47.5 (4)
O16—O6—O22	87.7 (9)	O4—O29—O9^xx	149.2 (7)
O16—O6—O24	155.2 (10)	O4—O29—O11^ix	88.6 (4)
O16—O6—O29^iv	103.7 (8)	O4—O29—O11^xx	160.5 (7)
O16—O6—O31^v	112.6 (10)	O4—O29—O26	55.0 (5)
O19—O6—O22	93.4 (8)	O4—O29—O28^vii	112.4 (8)
O19—O6—O24	106.6 (10)	O4^xii—O29—O6^xiii	61.5 (7)
O19—O6—O29^iv	86.9 (9)	O4^xii—O29—O6ⁱ	111.4 (12)
O19—O6—O31^v	163.7 (11)	O4^xii—O29—O9^ix	149.2 (7)
O22—O6—O24	82.3 (8)	O4^xii—O29—O9^xx	47.5 (4)
O22—O6—O29^iv	165.3 (9)	O4^xii—O29—O11^ix	160.5 (7)
O22—O6—O31^v	83.2 (10)	O4^xii—O29—O11^xx	88.6 (4)
O24—O6—O29^iv	83.5 (9)	O4^xii—O29—O26	55.0 (5)
O24—O6—O31^v	88.8 (10)	O4^xii—O29—O28^vii	112.4 (8)
O29^iv—O6—O31^v	100.4 (9)	O6^xiii—O29—O6ⁱ	61.8 (9)
U4—O7—K3	119.8 (8)	O6^xiii—O29—O9^ix	139.6 (8)
U4—O7—K4^vi	122.7 (6)	O6^xiii—O29—O9^xx	78.4 (6)
U4—O7—O1^viii	51.2 (7)	O6^xiii—O29—O11^ix	107.1 (8)
U4—O7—O4	2.6 (2)	O6^xiii—O29—O11^xx	71.8 (7)
U4—O7—O7ⁱ	169.1 (8)	O6^xiii—O29—O26	82.4 (9)
U4—O7—O9^ix	53.7 (5)	O6^xiii—O29—O28^vii	134.7 (7)
U4—O7—O15^ix	93.6 (6)	O6ⁱ—O29—O9^ix	78.4 (6)
U4—O7—O16ⁱ	57.4 (5)	O6ⁱ—O29—O9^xx	139.6 (8)
U4—O7—O18^vii	89.2 (6)	O6ⁱ—O29—O11^ix	71.8 (7)
U4—O7—O19ⁱ	67.8 (5)	O6ⁱ—O29—O11^xx	107.1 (8)
U4—O7—O20ⁱ	52.2 (6)	O6ⁱ—O29—O26	82.4 (9)
U4—O7—O25	125.7 (5)	O6ⁱ—O29—O28^vii	134.7 (7)
U4—O7—O28^vi	107.4 (6)	O9^ix—O29—O9^xx	139.1 (10)
K3—O7—K4^vi	109.2 (5)	O9^ix—O29—O11^ix	49.5 (4)
K3—O7—O1^viii	153.5 (9)	O9^ix—O29—O11^xx	117.2 (9)
K3—O7—O4	119.3 (6)	O9^ix—O29—O26	99.9 (4)
K3—O7—O7ⁱ	54.2 (4)	O9^ix—O29—O28^vii	70.2 (5)
K3—O7—O9^ix	144.0 (5)	O9^xx—O29—O11^ix	117.2 (9)
K3—O7—O15^ix	110.0 (5)	O9^xx—O29—O11^xx	49.5 (4)
K3—O7—O16ⁱ	63.3 (5)	O9^xx—O29—O26	99.9 (4)
K3—O7—O18^vii	150.0 (6)	O9^xx—O29—O28^vii	70.2 (5)
K3—O7—O19ⁱ	87.7 (5)	O11^ix—O29—O11^xx	72.3 (7)
K3—O7—O20ⁱ	87.5 (8)	O11^ix—O29—O26	142.7 (6)
K3—O7—O25	57.7 (7)	O11^ix—O29—O28^vii	63.0 (7)
K3—O7—O28^vi	56.3 (5)	O11^xx—O29—O26	142.7 (6)
K4^vi—O7—O1^viii	71.6 (7)	O11^xx—O29—O28^vii	63.0 (7)
K4^vi—O7—O4	124.6 (5)	O26—O29—O28^vii	133.9 (9)
K4^vi—O7—O7ⁱ	58.1 (4)	U1^xiii—O30—U1ⁱ	118.4 (5)
K4^vi—O7—O9^ix	100.1 (7)	U1^xiii—O30—K2^xiii	74.0 (4)
K4^vi—O7—O15^ix	96.2 (7)	U1^xiii—O30—O2	129.9 (10)
K4^vi—O7—O16ⁱ	159.5 (7)	U1^xiii—O30—O2^xii	76.3 (5)
K4^vi—O7—O18^vii	52.9 (5)	U1^xiii—O30—O10^x	127.7 (6)
K4^vi—O7—O19ⁱ	144.6 (7)	U1^xiii—O30—O10^xiv	32.9 (2)
K4^vi—O7—O20ⁱ	106.1 (6)	U1^xiii—O30—O12^xiii	23.3 (3)
K4^vi—O7—O25	104.4 (7)	U1^xiii—O30—O12ⁱ	95.4 (6)
K4^vi—O7—O28^vi	76.0 (7)	U1^xiii—O30—O14^ix	160.1 (9)
O1^viii—O7—O4	53.0 (7)	U1^xiii—O30—O14^xx	42.7 (4)
O1^viii—O7—O7ⁱ	129.0 (7)	U1^xiii—O30—O21^xiii	77.8 (4)
O1^viii—O7—O9^ix	56.3 (6)	U1^xiii—O30—O21ⁱ	122.4 (9)
O1^viii—O7—O15^ix	96.1 (8)	U1^xiii—O30—O22^xiii	32.9 (2)
O1^viii—O7—O16ⁱ	106.3 (9)	U1^xiii—O30—O22ⁱ	119.4 (7)
O1^viii—O7—O18^vii	51.9 (8)	U1^xiii—O30—O28	119.8 (3)
O1^viii—O7—O19ⁱ	106.8 (7)	U1^xiii—O30—O32^x	69.0 (4)
O1^viii—O7—O20ⁱ	67.5 (10)	U1ⁱ—O30—K2^xiii	74.0 (4)
O1^viii—O7—O25	148.8 (10)	U1ⁱ—O30—O2	76.3 (5)
O1^viii—O7—O28^vi	100.0 (7)	U1ⁱ—O30—O2^xii	129.9 (10)
O4—O7—O7ⁱ	170.7 (7)	U1ⁱ—O30—O10^x	32.9 (2)
O4—O7—O9^ix	52.3 (5)	U1ⁱ—O30—O10^xiv	127.7 (6)
O4—O7—O15^ix	91.4 (6)	U1ⁱ—O30—O12^xiii	95.4 (6)
O4—O7—O16ⁱ	56.4 (5)	U1ⁱ—O30—O12ⁱ	23.3 (3)
O4—O7—O18^vii	89.3 (5)	U1ⁱ—O30—O14^ix	42.7 (4)
O4—O7—O19ⁱ	65.2 (4)	U1ⁱ—O30—O14^xx	160.1 (9)
O4—O7—O20ⁱ	54.2 (6)	U1ⁱ—O30—O21^xiii	122.4 (9)
O4—O7—O25	123.0 (4)	U1ⁱ—O30—O21ⁱ	77.8 (4)
O4—O7—O28^vi	109.4 (5)	U1ⁱ—O30—O22^xiii	119.4 (7)
O7ⁱ—O7—O9^ix	136.9 (7)	U1ⁱ—O30—O22ⁱ	32.9 (2)
O7ⁱ—O7—O15^ix	97.1 (6)	U1ⁱ—O30—O28	119.8 (3)
O7ⁱ—O7—O16ⁱ	117.5 (7)	U1ⁱ—O30—O32^x	69.0 (4)
O7ⁱ—O7—O18^vii	98.4 (6)	K2^xiii—O30—O2	148.9 (5)
O7ⁱ—O7—O19ⁱ	118.5 (5)	K2^xiii—O30—O2^xii	148.9 (5)
O7ⁱ—O7—O20ⁱ	117.0 (8)	K2^xiii—O30—O10^x	106.9 (5)
O7ⁱ—O7—O25	60.8 (4)	K2^xiii—O30—O10^xiv	106.9 (5)
O7ⁱ—O7—O28^vi	61.8 (5)	K2^xiii—O30—O12^xiii	67.9 (8)
O9^ix—O7—O15^ix	44.8 (5)	K2^xiii—O30—O12ⁱ	67.9 (8)
O9^ix—O7—O16ⁱ	94.9 (6)	K2^xiii—O30—O14^ix	91.7 (10)
O9^ix—O7—O18^vii	47.6 (5)	K2^xiii—O30—O14^xx	91.7 (10)
O9^ix—O7—O19ⁱ	56.5 (5)	K2^xiii—O30—O21^xiii	57.3 (7)
O9^ix—O7—O20ⁱ	104.3 (8)	K2^xiii—O30—O21ⁱ	57.3 (7)
O9^ix—O7—O25	95.5 (6)	K2^xiii—O30—O22^xiii	50.7 (4)
O9^ix—O7—O28^vi	155.3 (6)	K2^xiii—O30—O22ⁱ	50.7 (4)
O15^ix—O7—O16ⁱ	104.3 (6)	K2^xiii—O30—O28	136.4 (11)
O15^ix—O7—O18^vii	56.4 (6)	K2^xiii—O30—O32^x	103.2 (8)
O15^ix—O7—O19ⁱ	48.4 (6)	O2—O30—O2^xii	61.5 (9)
O15^ix—O7—O20ⁱ	145.5 (8)	O2—O30—O10^x	44.3 (5)
O15^ix—O7—O25	53.0 (7)	O2—O30—O10^xiv	98.5 (9)
O15^ix—O7—O28^vi	158.7 (6)	O2—O30—O12^xiii	124.6 (12)
O16ⁱ—O7—O18^vii	142.0 (6)	O2—O30—O12ⁱ	88.0 (8)
O16ⁱ—O7—O19ⁱ	55.9 (5)	O2—O30—O14^ix	59.5 (9)
O16ⁱ—O7—O20ⁱ	56.3 (6)	O2—O30—O14^xx	119.3 (12)
O16ⁱ—O7—O25	87.8 (7)	O2—O30—O21^xiii	137.8 (7)
O16ⁱ—O7—O28^vi	84.6 (7)	O2—O30—O21ⁱ	107.2 (5)
O18^vii—O7—O19ⁱ	97.3 (6)	O2—O30—O22^xiii	159.7 (9)
O18^vii—O7—O20ⁱ	119.1 (7)	O2—O30—O22ⁱ	98.4 (5)
O18^vii—O7—O25	100.2 (8)	O2—O30—O28	55.5 (7)
O18^vii—O7—O28^vi	125.9 (7)	O2—O30—O32^x	74.3 (8)
O19ⁱ—O7—O20ⁱ	105.6 (7)	O2^xii—O30—O10^x	98.5 (9)
O19ⁱ—O7—O25	58.0 (4)	O2^xii—O30—O10^xiv	44.3 (5)
O19ⁱ—O7—O28^vi	136.8 (9)	O2^xii—O30—O12^xiii	88.0 (8)
O20ⁱ—O7—O25	139.7 (10)	O2^xii—O30—O12ⁱ	124.6 (12)
O20ⁱ—O7—O28^vi	55.2 (6)	O2^xii—O30—O14^ix	119.3 (12)
O25—O7—O28^vi	109.1 (7)	O2^xii—O30—O14^xx	59.5 (9)
U1—O8—U3	70.6 (6)	O2^xii—O30—O21^xiii	107.2 (5)
U1—O8—U6	74.6 (7)	O2^xii—O30—O21ⁱ	137.8 (7)
U1—O8—Sr2	148.3 (10)	O2^xii—O30—O22^xiii	98.4 (5)
U1—O8—Sr2'	148.3 (10)	O2^xii—O30—O22ⁱ	159.7 (9)
U1—O8—O3	53.0 (7)	O2^xii—O30—O28	55.5 (7)
U1—O8—O5	97.6 (9)	O2^xii—O30—O32^x	74.3 (8)
U1—O8—O8ⁱ	165.6 (6)	O10^x—O30—O10^xiv	115.1 (8)
U1—O8—O10ⁱⁱ	48.0 (6)	O10^x—O30—O12^xiii	106.6 (7)
U1—O8—O12	1.6 (5)	O10^x—O30—O12ⁱ	44.8 (5)
U1—O8—O13ⁱⁱ	51.9 (5)	O10^x—O30—O14^ix	42.8 (7)
U1—O8—O14ⁱⁱⁱ	54.3 (7)	O10^x—O30—O14^xx	155.9 (13)
U1—O8—O17	101.6 (9)	O10^x—O30—O21^xiii	148.1 (7)
U1—O8—O18ⁱ	92.8 (7)	O10^x—O30—O21ⁱ	96.6 (4)
U1—O8—O22	52.6 (7)	O10^x—O30—O22^xiii	146.9 (6)
U1—O8—O23	126.8 (6)	O10^x—O30—O22ⁱ	62.0 (3)
U1—O8—O24^x	109.0 (6)	O10^x—O30—O28	95.7 (6)
U1—O8—O27	139.4 (8)	O10^x—O30—O32^x	59.7 (4)
U3—O8—U6	59.8 (3)	O10^xiv—O30—O12^xiii	44.8 (5)
U3—O8—Sr2	79.7 (4)	O10^xiv—O30—O12ⁱ	106.6 (7)
U3—O8—Sr2'	79.7 (4)	O10^xiv—O30—O14^ix	155.9 (13)
U3—O8—O3	37.2 (5)	O10^xiv—O30—O14^xx	42.8 (7)
U3—O8—O5	27.0 (5)	O10^xiv—O30—O21^xiii	96.6 (4)
U3—O8—O8ⁱ	114.9 (6)	O10^xiv—O30—O21ⁱ	148.1 (7)
U3—O8—O10ⁱⁱ	116.9 (9)	O10^xiv—O30—O22^xiii	62.0 (3)
U3—O8—O12	69.4 (6)	O10^xiv—O30—O22ⁱ	146.9 (6)
U3—O8—O13ⁱⁱ	102.7 (6)	O10^xiv—O30—O28	95.7 (6)
U3—O8—O14ⁱⁱⁱ	85.7 (8)	O10^xiv—O30—O32^x	59.7 (4)
U3—O8—O17	72.1 (5)	O12^xiii—O30—O12ⁱ	72.3 (6)
U3—O8—O18ⁱ	134.0 (7)	O12^xiii—O30—O14^ix	138.0 (8)
U3—O8—O22	35.0 (4)	O12^xiii—O30—O14^xx	66.0 (5)
U3—O8—O23	81.9 (7)	O12^xiii—O30—O21^xiii	93.2 (8)
U3—O8—O24^x	123.4 (6)	O12^xiii—O30—O21ⁱ	124.6 (12)
U3—O8—O27	125.4 (8)	O12^xiii—O30—O22^xiii	46.0 (6)
U6—O8—Sr2	81.0 (4)	O12^xiii—O30—O22ⁱ	102.6 (8)
U6—O8—Sr2'	81.0 (4)	O12^xiii—O30—O28	139.9 (7)
U6—O8—O3	88.8 (6)	O12^xiii—O30—O32^x	52.4 (7)
U6—O8—O5	65.0 (5)	O12ⁱ—O30—O14^ix	66.0 (5)
U6—O8—O8ⁱ	119.8 (5)	O12ⁱ—O30—O14^xx	138.0 (8)
U6—O8—O10ⁱⁱ	87.6 (6)	O12ⁱ—O30—O21^xiii	124.6 (12)
U6—O8—O12	73.1 (6)	O12ⁱ—O30—O21ⁱ	93.2 (8)
U6—O8—O13ⁱⁱ	126.0 (9)	O12ⁱ—O30—O22^xiii	102.6 (8)
U6—O8—O14ⁱⁱⁱ	37.9 (6)	O12ⁱ—O30—O22ⁱ	46.0 (6)
U6—O8—O17	27.2 (3)	O12ⁱ—O30—O28	139.9 (7)
U6—O8—O18ⁱ	74.6 (5)	O12ⁱ—O30—O32^x	52.4 (7)
U6—O8—O22	33.4 (3)	O14^ix—O30—O14^xx	154.4 (10)
U6—O8—O23	127.9 (9)	O14^ix—O30—O21^xiii	106.4 (11)
U6—O8—O24^x	175.6 (7)	O14^ix—O30—O21ⁱ	55.6 (8)
U6—O8—O27	83.3 (5)	O14^ix—O30—O22^xiii	140.7 (13)
Sr2—O8—Sr2'	0	O14^ix—O30—O22ⁱ	42.6 (7)
Sr2—O8—O3	107.4 (8)	O14^ix—O30—O28	80.0 (6)
Sr2—O8—O5	53.0 (6)	O14^ix—O30—O32^x	101.9 (8)
Sr2—O8—O8ⁱ	43.3 (5)	O14^xx—O30—O21^xiii	55.6 (8)
Sr2—O8—O10ⁱⁱ	151.2 (5)	O14^xx—O30—O21ⁱ	106.4 (11)
Sr2—O8—O12	146.7 (9)	O14^xx—O30—O22^xiii	42.6 (7)
Sr2—O8—O13ⁱⁱ	150.6 (8)	O14^xx—O30—O22ⁱ	140.7 (13)
Sr2—O8—O14ⁱⁱⁱ	113.5 (6)	O14^xx—O30—O28	80.0 (6)
Sr2—O8—O17	57.3 (4)	O14^xx—O30—O32^x	101.9 (8)
Sr2—O8—O18ⁱ	100.0 (6)	O21^xiii—O30—O21ⁱ	51.5 (6)
Sr2—O8—O22	96.2 (6)	O21^xiii—O30—O22^xiii	47.3 (4)
Sr2—O8—O23	57.0 (7)	O21^xiii—O30—O22ⁱ	89.7 (8)
Sr2—O8—O24^x	96.5 (8)	O21^xiii—O30—O28	83.9 (7)
Sr2—O8—O27	54.2 (7)	O21^xiii—O30—O32^x	145.5 (6)
Sr2'—O8—O3	107.4 (8)	O21ⁱ—O30—O22^xiii	89.7 (8)
Sr2'—O8—O5	53.0 (6)	O21ⁱ—O30—O22ⁱ	47.3 (4)
Sr2'—O8—O8ⁱ	43.3 (5)	O21ⁱ—O30—O28	83.9 (7)
Sr2'—O8—O10ⁱⁱ	151.2 (5)	O21ⁱ—O30—O32^x	145.5 (6)
Sr2'—O8—O12	146.7 (9)	O22^xiii—O30—O22ⁱ	101.5 (8)
Sr2'—O8—O13ⁱⁱ	150.6 (8)	O22^xiii—O30—O28	117.3 (5)
Sr2'—O8—O14ⁱⁱⁱ	113.5 (6)	O22^xiii—O30—O32^x	98.2 (5)
Sr2'—O8—O17	57.3 (4)	O22ⁱ—O30—O28	117.3 (5)
Sr2'—O8—O18ⁱ	100.0 (6)	O22ⁱ—O30—O32^x	98.2 (5)
Sr2'—O8—O22	96.2 (6)	O28—O30—O32^x	120.5 (12)
Sr2'—O8—O23	57.0 (7)	Sr1^xviii—O31—Sr1'^xviii	0
Sr2'—O8—O24^x	96.5 (8)	Sr1^xviii—O31—K2^ix	107.2 (12)
Sr2'—O8—O27	54.2 (7)	Sr1^xviii—O31—O3^ix	92.6 (7)
O3—O8—O5	57.7 (7)	Sr1^xviii—O31—O3ⁱⁱⁱ	92.6 (7)
O3—O8—O8ⁱ	122.8 (7)	Sr1^xviii—O31—O6^ix	54.4 (8)
O3—O8—O10ⁱⁱ	98.6 (9)	Sr1^xviii—O31—O6ⁱⁱⁱ	54.4 (8)
O3—O8—O12	52.6 (7)	Sr1^xviii—O31—O12^ix	142.5 (6)
O3—O8—O13ⁱⁱ	66.3 (6)	Sr1^xviii—O31—O12ⁱⁱⁱ	142.5 (6)
O3—O8—O14ⁱⁱⁱ	96.8 (10)	Sr1^xviii—O31—O15^ix	54.2 (8)
O3—O8—O17	107.9 (8)	Sr1^xviii—O31—O15ⁱⁱⁱ	54.2 (8)
O3—O8—O18ⁱ	145.2 (10)	Sr1^xviii—O31—O25	95.3 (9)
O3—O8—O22	55.8 (6)	Sr1'^xviii—O31—K2^ix	107.2 (12)
O3—O8—O23	77.6 (6)	Sr1'^xviii—O31—O3^ix	92.6 (7)
O3—O8—O24^x	95.4 (5)	Sr1'^xviii—O31—O3ⁱⁱⁱ	92.6 (7)
O3—O8—O27	160.9 (11)	Sr1'^xviii—O31—O6^ix	54.4 (8)
O5—O8—O8ⁱ	89.0 (8)	Sr1'^xviii—O31—O6ⁱⁱⁱ	54.4 (8)
O5—O8—O10ⁱⁱ	142.3 (11)	Sr1'^xviii—O31—O12^ix	142.5 (6)
O5—O8—O12	96.4 (9)	Sr1'^xviii—O31—O12ⁱⁱⁱ	142.5 (6)
O5—O8—O13ⁱⁱ	123.0 (7)	Sr1'^xviii—O31—O15^ix	54.2 (8)
O5—O8—O14ⁱⁱⁱ	100.4 (9)	Sr1'^xviii—O31—O15ⁱⁱⁱ	54.2 (8)
O5—O8—O17	63.8 (6)	Sr1'^xviii—O31—O25	95.3 (9)
O5—O8—O18ⁱ	133.5 (7)	K2^ix—O31—O3^ix	89.1 (4)
O5—O8—O22	54.6 (7)	K2^ix—O31—O3ⁱⁱⁱ	89.1 (4)
O5—O8—O23	65.3 (9)	K2^ix—O31—O6^ix	69.3 (7)
O5—O8—O24^x	116.3 (8)	K2^ix—O31—O6ⁱⁱⁱ	69.3 (7)
O5—O8—O27	103.2 (10)	K2^ix—O31—O12^ix	70.5 (7)
O8ⁱ—O8—O10ⁱⁱ	128.2 (7)	K2^ix—O31—O12ⁱⁱⁱ	70.5 (7)
O8ⁱ—O8—O12	167.0 (6)	K2^ix—O31—O15^ix	131.1 (9)
O8ⁱ—O8—O13ⁱⁱ	113.9 (7)	K2^ix—O31—O15ⁱⁱⁱ	131.1 (9)
O8ⁱ—O8—O14ⁱⁱⁱ	137.0 (6)	K2^ix—O31—O25	157.5 (15)
O8ⁱ—O8—O17	92.7 (7)	O3^ix—O31—O3ⁱⁱⁱ	174.8 (12)
O8ⁱ—O8—O18ⁱ	91.8 (5)	O3^ix—O31—O6^ix	55.1 (7)
O8ⁱ—O8—O22	139.4 (7)	O3^ix—O31—O6ⁱⁱⁱ	128.5 (11)
O8ⁱ—O8—O23	45.3 (6)	O3^ix—O31—O12^ix	50.5 (6)
O8ⁱ—O8—O24^x	56.7 (5)	O3^ix—O31—O12ⁱⁱⁱ	124.3 (10)
O8ⁱ—O8—O27	49.5 (5)	O3^ix—O31—O15^ix	52.8 (6)
O10ⁱⁱ—O8—O12	49.0 (6)	O3^ix—O31—O15ⁱⁱⁱ	131.4 (8)
O10ⁱⁱ—O8—O13ⁱⁱ	53.1 (5)	O3^ix—O31—O25	89.9 (4)
O10ⁱⁱ—O8—O14ⁱⁱⁱ	49.8 (7)	O3ⁱⁱⁱ—O31—O6^ix	128.5 (11)
O10ⁱⁱ—O8—O17	103.4 (6)	O3ⁱⁱⁱ—O31—O6ⁱⁱⁱ	55.1 (7)
O10ⁱⁱ—O8—O18ⁱ	51.3 (5)	O3ⁱⁱⁱ—O31—O12^ix	124.3 (10)
O10ⁱⁱ—O8—O22	88.2 (9)	O3ⁱⁱⁱ—O31—O12ⁱⁱⁱ	50.5 (6)
O10ⁱⁱ—O8—O23	143.8 (9)	O3ⁱⁱⁱ—O31—O15^ix	131.4 (8)
O10ⁱⁱ—O8—O24^x	93.1 (7)	O3ⁱⁱⁱ—O31—O15ⁱⁱⁱ	52.8 (6)
O10ⁱⁱ—O8—O27	98.4 (7)	O3ⁱⁱⁱ—O31—O25	89.9 (4)
O12—O8—O13ⁱⁱ	53.4 (7)	O6^ix—O31—O6ⁱⁱⁱ	73.5 (11)
O12—O8—O14ⁱⁱⁱ	53.6 (6)	O6^ix—O31—O12^ix	92.6 (8)
O12—O8—O17	100.2 (8)	O6^ix—O31—O12ⁱⁱⁱ	139.8 (10)
O12—O8—O18ⁱ	93.0 (6)	O6^ix—O31—O15^ix	63.9 (8)
O12—O8—O22	51.0 (7)	O6^ix—O31—O15ⁱⁱⁱ	108.6 (13)
O12—O8—O23	127.1 (6)	O6^ix—O31—O25	127.0 (8)
O12—O8—O24^x	110.5 (6)	O6ⁱⁱⁱ—O31—O12^ix	139.8 (10)
O12—O8—O27	139.2 (7)	O6ⁱⁱⁱ—O31—O12ⁱⁱⁱ	92.6 (8)
O13ⁱⁱ—O8—O14ⁱⁱⁱ	95.8 (9)	O6ⁱⁱⁱ—O31—O15^ix	108.6 (13)
O13ⁱⁱ—O8—O17	151.7 (11)	O6ⁱⁱⁱ—O31—O15ⁱⁱⁱ	63.9 (8)
O13ⁱⁱ—O8—O18ⁱ	98.8 (7)	O6ⁱⁱⁱ—O31—O25	127.0 (8)
O13ⁱⁱ—O8—O22	102.1 (9)	O12^ix—O31—O12ⁱⁱⁱ	73.8 (9)
O13ⁱⁱ—O8—O23	94.1 (7)	O12^ix—O31—O15^ix	97.8 (7)
O13ⁱⁱ—O8—O24^x	57.4 (4)	O12^ix—O31—O15ⁱⁱⁱ	153.7 (14)
O13ⁱⁱ—O8—O27	131.9 (10)	O12^ix—O31—O25	91.7 (11)
O14ⁱⁱⁱ—O8—O17	56.5 (6)	O12ⁱⁱⁱ—O31—O15^ix	153.7 (14)
O14ⁱⁱⁱ—O8—O18ⁱ	51.9 (6)	O12ⁱⁱⁱ—O31—O15ⁱⁱⁱ	97.8 (7)
O14ⁱⁱⁱ—O8—O22	50.7 (7)	O12ⁱⁱⁱ—O31—O25	91.7 (11)
O14ⁱⁱⁱ—O8—O23	165.5 (11)	O15^ix—O31—O15ⁱⁱⁱ	78.6 (9)
O14ⁱⁱⁱ—O8—O24^x	142.2 (10)	O15^ix—O31—O25	63.2 (8)
O14ⁱⁱⁱ—O8—O27	87.6 (6)	O15ⁱⁱⁱ—O31—O25	63.2 (8)
O17—O8—O18ⁱ	69.8 (6)	Sr2—O32—Sr2'	0
O17—O8—O22	57.3 (5)	Sr2—O32—K1^xviii	86.6 (10)
O17—O8—O23	112.1 (10)	Sr2—O32—O2^xviii	121.7 (11)
O17—O8—O24^x	148.8 (10)	Sr2—O32—O2^xx	121.7 (11)
O17—O8—O27	59.4 (6)	Sr2—O32—O5	53.9 (7)
O18ⁱ—O8—O22	100.9 (7)	Sr2—O32—O5ⁱ	53.9 (7)
O18ⁱ—O8—O23	136.5 (10)	Sr2—O32—O10	110.2 (6)
O18ⁱ—O8—O24^x	102.4 (8)	Sr2—O32—O10ⁱ	110.2 (6)
O18ⁱ—O8—O27	48.1 (6)	Sr2—O32—O12^ix	133.9 (6)
O22—O8—O23	116.7 (9)	Sr2—O32—O12ⁱⁱⁱ	133.9 (6)
O22—O8—O24^x	151.0 (6)	Sr2—O32—O17	61.4 (7)
O22—O8—O27	116.2 (6)	Sr2—O32—O17ⁱ	61.4 (7)
O23—O8—O24^x	52.2 (9)	Sr2—O32—O30^xviii	167.8 (12)
O23—O8—O27	93.6 (9)	Sr2'—O32—K1^xviii	86.6 (10)
O24^x—O8—O27	92.4 (8)	Sr2'—O32—O2^xviii	121.7 (11)
U2—O9—U4^v	126.1 (7)	Sr2'—O32—O2^xx	121.7 (11)
U2—O9—U5^vi	122.5 (7)	Sr2'—O32—O5	53.9 (7)
U2—O9—O1^xxv	179.0 (7)	Sr2'—O32—O5ⁱ	53.9 (7)
U2—O9—O2^vi	115.4 (6)	Sr2'—O32—O10	110.2 (6)
U2—O9—O4^v	115.8 (6)	Sr2'—O32—O10ⁱ	110.2 (6)
U2—O9—O7^v	116.4 (6)	Sr2'—O32—O12^ix	133.9 (6)
U2—O9—O11	38.7 (3)	Sr2'—O32—O12ⁱⁱⁱ	133.9 (6)
U2—O9—O15	40.9 (6)	Sr2'—O32—O17	61.4 (7)
U2—O9—O18^vi	113.3 (8)	Sr2'—O32—O17ⁱ	61.4 (7)
U2—O9—O19ⁱⁱ	58.7 (4)	Sr2'—O32—O30^xviii	167.8 (12)
U2—O9—O20	64.8 (6)	K1^xviii—O32—O2^xviii	43.8 (6)
U2—O9—O29^v	85.3 (5)	K1^xviii—O32—O2^xx	43.8 (6)
U4^v—O9—U5^vi	111.0 (4)	K1^xviii—O32—O5	122.2 (10)
U4^v—O9—O1^xxv	53.9 (10)	K1^xviii—O32—O5ⁱ	122.2 (10)
U4^v—O9—O2^vi	102.8 (6)	K1^xviii—O32—O10	75.5 (4)
U4^v—O9—O4^v	37.2 (4)	K1^xviii—O32—O10ⁱ	75.5 (4)
U4^v—O9—O7^v	40.1 (4)	K1^xviii—O32—O12^ix	116.1 (6)
U4^v—O9—O11	109.8 (7)	K1^xviii—O32—O12ⁱⁱⁱ	116.1 (6)
U4^v—O9—O15	123.2 (9)	K1^xviii—O32—O17	58.8 (6)
U4^v—O9—O18^vi	111.5 (7)	K1^xviii—O32—O17ⁱ	58.8 (6)
U4^v—O9—O19ⁱⁱ	68.6 (5)	K1^xviii—O32—O30^xviii	81.2 (7)
U4^v—O9—O20	165.7 (8)	O2^xviii—O32—O2^xx	46.2 (4)
U4^v—O9—O29^v	80.1 (6)	O2^xviii—O32—O5	120.9 (5)
U5^vi—O9—O1^xxv	57.4 (10)	O2^xviii—O32—O5ⁱ	164.6 (10)
U5^vi—O9—O2^vi	37.0 (6)	O2^xviii—O32—O10	42.3 (4)
U5^vi—O9—O4^v	104.8 (5)	O2^xviii—O32—O10ⁱ	88.0 (5)
U5^vi—O9—O7^v	110.8 (5)	O2^xviii—O32—O12^ix	99.9 (8)
U5^vi—O9—O11	118.4 (7)	O2^xviii—O32—O12ⁱⁱⁱ	72.7 (7)
U5^vi—O9—O15	112.0 (9)	O2^xviii—O32—O17	66.1 (5)
U5^vi—O9—O18^vi	39.7 (5)	O2^xviii—O32—O17ⁱ	99.6 (8)
U5^vi—O9—O19ⁱⁱ	174.5 (7)	O2^xviii—O32—O30^xviii	47.7 (7)
U5^vi—O9—O20	57.8 (6)	O2^xx—O32—O5	164.6 (10)
U5^vi—O9—O29^v	99.3 (6)	O2^xx—O32—O5ⁱ	120.9 (5)
O1^xxv—O9—O2^vi	63.9 (7)	O2^xx—O32—O10	88.0 (5)
O1^xxv—O9—O4^v	63.5 (9)	O2^xx—O32—O10ⁱ	42.3 (4)
O1^xxv—O9—O7^v	64.3 (7)	O2^xx—O32—O12^ix	72.7 (7)
O1^xxv—O9—O11	140.3 (7)	O2^xx—O32—O12ⁱⁱⁱ	99.9 (8)
O1^xxv—O9—O15	140.1 (8)	O2^xx—O32—O17	99.6 (8)
O1^xxv—O9—O18^vi	67.4 (10)	O2^xx—O32—O17ⁱ	66.1 (5)
O1^xxv—O9—O19ⁱⁱ	121.4 (11)	O2^xx—O32—O30^xviii	47.7 (7)
O1^xxv—O9—O20	115.1 (12)	O5—O32—O5ⁱ	70.0 (8)
O1^xxv—O9—O29^v	93.7 (6)	O5—O32—O10	81.0 (5)
O2^vi—O9—O4^v	77.9 (7)	O5—O32—O10ⁱ	150.9 (7)
O2^vi—O9—O7^v	128.1 (5)	O5—O32—O12^ix	121.7 (11)
O2^vi—O9—O11	90.3 (6)	O5—O32—O12ⁱⁱⁱ	80.6 (8)
O2^vi—O9—O15	133.7 (10)	O5—O32—O17	65.1 (7)
O2^vi—O9—O18^vi	76.7 (8)	O5—O32—O17ⁱ	114.5 (11)
O2^vi—O9—O19ⁱⁱ	148.3 (9)	O5—O32—O30^xviii	134.1 (10)
O2^vi—O9—O20	62.9 (7)	O5ⁱ—O32—O10	150.9 (7)
O2^vi—O9—O29^v	62.3 (8)	O5ⁱ—O32—O10ⁱ	81.0 (5)
O4^v—O9—O7^v	77.3 (6)	O5ⁱ—O32—O12^ix	80.6 (8)
O4^v—O9—O11	82.7 (5)	O5ⁱ—O32—O12ⁱⁱⁱ	121.7 (11)
O4^v—O9—O15	143.2 (9)	O5ⁱ—O32—O17	114.5 (11)
O4^v—O9—O18^vi	130.6 (6)	O5ⁱ—O32—O17ⁱ	65.1 (7)
O4^v—O9—O19ⁱⁱ	78.3 (6)	O5ⁱ—O32—O30^xviii	134.1 (10)
O4^v—O9—O20	132.6 (9)	O10—O32—O10ⁱ	127.8 (6)
O4^v—O9—O29^v	43.6 (5)	O10—O32—O12^ix	114.0 (10)
O7^v—O9—O11	130.1 (7)	O10—O32—O12ⁱⁱⁱ	48.0 (5)
O7^v—O9—O15	90.1 (8)	O10—O32—O17	51.5 (4)
O7^v—O9—O18^vi	86.3 (7)	O10—O32—O17ⁱ	133.3 (10)
O7^v—O9—O19ⁱⁱ	65.2 (5)	O10—O32—O30^xviii	66.7 (4)
O7^v—O9—O20	148.4 (9)	O10ⁱ—O32—O12^ix	48.0 (5)
O7^v—O9—O29^v	119.0 (8)	O10ⁱ—O32—O12ⁱⁱⁱ	114.0 (10)
O11—O9—O15	79.5 (6)	O10ⁱ—O32—O17	133.3 (10)
O11—O9—O18^vi	138.5 (9)	O10ⁱ—O32—O17ⁱ	51.5 (4)
O11—O9—O19ⁱⁱ	66.2 (5)	O10ⁱ—O32—O30^xviii	66.7 (4)
O11—O9—O20	72.4 (7)	O12^ix—O32—O12ⁱⁱⁱ	73.7 (10)
O11—O9—O29^v	46.6 (4)	O12^ix—O32—O17	164.7 (9)
O15—O9—O18^vi	81.7 (8)	O12^ix—O32—O17ⁱ	95.2 (5)
O15—O9—O19ⁱⁱ	65.2 (8)	O12^ix—O32—O30^xviii	53.6 (7)
O15—O9—O20	71.0 (9)	O12ⁱⁱⁱ—O32—O17	95.2 (5)
O15—O9—O29^v	126.0 (7)	O12ⁱⁱⁱ—O32—O17ⁱ	164.7 (9)
O18^vi—O9—O19ⁱⁱ	135.0 (8)	O12ⁱⁱⁱ—O32—O30^xviii	53.6 (7)
O18^vi—O9—O20	66.6 (9)	O17—O32—O17ⁱ	93.5 (11)
O18^vi—O9—O29^v	139.0 (8)	O17—O32—O30^xviii	111.3 (6)
O19ⁱⁱ—O9—O20	123.5 (7)	O17ⁱ—O32—O30^xviii	111.3 (6)
O19ⁱⁱ—O9—O29^v	86.0 (6)

Symmetry codes: (i) x, −y+1, z; (ii) x−1/2, −y+3/2, z; (iii) x+1/2, −y+3/2, z; (iv) x, y+1, z; (v) x−1/2, y+1/2, z; (vi) x−1/2, y+1/2, z−1; (vii) x, y, z−1; (viii) x−1/2, y−1/2, z−1; (ix) x+1/2, y−1/2, z; (x) x−1/2, y−1/2, z; (xi) x+1/2, y−1/2, z+1; (xii) x, −y, z; (xiii) x, y−1, z; (xiv) x−1/2, −y+1/2, z; (xv) x, y, z+1; (xvi) x, −y, z+1; (xvii) x, −y+2, z; (xviii) x+1/2, y+1/2, z; (xix) x+1/2, −y+1/2, z+1; (xx) x+1/2, −y+1/2, z; (xxi) x+1/2, y+1/2, z+1; (xxii) x+1, y, z+1; (xxiii) x+1/2, −y+3/2, z+1; (xxiv) x+1, y, z; (xxv) x−1, y, z−1; (xxvi) x−1, y, z; (xxvii) x−1/2, −y+3/2, z−1; (xxviii) x−1/2, −y+1/2, z−1; (xxix) x, −y, z−1.

(rameauite) top

Crystal data top

Ca₂K₄O₅₆U₁₂	F(000) = 3336
M_r = 1994.4	D_x = 5.442 Mg m⁻³
Monoclinic, Cc	Mo Kα radiation, λ = 0.71073 Å
Hall symbol: C -2yc	Cell parameters from 2314 reflections
a = 13.947 (3) Å	θ = 5.2–27.2°
b = 14.300 (3) Å	µ = 40.44 mm⁻¹
c = 13.888 (3) Å	T = 296 K
β = 118.50 (3)°	Tabular, orange
V = 2434.3 (11) Å³	0.09 × 0.06 × 0.03 mm
Z = 2

Data collection top

SuperNova, Dual, Cu at home/near, AtlasS2 diffractometer	3280 independent reflections
Radiation source: X-ray tube	2344 reflections with I > 3σ(I)
Mirror monochromator	R_int = 0.045
Detector resolution: 5.2027 pixels mm^-1	θ_max = 27.8°, θ_min = 5.2°
ω scans	h = −18→11
Absorption correction: multi-scan CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.	k = −18→18
T_min = 0.417, T_max = 1	l = −18→16
7145 measured reflections

Refinement top

Refinement on F²	2 constraints
Least-squares matrix: full	Primary atom site location: structure-invariant direct methods
R[F² > 2σ(F²)] = 0.042	Secondary atom site location: difference Fourier map
wR(F²) = 0.091	Weighting scheme based on measured s.u.'s w = 1/(σ²(I) + 0.000485I²)
S = 1.34	(Δ/σ)_max = 0.027
3280 reflections	Δρ_max = 5.41 e Å⁻³
196 parameters	Δρ_min = −7.11 e Å⁻³
0 restraints	Absolute structure: 610 of Friedel pairs used in the refinement

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å²) top

	x	y	z	U_iso*/U_eq
U1	0.2214 (11)	0.50151 (9)	0.1010 (10)	0.0168 (6)
U2	0.0881 (11)	0.52239 (9)	0.2828 (10)	0.0196 (6)
U3	0.2102 (11)	0.00417 (9)	0.0935 (10)	0.0173 (5)
U4	0.4099 (11)	0.51689 (10)	0.4037 (10)	0.0173 (5)
U5	0.0692 (11)	−0.01326 (10)	0.2565 (10)	0.0170 (6)
U6	0.9025 (11)	0.51586 (10)	0.9074 (10)	0.0185 (6)
Ca1	0.0961 (13)	0.2526 (6)	0.1526 (12)	0.031 (3)
K1	0.2419 (13)	0.7507 (6)	0.2578 (12)	0.035 (3)
O1	0.200 (2)	0.3786 (16)	0.123 (2)	0.027 (6)*
O2	0.076 (2)	0.5070 (19)	0.429 (2)	0.026 (6)*
O3	0.092 (2)	0.6491 (13)	0.297 (2)	0.015 (4)*
K2	0.0953 (14)	0.7511 (7)	0.9147 (13)	0.037 (4)
O4	0.395 (2)	0.4876 (16)	0.2248 (19)	0.023 (6)*
O5	0.579 (2)	0.5040 (17)	0.9191 (19)	0.019 (5)*
O6	0.539 (2)	0.5270 (17)	0.584 (2)	0.018 (5)*
O7	0.038 (2)	0.5519 (17)	0.0945 (19)	0.024 (5)*
O8	0.238 (2)	0.5312 (18)	0.266 (2)	0.026 (6)*
O9	0.899 (2)	0.5389 (17)	0.236 (2)	0.024 (6)*
O10	0.028 (2)	0.747 (2)	0.084 (2)	0.033 (7)*
O11	0.283 (2)	0.5487 (17)	0.4747 (19)	0.031 (5)*
O12	0.240 (2)	0.623 (2)	0.082 (2)	0.037 (7)*
O13	0.892 (3)	0.396 (2)	0.942 (3)	0.052 (9)*
O14	0.419 (2)	0.8612 (14)	0.3798 (19)	0.015 (5)*
O15	0.735 (2)	0.518 (2)	0.763 (2)	0.038 (7)*
O16	0.081 (2)	0.3996 (17)	0.258 (2)	0.029 (7)*
O17	0.191 (2)	0.1289 (15)	0.110 (2)	0.022 (5)*
O18	0.073 (2)	0.1140 (14)	0.250 (2)	0.018 (5)*
O19	0.393 (3)	0.3907 (17)	0.420 (2)	0.031 (6)*
O20	0.253 (3)	0.2505 (17)	0.334 (3)	0.033 (6)*
O21	0.049 (3)	0.2527 (18)	−0.039 (2)	0.041 (8)*
O22	−0.111 (3)	0.7486 (18)	0.217 (3)	0.035 (7)*
O23	0.244 (2)	−0.1166 (19)	0.087 (2)	0.020 (6)*
O24	0.422 (2)	0.6448 (16)	0.391 (2)	0.031 (6)*
O25	0.073 (2)	−0.1438 (15)	0.2669 (18)	0.024 (6)*
O26	0.795 (2)	0.5542 (16)	0.9874 (19)	0.028 (5)*
O27	−0.231 (2)	0.7514 (19)	−0.018 (2)	0.035 (7)*
O28	−0.086 (3)	0.254 (2)	0.127 (3)	0.055 (8)*

Atomic displacement parameters (Å²) top

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
U1	0.0183 (9)	0.0148 (7)	0.0153 (7)	0.0007 (6)	0.0064 (6)	0.0014 (6)
U2	0.0287 (9)	0.0134 (8)	0.0201 (7)	0.0026 (6)	0.0144 (6)	0.0017 (5)
U3	0.0218 (8)	0.0141 (7)	0.0149 (6)	−0.0010 (6)	0.0079 (5)	−0.0010 (5)
U4	0.0188 (7)	0.0155 (8)	0.0164 (7)	0.0007 (6)	0.0073 (5)	−0.0012 (6)
U5	0.0243 (9)	0.0112 (7)	0.0175 (7)	−0.0013 (7)	0.0116 (6)	−0.0012 (6)
U6	0.0191 (8)	0.0158 (8)	0.0178 (7)	−0.0010 (6)	0.0067 (6)	−0.0002 (6)
Ca1	0.047 (4)	0.016 (4)	0.038 (4)	−0.001 (4)	0.025 (4)	0.000 (3)
K1	0.034 (5)	0.025 (4)	0.031 (4)	0.000 (4)	0.002 (4)	−0.004 (3)
K2	0.048 (5)	0.034 (5)	0.031 (4)	0.004 (4)	0.020 (4)	0.002 (4)

Geometric parameters (Å, º) top

U1—U2	3.79 (2)	O4—O6ⁱ	3.42 (5)
U1—U2ⁱ	3.905 (18)	O4—O8	2.59 (5)
U1—U4	3.758 (16)	O4—O11ⁱ	3.10 (4)
U1—U6ⁱⁱ	3.957 (16)	O4—O12	2.87 (3)
U1—O1	1.83 (3)	O4—O18^viii	2.95 (4)
U1—O2ⁱ	2.28 (2)	O4—O19	3.05 (5)
U1—O4	2.21 (2)	O4—O22^xiii	3.42 (4)
U1—O7	2.61 (3)	O4—O24	3.11 (4)
U1—O8	2.23 (3)	O4—O25^viii	2.95 (4)
U1—O11ⁱ	2.40 (4)	O5—O6^xii	2.64 (5)
U1—O12	1.80 (3)	O5—O15	3.74 (5)
U1—O16	3.84 (4)	O5—O17^xx	2.95 (4)
U2—U4	3.975 (19)	O5—O18^xxi	2.86 (4)
U2—U6ⁱⁱⁱ	3.78 (2)	O5—O19^xii	3.00 (5)
U2—O1	3.86 (4)	O5—O21^xx	3.66 (4)
U2—O2	2.12 (4)	O5—O23^xx	2.93 (3)
U2—O3	1.819 (15)	O5—O24^xii	2.95 (4)
U2—O7	2.41 (3)	O5—O25^xxi	2.88 (4)
U2—O8	2.22 (4)	O5—O26	2.79 (4)
U2—O9^iv	2.41 (3)	O6—O10^ix	3.24 (4)
U2—O11	2.78 (2)	O6—O11	3.16 (4)
U2—O14^v	3.97 (3)	O6—O15	2.68 (3)
U2—O16	1.78 (3)	O6—O17^xxi	2.98 (4)
U3—U4^vi	3.745 (16)	O6—O18^xxi	2.93 (4)
U3—U5	3.65 (2)	O6—O19	2.95 (4)
U3—U6^vi	3.878 (16)	O6—O23^xxi	3.12 (4)
U3—O5^vii	2.24 (2)	O6—O24	2.92 (4)
U3—O6^vi	2.36 (3)	O6—O25^xxi	2.89 (4)
U3—O9^v	2.47 (2)	O7—O8	2.69 (3)
U3—O15^vi	2.22 (3)	O7—O9^iv	3.37 (5)
U3—O17	1.83 (3)	O7—O10	2.79 (4)
U3—O18	3.84 (4)	O7—O12	3.07 (4)
U3—O23	1.81 (3)	O7—O13ⁱⁱ	3.08 (4)
U3—O26^vii	2.41 (4)	O7—O14^xiv	2.90 (3)
U4—U5^viii	3.69 (2)	O7—O16	2.99 (4)
U4—O4	2.43 (3)	O7—O26ⁱⁱ	2.98 (4)
U4—O5ⁱ	2.28 (3)	O8—O11	2.67 (4)
U4—O6	2.28 (2)	O8—O12	2.89 (4)
U4—O8	2.25 (2)	O8—O16	2.84 (4)
U4—O11	2.45 (4)	O8—O19	2.97 (4)
U4—O19	1.84 (3)	O8—O24	2.83 (3)
U4—O24	1.86 (3)	O9—O13ⁱ	3.05 (5)
U5—O4^v	2.25 (3)	O9—O14^xiii	3.17 (4)
U5—O5^vi	2.19 (3)	O9—O15ⁱ	2.62 (4)
U5—O6^vi	2.24 (3)	O9—O16^xxii	3.12 (4)
U5—O15^vi	2.28 (3)	O9—O17^viii	2.88 (3)
U5—O17	3.81 (4)	O9—O22^xxii	3.01 (4)
U5—O18	1.825 (15)	O9—O23^viii	3.11 (4)
U5—O25	1.87 (3)	O9—O26^xxiii	3.05 (4)
U5—O26^vi	3.30 (2)	O10—O12	3.46 (4)
U6—K1^ix	3.999 (11)	O10—O14^xiv	2.93 (3)
U6—O2^x	2.32 (3)	O10—O22	3.25 (6)
U6—O7^xi	2.43 (2)	O10—O23^xv	3.57 (4)
U6—O9^xii	2.48 (3)	O10—O24^xiv	2.82 (4)
U6—O10^xi	3.99 (3)	O10—O25^xv	2.79 (4)
U6—O13	1.81 (3)	O10—O26ⁱⁱ	3.98 (4)
U6—O14^ix	1.839 (18)	O10—O27	3.19 (4)
U6—O15	2.23 (2)	O11—O12^xii	3.08 (4)
U6—O26	2.31 (4)	O11—O16	3.67 (3)
Ca1—O1	2.47 (3)	O11—O19	3.03 (5)
Ca1—K2ⁱ	3.65 (2)	O11—O24	3.03 (5)
Ca1—O13ⁱⁱ	3.60 (3)	O11—O27^ix	2.87 (4)
Ca1—O16	2.63 (3)	O12—O14^xiv	4.00 (3)
Ca1—O17	2.45 (3)	O12—O16ⁱ	3.97 (3)
Ca1—O18	2.50 (3)	O12—O19ⁱ	3.77 (5)
Ca1—O19^vi	3.74 (3)	O12—O20ⁱ	3.97 (5)
Ca1—O20	2.42 (3)	O12—O23^xv	3.72 (4)
Ca1—O21	2.42 (3)	O12—O24	3.82 (3)
Ca1—O22^xiii	3.75 (4)	O12—O28^viii	2.89 (5)
Ca1—O28	2.39 (5)	O13—O14^ix	3.64 (4)
K1—O3	2.80 (3)	O13—O15	2.97 (4)
K1—O7	3.90 (3)	O13—O16^xi	3.90 (4)
K1—O8	3.15 (3)	O13—O18^xxi	3.95 (4)
K1—O10	2.81 (2)	O13—O20^xxi	2.77 (4)
K1—O12	3.04 (3)	O13—O21^xi	2.91 (5)
K1—O14	2.73 (2)	O13—O22^x	3.73 (6)
K1—O15^xiv	3.31 (3)	O13—O23^xx	3.51 (6)
K1—O23^xv	3.05 (3)	O13—O26	2.85 (5)
K1—O24	2.75 (3)	O13—O28^xi	3.17 (5)
K1—O25^xv	2.85 (3)	O14—O15^xiv	2.87 (3)
K1—O27^ix	2.95 (3)	O14—O16^viii	3.46 (5)
K1—O28^viii	3.64 (5)	O14—O23^xv	3.62 (3)
O1—O2ⁱ	2.91 (3)	O14—O24	3.09 (3)
O1—O4	2.86 (4)	O14—O26^xiv	3.02 (5)
O1—O7	3.24 (4)	O14—O27^ix	3.43 (4)
O1—O8	2.82 (4)	O14—O28^viii	3.80 (5)
O1—O11ⁱ	2.98 (5)	O15—O17^xxi	2.84 (4)
O1—O12	3.62 (4)	O15—O18^xxi	2.88 (4)
O1—O13ⁱⁱ	3.81 (4)	O15—O20^xxi	3.95 (4)
O1—O16	3.05 (5)	O15—O23^xxi	2.88 (4)
O1—O17	3.58 (4)	O15—O25^xxi	2.91 (4)
O1—O19	3.70 (3)	O15—O26	2.86 (4)
O1—O20	3.23 (5)	O16—O19	3.83 (4)
O1—O21	2.87 (4)	O16—O20	3.00 (4)
O1—O22^xiii	2.97 (4)	O16—O28	3.01 (4)
O1—O27^xiii	3.15 (5)	O17—O18	3.10 (5)
O2—O3	2.82 (4)	O17—O19^vi	3.72 (4)
O2—K2ⁱ	3.71 (3)	O17—O20	3.30 (5)
O2—O7^xii	2.72 (5)	O17—O21	2.73 (4)
O2—O8	3.90 (5)	O17—O22^xiii	2.98 (4)
O2—O9^iv	2.68 (3)	O17—O23	3.64 (4)
O2—O11	2.71 (4)	O17—O26^vii	2.92 (5)
O2—O12^xii	2.93 (3)	O17—O27^xiii	3.04 (5)
O2—O13ⁱⁱⁱ	3.00 (5)	O18—O20	2.95 (4)
O2—O14^v	2.86 (4)	O18—O24^v	3.52 (5)
O2—O16	2.85 (4)	O18—O25	3.70 (3)
O2—O21^xii	3.50 (4)	O18—O28	2.87 (4)
O3—O7	2.90 (4)	O19—O20	2.65 (4)
O3—O8	2.83 (4)	O19—O21^xxi	2.85 (5)
O3—O9^iv	2.87 (4)	O19—O22^xiii	3.45 (5)
O3—O10	3.00 (4)	O19—O24	3.70 (4)
O3—O11	2.99 (3)	O19—O28^xxi	3.44 (5)
O3—O16	3.59 (3)	O20—O21^xxi	3.63 (5)
O3—O21^xii	2.97 (5)	O20—O22^xiii	3.03 (7)
O3—O22	2.88 (4)	O20—O28^xxi	3.59 (5)
O3—O25^xv	2.98 (3)	O21—O22ⁱ	3.04 (4)
O3—O27^ix	2.95 (3)	O21—O25^xxiv	3.27 (5)
K2—O5^xvi	3.63 (3)	O21—O27^xiii	2.94 (5)
K2—O10^xvii	2.91 (4)	O21—O28	3.61 (7)
K2—O12^xvii	2.89 (3)	O22—O25^xv	2.78 (5)
K2—O14^xviii	2.77 (3)	O22—O26ⁱⁱ	3.96 (4)
K2—O16^xii	3.01 (3)	O22—O27	2.87 (4)
K2—O18^xii	2.90 (3)	O23—O26^vii	3.06 (4)
K2—O20^xii	2.91 (5)	O23—O28^xiii	2.84 (5)
K2—O23^xix	2.97 (3)	O24—O27^ix	3.31 (5)
K2—O24^xviii	2.72 (3)	O24—O28^viii	3.94 (5)
K2—O28^xx	4.00 (3)	O25—O26^vi	3.40 (3)
K2—O28^xii	3.57 (4)	O25—O27^xxi	3.31 (3)
O4—O5ⁱ	2.69 (3)	O26—O27^xi	2.84 (4)

U2—U1—U2ⁱ	129.9 (4)	O2ⁱ—O12—O8	91.1 (11)
U2—U1—U4	63.5 (4)	O2ⁱ—O12—O10	87.5 (10)
U2—U1—U6ⁱⁱ	72.6 (4)	O2ⁱ—O12—O11ⁱ	53.6 (9)
U2—U1—O1	78.2 (12)	O2ⁱ—O12—O14^xiv	45.7 (7)
U2—U1—O2ⁱ	103.4 (10)	O2ⁱ—O12—O16ⁱ	45.9 (8)
U2—U1—O4	101.0 (10)	O2ⁱ—O12—O19ⁱ	90.1 (11)
U2—U1—O7	39.0 (6)	O2ⁱ—O12—O20ⁱ	90.1 (10)
U2—U1—O8	31.4 (7)	O2ⁱ—O12—O23^xv	130.4 (9)
U2—U1—O11ⁱ	165.7 (7)	O2ⁱ—O12—O24	137.6 (12)
U2—U1—O12	100.1 (12)	O2ⁱ—O12—O28^viii	148.7 (16)
U2—U1—O16	26.9 (5)	K2^xxiii—O12—O4	171.5 (15)
U2ⁱ—U1—U4	166.6 (6)	K2^xxiii—O12—O7	86.8 (9)
U2ⁱ—U1—U6ⁱⁱ	57.4 (3)	K2^xxiii—O12—O8	134.5 (13)
U2ⁱ—U1—O1	94.5 (9)	K2^xxiii—O12—O10	53.7 (7)
U2ⁱ—U1—O2ⁱ	26.5 (9)	K2^xxiii—O12—O11ⁱ	110.0 (10)
U2ⁱ—U1—O4	128.7 (11)	K2^xxiii—O12—O14^xiv	43.9 (5)
U2ⁱ—U1—O7	93.1 (6)	K2^xxiii—O12—O16ⁱ	49.0 (6)
U2ⁱ—U1—O8	160.0 (9)	K2^xxiii—O12—O19ⁱ	86.2 (9)
U2ⁱ—U1—O11ⁱ	44.9 (6)	K2^xxiii—O12—O20ⁱ	47.1 (8)
U2ⁱ—U1—O12	86.7 (9)	K2^xxiii—O12—O23^xv	51.7 (6)
U2ⁱ—U1—O16	120.9 (5)	K2^xxiii—O12—O24	133.3 (11)
U4—U1—U6ⁱⁱ	136.0 (6)	K2^xxiii—O12—O28^viii	87.5 (10)
U4—U1—O1	87.2 (8)	O4—O12—O7	98.5 (12)
U4—U1—O2ⁱ	166.9 (11)	O4—O12—O8	53.4 (10)
U4—U1—O4	37.9 (9)	O4—O12—O10	134.7 (14)
U4—U1—O7	100.2 (7)	O4—O12—O11ⁱ	62.7 (9)
U4—U1—O8	33.3 (7)	O4—O12—O14^xiv	138.2 (11)
U4—U1—O11ⁱ	121.9 (7)	O4—O12—O16ⁱ	123.9 (12)
U4—U1—O12	92.0 (8)	O4—O12—O19ⁱ	85.6 (11)
U4—U1—O16	70.2 (5)	O4—O12—O20ⁱ	125.1 (13)
U6ⁱⁱ—U1—O1	86.9 (8)	O4—O12—O23^xv	131.3 (9)
U6ⁱⁱ—U1—O2ⁱ	31.0 (9)	O4—O12—O24	53.2 (8)
U6ⁱⁱ—U1—O4	173.2 (11)	O4—O12—O28^viii	90.5 (10)
U6ⁱⁱ—U1—O7	36.7 (6)	O7—O12—O8	53.5 (9)
U6ⁱⁱ—U1—O8	102.9 (9)	O7—O12—O10	50.2 (9)
U6ⁱⁱ—U1—O11ⁱ	101.4 (6)	O7—O12—O11ⁱ	99.0 (11)
U6ⁱⁱ—U1—O12	92.7 (8)	O7—O12—O14^xiv	46.2 (7)
U6ⁱⁱ—U1—O16	72.2 (5)	O7—O12—O16ⁱ	90.2 (8)
O1—U1—O2ⁱ	89.5 (10)	O7—O12—O19ⁱ	144.0 (10)
O1—U1—O4	89.4 (11)	O7—O12—O20ⁱ	128.3 (9)
O1—U1—O7	92.3 (13)	O7—O12—O23^xv	109.6 (11)
O1—U1—O8	87.5 (13)	O7—O12—O24	95.8 (10)
O1—U1—O11ⁱ	88.6 (13)	O7—O12—O28^viii	154.2 (15)
O1—U1—O12	178.3 (18)	O8—O12—O10	81.8 (11)
O1—U1—O16	51.4 (12)	O8—O12—O11ⁱ	98.6 (12)
O2ⁱ—U1—O4	154.8 (14)	O8—O12—O14^xiv	99.6 (10)
O2ⁱ—U1—O7	67.2 (10)	O8—O12—O16ⁱ	136.9 (11)
O2ⁱ—U1—O8	133.9 (13)	O8—O12—O19ⁱ	138.7 (11)
O2ⁱ—U1—O11ⁱ	70.6 (10)	O8—O12—O20ⁱ	178.2 (11)
O2ⁱ—U1—O12	91.0 (10)	O8—O12—O23^xv	116.5 (12)
O2ⁱ—U1—O16	97.9 (10)	O8—O12—O24	47.5 (7)
O4—U1—O7	138.0 (12)	O8—O12—O28^viii	117.8 (11)
O4—U1—O8	71.2 (11)	O10—O12—O11ⁱ	141.1 (10)
O4—U1—O11ⁱ	84.2 (11)	O10—O12—O14^xiv	45.6 (6)
O4—U1—O12	90.9 (11)	O10—O12—O16ⁱ	92.0 (8)
O4—U1—O16	101.0 (10)	O10—O12—O19ⁱ	139.5 (10)
O7—U1—O8	66.9 (9)	O10—O12—O20ⁱ	99.6 (10)
O7—U1—O11ⁱ	137.9 (9)	O10—O12—O23^xv	59.5 (8)
O7—U1—O12	86.4 (12)	O10—O12—O24	93.5 (9)
O7—U1—O16	51.1 (8)	O10—O12—O28^viii	107.4 (12)
O8—U1—O11ⁱ	155.1 (10)	O11ⁱ—O12—O14^xiv	96.8 (8)
O8—U1—O12	91.0 (13)	O11ⁱ—O12—O16ⁱ	61.2 (7)
O8—U1—O16	47.2 (9)	O11ⁱ—O12—O19ⁱ	51.2 (9)
O11ⁱ—U1—O12	93.1 (14)	O11ⁱ—O12—O20ⁱ	81.0 (10)
O11ⁱ—U1—O16	139.2 (8)	O11ⁱ—O12—O23^xv	143.5 (13)
O12—U1—O16	126.9 (13)	O11ⁱ—O12—O24	115.5 (9)
U1—U2—U1^xii	128.9 (4)	O11ⁱ—O12—O28^viii	106.6 (14)
U1—U2—U4	57.8 (3)	O14^xiv—O12—O16ⁱ	51.4 (7)
U1—U2—U6ⁱⁱⁱ	162.4 (3)	O14^xiv—O12—O19ⁱ	110.3 (9)
U1—U2—O1	27.6 (5)	O14^xiv—O12—O20ⁱ	82.2 (8)
U1—U2—O2	156.1 (8)	O14^xiv—O12—O23^xv	87.6 (7)
U1—U2—O3	98.6 (12)	O14^xiv—O12—O24	134.9 (11)
U1—U2—O7	42.9 (8)	O14^xiv—O12—O28^viii	131.2 (11)
U1—U2—O8	31.5 (7)	O16ⁱ—O12—O19ⁱ	59.2 (7)
U1—U2—O9^iv	130.4 (8)	O16ⁱ—O12—O20ⁱ	44.4 (7)
U1—U2—O11	94.8 (8)	O16ⁱ—O12—O23^xv	95.7 (8)
U1—U2—O14^v	137.7 (4)	O16ⁱ—O12—O24	173.6 (11)
U1—U2—O16	77.9 (12)	O16ⁱ—O12—O28^viii	104.9 (13)
U1^xii—U2—U4	71.9 (4)	O19ⁱ—O12—O20ⁱ	39.9 (8)
U1^xii—U2—U6ⁱⁱⁱ	62.0 (4)	O19ⁱ—O12—O23^xv	93.2 (10)
U1^xii—U2—O1	120.0 (4)	O19ⁱ—O12—O24	114.4 (9)
U1^xii—U2—O2	28.7 (7)	O19ⁱ—O12—O28^viii	60.5 (12)
U1^xii—U2—O3	89.6 (9)	O20ⁱ—O12—O23^xv	63.6 (8)
U1^xii—U2—O7	169.0 (8)	O20ⁱ—O12—O24	131.1 (10)
U1^xii—U2—O8	99.3 (7)	O20ⁱ—O12—O28^viii	60.8 (11)
U1^xii—U2—O9^iv	100.6 (9)	O23^xv—O12—O24	84.3 (8)
U1^xii—U2—O11	37.6 (7)	O23^xv—O12—O28^viii	49.0 (9)
U1^xii—U2—O14^v	66.6 (4)	O24—O12—O28^viii	70.4 (10)
U1^xii—U2—O16	95.0 (9)	U6—O13—Ca1^xi	128.9 (15)
U4—U2—U6ⁱⁱⁱ	133.5 (4)	U6—O13—O1^xi	91.8 (14)
U4—U2—O1	63.1 (4)	U6—O13—O2^x	50.7 (13)
U4—U2—O2	100.5 (7)	U6—O13—O7^xi	52.1 (9)
U4—U2—O3	90.2 (9)	U6—O13—O9^xii	54.4 (14)
U4—U2—O7	98.4 (9)	U6—O13—O14^ix	1.8 (7)
U4—U2—O8	27.5 (7)	U6—O13—O15	48.5 (9)
U4—U2—O9^iv	170.9 (8)	U6—O13—O16^xi	101.1 (13)
U4—U2—O11	37.5 (7)	U6—O13—O18^xxi	93.4 (12)
U4—U2—O14^v	125.4 (4)	U6—O13—O20^xxi	134.4 (17)
U4—U2—O16	90.5 (9)	U6—O13—O21^xi	123 (2)
U6ⁱⁱⁱ—U2—O1	137.8 (5)	U6—O13—O22^x	105.9 (19)
U6ⁱⁱⁱ—U2—O2	33.4 (7)	U6—O13—O23^xx	110.3 (19)
U6ⁱⁱⁱ—U2—O3	95.1 (12)	U6—O13—O26	54.0 (13)
U6ⁱⁱⁱ—U2—O7	128.1 (8)	U6—O13—O28^xi	147 (2)
U6ⁱⁱⁱ—U2—O8	160.9 (8)	Ca1^xi—O13—O1^xi	38.9 (6)
U6ⁱⁱⁱ—U2—O9^iv	40.2 (7)	Ca1^xi—O13—O2^x	86.9 (10)
U6ⁱⁱⁱ—U2—O11	98.8 (8)	Ca1^xi—O13—O7^xi	81.2 (8)
U6ⁱⁱⁱ—U2—O14^v	27.3 (4)	Ca1^xi—O13—O9^xii	124.8 (15)
U6ⁱⁱⁱ—U2—O16	87.7 (12)	Ca1^xi—O13—O14^ix	127.3 (10)
O1—U2—O2	137.1 (9)	Ca1^xi—O13—O15	176.0 (18)
O1—U2—O3	126.2 (13)	Ca1^xi—O13—O16^xi	40.8 (6)
O1—U2—O7	56.8 (8)	Ca1^xi—O13—O18^xxi	136.7 (11)
O1—U2—O8	46.1 (8)	Ca1^xi—O13—O20^xxi	94.9 (10)
O1—U2—O9^iv	126.0 (8)	Ca1^xi—O13—O21^xi	42.1 (7)
O1—U2—O11	98.4 (8)	Ca1^xi—O13—O22^x	93.1 (10)
O1—U2—O14^v	110.8 (6)	Ca1^xi—O13—O23^xx	87.4 (10)
O1—U2—O16	50.5 (12)	Ca1^xi—O13—O26	123.2 (14)
O2—U2—O3	90.8 (14)	Ca1^xi—O13—O28^xi	40.7 (9)
O2—U2—O7	160.8 (11)	O1^xi—O13—O2^x	48.8 (8)
O2—U2—O8	128.0 (10)	O1^xi—O13—O7^xi	54.9 (8)
O2—U2—O9^iv	72.2 (11)	O1^xi—O13—O9^xii	96.2 (14)
O2—U2—O11	65.5 (10)	O1^xi—O13—O14^ix	90.3 (10)
O2—U2—O14^v	44.4 (8)	O1^xi—O13—O15	137.6 (15)
O2—U2—O16	93.6 (14)	O1^xi—O13—O16^xi	46.7 (8)
O3—U2—O7	85.4 (12)	O1^xi—O13—O18^xxi	174.2 (10)
O3—U2—O8	88.5 (13)	O1^xi—O13—O20^xxi	125.9 (13)
O3—U2—O9^iv	84.5 (12)	O1^xi—O13—O21^xi	48.2 (9)
O3—U2—O11	78.2 (9)	O1^xi—O13—O22^x	94.3 (12)
O3—U2—O14^v	122.4 (13)	O1^xi—O13—O23^xx	113.9 (11)
O3—U2—O16	175.4 (15)	O1^xi—O13—O26	114.2 (11)
O7—U2—O8	70.8 (10)	O1^xi—O13—O28^xi	77.4 (10)
O7—U2—O9^iv	88.7 (10)	O2^x—O13—O7^xi	53.2 (10)
O7—U2—O11	131.5 (11)	O2^x—O13—O9^xii	52.5 (10)
O7—U2—O14^v	124.2 (8)	O2^x—O13—O14^ix	49.9 (9)
O7—U2—O16	90.0 (12)	O2^x—O13—O15	89.3 (13)
O8—U2—O9^iv	158.8 (11)	O2^x—O13—O16^xi	85.6 (10)
O8—U2—O11	63.5 (10)	O2^x—O13—O18^xxi	134.2 (12)
O8—U2—O14^v	144.3 (8)	O2^x—O13—O20^xxi	136 (2)
O8—U2—O16	90.0 (14)	O2^x—O13—O21^xi	72.7 (14)
O9^iv—U2—O11	133.7 (11)	O2^x—O13—O22^x	82.8 (14)
O9^iv—U2—O14^v	53.0 (8)	O2^x—O13—O23^xx	144.5 (13)
O9^iv—U2—O16	95.3 (12)	O2^x—O13—O26	99.0 (12)
O11—U2—O14^v	102.8 (8)	O2^x—O13—O28^xi	126.2 (13)
O11—U2—O16	105.0 (10)	O7^xi—O13—O9^xii	96.6 (13)
O14^v—U2—O16	60.5 (12)	O7^xi—O13—O14^ix	50.3 (7)
U4^vi—U3—U5	71.3 (4)	O7^xi—O13—O15	97.5 (11)
U4^vi—U3—U6^vi	136.5 (6)	O7^xi—O13—O16^xi	49.2 (8)
U4^vi—U3—O5^vii	34.5 (9)	O7^xi—O13—O18^xxi	130.7 (12)
U4^vi—U3—O6^vi	35.6 (7)	O7^xi—O13—O20^xxi	170 (2)
U4^vi—U3—O9^v	170.0 (9)	O7^xi—O13—O21^xi	102.9 (13)
U4^vi—U3—O15^vi	107.0 (9)	O7^xi—O13—O22^x	135.7 (18)
U4^vi—U3—O17	89.2 (8)	O7^xi—O13—O23^xx	91.3 (13)
U4^vi—U3—O18	75.0 (5)	O7^xi—O13—O26	60.2 (9)
U4^vi—U3—O23	96.8 (8)	O7^xi—O13—O28^xi	97.6 (12)
U4^vi—U3—O26^vii	107.6 (6)	O9^xii—O13—O14^ix	55.6 (9)
U5—U3—U6^vi	65.6 (4)	O9^xii—O13—O15	51.5 (10)
U5—U3—O5^vii	105.7 (10)	O9^xii—O13—O16^xi	138.1 (14)
U5—U3—O6^vi	36.5 (7)	O9^xii—O13—O18^xxi	84.7 (9)
U5—U3—O9^v	101.8 (9)	O9^xii—O13—O20^xxi	92.9 (15)
U5—U3—O15^vi	36.4 (8)	O9^xii—O13—O21^xi	86.6 (16)
U5—U3—O17	80.8 (12)	O9^xii—O13—O22^x	51.5 (10)
U5—U3—O18	28.1 (3)	O9^xii—O13—O23^xx	147.6 (13)
U5—U3—O23	101.6 (12)	O9^xii—O13—O26	101.2 (12)
U5—U3—O26^vii	166.6 (7)	O9^xii—O13—O28^xi	156.9 (16)
U6^vi—U3—O5^vii	170.6 (10)	O14^ix—O13—O15	50.2 (8)
U6^vi—U3—O6^vi	100.9 (8)	O14^ix—O13—O16^xi	99.3 (9)
U6^vi—U3—O9^v	38.6 (8)	O14^ix—O13—O18^xxi	94.9 (8)
U6^vi—U3—O15^vi	29.6 (7)	O14^ix—O13—O20^xxi	136.2 (13)
U6^vi—U3—O17	89.9 (8)	O14^ix—O13—O21^xi	122.2 (17)
U6^vi—U3—O18	70.2 (4)	O14^ix—O13—O22^x	107.0 (14)
U6^vi—U3—O23	86.0 (8)	O14^ix—O13—O23^xx	110.0 (12)
U6^vi—U3—O26^vii	115.7 (7)	O14^ix—O13—O26	53.8 (10)
O5^vii—U3—O6^vi	70.0 (11)	O14^ix—O13—O28^xi	145.2 (14)
O5^vii—U3—O9^v	150.8 (13)	O15—O13—O16^xi	140.1 (13)
O5^vii—U3—O15^vi	141.4 (13)	O15—O13—O18^xxi	46.6 (8)
O5^vii—U3—O17	92.4 (10)	O15—O13—O20^xxi	86.9 (12)
O5^vii—U3—O18	104.2 (10)	O15—O13—O21^xi	135.2 (19)
O5^vii—U3—O23	92.3 (11)	O15—O13—O22^x	85.2 (12)
O5^vii—U3—O26^vii	73.6 (11)	O15—O13—O23^xx	96.4 (14)
O6^vi—U3—O9^v	138.2 (12)	O15—O13—O26	58.7 (10)
O6^vi—U3—O15^vi	71.4 (10)	O15—O13—O28^xi	143.3 (19)
O6^vi—U3—O17	89.5 (13)	O16^xi—O13—O18^xxi	134.4 (15)
O6^vi—U3—O18	49.5 (8)	O16^xi—O13—O20^xxi	123.0 (15)
O6^vi—U3—O23	95.7 (12)	O16^xi—O13—O21^xi	80.4 (9)
O6^vi—U3—O26^vii	143.0 (9)	O16^xi—O13—O22^x	133.0 (11)
O9^v—U3—O15^vi	67.5 (11)	O16^xi—O13—O23^xx	67.8 (10)
O9^v—U3—O17	82.4 (10)	O16^xi—O13—O26	83.0 (11)
O9^v—U3—O18	95.5 (9)	O16^xi—O13—O28^xi	49.1 (9)
O9^v—U3—O23	91.6 (10)	O18^xxi—O13—O20^xxi	48.3 (9)
O9^v—U3—O26^vii	77.4 (10)	O18^xxi—O13—O21^xi	126.2 (11)
O15^vi—U3—O17	88.3 (13)	O18^xxi—O13—O22^x	81.7 (9)
O15^vi—U3—O18	48.2 (8)	O18^xxi—O13—O23^xx	66.7 (9)
O15^vi—U3—O23	90.4 (12)	O18^xxi—O13—O26	71.2 (9)
O15^vi—U3—O26^vii	144.8 (10)	O18^xxi—O13—O28^xi	99.6 (13)
O17—U3—O18	52.7 (12)	O20^xxi—O13—O21^xi	79.5 (13)
O17—U3—O23	174.0 (13)	O20^xxi—O13—O22^x	53.1 (14)
O17—U3—O26^vii	85.9 (13)	O20^xxi—O13—O23^xx	79.6 (16)
O18—U3—O23	129.4 (13)	O20^xxi—O13—O26	116.0 (18)
O18—U3—O26^vii	138.6 (7)	O20^xxi—O13—O28^xi	74.0 (13)
O23—U3—O26^vii	91.8 (14)	O21^xi—O13—O22^x	52.7 (9)
U1—U4—U2	58.7 (4)	O21^xi—O13—O23^xx	122.2 (14)
U1—U4—U3^xxi	137.3 (6)	O21^xi—O13—O26	161.9 (13)
U1—U4—U5^viii	70.1 (4)	O21^xi—O13—O28^xi	72.5 (12)
U1—U4—O4	34.1 (7)	O22^x—O13—O23^xx	132.5 (12)
U1—U4—O5ⁱ	103.7 (8)	O22^x—O13—O26	143.7 (12)
U1—U4—O6	174.2 (11)	O22^x—O13—O28^xi	106.3 (12)
U1—U4—O8	32.8 (9)	O23^xx—O13—O26	56.3 (12)
U1—U4—O11	101.9 (6)	O23^xx—O13—O28^xi	50.0 (11)
U1—U4—O19	90.9 (8)	O26—O13—O28^xi	101.7 (18)
U1—U4—O24	89.8 (8)	U2^viii—O14—U6^xiv	70.6 (9)
U2—U4—U3^xxi	163.1 (6)	U2^viii—O14—K1	129.3 (10)
U2—U4—U5^viii	128.7 (4)	U2^viii—O14—O2^viii	31.3 (7)
U2—U4—O4	92.4 (7)	U2^viii—O14—K2^xxv	77.1 (8)
U2—U4—O5ⁱ	161.7 (8)	U2^viii—O14—O7^ix	87.5 (8)
U2—U4—O6	127.1 (10)	U2^viii—O14—O9^xvi	37.4 (6)
U2—U4—O8	27.0 (9)	U2^viii—O14—O10^ix	121.1 (9)
U2—U4—O11	43.7 (6)	U2^viii—O14—O12^ix	63.7 (6)
U2—U4—O19	83.4 (13)	U2^viii—O14—O13^xiv	70.8 (8)
U2—U4—O24	94.3 (9)	U2^viii—O14—O15^xiv	88.4 (8)
U3^xxi—U4—U5^viii	67.4 (4)	U2^viii—O14—O16^viii	26.6 (5)
U3^xxi—U4—O4	103.2 (8)	U2^viii—O14—O23^xv	76.1 (7)
U3^xxi—U4—O5ⁱ	33.7 (7)	U2^viii—O14—O24	127.0 (11)
U3^xxi—U4—O6	37.1 (9)	U2^viii—O14—O26^xiv	120.4 (7)
U3^xxi—U4—O8	169.8 (11)	U2^viii—O14—O27^ix	171.9 (9)
U3^xxi—U4—O11	120.8 (7)	U2^viii—O14—O28^viii	70.9 (8)
U3^xxi—U4—O19	90.1 (11)	U6^xiv—O14—K1	120.9 (12)
U3^xxi—U4—O24	91.5 (8)	U6^xiv—O14—O2^viii	54.0 (9)
U5^viii—U4—O4	36.3 (7)	U6^xiv—O14—K2^xxv	135.0 (12)
U5^viii—U4—O5ⁱ	33.7 (7)	U6^xiv—O14—O7^ix	56.4 (8)
U5^viii—U4—O6	104.2 (10)	U6^xiv—O14—O9^xvi	51.5 (9)
U5^viii—U4—O8	102.5 (10)	U6^xiv—O14—O10^ix	111.4 (13)
U5^viii—U4—O11	170.9 (7)	U6^xiv—O14—O12^ix	90.7 (9)
U5^viii—U4—O19	95.6 (14)	U6^xiv—O14—O13^xiv	1.7 (7)
U5^viii—U4—O24	87.5 (12)	U6^xiv—O14—O15^xiv	51.0 (8)
O4—U4—O5ⁱ	69.7 (10)	U6^xiv—O14—O16^viii	97.1 (12)
O4—U4—O6	140.3 (12)	U6^xiv—O14—O23^xv	93.6 (9)
O4—U4—O8	66.9 (11)	U6^xiv—O14—O24	161.2 (18)
O4—U4—O11	136.0 (9)	U6^xiv—O14—O26^xiv	49.8 (11)
O4—U4—O19	90.2 (13)	U6^xiv—O14—O27^ix	101.5 (15)
O4—U4—O24	92.1 (13)	U6^xiv—O14—O28^viii	128.8 (13)
O5ⁱ—U4—O6	70.7 (11)	K1—O14—O2^viii	158.6 (11)
O5ⁱ—U4—O8	136.2 (13)	K1—O14—K2^xxv	103.7 (7)
O5ⁱ—U4—O11	154.4 (10)	K1—O14—O7^ix	142.0 (15)
O5ⁱ—U4—O19	92.7 (16)	K1—O14—O9^xvi	106.9 (8)
O5ⁱ—U4—O24	90.1 (13)	K1—O14—O10^ix	101.2 (9)
O6—U4—O8	152.6 (14)	K1—O14—O12^ix	147.8 (7)
O6—U4—O11	83.7 (11)	K1—O14—O13^xiv	122.2 (10)
O6—U4—O19	90.5 (11)	K1—O14—O15^xiv	72.4 (8)
O6—U4—O24	89.1 (10)	K1—O14—O16^viii	113.4 (10)
O8—U4—O11	69.2 (11)	K1—O14—O23^xv	55.1 (7)
O8—U4—O19	92.5 (12)	K1—O14—O24	56.0 (5)
O8—U4—O24	86.4 (10)	K1—O14—O26^xiv	88.7 (10)
O11—U4—O19	88.6 (16)	K1—O14—O27^ix	55.8 (7)
O11—U4—O24	88.3 (13)	K1—O14—O28^viii	65.3 (8)
O19—U4—O24	177 (2)	O2^viii—O14—K2^xxv	82.4 (10)
U3—U5—U4^v	168.69 (14)	O2^viii—O14—O7^ix	56.3 (9)
U3—U5—O4^v	136.7 (8)	O2^viii—O14—O9^xvi	52.5 (7)
U3—U5—O5^vi	147.6 (8)	O2^viii—O14—O10^ix	99.7 (9)
U3—U5—O6^vi	38.8 (8)	O2^viii—O14—O12^ix	47.0 (7)
U3—U5—O15^vi	35.4 (7)	O2^viii—O14—O13^xiv	53.2 (10)
U3—U5—O17	28.4 (5)	O2^viii—O14—O15^xiv	94.1 (9)
U3—U5—O18	81.9 (12)	O2^viii—O14—O16^viii	52.7 (9)
U3—U5—O25	96.2 (12)	O2^viii—O14—O23^xv	103.4 (10)
U3—U5—O26^vi	93.7 (7)	O2^viii—O14—O24	136.6 (12)
U4^v—U5—O4^v	39.7 (8)	O2^viii—O14—O26^xiv	98.2 (10)
U4^v—U5—O5^vi	35.4 (7)	O2^viii—O14—O27^ix	142.2 (12)
U4^v—U5—O6^vi	138.6 (8)	O2^viii—O14—O28^viii	100.8 (13)
U4^v—U5—O15^vi	148.5 (8)	K2^xxv—O14—O7^ix	92.4 (8)
U4^v—U5—O17	140.8 (5)	K2^xxv—O14—O9^xvi	112.3 (12)
U4^v—U5—O18	87.4 (12)	K2^xxv—O14—O10^ix	61.3 (8)
U4^v—U5—O25	94.6 (12)	K2^xxv—O14—O12^ix	46.3 (6)
U4^v—U5—O26^vi	91.9 (7)	K2^xxv—O14—O13^xiv	133.8 (10)
O4^v—U5—O5^vi	74.7 (11)	K2^xxv—O14—O15^xiv	157.7 (14)
O4^v—U5—O6^vi	99.0 (10)	K2^xxv—O14—O16^viii	56.5 (8)
O4^v—U5—O15^vi	171.8 (11)	K2^xxv—O14—O23^xv	108.2 (10)
O4^v—U5—O17	127.3 (8)	K2^xxv—O14—O24	54.8 (7)
O4^v—U5—O18	92.2 (12)	K2^xxv—O14—O26^xiv	144.4 (10)
O4^v—U5—O25	90.8 (12)	K2^xxv—O14—O27^ix	108.7 (8)
O4^v—U5—O26^vi	129.5 (11)	K2^xxv—O14—O28^viii	63.5 (8)
O5^vi—U5—O6^vi	173.6 (12)	O7^ix—O14—O9^xvi	97.9 (8)
O5^vi—U5—O15^vi	113.5 (10)	O7^ix—O14—O10^ix	57.1 (9)
O5^vi—U5—O17	133.8 (9)	O7^ix—O14—O12^ix	49.9 (8)
O5^vi—U5—O18	90.3 (13)	O7^ix—O14—O13^xiv	54.7 (8)
O5^vi—U5—O25	90.0 (13)	O7^ix—O14—O15^xiv	104.0 (10)
O5^vi—U5—O26^vi	56.8 (9)	O7^ix—O14—O16^viii	104.2 (10)
O6^vi—U5—O15^vi	72.7 (11)	O7^ix—O14—O23^xv	149.5 (9)
O6^vi—U5—O17	51.3 (9)	O7^ix—O14—O24	112.9 (10)
O6^vi—U5—O18	91.4 (13)	O7^ix—O14—O26^xiv	60.4 (9)
O6^vi—U5—O25	88.6 (12)	O7^ix—O14—O27^ix	86.6 (11)
O6^vi—U5—O26^vi	128.8 (11)	O7^ix—O14—O28^viii	150.2 (13)
O15^vi—U5—O17	47.9 (8)	O9^xvi—O14—O10^ix	151.9 (9)
O15^vi—U5—O18	88.6 (13)	O9^xvi—O14—O12^ix	97.4 (9)
O15^vi—U5—O25	88.5 (13)	O9^xvi—O14—O13^xiv	52.7 (9)
O15^vi—U5—O26^vi	58.3 (9)	O9^xvi—O14—O15^xiv	51.1 (9)
O17—U5—O18	53.6 (12)	O9^xvi—O14—O16^viii	56.1 (9)
O17—U5—O25	124.6 (13)	O9^xvi—O14—O23^xv	54.0 (7)
O17—U5—O26^vi	98.5 (7)	O9^xvi—O14—O24	146.0 (12)
O18—U5—O25	176.9 (14)	O9^xvi—O14—O26^xiv	95.1 (9)
O18—U5—O26^vi	100.9 (9)	O9^xvi—O14—O27^ix	138.5 (11)
O25—U5—O26^vi	76.8 (8)	O9^xvi—O14—O28^viii	77.4 (10)
U1^xi—U6—U2^x	60.6 (4)	O10^ix—O14—O12^ix	57.4 (8)
U1^xi—U6—U3^xxi	135.2 (6)	O10^ix—O14—O13^xiv	109.8 (11)
U1^xi—U6—K1^ix	124.3 (3)	O10^ix—O14—O15^xiv	140.8 (16)
U1^xi—U6—O2^x	30.4 (7)	O10^ix—O14—O16^viii	113.6 (11)
U1^xi—U6—O7^xi	39.9 (8)	O10^ix—O14—O23^xv	153.0 (9)
U1^xi—U6—O9^xii	97.8 (7)	O10^ix—O14—O24	55.8 (7)
U1^xi—U6—O10^xi	66.6 (4)	O10^ix—O14—O26^xiv	83.8 (11)
U1^xi—U6—O13	88.5 (11)	O10^ix—O14—O27^ix	59.5 (9)
U1^xi—U6—O14^ix	88.6 (8)	O10^ix—O14—O28^viii	116.9 (9)
U1^xi—U6—O15	164.7 (11)	O12^ix—O14—O13^xiv	89.3 (8)
U1^xi—U6—O26	117.3 (7)	O12^ix—O14—O15^xiv	139.6 (8)
U2^x—U6—U3^xxi	74.6 (4)	O12^ix—O14—O16^viii	63.9 (7)
U2^x—U6—K1^ix	102.7 (4)	O12^ix—O14—O23^xv	135.4 (12)
U2^x—U6—O2^x	30.3 (7)	O12^ix—O14—O24	92.2 (8)
U2^x—U6—O7^xi	99.3 (9)	O12^ix—O14—O26^xiv	110.1 (9)
U2^x—U6—O9^xii	38.7 (7)	O12^ix—O14—O27^ix	115.9 (8)
U2^x—U6—O10^xi	101.8 (6)	O12^ix—O14—O28^viii	101.1 (10)
U2^x—U6—O13	98.2 (16)	O13^xiv—O14—O15^xiv	52.7 (8)
U2^x—U6—O14^ix	82.1 (12)	O13^xiv—O14—O16^viii	97.3 (10)
U2^x—U6—O15	104.1 (10)	O13^xiv—O14—O23^xv	95.3 (8)
U2^x—U6—O26	174.4 (7)	O13^xiv—O14—O24	160.4 (15)
U3^xxi—U6—K1^ix	64.2 (2)	O13^xiv—O14—O26^xiv	49.6 (10)
U3^xxi—U6—O2^x	104.9 (8)	O13^xiv—O14—O27^ix	101.3 (12)
U3^xxi—U6—O7^xi	169.3 (9)	O13^xiv—O14—O28^viii	130.1 (11)
U3^xxi—U6—O9^xii	38.5 (6)	O15^xiv—O14—O16^viii	104.0 (11)
U3^xxi—U6—O10^xi	128.1 (4)	O15^xiv—O14—O23^xv	51.0 (8)
U3^xxi—U6—O13	97.5 (11)	O15^xiv—O14—O24	128.1 (10)
U3^xxi—U6—O14^ix	86.0 (8)	O15^xiv—O14—O26^xiv	57.9 (9)
U3^xxi—U6—O15	29.5 (9)	O15^xiv—O14—O27^ix	87.6 (11)
U3^xxi—U6—O26	107.3 (7)	O15^xiv—O14—O28^viii	95.9 (10)
K1^ix—U6—O2^x	118.4 (8)	O16^viii—O14—O23^xv	71.5 (8)
K1^ix—U6—O7^xi	109.5 (7)	O16^viii—O14—O24	100.9 (11)
K1^ix—U6—O9^xii	91.1 (7)	O16^viii—O14—O26^xiv	146.9 (9)
K1^ix—U6—O10^xi	66.5 (4)	O16^viii—O14—O27^ix	161.4 (9)
K1^ix—U6—O13	146.7 (13)	O16^viii—O14—O28^viii	48.7 (8)
K1^ix—U6—O14^ix	35.9 (8)	O23^xv—O14—O24	97.4 (8)
K1^ix—U6—O15	55.9 (8)	O23^xv—O14—O26^xiv	106.3 (9)
K1^ix—U6—O26	73.9 (7)	O23^xv—O14—O27^ix	106.7 (8)
O2^x—U6—O7^xi	69.8 (10)	O23^xv—O14—O28^viii	44.9 (8)
O2^x—U6—O9^xii	67.7 (10)	O24—O14—O26^xiv	112.0 (12)
O2^x—U6—O10^xi	84.9 (8)	O24—O14—O27^ix	60.7 (9)
O2^x—U6—O13	92.3 (16)	O24—O14—O28^viii	68.7 (9)
O2^x—U6—O14^ix	86.2 (13)	O26^xiv—O14—O27^ix	51.7 (9)
O2^x—U6—O15	134.3 (13)	O26^xiv—O14—O28^viii	148.6 (10)
O2^x—U6—O26	147.7 (10)	O27^ix—O14—O28^viii	116.6 (9)
O7^xi—U6—O9^xii	137.5 (11)	U3^xxi—O15—U5^xxi	108.2 (10)
O7^xi—U6—O10^xi	43.6 (8)	U3^xxi—O15—U6	121.0 (15)
O7^xi—U6—O13	92.0 (13)	U3^xxi—O15—K1^ix	96.4 (10)
O7^xi—U6—O14^ix	84.5 (10)	U3^xxi—O15—O5	139.7 (10)
O7^xi—U6—O15	154.6 (13)	U3^xxi—O15—O6	56.7 (9)
O7^xi—U6—O26	77.9 (10)	U3^xxi—O15—O9^xii	60.8 (10)
O9^xii—U6—O10^xi	130.7 (9)	U3^xxi—O15—O13	118.8 (15)
O9^xii—U6—O13	89.4 (16)	U3^xxi—O15—O14^ix	109.3 (14)
O9^xii—U6—O14^ix	93.0 (13)	U3^xxi—O15—O17^xxi	40.2 (8)
O9^xii—U6—O15	67.2 (11)	U3^xxi—O15—O18^xxi	96.7 (10)
O9^xii—U6—O26	144.5 (9)	U3^xxi—O15—O20^xxi	94.8 (11)
O10^xi—U6—O13	133.5 (13)	U3^xxi—O15—O23^xxi	39.0 (7)
O10^xi—U6—O14^ix	43.2 (9)	U3^xxi—O15—O25^xxi	112.1 (10)
O10^xi—U6—O15	120.4 (8)	U3^xxi—O15—O26	172.6 (14)
O10^xi—U6—O26	72.8 (8)	U5^xxi—O15—U6	129.8 (15)
O13—U6—O14^ix	176.5 (13)	U5^xxi—O15—K1^ix	93.9 (10)
O13—U6—O15	94.2 (13)	U5^xxi—O15—O5	32.5 (6)
O13—U6—O26	86.8 (18)	U5^xxi—O15—O6	53.0 (9)
O14^ix—U6—O15	89.2 (10)	U5^xxi—O15—O9^xii	158.1 (14)
O14^ix—U6—O26	92.8 (13)	U5^xxi—O15—O13	110.1 (15)
O15—U6—O26	77.9 (11)	U5^xxi—O15—O14^ix	131.1 (14)
O1—Ca1—K2ⁱ	117.4 (7)	U5^xxi—O15—O17^xxi	95.6 (10)
O1—Ca1—O13ⁱⁱ	75.3 (9)	U5^xxi—O15—O18^xxi	39.3 (7)
O1—Ca1—O16	73.5 (10)	U5^xxi—O15—O20^xxi	85.6 (11)
O1—Ca1—O17	93.3 (12)	U5^xxi—O15—O23^xxi	116.0 (10)
O1—Ca1—O18	154.9 (8)	U5^xxi—O15—O25^xxi	40.0 (8)
O1—Ca1—O19^vi	121.2 (9)	U5^xxi—O15—O26	79.0 (12)
O1—Ca1—O20	82.5 (11)	U6—O15—K1^ix	90.2 (8)
O1—Ca1—O21	71.7 (11)	U6—O15—O5	97.3 (11)
O1—Ca1—O22^xiii	52.3 (8)	U6—O15—O6	176.6 (17)
O1—Ca1—O28	129.4 (10)	U6—O15—O9^xii	61.0 (9)
K2ⁱ—Ca1—O13ⁱⁱ	116.3 (9)	U6—O15—O13	37.3 (7)
K2ⁱ—Ca1—O16	54.4 (7)	U6—O15—O14^ix	39.8 (6)
K2ⁱ—Ca1—O17	119.6 (7)	U6—O15—O17^xxi	114.9 (13)
K2ⁱ—Ca1—O18	52.3 (7)	U6—O15—O18^xxi	119.9 (12)
K2ⁱ—Ca1—O19^vi	119.6 (7)	U6—O15—O20^xxi	81.3 (9)
K2ⁱ—Ca1—O20	52.8 (12)	U6—O15—O23^xxi	108.5 (13)
K2ⁱ—Ca1—O21	166.0 (11)	U6—O15—O25^xxi	118.6 (12)
K2ⁱ—Ca1—O22^xiii	106.6 (7)	U6—O15—O26	52.3 (9)
K2ⁱ—Ca1—O28	69.0 (10)	K1^ix—O15—O5	95.6 (9)
O13ⁱⁱ—Ca1—O16	75.7 (8)	K1^ix—O15—O6	87.7 (9)
O13ⁱⁱ—Ca1—O17	121.5 (10)	K1^ix—O15—O9^xii	105.8 (12)
O13ⁱⁱ—Ca1—O18	129.5 (10)	K1^ix—O15—O13	125.9 (9)
O13ⁱⁱ—Ca1—O19^vi	68.3 (7)	K1^ix—O15—O14^ix	51.9 (6)
O13ⁱⁱ—Ca1—O20	145.4 (9)	K1^ix—O15—O17^xxi	136.2 (12)
O13ⁱⁱ—Ca1—O21	53.7 (11)	K1^ix—O15—O18^xxi	133.1 (11)
O13ⁱⁱ—Ca1—O22^xiii	123.4 (10)	K1^ix—O15—O20^xxi	168.3 (10)
O13ⁱⁱ—Ca1—O28	60.1 (12)	K1^ix—O15—O23^xxi	58.5 (8)
O16—Ca1—O17	155.6 (9)	K1^ix—O15—O25^xxi	54.1 (8)
O16—Ca1—O18	105.8 (11)	K1^ix—O15—O26	81.2 (9)
O16—Ca1—O19^vi	133.9 (9)	O5—O15—O6	85.5 (11)
O16—Ca1—O20	72.7 (10)	O5—O15—O9^xii	148.9 (12)
O16—Ca1—O21	123.9 (10)	O5—O15—O13	83.3 (13)
O16—Ca1—O22^xiii	104.2 (8)	O5—O15—O14^ix	108.3 (11)
O16—Ca1—O28	73.5 (11)	O5—O15—O17^xxi	114.6 (12)
O17—Ca1—O18	77.4 (10)	O5—O15—O18^xxi	49.1 (9)
O17—Ca1—O19^vi	70.5 (8)	O5—O15—O20^xxi	77.8 (10)
O17—Ca1—O20	85.4 (11)	O5—O15—O23^xxi	142.4 (11)
O17—Ca1—O21	68.1 (11)	O5—O15—O25^xxi	49.5 (9)
O17—Ca1—O22^xiii	52.5 (8)	O5—O15—O26	47.7 (8)
O17—Ca1—O28	129.0 (10)	O6—O15—O9^xii	117.1 (14)
O18—Ca1—O19^vi	78.0 (7)	O6—O15—O13	145.4 (14)
O18—Ca1—O20	73.6 (10)	O6—O15—O14^ix	137.5 (13)
O18—Ca1—O21	123.9 (10)	O6—O15—O17^xxi	65.2 (9)
O18—Ca1—O22^xiii	105.5 (8)	O6—O15—O18^xxi	63.3 (9)
O18—Ca1—O28	71.8 (11)	O6—O15—O20^xxi	101.2 (11)
O19^vi—Ca1—O20	146.1 (9)	O6—O15—O23^xxi	68.1 (10)
O19^vi—Ca1—O21	49.7 (10)	O6—O15—O25^xxi	62.0 (10)
O19^vi—Ca1—O22^xiii	119.2 (9)	O6—O15—O26	129.8 (15)
O19^vi—Ca1—O28	64.0 (11)	O9^xii—O15—O13	65.9 (13)
O20—Ca1—O21	141.1 (17)	O9^xii—O15—O14^ix	70.3 (10)
O20—Ca1—O22^xiii	53.8 (14)	O9^xii—O15—O17^xxi	63.5 (11)
O20—Ca1—O28	121.8 (17)	O9^xii—O15—O18^xxi	120.0 (13)
O21—Ca1—O22^xiii	87.3 (12)	O9^xii—O15—O20^xxi	77.1 (12)
O21—Ca1—O28	97.1 (14)	O9^xii—O15—O23^xxi	68.7 (11)
O22^xiii—Ca1—O28	175.6 (12)	O9^xii—O15—O25^xxi	159.1 (15)
U6^xiv—K1—O3	128.0 (7)	O9^xii—O15—O26	113.0 (10)
U6^xiv—K1—O7	169.4 (5)	O13—O15—O14^ix	77.1 (9)
U6^xiv—K1—O8	146.1 (5)	O13—O15—O17^xxi	90.1 (11)
U6^xiv—K1—O10	124.3 (7)	O13—O15—O18^xxi	84.9 (11)
U6^xiv—K1—O12	134.9 (8)	O13—O15—O20^xxi	44.4 (8)
U6^xiv—K1—O14	23.2 (5)	O13—O15—O23^xxi	133.3 (16)
U6^xiv—K1—O15^xiv	33.9 (4)	O13—O15—O25^xxi	128.1 (15)
U6^xiv—K1—O23^xv	71.0 (5)	O13—O15—O26	58.6 (11)
U6^xiv—K1—O24	90.3 (6)	O14^ix—O15—O17^xxi	133.3 (15)
U6^xiv—K1—O25^xv	78.8 (6)	O14^ix—O15—O18^xxi	153.2 (13)
U6^xiv—K1—O27^ix	72.7 (6)	O14^ix—O15—O20^xxi	120.8 (9)
U6^xiv—K1—O28^viii	84.8 (6)	O14^ix—O15—O23^xxi	78.2 (11)
O3—K1—O7	48.0 (7)	O14^ix—O15—O25^xxi	96.2 (11)
O3—K1—O8	56.5 (8)	O14^ix—O15—O26	63.7 (10)
O3—K1—O10	64.6 (8)	O17^xxi—O15—O18^xxi	65.5 (10)
O3—K1—O12	97.0 (8)	O17^xxi—O15—O20^xxi	55.3 (9)
O3—K1—O14	135.7 (10)	O17^xxi—O15—O23^xxi	79.1 (11)
O3—K1—O15^xiv	118.8 (9)	O17^xxi—O15—O25^xxi	125.4 (10)
O3—K1—O23^xv	139.3 (7)	O17^xxi—O15—O26	142.6 (14)
O3—K1—O24	96.4 (8)	O18^xxi—O15—O20^xxi	48.1 (8)
O3—K1—O25^xv	63.7 (8)	O18^xxi—O15—O23^xxi	128.3 (10)
O3—K1—O27^ix	61.6 (8)	O18^xxi—O15—O25^xxi	79.3 (11)
O3—K1—O28^viii	146.5 (7)	O18^xxi—O15—O26	90.0 (12)
O7—K1—O8	43.3 (5)	O20^xxi—O15—O23^xxi	131.9 (13)
O7—K1—O10	45.8 (7)	O20^xxi—O15—O25^xxi	123.8 (13)
O7—K1—O12	50.8 (8)	O20^xxi—O15—O26	87.3 (11)
O7—K1—O14	167.4 (7)	O23^xxi—O15—O25^xxi	93.5 (11)
O7—K1—O15^xiv	136.1 (6)	O23^xxi—O15—O26	136.7 (13)
O7—K1—O23^xv	105.8 (7)	O25^xxi—O15—O26	72.2 (10)
O7—K1—O24	99.8 (7)	U1—O16—U2	75.1 (12)
O7—K1—O25^xv	91.3 (7)	U1—O16—Ca1	78.0 (9)
O7—K1—O27^ix	107.5 (8)	U1—O16—O1	27.9 (6)
O7—K1—O28^viii	100.9 (7)	U1—O16—O2	119.4 (11)
O8—K1—O10	89.0 (7)	U1—O16—O3	73.4 (8)
O8—K1—O12	55.6 (8)	U1—O16—K2ⁱ	143.9 (10)
O8—K1—O14	125.5 (6)	U1—O16—O7	42.7 (7)
O8—K1—O15^xiv	174.9 (10)	U1—O16—O8	35.1 (7)
O8—K1—O23^xv	130.9 (9)	U1—O16—O9^iv	108.3 (10)
O8—K1—O24	56.9 (7)	U1—O16—O11	81.2 (8)
O8—K1—O25^xv	119.8 (10)	U1—O16—O12^xii	121.0 (8)
O8—K1—O27^ix	87.1 (8)	U1—O16—O13ⁱⁱ	67.7 (8)
O8—K1—O28^viii	93.3 (8)	U1—O16—O14^v	165.5 (9)
O10—K1—O12	72.4 (8)	U1—O16—O19	66.6 (7)
O10—K1—O14	145.1 (8)	U1—O16—O20	86.0 (12)
O10—K1—O15^xiv	90.4 (7)	U1—O16—O28	112.1 (12)
O10—K1—O23^xv	75.0 (8)	U2—O16—Ca1	152.4 (18)
O10—K1—O24	145.4 (9)	U2—O16—O1	102.8 (15)
O10—K1—O25^xv	59.0 (8)	U2—O16—O2	48.0 (11)
O10—K1—O27^ix	117.2 (10)	U2—O16—O3	2.3 (8)
O10—K1—O28^viii	104.7 (9)	U2—O16—K2ⁱ	125.9 (15)
O12—K1—O14	120.3 (10)	U2—O16—O7	53.6 (10)
O12—K1—O15^xiv	128.9 (9)	U2—O16—O8	51.3 (11)
O12—K1—O23^xv	75.3 (9)	U2—O16—O9^iv	50.1 (10)
O12—K1—O24	82.3 (8)	U2—O16—O11	47.1 (7)
O12—K1—O25^xv	131.5 (7)	U2—O16—O12^xii	84.9 (10)
O12—K1—O27^ix	142.2 (8)	U2—O16—O13ⁱⁱ	100.3 (11)
O12—K1—O28^viii	50.3 (8)	U2—O16—O14^v	92.9 (14)
O14—K1—O15^xiv	55.7 (6)	U2—O16—O19	88.7 (10)
O14—K1—O23^xv	77.5 (7)	U2—O16—O20	132.1 (13)
O14—K1—O24	68.6 (7)	U2—O16—O28	139.1 (13)
O14—K1—O25^xv	100.9 (8)	Ca1—O16—O1	51.0 (9)
O14—K1—O27^ix	74.2 (9)	Ca1—O16—O2	158.7 (13)
O14—K1—O28^viii	71.7 (9)	Ca1—O16—O3	150.4 (13)
O15^xiv—K1—O23^xv	53.7 (8)	Ca1—O16—K2ⁱ	80.3 (8)
O15^xiv—K1—O24	124.1 (7)	Ca1—O16—O7	101.5 (11)
O15^xiv—K1—O25^xv	55.8 (8)	Ca1—O16—O8	106.6 (13)
O15^xiv—K1—O27^ix	88.6 (8)	Ca1—O16—O9^iv	137.1 (9)
O15^xiv—K1—O28^viii	91.8 (8)	Ca1—O16—O11	133.5 (11)
O23^xv—K1—O24	121.3 (10)	Ca1—O16—O12^xii	114.4 (9)
O23^xv—K1—O25^xv	91.2 (9)	Ca1—O16—O13ⁱⁱ	63.5 (7)
O23^xv—K1—O27^ix	141.5 (8)	Ca1—O16—O14^v	112.7 (10)
O23^xv—K1—O28^viii	49.4 (8)	Ca1—O16—O19	86.0 (9)
O24—K1—O25^xv	140.3 (10)	Ca1—O16—O20	50.4 (9)
O24—K1—O27^ix	70.8 (9)	Ca1—O16—O28	49.6 (10)
O24—K1—O28^viii	74.6 (9)	O1—O16—O2	143.1 (13)
O25^xv—K1—O27^ix	69.5 (8)	O1—O16—O3	101.1 (11)
O25^xv—K1—O28^viii	140.5 (8)	O1—O16—K2ⁱ	120.5 (11)
O27^ix—K1—O28^viii	138.1 (8)	O1—O16—O7	64.8 (10)
U1—O1—U2	74.2 (11)	O1—O16—O8	57.0 (10)
U1—O1—Ca1	152.0 (17)	O1—O16—O9^iv	131.1 (12)
U1—O1—O2ⁱ	51.6 (9)	O1—O16—O11	97.6 (10)
U1—O1—O4	50.8 (9)	O1—O16—O12^xii	121.0 (9)
U1—O1—O7	53.5 (10)	O1—O16—O13ⁱⁱ	65.2 (10)
U1—O1—O8	52.2 (10)	O1—O16—O14^v	163.5 (11)
U1—O1—O11ⁱ	53.7 (11)	O1—O16—O19	63.9 (8)
U1—O1—O12	0.8 (9)	O1—O16—O20	64.4 (12)
U1—O1—O13ⁱⁱ	92.8 (10)	O1—O16—O28	92.9 (13)
U1—O1—O16	100.7 (14)	O2—O16—O3	50.2 (9)
U1—O1—O17	162.7 (17)	O2—O16—K2ⁱ	78.5 (10)
U1—O1—O19	93.0 (10)	O2—O16—O7	99.7 (12)
U1—O1—O20	135.3 (13)	O2—O16—O8	86.5 (11)
U1—O1—O21	126.0 (12)	O2—O16—O9^iv	53.0 (8)
U1—O1—O22^xiii	119.6 (15)	O2—O16—O11	47.1 (8)
U1—O1—O27^xiii	109.4 (16)	O2—O16—O12^xii	47.4 (7)
U2—O1—Ca1	82.0 (9)	O2—O16—O13ⁱⁱ	132.3 (11)
U2—O1—O2ⁱ	90.6 (10)	O2—O16—O14^v	52.9 (9)
U2—O1—O4	88.6 (10)	O2—O16—O19	90.1 (9)
U2—O1—O7	38.5 (6)	O2—O16—O20	114.9 (11)
U2—O1—O8	34.5 (7)	O2—O16—O28	123.8 (16)
U2—O1—O11ⁱ	127.6 (10)	O3—O16—K2ⁱ	128.2 (11)
U2—O1—O12	73.4 (8)	O3—O16—O7	51.3 (8)
U2—O1—O13ⁱⁱ	73.0 (9)	O3—O16—O8	50.6 (9)
U2—O1—O16	26.7 (6)	O3—O16—O9^iv	50.1 (8)
U2—O1—O17	123.1 (10)	O3—O16—O11	48.7 (6)
U2—O1—O19	67.2 (8)	O3—O16—O12^xii	87.2 (8)
U2—O1—O20	76.0 (10)	O3—O16—O13ⁱⁱ	98.1 (8)
U2—O1—O21	116.0 (12)	O3—O16—O14^v	94.4 (10)
U2—O1—O22^xiii	126.7 (11)	O3—O16—O19	89.4 (8)
U2—O1—O27^xiii	174.2 (10)	O3—O16—O20	133.0 (10)
Ca1—O1—O2ⁱ	115.4 (10)	O3—O16—O28	138.1 (10)
Ca1—O1—O4	144.2 (11)	K2ⁱ—O16—O7	173.0 (12)
Ca1—O1—O7	98.5 (11)	K2ⁱ—O16—O8	131.5 (9)
Ca1—O1—O8	111.9 (14)	K2ⁱ—O16—O9^iv	107.3 (12)
Ca1—O1—O11ⁱ	145.1 (12)	K2ⁱ—O16—O11	93.6 (8)
Ca1—O1—O12	151.3 (13)	K2ⁱ—O16—O12^xii	46.4 (6)
Ca1—O1—O13ⁱⁱ	65.8 (8)	K2ⁱ—O16—O13ⁱⁱ	125.5 (9)
Ca1—O1—O16	55.6 (9)	K2ⁱ—O16—O14^v	50.2 (6)
Ca1—O1—O17	43.1 (8)	K2ⁱ—O16—O19	83.5 (7)
Ca1—O1—O19	91.1 (10)	K2ⁱ—O16—O20	58.0 (11)
Ca1—O1—O20	48.0 (8)	K2ⁱ—O16—O28	72.8 (10)
Ca1—O1—O21	53.3 (9)	O7—O16—O8	54.7 (8)
Ca1—O1—O22^xiii	86.4 (11)	O7—O16—O9^iv	66.7 (10)
Ca1—O1—O27^xiii	93.3 (11)	O7—O16—O11	90.0 (9)
O2ⁱ—O1—O4	99.1 (12)	O7—O16—O12^xii	136.3 (10)
O2ⁱ—O1—O7	52.2 (9)	O7—O16—O13ⁱⁱ	51.1 (7)
O2ⁱ—O1—O8	92.8 (11)	O7—O16—O14^v	123.3 (11)
O2ⁱ—O1—O11ⁱ	54.8 (9)	O7—O16—O19	103.3 (11)
O2ⁱ—O1—O12	51.9 (8)	O7—O16—O20	128.3 (16)
O2ⁱ—O1—O13ⁱⁱ	50.8 (9)	O7—O16—O28	103.1 (10)
O2ⁱ—O1—O16	104.9 (12)	O8—O16—O9^iv	99.2 (12)
O2ⁱ—O1—O17	121.5 (10)	O8—O16—O11	46.4 (8)
O2ⁱ—O1—O19	143.3 (12)	O8—O16—O12^xii	90.4 (8)
O2ⁱ—O1—O20	159.4 (15)	O8—O16—O13ⁱⁱ	98.5 (11)
O2ⁱ—O1—O21	74.7 (9)	O8—O16—O14^v	139.4 (12)
O2ⁱ—O1—O22^xiii	140.2 (17)	O8—O16—O19	50.3 (8)
O2ⁱ—O1—O27^xiii	88.4 (11)	O8—O16—O20	89.0 (12)
O4—O1—O7	95.0 (11)	O8—O16—O28	147.2 (16)
O4—O1—O8	54.2 (10)	O9^iv—O16—O11	88.9 (9)
O4—O1—O11ⁱ	64.1 (10)	O9^iv—O16—O12^xii	98.7 (10)
O4—O1—O12	51.0 (8)	O9^iv—O16—O13ⁱⁱ	79.5 (9)
O4—O1—O13ⁱⁱ	143.1 (12)	O9^iv—O16—O14^v	57.3 (8)
O4—O1—O16	108.0 (12)	O9^iv—O16—O19	136.2 (10)
O4—O1—O17	124.9 (11)	O9^iv—O16—O20	164.4 (16)
O4—O1—O19	53.7 (9)	O9^iv—O16—O28	91.4 (11)
O4—O1—O20	96.2 (10)	O11—O16—O12^xii	47.3 (7)
O4—O1—O21	154.3 (17)	O11—O16—O13ⁱⁱ	140.9 (11)
O4—O1—O22^xiii	71.8 (10)	O11—O16—O14^v	96.7 (9)
O4—O1—O27^xiii	97.2 (12)	O11—O16—O19	47.5 (7)
O7—O1—O8	52.0 (8)	O11—O16—O20	87.2 (9)
O7—O1—O11ⁱ	97.3 (11)	O11—O16—O28	165.8 (14)
O7—O1—O12	52.8 (8)	O12^xii—O16—O13ⁱⁱ	171.1 (12)
O7—O1—O13ⁱⁱ	51.0 (7)	O12^xii—O16—O14^v	64.7 (8)
O7—O1—O16	56.7 (9)	O12^xii—O16—O19	57.8 (7)
O7—O1—O17	138.6 (11)	O12^xii—O16—O20	67.8 (10)
O7—O1—O19	101.3 (10)	O12^xii—O16—O28	118.7 (12)
O7—O1—O20	112.9 (14)	O13ⁱⁱ—O16—O14^v	107.5 (10)
O7—O1—O21	100.1 (10)	O13ⁱⁱ—O16—O19	129.0 (13)
O7—O1—O22^xiii	162.1 (12)	O13ⁱⁱ—O16—O20	112.6 (13)
O7—O1—O27^xiii	140.2 (10)	O13ⁱⁱ—O16—O28	52.8 (10)
O8—O1—O11ⁱ	102.4 (12)	O14^v—O16—O19	122.1 (9)
O8—O1—O12	51.4 (9)	O14^v—O16—O20	108.2 (13)
O8—O1—O13ⁱⁱ	100.9 (11)	O14^v—O16—O28	71.7 (12)
O8—O1—O16	57.7 (10)	O19—O16—O20	43.6 (8)
O8—O1—O17	142.8 (12)	O19—O16—O28	131.8 (12)
O8—O1—O19	52.2 (8)	O20—O16—O28	88.8 (12)
O8—O1—O20	85.0 (11)	U3—O17—U5	70.9 (11)
O8—O1—O21	149.1 (15)	U3—O17—Ca1	149.2 (18)
O8—O1—O22^xiii	110.1 (10)	U3—O17—O1	167.2 (17)
O8—O1—O27^xiii	151.2 (13)	U3—O17—O5^vii	49.2 (8)
O11ⁱ—O1—O12	54.5 (9)	U3—O17—O6^vi	52.5 (10)
O11ⁱ—O1—O13ⁱⁱ	102.1 (10)	U3—O17—O9^v	58.4 (9)
O11ⁱ—O1—O16	153.2 (13)	U3—O17—O15^vi	51.5 (10)
O11ⁱ—O1—O17	109.0 (12)	U3—O17—O18	99.2 (14)
O11ⁱ—O1—O19	115.9 (11)	U3—O17—O19^vi	90.9 (10)
O11ⁱ—O1—O20	145.6 (13)	U3—O17—O20	129.8 (13)
O11ⁱ—O1—O21	93.3 (12)	U3—O17—O21	129.5 (12)
O11ⁱ—O1—O22^xiii	87.9 (14)	U3—O17—O22^xiii	117.9 (14)
O11ⁱ—O1—O27^xiii	55.8 (10)	U3—O17—O23	3.0 (6)
O12—O1—O13ⁱⁱ	92.6 (8)	U3—O17—O26^vii	55.3 (11)
O12—O1—O16	99.9 (11)	U3—O17—O27^xiii	112.0 (16)
O12—O1—O17	163.5 (13)	U5—O17—Ca1	79.8 (9)
O12—O1—O19	92.6 (8)	U5—O17—O1	121.4 (10)
O12—O1—O20	134.7 (10)	U5—O17—O5^vii	88.7 (10)
O12—O1—O21	126.3 (10)	U5—O17—O6^vi	36.0 (7)
O12—O1—O22^xiii	120.1 (12)	U5—O17—O9^v	90.8 (10)
O12—O1—O27^xiii	110.3 (12)	U5—O17—O15^vi	36.5 (7)
O13ⁱⁱ—O1—O16	68.1 (10)	U5—O17—O18	28.3 (4)
O13ⁱⁱ—O1—O17	91.7 (8)	U5—O17—O19^vi	72.9 (8)
O13ⁱⁱ—O1—O19	136.4 (14)	U5—O17—O20	76.1 (10)
O13ⁱⁱ—O1—O20	109.4 (13)	U5—O17—O21	113.9 (13)
O13ⁱⁱ—O1—O21	49.3 (10)	U5—O17—O22^xiii	125.8 (12)
O13ⁱⁱ—O1—O22^xiii	144.5 (11)	U5—O17—O23	72.1 (8)
O13ⁱⁱ—O1—O27^xiii	102.1 (9)	U5—O17—O26^vii	126.2 (11)
O16—O1—O17	96.5 (11)	U5—O17—O27^xiii	175.0 (10)
O16—O1—O19	68.3 (10)	Ca1—O17—O1	43.6 (8)
O16—O1—O20	56.9 (11)	Ca1—O17—O5^vii	122.7 (10)
O16—O1—O21	97.6 (13)	Ca1—O17—O6^vi	97.7 (12)
O16—O1—O22^xiii	114.8 (14)	Ca1—O17—O9^v	132.9 (11)
O16—O1—O27^xiii	148.9 (13)	Ca1—O17—O15^vi	107.5 (14)
O17—O1—O19	95.3 (8)	Ca1—O17—O18	52.1 (8)
O17—O1—O20	57.8 (9)	Ca1—O17—O19^vi	71.2 (8)
O17—O1—O21	48.5 (8)	Ca1—O17—O20	47.0 (8)
O17—O1—O22^xiii	53.1 (8)	Ca1—O17—O21	55.5 (10)
O17—O1—O27^xiii	53.2 (9)	Ca1—O17—O22^xiii	86.7 (12)
O19—O1—O20	44.3 (8)	Ca1—O17—O23	151.1 (14)
O19—O1—O21	140.8 (12)	Ca1—O17—O26^vii	152.3 (14)
O19—O1—O22^xiii	61.2 (10)	Ca1—O17—O27^xiii	96.6 (11)
O19—O1—O27^xiii	116.4 (10)	O1—O17—O5^vii	129.9 (10)
O20—O1—O21	96.9 (12)	O1—O17—O6^vi	139.5 (12)
O20—O1—O22^xiii	58.4 (13)	O1—O17—O9^v	114.5 (10)
O20—O1—O27^xiii	103.3 (12)	O1—O17—O15^vi	135.4 (12)
O21—O1—O22^xiii	96.7 (12)	O1—O17—O18	93.1 (10)
O21—O1—O27^xiii	58.3 (11)	O1—O17—O19^vi	96.5 (8)
O22^xiii—O1—O27^xiii	55.9 (10)	O1—O17—O20	55.8 (8)
U1^xii—O2—U2	124.8 (15)	O1—O17—O21	52.0 (8)
U1^xii—O2—U6ⁱⁱⁱ	118.7 (15)	O1—O17—O22^xiii	52.9 (8)
U1^xii—O2—O1^xii	38.9 (6)	O1—O17—O23	165.1 (12)
U1^xii—O2—O3	114.5 (12)	O1—O17—O26^vii	112.4 (12)
U1^xii—O2—K2ⁱ	87.2 (8)	O1—O17—O27^xiii	56.1 (9)
U1^xii—O2—O7^xii	62.2 (9)	O5^vii—O17—O6^vi	52.9 (10)
U1^xii—O2—O8	98.2 (11)	O5^vii—O17—O9^v	102.9 (12)
U1^xii—O2—O9^iv	172.1 (16)	O5^vii—O17—O15^vi	93.3 (11)
U1^xii—O2—O11	56.8 (9)	O5^vii—O17—O18	108.1 (11)
U1^xii—O2—O12^xii	37.8 (6)	O5^vii—O17—O19^vi	51.9 (8)
U1^xii—O2—O13ⁱⁱⁱ	108.6 (14)	O5^vii—O17—O20	162.7 (15)
U1^xii—O2—O14^v	113.9 (12)	O5^vii—O17—O21	80.2 (9)
U1^xii—O2—O16	118.8 (13)	O5^vii—O17—O22^xiii	139.9 (17)
U1^xii—O2—O21^xii	90.8 (9)	O5^vii—O17—O23	51.6 (7)
U2—O2—U6ⁱⁱⁱ	116.3 (10)	O5^vii—O17—O26^vii	56.6 (9)
U2—O2—O1^xii	122.9 (14)	O5^vii—O17—O27^xiii	90.3 (11)
U2—O2—O3	40.2 (7)	O6^vi—O17—O9^v	101.0 (11)
U2—O2—K2ⁱ	90.7 (10)	O6^vi—O17—O15^vi	54.8 (8)
U2—O2—O7^xii	166.4 (14)	O6^vi—O17—O18	57.6 (9)
U2—O2—O8	26.6 (6)	O6^vi—O17—O19^vi	50.7 (7)
U2—O2—O9^iv	58.8 (10)	O6^vi—O17—O20	111.2 (14)
U2—O2—O11	69.0 (11)	O6^vi—O17—O21	100.2 (11)
U2—O2—O12^xii	111.6 (14)	O6^vi—O17—O22^xiii	158.3 (12)
U2—O2—O13ⁱⁱⁱ	118.0 (12)	O6^vi—O17—O23	55.1 (9)
U2—O2—O14^v	104.4 (11)	O6^vi—O17—O26^vii	100.2 (12)
U2—O2—O16	38.4 (8)	O6^vi—O17—O27^xiii	142.4 (11)
U2—O2—O21^xii	94.7 (11)	O9^v—O17—O15^vi	54.5 (10)
U6ⁱⁱⁱ—O2—O1^xii	108.9 (14)	O9^v—O17—O18	105.7 (11)
U6ⁱⁱⁱ—O2—O3	114.8 (10)	O9^v—O17—O19^vi	149.0 (12)
U6ⁱⁱⁱ—O2—K2ⁱ	87.1 (8)	O9^v—O17—O20	85.9 (10)
U6ⁱⁱⁱ—O2—O7^xii	57.0 (9)	O9^v—O17—O21	155.2 (17)
U6ⁱⁱⁱ—O2—O8	142.6 (10)	O9^v—O17—O22^xiii	61.9 (9)
U6ⁱⁱⁱ—O2—O9^iv	59.0 (9)	O9^v—O17—O23	55.5 (8)
U6ⁱⁱⁱ—O2—O11	172.8 (15)	O9^v—O17—O26^vii	63.5 (10)
U6ⁱⁱⁱ—O2—O12^xii	114.3 (13)	O9^v—O17—O27^xiii	94.2 (12)
U6ⁱⁱⁱ—O2—O13ⁱⁱⁱ	37.0 (8)	O15^vi—O17—O18	57.9 (9)
U6ⁱⁱⁱ—O2—O14^v	39.9 (7)	O15^vi—O17—O19^vi	104.1 (11)
U6ⁱⁱⁱ—O2—O16	104.7 (10)	O15^vi—O17—O20	79.6 (10)
U6ⁱⁱⁱ—O2—O21^xii	89.2 (11)	O15^vi—O17—O21	150.3 (16)
O1^xii—O2—O3	90.1 (11)	O15^vi—O17—O22^xiii	103.6 (10)
O1^xii—O2—K2ⁱ	125.4 (9)	O15^vi—O17—O23	50.9 (9)
O1^xii—O2—O7^xii	70.3 (11)	O15^vi—O17—O26^vii	100.1 (12)
O1^xii—O2—O8	103.6 (11)	O15^vi—O17—O27^xiii	148.5 (13)
O1^xii—O2—O9^iv	133.5 (13)	O18—O17—O19^vi	72.0 (9)
O1^xii—O2—O11	64.0 (10)	O18—O17—O20	54.8 (10)
O1^xii—O2—O12^xii	76.7 (9)	O18—O17—O21	96.3 (13)
O1^xii—O2—O13ⁱⁱⁱ	80.4 (11)	O18—O17—O22^xiii	111.8 (13)
O1^xii—O2—O14^v	132.7 (15)	O18—O17—O23	100.3 (10)
O1^xii—O2—O16	146.3 (14)	O18—O17—O26^vii	154.5 (12)
O1^xii—O2—O21^xii	52.1 (8)	O18—O17—O27^xiii	148.5 (12)
O3—O2—K2ⁱ	130.8 (12)	O19^vi—O17—O20	114.2 (12)
O3—O2—O7^xii	151.6 (15)	O19^vi—O17—O21	49.5 (9)
O3—O2—O8	46.5 (9)	O19^vi—O17—O22^xiii	148.7 (12)
O3—O2—O9^iv	63.0 (10)	O19^vi—O17—O23	93.9 (8)
O3—O2—O11	65.6 (10)	O19^vi—O17—O26^vii	104.8 (10)
O3—O2—O12^xii	130.8 (14)	O19^vi—O17—O27^xiii	102.7 (9)
O3—O2—O13ⁱⁱⁱ	92.4 (12)	O20—O17—O21	98.1 (12)
O3—O2—O14^v	131.3 (10)	O20—O17—O22^xiii	57.4 (13)
O3—O2—O16	78.7 (11)	O20—O17—O23	128.4 (10)
O3—O2—O21^xii	54.7 (9)	O20—O17—O26^vii	139.9 (12)
K2ⁱ—O2—O7^xii	77.5 (9)	O20—O17—O27^xiii	104.0 (12)
K2ⁱ—O2—O8	88.9 (8)	O21—O17—O22^xiii	99.7 (13)
K2ⁱ—O2—O9^iv	99.9 (10)	O21—O17—O23	131.8 (10)
K2ⁱ—O2—O11	97.9 (10)	O21—O17—O26^vii	100.3 (13)
K2ⁱ—O2—O12^xii	49.9 (7)	O21—O17—O27^xiii	61.0 (12)
K2ⁱ—O2—O13ⁱⁱⁱ	123.2 (11)	O22^xiii—O17—O23	115.0 (11)
K2ⁱ—O2—O14^v	47.8 (7)	O22^xiii—O17—O26^vii	84.4 (13)
K2ⁱ—O2—O16	52.6 (8)	O22^xiii—O17—O27^xiii	57.0 (11)
K2ⁱ—O2—O21^xii	174.4 (13)	O23—O17—O26^vii	54.2 (9)
O7^xii—O2—O8	156.2 (11)	O23—O17—O27^xiii	111.0 (12)
O7^xii—O2—O9^iv	116.0 (14)	O26^vii—O17—O27^xiii	56.8 (10)
O7^xii—O2—O11	118.9 (11)	U3—O18—U5	70.0 (10)
O7^xii—O2—O12^xii	65.8 (10)	U3—O18—Ca1	78.1 (9)
O7^xii—O2—O13ⁱⁱⁱ	64.9 (12)	U3—O18—K2ⁱ	145.5 (9)
O7^xii—O2—O14^v	62.6 (10)	U3—O18—O4^v	107.5 (8)
O7^xii—O2—O16	128.8 (14)	U3—O18—O5^vi	113.2 (8)
O7^xii—O2—O21^xii	96.9 (12)	U3—O18—O6^vi	37.9 (7)
O8—O2—O9^iv	85.2 (11)	U3—O18—O13^vi	70.3 (8)
O8—O2—O11	43.2 (8)	U3—O18—O15^vi	35.1 (7)
O8—O2—O12^xii	90.5 (11)	U3—O18—O17	28.1 (6)
O8—O2—O13ⁱⁱⁱ	138.0 (12)	U3—O18—O20	86.3 (12)
O8—O2—O14^v	121.0 (11)	U3—O18—O24^v	162.8 (7)
O8—O2—O16	46.7 (9)	U3—O18—O25	69.1 (7)
O8—O2—O21^xii	96.6 (11)	U3—O18—O28	113.6 (13)
O9^iv—O2—O11	124.6 (15)	U5—O18—Ca1	146.5 (17)
O9^iv—O2—O12^xii	149.7 (14)	U5—O18—K2ⁱ	128.0 (14)
O9^iv—O2—O13ⁱⁱⁱ	64.8 (11)	U5—O18—O4^v	49.6 (9)
O9^iv—O2—O14^v	69.6 (9)	U5—O18—O5^vi	50.0 (10)
O9^iv—O2—O16	68.6 (10)	U5—O18—O6^vi	50.0 (9)
O9^iv—O2—O21^xii	81.7 (10)	U5—O18—O13^vi	88.9 (9)
O11—O2—O12^xii	66.0 (10)	U5—O18—O15^vi	52.2 (10)
O11—O2—O13ⁱⁱⁱ	136.9 (13)	U5—O18—O17	98.1 (14)
O11—O2—O14^v	145.7 (14)	U5—O18—O20	133.1 (13)
O11—O2—O16	82.5 (12)	U5—O18—O24^v	93.1 (13)
O11—O2—O21^xii	85.4 (12)	U5—O18—O25	1.6 (7)
O12^xii—O2—O13ⁱⁱⁱ	130.2 (15)	U5—O18—O28	133.9 (12)
O12^xii—O2—O14^v	87.3 (10)	Ca1—O18—K2ⁱ	84.6 (6)
O12^xii—O2—O16	86.7 (11)	Ca1—O18—O4^v	137.5 (9)
O12^xii—O2—O21^xii	128.6 (10)	Ca1—O18—O5^vi	161.5 (10)
O13ⁱⁱⁱ—O2—O14^v	76.8 (11)	Ca1—O18—O6^vi	97.8 (12)
O13ⁱⁱⁱ—O2—O16	131.3 (11)	Ca1—O18—O13^vi	90.0 (9)
O13ⁱⁱⁱ—O2—O21^xii	52.6 (11)	Ca1—O18—O15^vi	104.7 (13)
O14^v—O2—O16	74.4 (11)	Ca1—O18—O17	50.5 (9)
O14^v—O2—O21^xii	128.9 (13)	Ca1—O18—O20	51.9 (8)
O16—O2—O21^xii	132.6 (13)	Ca1—O18—O24^v	117.6 (9)
U2—O3—K1	118.9 (15)	Ca1—O18—O25	146.0 (13)
U2—O3—O2	49.0 (10)	Ca1—O18—O28	52.2 (10)
U2—O3—O7	55.9 (10)	K2ⁱ—O18—O4^v	105.4 (12)
U2—O3—O8	51.5 (10)	K2ⁱ—O18—O5^vi	78.1 (10)
U2—O3—O9^iv	56.4 (9)	K2ⁱ—O18—O6^vi	176.4 (13)
U2—O3—O10	112.3 (13)	K2ⁱ—O18—O13^vi	80.2 (8)
U2—O3—O11	65.3 (8)	K2ⁱ—O18—O15^vi	127.0 (9)
U2—O3—O16	2.3 (7)	K2ⁱ—O18—O17	124.3 (9)
U2—O3—O21^xii	123.0 (16)	K2ⁱ—O18—O20	59.7 (10)
U2—O3—O22	118.6 (13)	K2ⁱ—O18—O24^v	48.9 (7)
U2—O3—O25^xv	167.6 (14)	K2ⁱ—O18—O25	128.1 (10)
U2—O3—O27^ix	123.1 (11)	K2ⁱ—O18—O28	76.5 (9)
K1—O3—O2	142.9 (10)	O4^v—O18—O5^vi	55.2 (8)
K1—O3—O7	86.1 (11)	O4^v—O18—O6^vi	71.1 (9)
K1—O3—O8	67.8 (10)	O4^v—O18—O13^vi	132.1 (9)
K1—O3—O9^iv	155.1 (12)	O4^v—O18—O15^vi	101.4 (9)
K1—O3—O10	57.7 (8)	O4^v—O18—O17	129.6 (11)
K1—O3—O11	87.4 (9)	O4^v—O18—O20	164.0 (16)
K1—O3—O16	117.8 (11)	O4^v—O18—O24^v	56.6 (9)
K1—O3—O21^xii	110.2 (9)	O4^v—O18—O25	51.1 (7)
K1—O3—O22	110.8 (10)	O4^v—O18—O28	89.3 (12)
K1—O3—O25^xv	58.9 (8)	O5^vi—O18—O6^vi	99.8 (9)
K1—O3—O27^ix	61.6 (8)	O5^vi—O18—O13^vi	80.9 (9)
O2—O3—O7	102.9 (9)	O5^vi—O18—O15^vi	81.2 (10)
O2—O3—O8	87.4 (10)	O5^vi—O18—O17	137.7 (11)
O2—O3—O9^iv	56.2 (8)	O5^vi—O18—O20	112.4 (11)
O2—O3—O10	154.3 (10)	O5^vi—O18—O24^v	53.8 (9)
O2—O3—O11	55.5 (9)	O5^vi—O18—O25	50.2 (8)
O2—O3—O16	51.1 (8)	O5^vi—O18—O28	127.8 (16)
O2—O3—O21^xii	74.5 (12)	O6^vi—O18—O13^vi	102.3 (10)
O2—O3—O22	103.9 (15)	O6^vi—O18—O15^vi	55.0 (8)
O2—O3—O25^xv	141.0 (14)	O6^vi—O18—O17	59.2 (10)
O2—O3—O27^ix	94.4 (10)	O6^vi—O18—O20	123.8 (16)
O7—O3—O8	55.9 (8)	O6^vi—O18—O24^v	127.6 (11)
O7—O3—O9^iv	71.3 (10)	O6^vi—O18—O25	50.0 (7)
O7—O3—O10	56.5 (9)	O6^vi—O18—O28	102.9 (11)
O7—O3—O11	106.9 (10)	O13^vi—O18—O15^vi	48.5 (8)
O7—O3—O16	53.6 (8)	O13^vi—O18—O17	70.2 (10)
O7—O3—O21^xii	156.6 (13)	O13^vi—O18—O20	44.4 (8)
O7—O3—O22	96.4 (11)	O13^vi—O18—O24^v	114.1 (10)
O7—O3—O25^xv	112.0 (11)	O13^vi—O18—O25	87.4 (7)
O7—O3—O27^ix	143.2 (15)	O13^vi—O18—O28	136.8 (10)
O8—O3—O9^iv	105.6 (10)	O15^vi—O18—O17	56.6 (10)
O8—O3—O10	91.5 (12)	O15^vi—O18—O20	85.2 (12)
O8—O3—O11	54.5 (9)	O15^vi—O18—O24^v	134.9 (11)
O8—O3—O16	50.9 (8)	O15^vi—O18—O25	50.7 (8)
O8—O3—O21^xii	145.2 (10)	O15^vi—O18—O28	148.7 (16)
O8—O3—O22	152.0 (13)	O17—O18—O20	66.1 (12)
O8—O3—O25^xv	126.3 (14)	O17—O18—O24^v	168.1 (9)
O8—O3—O27^ix	93.3 (10)	O17—O18—O25	97.2 (10)
O9^iv—O3—O10	99.7 (9)	O17—O18—O28	94.0 (13)
O9^iv—O3—O11	108.7 (10)	O20—O18—O24^v	108.6 (12)
O9^iv—O3—O16	56.4 (8)	O20—O18—O25	131.5 (10)
O9^iv—O3—O21^xii	88.9 (13)	O20—O18—O28	92.4 (10)
O9^iv—O3—O22	63.1 (10)	O24^v—O18—O25	94.1 (9)
O9^iv—O3—O25^xv	119.6 (11)	O24^v—O18—O28	75.3 (13)
O9^iv—O3—O27^ix	143.1 (15)	O25—O18—O28	135.3 (10)
O10—O3—O11	140.0 (15)	U4—O19—Ca1^xxi	123.6 (12)
O10—O3—O16	110.1 (10)	U4—O19—O1	88.7 (10)
O10—O3—O21^xii	117.5 (10)	U4—O19—O4	52.7 (11)
O10—O3—O22	67.2 (12)	U4—O19—O5ⁱ	49.5 (12)
O10—O3—O25^xv	55.5 (8)	U4—O19—O6	50.8 (9)
O10—O3—O27^ix	111.4 (10)	U4—O19—O8	49.2 (9)
O11—O3—O16	67.0 (7)	U4—O19—O11	53.9 (12)
O11—O3—O21^xii	91.0 (11)	U4—O19—O12^xii	105.4 (16)
O11—O3—O22	151.5 (16)	U4—O19—O16	94.1 (13)
O11—O3—O25^xv	125.0 (9)	U4—O19—O17^xxi	89.8 (13)
O11—O3—O27^ix	57.8 (8)	U4—O19—O20	142.5 (15)
O16—O3—O21^xii	125.0 (12)	U4—O19—O21^xxi	127 (2)
O16—O3—O22	118.1 (10)	U4—O19—O22^xiii	115.4 (17)
O16—O3—O25^xv	165.3 (11)	U4—O19—O24	1.6 (10)
O16—O3—O27^ix	124.7 (8)	U4—O19—O28^xxi	136.4 (14)
O21^xii—O3—O22	62.6 (11)	Ca1^xxi—O19—O1	141.9 (10)
O21^xii—O3—O25^xv	66.5 (9)	Ca1^xxi—O19—O4	133.9 (15)
O21^xii—O3—O27^ix	59.6 (10)	Ca1^xxi—O19—O5ⁱ	88.8 (10)
O22—O3—O25^xv	56.5 (9)	Ca1^xxi—O19—O6	74.6 (7)
O22—O3—O27^ix	110.8 (11)	Ca1^xxi—O19—O8	169.5 (12)
O25^xv—O3—O27^ix	67.8 (7)	Ca1^xxi—O19—O11	117.2 (10)
Ca1^xii—K2—O2^xii	94.1 (6)	Ca1^xxi—O19—O12^xii	82.2 (8)
Ca1^xii—K2—O5^xvi	93.4 (6)	Ca1^xxi—O19—O16	134.9 (12)
Ca1^xii—K2—O10^xvii	163.7 (6)	Ca1^xxi—O19—O17^xxi	38.3 (6)
Ca1^xii—K2—O12^xvii	117.2 (8)	Ca1^xxi—O19—O20	93.8 (10)
Ca1^xii—K2—O14^xviii	104.0 (7)	Ca1^xxi—O19—O21^xxi	40.4 (7)
Ca1^xii—K2—O16^xii	45.3 (6)	Ca1^xxi—O19—O22^xiii	95.4 (9)
Ca1^xii—K2—O18^xii	43.1 (5)	Ca1^xxi—O19—O24	123.9 (8)
Ca1^xii—K2—O20^xii	41.5 (7)	Ca1^xxi—O19—O28^xxi	38.6 (8)
Ca1^xii—K2—O23^xix	118.5 (8)	O1—O19—O4	48.9 (7)
Ca1^xii—K2—O24^xviii	108.2 (7)	O1—O19—O5ⁱ	100.9 (11)
Ca1^xii—K2—O28^xx	101.7 (8)	O1—O19—O6	139.4 (12)
Ca1^xii—K2—O28^xii	38.6 (8)	O1—O19—O8	48.5 (8)
O2^xii—K2—O5^xvi	169.9 (9)	O1—O19—O11	97.4 (10)
O2^xii—K2—O10^xvii	83.1 (8)	O1—O19—O12^xii	110.2 (11)
O2^xii—K2—O12^xvii	50.8 (6)	O1—O19—O16	47.8 (8)
O2^xii—K2—O14^xviii	49.8 (6)	O1—O19—O17^xxi	139.4 (14)
O2^xii—K2—O16^xii	48.9 (8)	O1—O19—O20	58.3 (10)
O2^xii—K2—O18^xii	136.1 (7)	O1—O19—O21^xxi	105.6 (11)
O2^xii—K2—O20^xii	95.5 (8)	O1—O19—O22^xiii	48.9 (8)
O2^xii—K2—O23^xix	128.9 (7)	O1—O19—O24	89.0 (8)
O2^xii—K2—O24^xviii	118.0 (9)	O1—O19—O28^xxi	129.0 (12)
O2^xii—K2—O28^xx	93.1 (6)	O4—O19—O5ⁱ	52.8 (9)
O2^xii—K2—O28^xii	90.5 (6)	O4—O19—O6	95.2 (12)
O5^xvi—K2—O10^xvii	87.8 (8)	O4—O19—O8	50.8 (9)
O5^xvi—K2—O12^xvii	130.1 (7)	O4—O19—O11	96.0 (11)
O5^xvi—K2—O14^xviii	121.6 (8)	O4—O19—O12^xii	143.1 (13)
O5^xvi—K2—O16^xii	138.1 (8)	O4—O19—O16	87.3 (9)
O5^xvi—K2—O18^xii	50.5 (7)	O4—O19—O17^xxi	100.6 (13)
O5^xvi—K2—O20^xii	94.6 (8)	O4—O19—O20	105.1 (13)
O5^xvi—K2—O23^xix	51.7 (6)	O4—O19—O21^xxi	100.2 (16)
O5^xvi—K2—O24^xviii	53.0 (8)	O4—O19—O22^xiii	63.0 (10)
O5^xvi—K2—O28^xx	91.9 (6)	O4—O19—O24	53.8 (9)
O5^xvi—K2—O28^xii	91.2 (6)	O4—O19—O28^xxi	168.8 (16)
O10^xvii—K2—O12^xvii	73.2 (9)	O5ⁱ—O19—O6	52.7 (10)
O10^xvii—K2—O14^xviii	62.1 (8)	O5ⁱ—O19—O8	89.6 (11)
O10^xvii—K2—O16^xii	129.4 (9)	O5ⁱ—O19—O11	99.8 (12)
O10^xvii—K2—O18^xii	134.2 (9)	O5ⁱ—O19—O12^xii	139.9 (11)
O10^xvii—K2—O20^xii	154.7 (8)	O5ⁱ—O19—O16	136.2 (10)
O10^xvii—K2—O23^xix	74.7 (9)	O5ⁱ—O19—O17^xxi	50.7 (8)
O10^xvii—K2—O24^xviii	60.1 (9)	O5ⁱ—O19—O20	145.9 (19)
O10^xvii—K2—O28^xx	94.5 (9)	O5ⁱ—O19—O21^xxi	77.5 (14)
O10^xvii—K2—O28^xii	125.1 (10)	O5ⁱ—O19—O22^xiii	88.2 (14)
O12^xvii—K2—O14^xviii	89.8 (8)	O5ⁱ—O19—O24	50.9 (9)
O12^xvii—K2—O16^xii	84.5 (8)	O5ⁱ—O19—O28^xxi	125.1 (11)
O12^xvii—K2—O18^xii	145.7 (10)	O6—O19—O8	96.2 (11)
O12^xvii—K2—O20^xii	86.3 (10)	O6—O19—O11	63.8 (9)
O12^xvii—K2—O23^xix	78.7 (8)	O6—O19—O12^xii	87.3 (11)
O12^xvii—K2—O24^xviii	133.3 (11)	O6—O19—O16	127.2 (13)
O12^xvii—K2—O28^xx	46.2 (8)	O6—O19—O17^xxi	51.5 (8)
O12^xvii—K2—O28^xii	137.4 (8)	O6—O19—O20	159.3 (19)
O14^xviii—K2—O16^xii	73.3 (9)	O6—O19—O21^xxi	98.2 (12)
O14^xviii—K2—O18^xii	119.7 (7)	O6—O19—O22^xiii	139.0 (18)
O14^xviii—K2—O20^xii	134.1 (9)	O6—O19—O24	50.6 (8)
O14^xviii—K2—O23^xix	136.7 (11)	O6—O19—O28^xxi	90.0 (10)
O14^xviii—K2—O24^xviii	68.6 (8)	O8—O19—O11	52.9 (9)
O14^xviii—K2—O28^xx	135.8 (7)	O8—O19—O12^xii	92.3 (13)
O14^xviii—K2—O28^xii	72.4 (9)	O8—O19—O16	47.4 (9)
O16^xii—K2—O18^xii	87.7 (8)	O8—O19—O17^xxi	138.1 (13)
O16^xii—K2—O20^xii	60.8 (9)	O8—O19—O20	93.3 (12)
O16^xii—K2—O23^xix	144.7 (10)	O8—O19—O21^xxi	148.7 (16)
O16^xii—K2—O24^xviii	123.9 (8)	O8—O19—O22^xiii	94.9 (10)
O16^xii—K2—O28^xx	101.9 (8)	O8—O19—O24	48.7 (7)
O16^xii—K2—O28^xii	53.6 (7)	O8—O19—O28^xxi	138.5 (18)
O18^xii—K2—O20^xii	61.0 (9)	O11—O19—O12^xii	52.4 (10)
O18^xii—K2—O23^xix	89.0 (7)	O11—O19—O16	63.4 (9)
O18^xii—K2—O24^xviii	77.6 (9)	O11—O19—O17^xxi	114.0 (9)
O18^xii—K2—O28^xx	103.7 (8)	O11—O19—O20	108.9 (18)
O18^xii—K2—O28^xii	51.4 (7)	O11—O19—O21^xxi	156.9 (11)
O20^xii—K2—O23^xix	87.1 (9)	O11—O19—O22^xiii	146.3 (11)
O20^xii—K2—O24^xviii	138.6 (10)	O11—O19—O24	52.4 (9)
O20^xii—K2—O28^xx	60.2 (10)	O11—O19—O28^xxi	95.2 (14)
O20^xii—K2—O28^xii	80.1 (11)	O12^xii—O19—O16	62.9 (9)
O23^xix—K2—O24^xviii	89.5 (8)	O12^xii—O19—O17^xxi	109.3 (9)
O23^xix—K2—O28^xx	45.2 (7)	O12^xii—O19—O20	74.0 (15)
O23^xix—K2—O28^xii	139.7 (8)	O12^xii—O19—O21^xxi	116.0 (12)
O24^xviii—K2—O28^xx	134.2 (8)	O12^xii—O19—O22^xiii	131.5 (13)
O24^xviii—K2—O28^xii	76.2 (9)	O12^xii—O19—O24	103.9 (11)
O28^xx—K2—O28^xii	140.3 (12)	O12^xii—O19—O28^xxi	46.9 (10)
U1—O4—U4	108.0 (14)	O16—O19—O17^xxi	172.0 (13)
U1—O4—U5^viii	146.4 (16)	O16—O19—O20	51.3 (10)
U1—O4—O1	39.7 (7)	O16—O19—O21^xxi	133.4 (12)
U1—O4—O5ⁱ	160.3 (17)	O16—O19—O22^xiii	88.2 (9)
U1—O4—O6ⁱ	106.6 (11)	O16—O19—O24	93.2 (9)
U1—O4—O8	54.7 (9)	O16—O19—O28^xxi	97.5 (13)
U1—O4—O11ⁱ	50.5 (8)	O17^xxi—O19—O20	126.5 (13)
U1—O4—O12	38.7 (7)	O17^xxi—O19—O21^xxi	46.7 (9)
U1—O4—O18^viii	125.9 (12)	O17^xxi—O19—O22^xiii	96.4 (12)
U1—O4—O19	105.0 (14)	O17^xxi—O19—O24	90.5 (9)
U1—O4—O22^xiii	93.5 (10)	O17^xxi—O19—O28^xxi	74.9 (9)
U1—O4—O24	102.3 (12)	O20—O19—O21^xxi	82.7 (13)
U1—O4—O25^viii	135.8 (13)	O20—O19—O22^xiii	57.7 (14)
U4—O4—U5^viii	104.0 (9)	O20—O19—O24	142.0 (12)
U4—O4—O1	101.4 (13)	O20—O19—O28^xxi	70.9 (12)
U4—O4—O5ⁱ	52.7 (9)	O21^xxi—O19—O22^xiii	56.7 (9)
U4—O4—O6ⁱ	144.1 (10)	O21^xxi—O19—O24	128.2 (16)
U4—O4—O8	53.3 (9)	O21^xxi—O19—O28^xxi	69.2 (12)
U4—O4—O11ⁱ	158.0 (13)	O22^xiii—O19—O24	116.7 (12)
U4—O4—O12	105.2 (13)	O22^xiii—O19—O28^xxi	106.8 (11)
U4—O4—O18^viii	96.8 (10)	O24—O19—O28^xxi	135.4 (11)
U4—O4—O19	37.1 (7)	Ca1—O20—O1	49.5 (9)
U4—O4—O22^xiii	101.1 (12)	Ca1—O20—K2ⁱ	85.7 (13)
U4—O4—O24	36.6 (7)	Ca1—O20—O12^xii	120.3 (15)
U4—O4—O25^viii	104.7 (10)	Ca1—O20—O13^vi	128.5 (14)
U5^viii—O4—O1	140.9 (14)	Ca1—O20—O15^vi	80.3 (9)
U5^viii—O4—O5ⁱ	51.7 (9)	Ca1—O20—O16	56.8 (8)
U5^viii—O4—O6ⁱ	40.4 (7)	Ca1—O20—O17	47.6 (8)
U5^viii—O4—O8	154.9 (13)	Ca1—O20—O18	54.4 (8)
U5^viii—O4—O11ⁱ	98.0 (13)	Ca1—O20—O19	124.6 (15)
U5^viii—O4—O12	121.8 (14)	Ca1—O20—O21^xxi	139 (2)
U5^viii—O4—O18^viii	38.2 (6)	Ca1—O20—O22^xiii	86.0 (15)
U5^viii—O4—O19	106.6 (11)	Ca1—O20—O28^xxi	161 (2)
U5^viii—O4—O22^xiii	90.3 (11)	O1—O20—K2ⁱ	117.9 (12)
U5^viii—O4—O24	97.0 (10)	O1—O20—O12^xii	116.4 (11)
U5^viii—O4—O25^viii	39.5 (7)	O1—O20—O13^vi	136 (2)
O1—O4—O5ⁱ	138.3 (14)	O1—O20—O15^vi	111.5 (12)
O1—O4—O6ⁱ	111.3 (11)	O1—O20—O16	58.6 (10)
O1—O4—O8	62.2 (11)	O1—O20—O17	66.5 (11)
O1—O4—O11ⁱ	60.0 (9)	O1—O20—O18	103.6 (11)
O1—O4—O12	78.4 (9)	O1—O20—O19	77.4 (12)
O1—O4—O18^viii	160.1 (13)	O1—O20—O21^xxi	99.5 (14)
O1—O4—O19	77.4 (11)	O1—O20—O22^xiii	56.6 (11)
O1—O4—O22^xiii	55.6 (10)	O1—O20—O28^xxi	142.1 (12)
O1—O4—O24	120.8 (14)	K2ⁱ—O20—O12^xii	46.6 (8)
O1—O4—O25^viii	105.2 (12)	K2ⁱ—O20—O13^vi	104.3 (17)
O5ⁱ—O4—O6ⁱ	92.1 (11)	K2ⁱ—O20—O15^vi	96.7 (11)
O5ⁱ—O4—O8	105.8 (13)	K2ⁱ—O20—O16	61.2 (11)
O5ⁱ—O4—O11ⁱ	149.1 (15)	K2ⁱ—O20—O17	116.9 (12)
O5ⁱ—O4—O12	135.0 (13)	K2ⁱ—O20—O18	59.2 (11)
O5ⁱ—O4—O18^viii	60.7 (9)	K2ⁱ—O20—O19	111.4 (17)
O5ⁱ—O4—O19	62.6 (11)	K2ⁱ—O20—O21^xxi	134.9 (13)
O5ⁱ—O4—O22^xiii	94.1 (11)	K2ⁱ—O20—O22^xiii	171.6 (13)
O5ⁱ—O4—O24	60.5 (9)	K2ⁱ—O20—O28^xxi	75.0 (13)
O5ⁱ—O4—O25^viii	61.2 (9)	O12^xii—O20—O13^vi	100.7 (14)
O6ⁱ—O4—O8	158.8 (11)	O12^xii—O20—O15^vi	129.4 (13)
O6ⁱ—O4—O11ⁱ	57.8 (9)	O12^xii—O20—O16	67.8 (10)
O6ⁱ—O4—O12	95.8 (11)	O12^xii—O20—O17	163.3 (15)
O6ⁱ—O4—O18^viii	54.1 (9)	O12^xii—O20—O18	105.2 (16)
O6ⁱ—O4—O19	137.4 (12)	O12^xii—O20—O19	66.1 (12)
O6ⁱ—O4—O22^xiii	86.0 (12)	O12^xii—O20—O21^xxi	95.6 (9)
O6ⁱ—O4—O24	125.0 (12)	O12^xii—O20—O22^xiii	140.3 (12)
O6ⁱ—O4—O25^viii	53.3 (9)	O12^xii—O20—O28^xxi	44.6 (9)
O8—O4—O11ⁱ	105.1 (10)	O13^vi—O20—O15^vi	48.7 (8)
O8—O4—O12	63.6 (11)	O13^vi—O20—O16	165 (2)
O8—O4—O18^viii	125.6 (13)	O13^vi—O20—O17	84.8 (13)
O8—O4—O19	63.0 (12)	O13^vi—O20—O18	87.4 (11)
O8—O4—O22^xiii	103.6 (14)	O13^vi—O20—O19	98.9 (14)
O8—O4—O24	58.7 (10)	O13^vi—O20—O21^xxi	52.0 (11)
O8—O4—O25^viii	146.2 (15)	O13^vi—O20—O22^xiii	80.1 (16)
O11ⁱ—O4—O12	61.9 (9)	O13^vi—O20—O28^xxi	58.2 (11)
O11ⁱ—O4—O18^viii	100.5 (12)	O15^vi—O20—O16	131.2 (11)
O11ⁱ—O4—O19	134.7 (12)	O15^vi—O20—O17	45.0 (7)
O11ⁱ—O4—O22^xiii	78.5 (10)	O15^vi—O20—O18	46.7 (7)
O11ⁱ—O4—O24	140.5 (11)	O15^vi—O20—O19	142.5 (16)
O11ⁱ—O4—O25^viii	92.2 (11)	O15^vi—O20—O21^xxi	91.6 (10)
O12—O4—O18^viii	89.1 (11)	O15^vi—O20—O22^xiii	80.7 (11)
O12—O4—O19	126.6 (15)	O15^vi—O20—O28^xxi	101.2 (9)
O12—O4—O22^xiii	130.6 (10)	O16—O20—O17	103.8 (11)
O12—O4—O24	79.2 (10)	O16—O20—O18	86.9 (12)
O12—O4—O25^viii	148.5 (15)	O16—O20—O19	85.2 (12)
O18^viii—O4—O19	122.4 (10)	O16—O20—O21^xxi	135.6 (12)
O18^viii—O4—O22^xiii	128.3 (13)	O16—O20—O22^xiii	114.7 (15)
O18^viii—O4—O24	71.0 (10)	O16—O20—O28^xxi	112.1 (15)
O18^viii—O4—O25^viii	77.6 (10)	O17—O20—O18	59.1 (10)
O19—O4—O22^xiii	64.2 (11)	O17—O20—O19	129 (2)
O19—O4—O24	73.7 (10)	O17—O20—O21^xxi	100.1 (14)
O19—O4—O25^viii	84.1 (11)	O17—O20—O22^xiii	55.9 (11)
O22^xiii—O4—O24	137.6 (13)	O17—O20—O28^xxi	143.0 (12)
O22^xiii—O4—O25^viii	51.1 (10)	O18—O20—O19	170 (2)
O24—O4—O25^viii	121.5 (9)	O18—O20—O21^xxi	137.4 (12)
U3^xx—O5—U4^xii	111.8 (15)	O18—O20—O22^xiii	114.5 (15)
U3^xx—O5—U5^xxi	137.2 (15)	O18—O20—O28^xxi	112.9 (15)
U3^xx—O5—K2^xiii	89.6 (8)	O19—O20—O21^xxi	51.0 (11)
U3^xx—O5—O4^xii	168.7 (18)	O19—O20—O22^xiii	74.6 (15)
U3^xx—O5—O6^xii	57.2 (9)	O19—O20—O28^xxi	64.9 (10)
U3^xx—O5—O15	103.3 (11)	O21^xxi—O20—O22^xiii	53.4 (10)
U3^xx—O5—O17^xx	38.4 (6)	O21^xxi—O20—O28^xxi	59.9 (10)
U3^xx—O5—O18^xxi	125.5 (12)	O22^xiii—O20—O28^xxi	113.2 (14)
U3^xx—O5—O19^xii	104.7 (13)	Ca1—O21—O1	55.0 (8)
U3^xx—O5—O21^xx	85.5 (9)	Ca1—O21—O2ⁱ	98.8 (10)
U3^xx—O5—O23^xx	38.1 (7)	Ca1—O21—O3ⁱ	142.9 (13)
U3^xx—O5—O24^xii	108.3 (12)	Ca1—O21—O5^vii	100.5 (10)
U3^xx—O5—O25^xxi	121.2 (12)	Ca1—O21—O13ⁱⁱ	84.2 (14)
U3^xx—O5—O26	56.0 (9)	Ca1—O21—O17	56.4 (9)
U4^xii—O5—U5^xxi	110.9 (10)	Ca1—O21—O19^vi	89.9 (14)
U4^xii—O5—K2^xiii	86.4 (9)	Ca1—O21—O20^vi	100.5 (16)
U4^xii—O5—O4^xii	57.7 (9)	Ca1—O21—O22ⁱ	154 (2)
U4^xii—O5—O6^xii	54.7 (9)	Ca1—O21—O25^xxiv	145.7 (13)
U4^xii—O5—O15	144.6 (10)	Ca1—O21—O27^xiii	99.7 (11)
U4^xii—O5—O17^xx	104.0 (13)	Ca1—O21—O28	41.1 (9)
U4^xii—O5—O18^xxi	102.9 (10)	O1—O21—O2ⁱ	53.2 (8)
U4^xii—O5—O19^xii	37.8 (8)	O1—O21—O3ⁱ	87.9 (12)
U4^xii—O5—O21^xx	87.2 (11)	O1—O21—O5^vii	129.7 (12)
U4^xii—O5—O23^xx	112.3 (13)	O1—O21—O13ⁱⁱ	82.5 (11)
U4^xii—O5—O24^xii	39.1 (7)	O1—O21—O17	79.5 (10)
U4^xii—O5—O25^xxi	110.9 (10)	O1—O21—O19^vi	144.7 (16)
U4^xii—O5—O26	165.0 (15)	O1—O21—O20^vi	129.0 (15)
U5^xxi—O5—K2^xiii	91.1 (9)	O1—O21—O22ⁱ	138.9 (14)
U5^xxi—O5—O4^xii	53.6 (9)	O1—O21—O25^xxiv	128.4 (17)
U5^xxi—O5—O6^xii	164.7 (13)	O1—O21—O27^xiii	65.6 (11)
U5^xxi—O5—O15	34.0 (7)	O1—O21—O28	84.7 (12)
U5^xxi—O5—O17^xx	129.3 (14)	O2ⁱ—O21—O3ⁱ	50.7 (8)
U5^xxi—O5—O18^xxi	39.7 (7)	O2ⁱ—O21—O5^vii	154.7 (15)
U5^xxi—O5—O19^xii	110.0 (10)	O2ⁱ—O21—O13ⁱⁱ	54.8 (10)
U5^xxi—O5—O21^xx	98.5 (11)	O2ⁱ—O21—O17	130.5 (12)
U5^xxi—O5—O23^xx	119.6 (14)	O2ⁱ—O21—O19^vi	143.2 (14)
U5^xxi—O5—O24^xii	103.3 (10)	O2ⁱ—O21—O20^vi	96.9 (10)
U5^xxi—O5—O25^xxi	40.5 (8)	O2ⁱ—O21—O22ⁱ	86.2 (9)
U5^xxi—O5—O26	82.0 (12)	O2ⁱ—O21—O25^xxiv	107.7 (12)
K2^xiii—O5—O4^xii	93.6 (9)	O2ⁱ—O21—O27^xiii	81.5 (11)
K2^xiii—O5—O6^xii	83.4 (10)	O2ⁱ—O21—O28	101.4 (11)
K2^xiii—O5—O15	89.3 (9)	O3ⁱ—O21—O5^vii	104.9 (12)
K2^xiii—O5—O17^xx	127.4 (9)	O3ⁱ—O21—O13ⁱⁱ	91.0 (12)
K2^xiii—O5—O18^xxi	51.4 (7)	O3ⁱ—O21—O17	123.3 (18)
K2^xiii—O5—O19^xii	123.9 (11)	O3ⁱ—O21—O19^vi	127.0 (11)
K2^xiii—O5—O21^xx	169.8 (12)	O3ⁱ—O21—O20^vi	103.5 (10)
K2^xiii—O5—O23^xx	52.6 (7)	O3ⁱ—O21—O22ⁱ	57.2 (10)
K2^xiii—O5—O24^xii	47.4 (7)	O3ⁱ—O21—O25^xxiv	56.9 (9)
K2^xiii—O5—O25^xxi	131.5 (12)	O3ⁱ—O21—O27^xiii	59.8 (11)
K2^xiii—O5—O26	101.3 (10)	O3ⁱ—O21—O28	147.9 (13)
O4^xii—O5—O6^xii	112.3 (14)	O5^vii—O21—O13ⁱⁱ	143.6 (15)
O4^xii—O5—O15	87.6 (11)	O5^vii—O21—O17	52.6 (8)
O4^xii—O5—O17^xx	135.7 (13)	O5^vii—O21—O19^vi	53.1 (10)
O4^xii—O5—O18^xxi	64.1 (10)	O5^vii—O21—O20^vi	95.6 (9)
O4^xii—O5—O19^xii	64.6 (10)	O5^vii—O21—O22ⁱ	83.8 (9)
O4^xii—O5—O21^xx	89.5 (10)	O5^vii—O21—O25^xxiv	48.7 (8)
O4^xii—O5—O23^xx	146.3 (13)	O5^vii—O21—O27^xiii	79.2 (11)
O4^xii—O5—O24^xii	66.8 (9)	O5^vii—O21—O28	103.9 (11)
O4^xii—O5—O25^xxi	63.7 (10)	O13ⁱⁱ—O21—O17	140.1 (17)
O4^xii—O5—O26	133.5 (15)	O13ⁱⁱ—O21—O19^vi	91.1 (16)
O6^xii—O5—O15	159.1 (10)	O13ⁱⁱ—O21—O20^vi	48.5 (10)
O6^xii—O5—O17^xx	64.1 (10)	O13ⁱⁱ—O21—O22ⁱ	77.6 (12)
O6^xii—O5—O18^xxi	132.6 (14)	O13ⁱⁱ—O21—O25^xxiv	128.9 (12)
O6^xii—O5—O19^xii	62.6 (11)	O13ⁱⁱ—O21—O27^xiii	136.0 (15)
O6^xii—O5—O21^xx	86.4 (12)	O13ⁱⁱ—O21—O28	57.1 (12)
O6^xii—O5—O23^xx	67.8 (10)	O17—O21—O19^vi	83.7 (11)
O6^xii—O5—O24^xii	62.7 (10)	O17—O21—O20^vi	127.1 (15)
O6^xii—O5—O25^xxi	143.9 (15)	O17—O21—O22ⁱ	136.1 (14)
O6^xii—O5—O26	113.0 (11)	O17—O21—O25^xxiv	89.6 (12)
O15—O5—O17^xx	106.5 (11)	O17—O21—O27^xiii	64.7 (12)
O15—O5—O18^xxi	49.7 (9)	O17—O21—O28	85.9 (12)
O15—O5—O19^xii	136.0 (11)	O19^vi—O21—O20^vi	46.3 (10)
O15—O5—O21^xx	100.5 (11)	O19^vi—O21—O22ⁱ	71.7 (11)
O15—O5—O23^xx	92.3 (11)	O19^vi—O21—O25^xxiv	81.9 (11)
O15—O5—O24^xii	124.3 (12)	O19^vi—O21—O27^xiii	132.4 (15)
O15—O5—O25^xxi	50.2 (9)	O19^vi—O21—O28	63.2 (12)
O15—O5—O26	49.3 (9)	O20^vi—O21—O22ⁱ	53.1 (13)
O17^xx—O5—O18^xxi	152.9 (14)	O20^vi—O21—O25^xxiv	97.6 (10)
O17^xx—O5—O19^xii	77.4 (10)	O20^vi—O21—O27^xiii	159.7 (13)
O17^xx—O5—O21^xx	47.2 (7)	O20^vi—O21—O28	59.4 (11)
O17^xx—O5—O23^xx	76.4 (9)	O22ⁱ—O21—O25^xxiv	52.1 (10)
O17^xx—O5—O24^xii	126.7 (14)	O22ⁱ—O21—O27^xiii	106.7 (16)
O17^xx—O5—O25^xxi	93.2 (11)	O22ⁱ—O21—O28	112.5 (16)
O17^xx—O5—O26	61.1 (10)	O25^xxiv—O21—O27^xiii	64.2 (11)
O18^xxi—O5—O19^xii	127.7 (10)	O25^xxiv—O21—O28	145.1 (12)
O18^xxi—O5—O21^xx	138.0 (11)	O27^xiii—O21—O28	140.8 (10)
O18^xxi—O5—O23^xx	90.5 (11)	Ca1^xvi—O22—O1^xvi	41.2 (8)
O18^xxi—O5—O24^xii	74.7 (10)	Ca1^xvi—O22—O3	149.2 (12)
O18^xxi—O5—O25^xxi	80.2 (11)	Ca1^xvi—O22—O4^xvi	90.1 (10)
O18^xxi—O5—O26	91.9 (13)	Ca1^xvi—O22—O9^iv	92.0 (11)
O19^xii—O5—O21^xx	49.4 (10)	Ca1^xvi—O22—O10	138.0 (11)
O19^xii—O5—O23^xx	130.0 (14)	Ca1^xvi—O22—O13ⁱⁱⁱ	77.4 (11)
O19^xii—O5—O24^xii	76.9 (11)	Ca1^xvi—O22—O17^xvi	40.7 (8)
O19^xii—O5—O25^xxi	86.1 (11)	Ca1^xvi—O22—O19^xvi	77.1 (12)
O19^xii—O5—O26	131.8 (13)	Ca1^xvi—O22—O20^xvi	40.2 (8)
O21^xx—O5—O23^xx	123.5 (10)	Ca1^xvi—O22—O21^xii	113.7 (17)
O21^xx—O5—O24^xii	126.1 (13)	Ca1^xvi—O22—O25^xv	145.6 (12)
O21^xx—O5—O25^xxi	58.4 (10)	Ca1^xvi—O22—O26ⁱⁱ	85.1 (8)
O21^xx—O5—O26	83.3 (11)	Ca1^xvi—O22—O27	75.6 (10)
O23^xx—O5—O24^xii	86.0 (10)	O1^xvi—O22—O3	169.5 (18)
O23^xx—O5—O25^xxi	136.9 (14)	O1^xvi—O22—O4^xvi	52.5 (8)
O23^xx—O5—O26	64.6 (9)	O1^xvi—O22—O9^iv	131.0 (15)
O24^xii—O5—O25^xxi	130.2 (10)	O1^xvi—O22—O10	113.6 (14)
O24^xii—O5—O26	147.8 (13)	O1^xvi—O22—O13ⁱⁱⁱ	111.6 (17)
O25^xxi—O5—O26	73.7 (11)	O1^xvi—O22—O17^xvi	74.0 (11)
U3^xxi—O6—U4	107.3 (14)	O1^xvi—O22—O19^xvi	69.9 (11)
U3^xxi—O6—U5^xxi	104.7 (9)	O1^xvi—O22—O20^xvi	65.1 (13)
U3^xxi—O6—O4^xii	143.8 (10)	O1^xvi—O22—O21^xii	121.4 (16)
U3^xxi—O6—O5ⁱ	52.8 (9)	O1^xvi—O22—O25^xv	106.6 (12)
U3^xxi—O6—O10^ix	103.6 (11)	O1^xvi—O22—O26ⁱⁱ	101.7 (10)
U3^xxi—O6—O11	157.6 (13)	O1^xvi—O22—O27	65.2 (10)
U3^xxi—O6—O15	51.9 (9)	O3—O22—O4^xvi	118.7 (13)
U3^xxi—O6—O17^xxi	38.0 (7)	O3—O22—O9^iv	58.3 (9)
U3^xxi—O6—O18^xxi	92.5 (10)	O3—O22—O10	58.2 (11)
U3^xxi—O6—O19	103.1 (14)	O3—O22—O13ⁱⁱⁱ	77.6 (11)
U3^xxi—O6—O23^xxi	35.3 (7)	O3—O22—O17^xvi	114.4 (11)
U3^xxi—O6—O24	105.6 (13)	O3—O22—O19^xvi	110.3 (12)
U3^xxi—O6—O25^xxi	108.7 (10)	O3—O22—O20^xvi	123.3 (15)
U4—O6—U5^xxi	144.5 (16)	O3—O22—O21^xii	60.1 (11)
U4—O6—O4^xii	104.6 (11)	O3—O22—O25^xv	63.6 (11)
U4—O6—O5ⁱ	54.7 (9)	O3—O22—O26ⁱⁱ	81.2 (10)
U4—O6—O10^ix	92.9 (9)	O3—O22—O27	112.1 (18)
U4—O6—O11	50.3 (8)	O4^xvi—O22—O9^iv	173.9 (14)
U4—O6—O15	159.1 (17)	O4^xvi—O22—O10	90.9 (13)
U4—O6—O17^xxi	103.2 (12)	O4^xvi—O22—O13ⁱⁱⁱ	122.5 (14)
U4—O6—O18^xxi	124.5 (12)	O4^xvi—O22—O17^xvi	126.5 (13)
U4—O6—O19	38.7 (6)	O4^xvi—O22—O19^xvi	52.8 (9)
U4—O6—O23^xxi	106.2 (13)	O4^xvi—O22—O20^xvi	89.1 (13)
U4—O6—O24	39.5 (6)	O4^xvi—O22—O21^xii	88.8 (10)
U4—O6—O25^xxi	135.5 (13)	O4^xvi—O22—O25^xv	55.6 (9)
U5^xxi—O6—O4^xii	40.6 (7)	O4^xvi—O22—O26ⁱⁱ	136.3 (12)
U5^xxi—O6—O5ⁱ	155.0 (13)	O4^xvi—O22—O27	91.1 (11)
U5^xxi—O6—O10^ix	94.1 (11)	O9^iv—O22—O10	91.5 (14)
U5^xxi—O6—O11	96.5 (13)	O9^iv—O22—O13ⁱⁱⁱ	52.5 (10)
U5^xxi—O6—O15	54.2 (9)	O9^iv—O22—O17^xvi	57.5 (9)
U5^xxi—O6—O17^xxi	92.7 (10)	O9^iv—O22—O19^xvi	122.2 (15)
U5^xxi—O6—O18^xxi	38.6 (6)	O9^iv—O22—O20^xvi	88.7 (14)
U5^xxi—O6—O19	118.5 (14)	O9^iv—O22—O21^xii	85.1 (10)
U5^xxi—O6—O23^xxi	108.7 (9)	O9^iv—O22—O25^xv	121.9 (15)
U5^xxi—O6—O24	140.5 (15)	O9^iv—O22—O26ⁱⁱ	49.7 (8)
U5^xxi—O6—O25^xxi	40.4 (7)	O9^iv—O22—O27	95.0 (12)
O4^xii—O6—O5ⁱ	155.8 (11)	O10—O22—O13ⁱⁱⁱ	134.3 (13)
O4^xii—O6—O10^ix	91.3 (11)	O10—O22—O17^xvi	111.9 (14)
O4^xii—O6—O11	56.1 (8)	O10—O22—O19^xvi	133.4 (13)
O4^xii—O6—O15	94.8 (11)	O10—O22—O20^xvi	178.2 (13)
O4^xii—O6—O17^xxi	117.6 (12)	O10—O22—O21^xii	108.3 (15)
O4^xii—O6—O18^xxi	54.8 (9)	O10—O22—O25^xv	54.3 (12)
O4^xii—O6—O19	91.3 (12)	O10—O22—O26ⁱⁱ	66.0 (10)
O4^xii—O6—O23^xxi	143.6 (11)	O10—O22—O27	62.4 (12)
O4^xii—O6—O24	109.8 (11)	O13ⁱⁱⁱ—O22—O17^xvi	74.6 (11)
O4^xii—O6—O25^xxi	55.0 (9)	O13ⁱⁱⁱ—O22—O19^xvi	69.8 (11)
O5ⁱ—O6—O10^ix	101.4 (13)	O13ⁱⁱⁱ—O22—O20^xvi	46.9 (11)
O5ⁱ—O6—O11	105.0 (10)	O13ⁱⁱⁱ—O22—O21^xii	49.7 (10)
O5ⁱ—O6—O15	104.6 (13)	O13ⁱⁱⁱ—O22—O25^xv	117.2 (12)
O5ⁱ—O6—O17^xxi	63.1 (10)	O13ⁱⁱⁱ—O22—O26ⁱⁱ	98.7 (9)
O5ⁱ—O6—O18^xxi	123.1 (13)	O13ⁱⁱⁱ—O22—O27	136.4 (13)
O5ⁱ—O6—O19	64.7 (12)	O17^xvi—O22—O19^xvi	113.3 (18)
O5ⁱ—O6—O23^xxi	60.6 (10)	O17^xvi—O22—O20^xvi	66.7 (13)
O5ⁱ—O6—O24	63.7 (10)	O17^xvi—O22—O21^xii	124.3 (17)
O5ⁱ—O6—O25^xxi	147.9 (15)	O17^xvi—O22—O25^xv	166 (2)
O10^ix—O6—O11	81.8 (9)	O17^xvi—O22—O26ⁱⁱ	47.2 (9)
O10^ix—O6—O15	94.3 (10)	O17^xvi—O22—O27	62.6 (10)
O10^ix—O6—O17^xxi	141.2 (13)	O19^xvi—O22—O20^xvi	47.7 (11)
O10^ix—O6—O18^xxi	132.7 (12)	O19^xvi—O22—O21^xii	51.6 (10)
O10^ix—O6—O19	130.1 (10)	O19^xvi—O22—O25^xv	79.6 (12)
O10^ix—O6—O23^xxi	68.3 (10)	O19^xvi—O22—O26ⁱⁱ	160.4 (16)
O10^ix—O6—O24	54.3 (8)	O19^xvi—O22—O27	134.1 (13)
O10^ix—O6—O25^xxi	53.8 (9)	O20^xvi—O22—O21^xii	73.5 (14)
O11—O6—O15	150.3 (15)	O20^xvi—O22—O25^xv	126.9 (15)
O11—O6—O17^xxi	135.2 (12)	O20^xvi—O22—O26ⁱⁱ	112.8 (12)
O11—O6—O18^xxi	99.6 (12)	O20^xvi—O22—O27	115.8 (15)
O11—O6—O19	59.3 (10)	O21^xii—O22—O25^xv	68.1 (11)
O11—O6—O23^xxi	141.7 (12)	O21^xii—O22—O26ⁱⁱ	132.6 (11)
O11—O6—O24	59.6 (9)	O21^xii—O22—O27	171 (2)
O11—O6—O25^xxi	92.2 (11)	O25^xv—O22—O26ⁱⁱ	120.0 (17)
O15—O6—O17^xxi	60.0 (9)	O25^xv—O22—O27	104.3 (17)
O15—O6—O18^xxi	61.7 (9)	O26ⁱⁱ—O22—O27	45.7 (8)
O15—O6—O19	135.1 (14)	U3—O23—K1^xxvi	116.9 (15)
O15—O6—O23^xxi	59.0 (10)	U3—O23—K2^xxvii	123.3 (10)
O15—O6—O24	139.1 (14)	U3—O23—O5^vii	49.6 (8)
O15—O6—O25^xxi	62.9 (10)	U3—O23—O6^vi	49.0 (10)
O17^xxi—O6—O18^xxi	63.3 (10)	U3—O23—O9^v	52.7 (9)
O17^xxi—O6—O19	77.8 (11)	U3—O23—O10^xxvi	106.3 (14)
O17^xxi—O6—O23^xxi	73.3 (10)	U3—O23—O12^xxvi	162.8 (16)
O17^xxi—O6—O24	126.7 (14)	U3—O23—O13^vii	102.8 (14)
O17^xxi—O6—O25^xxi	121.3 (10)	U3—O23—O14^xxvi	94.4 (10)
O18^xxi—O6—O19	86.9 (10)	U3—O23—O15^vi	50.6 (10)
O18^xxi—O6—O23^xxi	118.1 (10)	U3—O23—O17	3.0 (6)
O18^xxi—O6—O24	158.6 (13)	U3—O23—O26^vii	51.9 (11)
O18^xxi—O6—O25^xxi	79.0 (10)	U3—O23—O28^xiii	145.7 (15)
O19—O6—O23^xxi	125.0 (15)	K1^xxvi—O23—K2^xxvii	88.3 (8)
O19—O6—O24	78.1 (9)	K1^xxvi—O23—O5^vii	133.7 (13)
O19—O6—O25^xxi	145.6 (16)	K1^xxvi—O23—O6^vi	85.3 (10)
O23^xxi—O6—O24	83.2 (11)	K1^xxvi—O23—O9^v	100.9 (9)
O23^xxi—O6—O25^xxi	89.1 (10)	K1^xxvi—O23—O10^xxvi	49.4 (6)
O24—O6—O25^xxi	105.0 (12)	K1^xxvi—O23—O12^xxvi	52.3 (7)
U1—O7—U2	98.1 (9)	K1^xxvi—O23—O13^vii	135.0 (11)
U1—O7—U6ⁱⁱ	103.4 (12)	K1^xxvi—O23—O14^xxvi	47.4 (5)
U1—O7—K1	75.6 (6)	K1^xxvi—O23—O15^vi	67.9 (9)
U1—O7—O1	34.2 (7)	K1^xxvi—O23—O17	117.0 (11)
U1—O7—O2ⁱ	50.6 (8)	K1^xxvi—O23—O26^vii	160.2 (10)
U1—O7—O3	107.5 (9)	K1^xxvi—O23—O28^xiii	76.2 (11)
U1—O7—O8	49.7 (9)	K2^xxvii—O23—O5^vii	75.7 (7)
U1—O7—O9^iv	142.1 (10)	K2^xxvii—O23—O6^vi	88.1 (8)
U1—O7—O10	107.6 (12)	K2^xxvii—O23—O9^v	170.9 (13)
U1—O7—O12	35.7 (7)	K2^xxvii—O23—O10^xxvi	51.9 (7)
U1—O7—O13ⁱⁱ	98.1 (13)	K2^xxvii—O23—O12^xxvi	49.6 (6)
U1—O7—O14^xiv	103.2 (13)	K2^xxvii—O23—O13^vii	87.1 (10)
U1—O7—O16	86.2 (9)	K2^xxvii—O23—O14^xxvi	133.2 (10)
U1—O7—O26ⁱⁱ	151.7 (12)	K2^xxvii—O23—O15^vi	134.2 (13)
U2—O7—U6ⁱⁱ	143.0 (14)	K2^xxvii—O23—O17	126.2 (8)
U2—O7—K1	74.9 (6)	K2^xxvii—O23—O26^vii	111.5 (10)
U2—O7—O1	84.7 (9)	K2^xxvii—O23—O28^xiii	86.8 (10)
U2—O7—O2ⁱ	142.3 (13)	O5^vii—O23—O6^vi	51.7 (9)
U2—O7—O3	38.7 (6)	O5^vii—O23—O9^v	98.0 (11)
U2—O7—O8	51.2 (9)	O5^vii—O23—O10^xxvi	88.5 (9)
U2—O7—O9^iv	45.6 (8)	O5^vii—O23—O12^xxvi	125.1 (9)
U2—O7—O10	102.2 (11)	O5^vii—O23—O13^vii	88.0 (11)
U2—O7—O12	108.7 (9)	O5^vii—O23—O14^xxvi	142.8 (12)
U2—O7—O13ⁱⁱ	111.9 (13)	O5^vii—O23—O15^vi	92.9 (11)
U2—O7—O14^xiv	156.5 (15)	O5^vii—O23—O17	52.0 (8)
U2—O7—O16	36.4 (7)	O5^vii—O23—O26^vii	55.4 (9)
U2—O7—O26ⁱⁱ	102.4 (13)	O5^vii—O23—O28^xiii	143.4 (16)
U6ⁱⁱ—O7—K1	139.4 (11)	O6^vi—O23—O9^v	93.1 (11)
U6ⁱⁱ—O7—O1	96.5 (10)	O6^vi—O23—O10^xxvi	57.4 (9)
U6ⁱⁱ—O7—O2ⁱ	53.2 (8)	O6^vi—O23—O12^xxvi	114.0 (11)
U6ⁱⁱ—O7—O3	148.0 (13)	O6^vi—O23—O13^vii	139.2 (11)
U6ⁱⁱ—O7—O8	151.2 (16)	O6^vi—O23—O14^xxvi	100.0 (11)
U6ⁱⁱ—O7—O9^iv	103.9 (10)	O6^vi—O23—O15^vi	52.9 (8)
U6ⁱⁱ—O7—O10	99.4 (9)	O6^vi—O23—O17	51.6 (8)
U6ⁱⁱ—O7—O12	106.3 (12)	O6^vi—O23—O26^vii	94.3 (11)
U6ⁱⁱ—O7—O13ⁱⁱ	35.9 (7)	O6^vi—O23—O28^xiii	160.9 (16)
U6ⁱⁱ—O7—O14^xiv	39.1 (5)	O9^v—O23—O10^xxvi	135.5 (13)
U6ⁱⁱ—O7—O16	115.4 (11)	O9^v—O23—O12^xxvi	136.8 (9)
U6ⁱⁱ—O7—O26ⁱⁱ	49.3 (8)	O9^v—O23—O13^vii	86.1 (11)
K1—O7—O1	102.3 (8)	O9^v—O23—O14^xxvi	55.5 (7)
K1—O7—O2ⁱ	109.7 (11)	O9^v—O23—O15^vi	51.7 (10)
K1—O7—O3	45.9 (7)	O9^v—O23—O17	49.7 (7)
K1—O7—O8	53.3 (8)	O9^v—O23—O26^vii	59.3 (9)
K1—O7—O9^iv	99.3 (9)	O9^v—O23—O28^xiii	94.9 (10)
K1—O7—O10	46.0 (6)	O10^xxvi—O23—O12^xxvi	56.6 (8)
K1—O7—O12	50.1 (7)	O10^xxvi—O23—O13^vii	138.3 (11)
K1—O7—O13ⁱⁱ	171.6 (15)	O10^xxvi—O23—O14^xxvi	94.5 (9)
K1—O7—O14^xiv	100.8 (9)	O10^xxvi—O23—O15^vi	84.2 (11)
K1—O7—O16	105.0 (7)	O10^xxvi—O23—O17	108.8 (11)
K1—O7—O26ⁱⁱ	128.6 (11)	O10^xxvi—O23—O26^vii	143.9 (9)
O1—O7—O2ⁱ	57.6 (9)	O10^xxvi—O23—O28^xiii	105.6 (12)
O1—O7—O3	113.7 (9)	O12^xxvi—O23—O13^vii	92.9 (10)
O1—O7—O8	55.8 (9)	O12^xxvi—O23—O14^xxvi	86.0 (7)
O1—O7—O9^iv	116.5 (11)	O12^xxvi—O23—O15^vi	120.1 (12)
O1—O7—O10	141.6 (13)	O12^xxvi—O23—O17	165.0 (12)
O1—O7—O12	69.9 (10)	O12^xxvi—O23—O26^vii	142.7 (13)
O1—O7—O13ⁱⁱ	74.1 (10)	O12^xxvi—O23—O28^xiii	50.1 (9)
O1—O7—O14^xiv	118.6 (13)	O13^vii—O23—O14^xxvi	112.5 (10)
O1—O7—O16	58.5 (10)	O13^vii—O23—O15^vi	137.5 (12)
O1—O7—O26ⁱⁱ	128.9 (11)	O13^vii—O23—O17	101.5 (10)
O2ⁱ—O7—O3	154.5 (13)	O13^vii—O23—O26^vii	50.9 (9)
O2ⁱ—O7—O8	100.2 (13)	O13^vii—O23—O28^xiii	58.8 (12)
O2ⁱ—O7—O9^iv	151.0 (12)	O14^xxvi—O23—O15^vi	50.8 (7)
O2ⁱ—O7—O10	107.0 (14)	O14^xxvi—O23—O17	92.4 (8)
O2ⁱ—O7—O12	60.3 (10)	O14^xxvi—O23—O26^vii	113.7 (9)
O2ⁱ—O7—O13ⁱⁱ	61.9 (12)	O14^xxvi—O23—O28^xiii	70.9 (10)
O2ⁱ—O7—O14^xiv	61.1 (10)	O15^vi—O23—O17	50.0 (9)
O2ⁱ—O7—O16	111.5 (13)	O15^vi—O23—O26^vii	96.1 (12)
O2ⁱ—O7—O26ⁱⁱ	102.4 (10)	O15^vi—O23—O28^xiii	121.6 (12)
O3—O7—O8	60.7 (9)	O17—O23—O26^vii	50.8 (9)
O3—O7—O9^iv	54.0 (9)	O17—O23—O28^xiii	142.7 (12)
O3—O7—O10	63.5 (9)	O26^vii—O23—O28^xiii	104.8 (14)
O3—O7—O12	94.3 (10)	U4—O24—K1	120.8 (11)
O3—O7—O13ⁱⁱ	142.5 (16)	U4—O24—K2^xxv	130.1 (14)
O3—O7—O14^xiv	123.1 (11)	U4—O24—O4	51.3 (10)
O3—O7—O16	75.1 (9)	U4—O24—O5ⁱ	50.9 (10)
O3—O7—O26ⁱⁱ	100.7 (13)	U4—O24—O6	51.5 (9)
O8—O7—O9^iv	96.7 (11)	U4—O24—O8	52.7 (9)
O8—O7—O10	99.3 (11)	U4—O24—O10^ix	118.6 (13)
O8—O7—O12	59.7 (10)	U4—O24—O11	53.9 (11)
O8—O7—O13ⁱⁱ	126.5 (13)	U4—O24—O12	89.2 (10)
O8—O7—O14^xiv	143.3 (15)	U4—O24—O14	172.3 (18)
O8—O7—O16	59.8 (9)	U4—O24—O18^viii	92.0 (13)
O8—O7—O26ⁱⁱ	153.5 (16)	U4—O24—O19	1.6 (10)
O9^iv—O7—O10	93.2 (12)	U4—O24—O27^ix	107.6 (15)
O9^iv—O7—O12	148.1 (10)	U4—O24—O28^viii	121.2 (13)
O9^iv—O7—O13ⁱⁱ	89.1 (13)	K1—O24—K2^xxv	104.7 (10)
O9^iv—O7—O14^xiv	114.6 (11)	K1—O24—O4	98.6 (8)
O9^iv—O7—O16	58.4 (10)	K1—O24—O5ⁱ	150.3 (12)
O9^iv—O7—O26ⁱⁱ	57.1 (9)	K1—O24—O6	149.9 (15)
O10—O7—O12	72.1 (11)	K1—O24—O8	68.6 (8)
O10—O7—O13ⁱⁱ	133.5 (10)	K1—O24—O10^ix	103.5 (11)
O10—O7—O14^xiv	62.0 (8)	K1—O24—O11	87.8 (10)
O10—O7—O16	138.6 (13)	K1—O24—O12	52.1 (6)
O10—O7—O26ⁱⁱ	87.0 (10)	K1—O24—O14	55.4 (7)
O12—O7—O13ⁱⁱ	121.7 (15)	K1—O24—O18^viii	107.0 (10)
O12—O7—O14^xiv	83.9 (11)	K1—O24—O19	120.0 (10)
O12—O7—O16	115.1 (10)	K1—O24—O27^ix	57.4 (8)
O12—O7—O26ⁱⁱ	145.4 (12)	K1—O24—O28^viii	63.0 (9)
O13ⁱⁱ—O7—O14^xiv	75.0 (9)	K2^xxv—O24—O4	105.8 (12)
O13ⁱⁱ—O7—O16	79.8 (11)	K2^xxv—O24—O5ⁱ	79.5 (10)
O13ⁱⁱ—O7—O26ⁱⁱ	56.1 (10)	K2^xxv—O24—O6	97.4 (9)
O14^xiv—O7—O16	154.0 (11)	K2^xxv—O24—O8	152.0 (14)
O14^xiv—O7—O26ⁱⁱ	61.8 (9)	K2^xxv—O24—O10^ix	63.4 (9)
O16—O7—O26ⁱⁱ	98.8 (12)	K2^xxv—O24—O11	153.6 (11)
U1—O8—U2	117.1 (10)	K2^xxv—O24—O12	105.0 (10)
U1—O8—U4	113.9 (15)	K2^xxv—O24—O14	56.6 (8)
U1—O8—K1	98.5 (10)	K2^xxv—O24—O18^viii	53.5 (7)
U1—O8—O1	40.3 (8)	K2^xxv—O24—O19	131.4 (11)
U1—O8—O2	140.6 (10)	K2^xxv—O24—O27^ix	113.9 (11)
U1—O8—O3	122.5 (10)	K2^xxv—O24—O28^viii	61.7 (8)
U1—O8—O4	54.2 (9)	O4—O24—O5ⁱ	52.8 (8)
U1—O8—O7	63.3 (9)	O4—O24—O6	94.6 (11)
U1—O8—O11	171.6 (14)	O4—O24—O8	51.4 (10)
U1—O8—O12	38.5 (7)	O4—O24—O10^ix	157.2 (12)
U1—O8—O16	97.6 (11)	O4—O24—O11	94.9 (11)
U1—O8—O19	107.2 (13)	O4—O24—O12	47.7 (7)
U1—O8—O24	111.1 (14)	O4—O24—O14	133.7 (12)
U2—O8—U4	125.4 (14)	O4—O24—O18^viii	52.4 (8)
U2—O8—K1	95.3 (10)	O4—O24—O19	52.5 (9)
U2—O8—O1	99.3 (11)	O4—O24—O27^ix	137.4 (11)
U2—O8—O2	25.4 (6)	O4—O24—O28^viii	69.9 (9)
U2—O8—O3	40.0 (7)	O5ⁱ—O24—O6	53.5 (10)
U2—O8—O4	162.0 (15)	O5ⁱ—O24—O8	93.7 (11)
U2—O8—O7	57.9 (9)	O5ⁱ—O24—O10^ix	104.5 (10)
U2—O8—O11	68.6 (11)	O5ⁱ—O24—O11	101.2 (12)
U2—O8—O12	121.8 (11)	O5ⁱ—O24—O12	98.2 (10)
U2—O8—O16	38.7 (8)	O5ⁱ—O24—O14	136.1 (13)
U2—O8—O19	106.6 (14)	O5ⁱ—O24—O18^viii	51.5 (9)
U2—O8—O24	126.3 (14)	O5ⁱ—O24—O19	52.3 (10)
U4—O8—K1	95.2 (9)	O5ⁱ—O24—O27^ix	148.2 (13)
U4—O8—O1	107.2 (12)	O5ⁱ—O24—O28^viii	95.6 (12)
U4—O8—O2	100.1 (11)	O6—O24—O8	100.2 (12)
U4—O8—O3	118.4 (12)	O6—O24—O10^ix	68.6 (9)
U4—O8—O4	59.8 (9)	O6—O24—O11	64.2 (10)
U4—O8—O7	176.5 (17)	O6—O24—O12	139.9 (11)
U4—O8—O11	58.8 (9)	O6—O24—O14	127.7 (11)
U4—O8—O12	109.7 (13)	O6—O24—O18^viii	102.5 (11)
U4—O8—O16	117.5 (12)	O6—O24—O19	51.3 (8)
U4—O8—O19	38.3 (7)	O6—O24—O27^ix	95.1 (12)
U4—O8—O24	40.9 (7)	O6—O24—O28^viii	147.1 (13)
K1—O8—O1	138.2 (12)	O8—O24—O10^ix	143.9 (16)
K1—O8—O2	97.7 (9)	O8—O24—O11	54.2 (9)
K1—O8—O3	55.7 (8)	O8—O24—O12	48.7 (8)
K1—O8—O4	101.5 (12)	O8—O24—O14	123.9 (10)
K1—O8—O7	83.4 (9)	O8—O24—O18^viii	101.2 (11)
K1—O8—O11	86.7 (10)	O8—O24—O19	52.2 (8)
K1—O8—O12	60.4 (9)	O8—O24—O27^ix	86.1 (11)
K1—O8—O16	133.1 (12)	O8—O24—O28^viii	92.4 (10)
K1—O8—O19	132.8 (9)	O10^ix—O24—O11	91.4 (12)
K1—O8—O24	54.5 (8)	O10^ix—O24—O12	151.5 (12)
O1—O8—O2	112.0 (12)	O10^ix—O24—O14	59.3 (9)
O1—O8—O3	131.3 (11)	O10^ix—O24—O18^viii	114.6 (11)
O1—O8—O4	63.6 (11)	O10^ix—O24—O19	118.0 (11)
O1—O8—O7	72.1 (10)	O10^ix—O24—O27^ix	62.1 (9)
O1—O8—O11	135.0 (14)	O10^ix—O24—O28^viii	115.9 (12)
O1—O8—O12	78.8 (11)	O11—O24—O12	101.0 (9)
O1—O8—O16	65.3 (11)	O11—O24—O14	118.4 (13)
O1—O8—O19	79.4 (10)	O11—O24—O18^viii	145.1 (11)
O1—O8—O24	133.4 (15)	O11—O24—O19	52.3 (10)
O2—O8—O3	46.1 (8)	O11—O24—O27^ix	53.7 (9)
O2—O8—O4	153.2 (11)	O11—O24—O28^viii	143.1 (9)
O2—O8—O7	83.3 (11)	O12—O24—O14	92.3 (9)
O2—O8—O11	43.9 (8)	O12—O24—O18^viii	67.5 (8)
O2—O8—O12	143.8 (11)	O12—O24—O19	89.6 (8)
O2—O8—O16	46.9 (9)	O12—O24—O27^ix	105.2 (8)
O2—O8—O19	87.0 (12)	O12—O24—O28^viii	43.7 (7)
O2—O8—O24	107.5 (11)	O14—O24—O18^viii	95.5 (11)
O3—O8—O4	157.1 (15)	O14—O24—O19	170.8 (15)
O3—O8—O7	63.4 (10)	O14—O24—O27^ix	64.8 (10)
O3—O8—O11	65.8 (11)	O14—O24—O28^viii	64.2 (9)
O3—O8—O12	100.0 (11)	O18^viii—O24—O19	93.6 (10)
O3—O8—O16	78.6 (11)	O18^viii—O24—O27^ix	159.3 (11)
O3—O8—O19	128.4 (14)	O18^viii—O24—O28^viii	44.8 (7)
O3—O8—O24	94.1 (11)	O19—O24—O27^ix	106.0 (12)
O4—O8—O7	117.4 (14)	O19—O24—O28^viii	122.3 (10)
O4—O8—O11	118.5 (11)	O27^ix—O24—O28^viii	116.2 (10)
O4—O8—O12	63.0 (11)	U5—O25—K1^xxvi	121.3 (15)
O4—O8—O16	123.5 (14)	U5—O25—O3^xxvi	176.3 (11)
O4—O8—O19	66.2 (12)	U5—O25—O4^v	49.7 (10)
O4—O8—O24	69.9 (11)	U5—O25—O5^vi	49.5 (10)
O7—O8—O11	124.1 (15)	U5—O25—O6^vi	50.9 (10)
O7—O8—O12	66.8 (10)	U5—O25—O10^xxvi	120.3 (14)
O7—O8—O16	65.5 (10)	U5—O25—O15^vi	51.5 (10)
O7—O8—O19	143.6 (14)	U5—O25—O18	1.5 (7)
O7—O8—O24	137.2 (14)	U5—O25—O21^xxviii	121.8 (15)
O11—O8—O12	145.2 (14)	U5—O25—O22^xxvi	122.7 (14)
O11—O8—O16	83.3 (12)	U5—O25—O26^vi	70.8 (9)
O11—O8—O19	64.6 (10)	U5—O25—O27^xxi	120.7 (11)
O11—O8—O24	66.7 (10)	K1^xxvi—O25—O3^xxvi	57.4 (9)
O12—O8—O16	126.8 (10)	K1^xxvi—O25—O4^v	165.0 (13)
O12—O8—O19	129.3 (15)	K1^xxvi—O25—O5^vi	131.6 (9)
O12—O8—O24	83.8 (11)	K1^xxvi—O25—O6^vi	93.4 (12)
O16—O8—O19	82.3 (12)	K1^xxvi—O25—O10^xxvi	59.7 (9)
O16—O8—O24	149.3 (14)	K1^xxvi—O25—O15^vi	70.2 (9)
O19—O8—O24	79.1 (10)	K1^xxvi—O25—O18	120.0 (11)
U2^xxii—O9—U3^viii	144.0 (14)	K1^xxvi—O25—O21^xxviii	101.3 (10)
U2^xxii—O9—U6ⁱ	101.1 (9)	K1^xxvi—O25—O22^xxvi	112.5 (13)
U2^xxii—O9—O2^xxii	49.0 (9)	K1^xxvi—O25—O26^vi	79.7 (8)
U2^xxii—O9—O3^xxii	39.0 (6)	K1^xxvi—O25—O27^xxi	56.7 (8)
U2^xxii—O9—O7^xxii	45.7 (7)	O3^xxvi—O25—O4^v	132.3 (13)
U2^xxii—O9—O13ⁱ	107.2 (10)	O3^xxvi—O25—O5^vi	128.1 (13)
U2^xxii—O9—O14^xiii	89.7 (9)	O3^xxvi—O25—O6^vi	131.6 (13)
U2^xxii—O9—O15ⁱ	148.1 (13)	O3^xxvi—O25—O10^xxvi	62.5 (10)
U2^xxii—O9—O16^xxii	34.5 (6)	O3^xxvi—O25—O15^vi	126.8 (13)
U2^xxii—O9—O17^viii	149.9 (15)	O3^xxvi—O25—O18	175.1 (9)
U2^xxii—O9—O22^xxii	97.0 (12)	O3^xxvi—O25—O21^xxviii	56.5 (10)
U2^xxii—O9—O23^viii	115.7 (12)	O3^xxvi—O25—O22^xxvi	59.9 (10)
U2^xxii—O9—O26^xxiii	100.4 (13)	O3^xxvi—O25—O26^vi	105.5 (9)
U3^viii—O9—U6ⁱ	102.9 (12)	O3^xxvi—O25—O27^xxi	55.6 (7)
U3^viii—O9—O2^xxii	152.3 (15)	O4^v—O25—O5^vi	55.1 (8)
U3^viii—O9—O3^xxii	146.8 (13)	O4^v—O25—O6^vi	71.7 (10)
U3^viii—O9—O7^xxii	103.7 (10)	O4^v—O25—O10^xxvi	112.1 (10)
U3^viii—O9—O13ⁱ	108.0 (14)	O4^v—O25—O15^vi	100.8 (12)
U3^viii—O9—O14^xiii	94.6 (10)	O4^v—O25—O18	51.2 (8)
U3^viii—O9—O15ⁱ	51.7 (8)	O4^v—O25—O21^xxviii	93.5 (13)
U3^viii—O9—O16^xxii	117.2 (11)	O4^v—O25—O22^xxvi	73.3 (11)
U3^viii—O9—O17^viii	39.1 (6)	O4^v—O25—O26^vi	104.8 (11)
U3^viii—O9—O22^xxii	98.3 (10)	O4^v—O25—O27^xxi	136.9 (13)
U3^viii—O9—O23^viii	35.6 (6)	O5^vi—O25—O6^vi	100.2 (12)
U3^viii—O9—O26^xxiii	50.3 (8)	O5^vi—O25—O10^xxvi	166.5 (12)
U6ⁱ—O9—O2^xxii	53.3 (9)	O5^vi—O25—O15^vi	80.4 (11)
U6ⁱ—O9—O3^xxii	107.8 (9)	O5^vi—O25—O18	49.6 (9)
U6ⁱ—O9—O7^xxii	145.7 (10)	O5^vi—O25—O21^xxviii	72.9 (11)
U6ⁱ—O9—O13ⁱ	36.2 (7)	O5^vi—O25—O22^xxvi	105.5 (15)
U6ⁱ—O9—O14^xiii	35.4 (6)	O5^vi—O25—O26^vi	51.9 (8)
U6ⁱ—O9—O15ⁱ	51.8 (9)	O5^vi—O25—O27^xxi	86.4 (9)
U6ⁱ—O9—O16^xxii	93.6 (10)	O6^vi—O25—O10^xxvi	69.5 (10)
U6ⁱ—O9—O17^viii	106.0 (13)	O6^vi—O25—O15^vi	55.1 (9)
U6ⁱ—O9—O22^xxii	112.2 (14)	O6^vi—O25—O18	51.0 (8)
U6ⁱ—O9—O23^viii	95.7 (11)	O6^vi—O25—O21^xxviii	164.7 (14)
U6ⁱ—O9—O26^xxiii	152.6 (12)	O6^vi—O25—O22^xxvi	110.8 (11)
O2^xxii—O9—O3^xxii	60.8 (9)	O6^vi—O25—O26^vi	105.6 (11)
O2^xxii—O9—O7^xxii	94.7 (11)	O6^vi—O25—O27^xxi	141.3 (13)
O2^xxii—O9—O13ⁱ	62.7 (11)	O10^xxvi—O25—O15^vi	99.7 (14)
O2^xxii—O9—O14^xiii	57.9 (9)	O10^xxvi—O25—O18	120.5 (11)
O2^xxii—O9—O15ⁱ	104.7 (13)	O10^xxvi—O25—O21^xxviii	114.7 (12)
O2^xxii—O9—O16^xxii	58.3 (9)	O10^xxvi—O25—O22^xxvi	71.6 (13)
O2^xxii—O9—O17^viii	149.9 (15)	O10^xxvi—O25—O26^vi	138.1 (13)
O2^xxii—O9—O22^xxii	103.9 (11)	O10^xxvi—O25—O27^xxi	107.1 (11)
O2^xxii—O9—O23^viii	124.0 (12)	O15^vi—O25—O18	50.0 (9)
O2^xxii—O9—O26^xxiii	149.1 (16)	O15^vi—O25—O21^xxviii	134.2 (10)
O3^xxii—O9—O7^xxii	54.7 (9)	O15^vi—O25—O22^xxvi	165.8 (13)
O3^xxii—O9—O13ⁱ	90.1 (11)	O15^vi—O25—O26^vi	53.2 (8)
O3^xxii—O9—O14^xiii	117.8 (9)	O15^vi—O25—O27^xxi	89.4 (9)
O3^xxii—O9—O15ⁱ	152.6 (14)	O18—O25—O21^xxviii	122.2 (12)
O3^xxii—O9—O16^xxii	73.5 (9)	O18—O25—O22^xxvi	124.2 (12)
O3^xxii—O9—O17^viii	117.7 (12)	O18—O25—O26^vi	69.6 (7)
O3^xxii—O9—O22^xxii	58.5 (10)	O18—O25—O27^xxi	119.6 (9)
O3^xxii—O9—O23^viii	147.7 (15)	O21^xxviii—O25—O22^xxvi	59.8 (11)
O3^xxii—O9—O26^xxiii	99.6 (12)	O21^xxviii—O25—O26^vi	81.2 (9)
O7^xxii—O9—O13ⁱ	144.8 (12)	O21^xxviii—O25—O27^xxi	53.1 (10)
O7^xxii—O9—O14^xiii	120.8 (12)	O22^xxvi—O25—O26^vi	140.4 (15)
O7^xxii—O9—O15ⁱ	152.6 (11)	O22^xxvi—O25—O27^xxi	103.8 (12)
O7^xxii—O9—O16^xxii	54.8 (9)	O26^vi—O25—O27^xxi	50.0 (7)
O7^xxii—O9—O17^viii	108.3 (11)	U3^xx—O26—U5^xxi	91.2 (9)
O7^xxii—O9—O22^xxii	84.8 (13)	U3^xx—O26—U6	148.0 (13)
O7^xxii—O9—O23^viii	93.5 (11)	U3^xx—O26—O5	50.4 (9)
O7^xxii—O9—O26^xxiii	55.1 (9)	U3^xx—O26—O7^xi	117.8 (10)
O13ⁱ—O9—O14^xiii	71.7 (10)	U3^xx—O26—O9^xvii	52.3 (8)
O13ⁱ—O9—O15ⁱ	62.6 (12)	U3^xx—O26—O10^xi	124.0 (10)
O13ⁱ—O9—O16^xxii	119.3 (10)	U3^xx—O26—O13	109.0 (14)
O13ⁱ—O9—O17^viii	87.7 (12)	U3^xx—O26—O14^ix	171.1 (12)
O13ⁱ—O9—O22^xxii	76.0 (13)	U3^xx—O26—O15	130.1 (12)
O13ⁱ—O9—O23^viii	121.3 (14)	U3^xx—O26—O17^xx	38.8 (8)
O13ⁱ—O9—O26^xxiii	146.0 (13)	U3^xx—O26—O22^xi	77.4 (10)
O14^xiii—O9—O15ⁱ	58.6 (10)	U3^xx—O26—O23^xx	36.3 (7)
O14^xiii—O9—O16^xxii	66.7 (10)	U3^xx—O26—O25^xxi	99.3 (10)
O14^xiii—O9—O17^viii	120.2 (13)	U3^xx—O26—O27^xi	102.4 (13)
O14^xiii—O9—O22^xxii	147.5 (14)	U5^xxi—O26—U6	91.8 (9)
O14^xiii—O9—O23^viii	70.6 (9)	U5^xxi—O26—O5	41.2 (7)
O14^xiii—O9—O26^xxiii	128.5 (11)	U5^xxi—O26—O7^xi	144.6 (13)
O15ⁱ—O9—O16^xxii	120.9 (13)	U5^xxi—O26—O9^xvii	143.4 (13)
O15ⁱ—O9—O17^viii	62.0 (10)	U5^xxi—O26—O10^xi	134.4 (9)
O15ⁱ—O9—O22^xxii	108.4 (15)	U5^xxi—O26—O13	89.0 (9)
O15ⁱ—O9—O23^viii	59.6 (10)	U5^xxi—O26—O14^ix	95.8 (9)
O15ⁱ—O9—O26^xxiii	102.0 (10)	U5^xxi—O26—O15	42.7 (7)
O16^xxii—O9—O17^viii	151.7 (12)	U5^xxi—O26—O17^xx	96.9 (9)
O16^xxii—O9—O22^xxii	130.2 (15)	U5^xxi—O26—O22^xi	134.5 (10)
O16^xxii—O9—O23^viii	83.3 (10)	U5^xxi—O26—O23^xx	88.7 (8)
O16^xxii—O9—O26^xxiii	94.6 (11)	U5^xxi—O26—O25^xxi	32.4 (5)
O17^viii—O9—O22^xxii	60.7 (10)	U5^xxi—O26—O27^xi	95.7 (8)
O17^viii—O9—O23^viii	74.8 (9)	U6—O26—O5	128.2 (12)
O17^viii—O9—O26^xxiii	58.9 (9)	U6—O26—O7^xi	52.9 (8)
O22^xxii—O9—O23^viii	132.0 (10)	U6—O26—O9^xvii	117.5 (10)
O22^xxii—O9—O26^xxiii	81.6 (11)	U6—O26—O10^xi	73.5 (9)
O23^viii—O9—O26^xxiii	59.5 (9)	U6—O26—O13	39.2 (10)
U6ⁱⁱ—O10—K1	121.4 (9)	U6—O26—O14^ix	37.4 (6)
U6ⁱⁱ—O10—O3	93.3 (8)	U6—O26—O15	49.8 (8)
U6ⁱⁱ—O10—K2^xxiii	74.7 (7)	U6—O26—O17^xx	169.2 (12)
U6ⁱⁱ—O10—O6^xiv	146.5 (8)	U6—O26—O22^xi	120.8 (11)
U6ⁱⁱ—O10—O7	36.9 (6)	U6—O26—O23^xx	111.9 (12)
U6ⁱⁱ—O10—O12	72.4 (7)	U6—O26—O25^xxi	100.2 (11)
U6ⁱⁱ—O10—O14^xiv	25.4 (5)	U6—O26—O27^xi	109.1 (13)
U6ⁱⁱ—O10—O22	98.7 (9)	O5—O26—O7^xi	162.7 (14)
U6ⁱⁱ—O10—O23^xv	125.4 (10)	O5—O26—O9^xvii	102.6 (13)
U6ⁱⁱ—O10—O24^xiv	89.5 (8)	O5—O26—O10^xi	150.4 (12)
U6ⁱⁱ—O10—O25^xv	150.1 (13)	O5—O26—O13	105.8 (13)
U6ⁱⁱ—O10—O26ⁱⁱ	33.7 (6)	O5—O26—O14^ix	135.8 (11)
U6ⁱⁱ—O10—O27	70.7 (7)	O5—O26—O15	82.9 (10)
K1—O10—O3	57.7 (7)	O5—O26—O17^xx	62.2 (10)
K1—O10—K2^xxiii	94.3 (10)	O5—O26—O22^xi	110.0 (13)
K1—O10—O6^xiv	87.1 (8)	O5—O26—O23^xx	60.0 (9)
K1—O10—O7	88.2 (8)	O5—O26—O25^xxi	54.4 (9)
K1—O10—O12	56.9 (7)	O5—O26—O27^xi	98.1 (12)
K1—O10—O14^xiv	133.6 (13)	O7^xi—O26—O9^xvii	67.8 (9)
K1—O10—O22	100.8 (10)	O7^xi—O26—O10^xi	44.5 (8)
K1—O10—O23^xv	55.6 (7)	O7^xi—O26—O13	63.7 (10)
K1—O10—O24^xiv	131.9 (13)	O7^xi—O26—O14^ix	57.8 (9)
K1—O10—O25^xv	61.3 (8)	O7^xi—O26—O15	102.3 (13)
K1—O10—O26ⁱⁱ	131.8 (10)	O7^xi—O26—O17^xx	118.4 (11)
K1—O10—O27	153.7 (14)	O7^xi—O26—O22^xi	75.2 (9)
O3—O10—K2^xxiii	138.2 (12)	O7^xi—O26—O23^xx	102.8 (10)
O3—O10—O6^xiv	118.4 (10)	O7^xi—O26—O25^xxi	141.5 (13)
O3—O10—O7	60.0 (9)	O7^xi—O26—O27^xi	97.1 (11)
O3—O10—O12	85.1 (9)	O9^xvii—O26—O10^xi	78.2 (8)
O3—O10—O14^xiv	118.7 (11)	O9^xvii—O26—O13	100.0 (12)
O3—O10—O22	54.7 (9)	O9^xvii—O26—O14^ix	120.7 (10)
O3—O10—O23^xv	113.0 (8)	O9^xvii—O26—O15	162.7 (13)
O3—O10—O24^xiv	165.2 (15)	O9^xvii—O26—O17^xx	57.6 (9)
O3—O10—O25^xv	62.0 (9)	O9^xvii—O26—O22^xi	48.8 (8)
O3—O10—O26ⁱⁱ	79.7 (9)	O9^xvii—O26—O23^xx	61.1 (9)
O3—O10—O27	100.8 (12)	O9^xvii—O26—O25^xxi	141.4 (13)
K2^xxiii—O10—O6^xiv	86.9 (10)	O9^xvii—O26—O27^xi	94.8 (11)
K2^xxiii—O10—O7	91.9 (11)	O10^xi—O26—O13	103.2 (12)
K2^xxiii—O10—O12	53.1 (7)	O10^xi—O26—O14^ix	47.2 (7)
K2^xxiii—O10—O14^xiv	56.6 (8)	O10^xi—O26—O15	105.2 (12)
K2^xxiii—O10—O22	164.7 (10)	O10^xi—O26—O17^xx	95.8 (10)
K2^xxiii—O10—O23^xv	53.5 (7)	O10^xi—O26—O22^xi	48.4 (9)
K2^xxiii—O10—O24^xiv	56.5 (9)	O10^xi—O26—O23^xx	136.9 (8)
K2^xxiii—O10—O25^xv	134.8 (13)	O10^xi—O26—O25^xxi	106.8 (9)
K2^xxiii—O10—O26ⁱⁱ	105.4 (9)	O10^xi—O26—O27^xi	52.7 (8)
K2^xxiii—O10—O27	111.9 (9)	O13—O26—O14^ix	76.6 (13)
O6^xiv—O10—O7	175.1 (11)	O13—O26—O15	62.7 (11)
O6^xiv—O10—O12	118.1 (12)	O13—O26—O17^xx	147.0 (15)
O6^xiv—O10—O14^xiv	121.9 (10)	O13—O26—O22^xi	136.5 (10)
O6^xiv—O10—O22	91.9 (11)	O13—O26—O23^xx	72.8 (13)
O6^xiv—O10—O23^xv	54.3 (9)	O13—O26—O25^xxi	115.3 (11)
O6^xiv—O10—O24^xiv	57.1 (9)	O13—O26—O27^xi	148.2 (17)
O6^xiv—O10—O25^xv	56.7 (9)	O14^ix—O26—O15	58.4 (9)
O6^xiv—O10—O26ⁱⁱ	136.4 (10)	O14^ix—O26—O17^xx	134.4 (12)
O6^xiv—O10—O27	91.5 (10)	O14^ix—O26—O22^xi	93.8 (10)
O7—O10—O12	57.7 (10)	O14^ix—O26—O23^xx	148.9 (13)
O7—O10—O14^xiv	60.9 (8)	O14^ix—O26—O25^xxi	84.0 (9)
O7—O10—O22	90.6 (12)	O14^ix—O26—O27^xi	71.6 (10)
O7—O10—O23^xv	121.4 (12)	O15—O26—O17^xx	137.2 (11)
O7—O10—O24^xiv	125.8 (12)	O15—O26—O22^xi	144.8 (13)
O7—O10—O25^xv	122.0 (13)	O15—O26—O23^xx	109.9 (11)
O7—O10—O26ⁱⁱ	48.5 (8)	O15—O26—O25^xxi	54.6 (9)
O7—O10—O27	93.4 (11)	O15—O26—O27^xi	100.6 (12)
O12—O10—O14^xiv	76.9 (10)	O17^xx—O26—O22^xi	48.4 (9)
O12—O10—O22	138.8 (11)	O17^xx—O26—O23^xx	74.9 (11)
O12—O10—O23^xv	63.9 (9)	O17^xx—O26—O25^xxi	83.9 (10)
O12—O10—O24^xiv	109.6 (13)	O17^xx—O26—O27^xi	63.7 (11)
O12—O10—O25^xv	118.2 (9)	O22^xi—O26—O23^xx	104.8 (11)
O12—O10—O26ⁱⁱ	101.8 (9)	O22^xi—O26—O25^xxi	105.5 (10)
O12—O10—O27	142.8 (11)	O22^xi—O26—O27^xi	46.4 (8)
O14^xiv—O10—O22	112.2 (12)	O23^xx—O26—O25^xxi	113.7 (10)
O14^xiv—O10—O23^xv	110.1 (12)	O23^xx—O26—O27^xi	138.6 (15)
O14^xiv—O10—O24^xiv	64.9 (8)	O25^xxi—O26—O27^xi	63.3 (8)
O14^xiv—O10—O25^xv	164.3 (14)	K1^xiv—O27—O1^xvi	137.5 (10)
O14^xiv—O10—O26ⁱⁱ	49.0 (8)	K1^xiv—O27—O3^xiv	56.8 (8)
O14^xiv—O10—O27	68.0 (9)	K1^xiv—O27—O10	90.9 (11)
O22—O10—O23^xv	135.8 (11)	K1^xiv—O27—O11^xiv	87.1 (10)
O22—O10—O24^xiv	110.5 (12)	K1^xiv—O27—O14^xiv	50.0 (7)
O22—O10—O25^xv	54.1 (10)	K1^xiv—O27—O17^xvi	135.3 (10)
O22—O10—O26ⁱⁱ	65.6 (9)	K1^xiv—O27—O21^xvi	107.1 (8)
O22—O10—O27	52.9 (9)	K1^xiv—O27—O22	155.6 (15)
O23^xv—O10—O24^xiv	76.7 (10)	K1^xiv—O27—O24^xiv	51.8 (7)
O23^xv—O10—O25^xv	82.1 (10)	K1^xiv—O27—O25^vi	53.8 (7)
O23^xv—O10—O26ⁱⁱ	158.6 (11)	K1^xiv—O27—O26ⁱⁱ	88.2 (10)
O23^xv—O10—O27	140.0 (11)	O1^xvi—O27—O3^xiv	83.3 (10)
O24^xiv—O10—O25^xv	110.4 (13)	O1^xvi—O27—O10	110.6 (10)
O24^xiv—O10—O26ⁱⁱ	94.9 (8)	O1^xvi—O27—O11^xiv	59.2 (10)
O24^xiv—O10—O27	66.4 (9)	O1^xvi—O27—O14^xiv	162.9 (10)
O25^xv—O10—O26ⁱⁱ	119.3 (13)	O1^xvi—O27—O17^xvi	70.7 (11)
O25^xv—O10—O27	96.3 (12)	O1^xvi—O27—O21^xvi	56.1 (9)
O26ⁱⁱ—O10—O27	45.0 (7)	O1^xvi—O27—O22	58.9 (10)
U1^xii—O11—U2	97.5 (10)	O1^xvi—O27—O24^xiv	114.9 (11)
U1^xii—O11—U4	144.9 (12)	O1^xvi—O27—O25^vi	117.7 (11)
U1^xii—O11—O1^xii	37.7 (7)	O1^xvi—O27—O26ⁱⁱ	129.5 (14)
U1^xii—O11—O2	52.6 (9)	O3^xiv—O27—O10	134.1 (14)
U1^xii—O11—O3	104.9 (12)	O3^xiv—O27—O11^xiv	61.9 (7)
U1^xii—O11—O4^xii	45.3 (8)	O3^xiv—O27—O14^xiv	106.8 (11)
U1^xii—O11—O6	109.8 (10)	O3^xiv—O27—O17^xvi	113.8 (12)
U1^xii—O11—O8	141.4 (12)	O3^xiv—O27—O21^xvi	60.6 (9)
U1^xii—O11—O12^xii	35.6 (7)	O3^xiv—O27—O22	141.9 (15)
U1^xii—O11—O16	91.2 (10)	O3^xiv—O27—O24^xiv	82.7 (10)
U1^xii—O11—O19	111.2 (12)	O3^xiv—O27—O25^vi	56.6 (7)
U1^xii—O11—O24	159.4 (11)	O3^xiv—O27—O26ⁱⁱ	123.2 (10)
U1^xii—O11—O27^ix	102.8 (13)	O10—O27—O11^xiv	87.2 (10)
U2—O11—U4	98.8 (10)	O10—O27—O14^xiv	52.5 (8)
U2—O11—O1^xii	100.6 (10)	O10—O27—O17^xvi	112.1 (10)
U2—O11—O2	45.5 (8)	O10—O27—O21^xvi	162.0 (13)
U2—O11—O3	36.5 (4)	O10—O27—O22	64.7 (12)
U2—O11—O4^xii	142.3 (13)	O10—O27—O24^xiv	51.5 (8)
U2—O11—O6	144.2 (13)	O10—O27—O25^vi	131.7 (13)
U2—O11—O8	47.9 (8)	O10—O27—O26ⁱⁱ	82.4 (10)
U2—O11—O12^xii	91.5 (9)	O11^xiv—O27—O14^xiv	112.7 (13)
U2—O11—O16	27.9 (5)	O11^xiv—O27—O17^xvi	129.9 (14)
U2—O11—O19	92.1 (9)	O11^xiv—O27—O21^xvi	94.1 (12)
U2—O11—O24	101.9 (10)	O11^xiv—O27—O22	92.1 (11)
U2—O11—O27^ix	96.8 (8)	O11^xiv—O27—O24^xiv	58.2 (10)
U4—O11—O1^xii	159.4 (11)	O11^xiv—O27—O25^vi	118.1 (10)
U4—O11—O2	139.3 (12)	O11^xiv—O27—O26ⁱⁱ	168.5 (15)
U4—O11—O3	106.7 (12)	O14^xiv—O27—O17^xvi	115.6 (11)
U4—O11—O4^xii	110.2 (10)	O14^xiv—O27—O21^xvi	140.9 (10)
U4—O11—O6	45.9 (7)	O14^xiv—O27—O22	109.0 (12)
U4—O11—O8	52.0 (9)	O14^xiv—O27—O24^xiv	54.6 (8)
U4—O11—O12^xii	113.0 (12)	O14^xiv—O27—O25^vi	79.4 (9)
U4—O11—O16	88.8 (10)	O14^xiv—O27—O26ⁱⁱ	56.7 (9)
U4—O11—O19	37.5 (8)	O17^xvi—O27—O21^xvi	54.2 (9)
U4—O11—O24	37.8 (7)	O17^xvi—O27—O22	60.4 (11)
U4—O11—O27^ix	105.9 (13)	O17^xvi—O27—O24^xiv	163.4 (10)
O1^xii—O11—O2	61.2 (10)	O17^xvi—O27—O25^vi	83.7 (10)
O1^xii—O11—O3	85.4 (11)	O17^xvi—O27—O26ⁱⁱ	59.5 (11)
O1^xii—O11—O4^xii	56.0 (9)	O21^xvi—O27—O22	97.3 (15)
O1^xii—O11—O6	115.2 (10)	O21^xvi—O27—O24^xiv	142.3 (11)
O1^xii—O11—O8	144.5 (12)	O21^xvi—O27—O25^vi	62.7 (9)
O1^xii—O11—O12^xii	73.4 (11)	O21^xvi—O27—O26ⁱⁱ	97.3 (12)
O1^xii—O11—O16	111.6 (11)	O22—O27—O24^xiv	107.8 (12)
O1^xii—O11—O19	147.3 (13)	O22—O27—O25^vi	143.5 (14)
O1^xii—O11—O24	129.8 (12)	O22—O27—O26ⁱⁱ	87.9 (10)
O1^xii—O11—O27^ix	65.0 (11)	O24^xiv—O27—O25^vi	105.6 (11)
O2—O11—O3	58.9 (9)	O24^xiv—O27—O26ⁱⁱ	111.0 (13)
O2—O11—O4^xii	97.9 (13)	O25^vi—O27—O26ⁱⁱ	66.7 (8)
O2—O11—O6	157.5 (13)	Ca1—O28—K1^v	146.3 (14)
O2—O11—O8	92.9 (11)	Ca1—O28—K2^vii	147.3 (17)
O2—O11—O12^xii	60.4 (10)	Ca1—O28—K2ⁱ	72.4 (8)
O2—O11—O16	50.5 (9)	Ca1—O28—O12^v	138.6 (14)
O2—O11—O19	112.7 (13)	Ca1—O28—O13ⁱⁱ	79.2 (15)
O2—O11—O24	144.7 (11)	Ca1—O28—O14^v	108.3 (11)
O2—O11—O27^ix	98.4 (12)	Ca1—O28—O16	56.9 (10)
O3—O11—O4^xii	141.3 (14)	Ca1—O28—O18	55.9 (10)
O3—O11—O6	143.1 (14)	Ca1—O28—O19^vi	77.4 (14)
O3—O11—O8	59.6 (9)	Ca1—O28—O20^vi	102.5 (17)
O3—O11—O12^xii	118.6 (11)	Ca1—O28—O21	41.8 (10)
O3—O11—O16	64.4 (6)	Ca1—O28—O23^xvi	139.7 (15)
O3—O11—O19	120.4 (11)	Ca1—O28—O24^v	107.5 (11)
O3—O11—O24	86.9 (10)	K1^v—O28—K2^vii	66.4 (8)
O3—O11—O27^ix	60.3 (7)	K1^v—O28—K2ⁱ	73.9 (9)
O4^xii—O11—O6	66.2 (9)	K1^v—O28—O12^v	54.1 (10)
O4^xii—O11—O8	158.7 (14)	K1^v—O28—O13ⁱⁱ	125.5 (13)
O4^xii—O11—O12^xii	55.4 (8)	K1^v—O28—O14^v	43.0 (7)
O4^xii—O11—O16	126.9 (12)	K1^v—O28—O16	102.2 (13)
O4^xii—O11—O19	96.3 (10)	K1^v—O28—O18	101.5 (14)
O4^xii—O11—O24	115.9 (10)	K1^v—O28—O19^vi	126.6 (12)
O4^xii—O11—O27^ix	97.9 (11)	K1^v—O28—O20^vi	111.2 (12)
O6—O11—O8	97.9 (13)	K1^v—O28—O21	171.8 (11)
O6—O11—O12^xii	97.2 (10)	K1^v—O28—O23^xvi	54.4 (11)
O6—O11—O16	125.8 (12)	K1^v—O28—O24^v	42.4 (7)
O6—O11—O19	56.9 (9)	K2^vii—O28—K2ⁱ	140.3 (15)
O6—O11—O24	56.3 (9)	K2^vii—O28—O12^v	46.3 (7)
O6—O11—O27^ix	99.4 (11)	K2^vii—O28—O13ⁱⁱ	76.5 (9)
O8—O11—O12^xii	116.6 (12)	K2^vii—O28—O14^v	102.0 (11)
O8—O11—O16	50.3 (9)	K2^vii—O28—O16	136.2 (11)
O8—O11—O19	62.5 (10)	K2^vii—O28—O18	134.8 (11)
O8—O11—O24	59.1 (10)	K2^vii—O28—O19^vi	75.9 (9)
O8—O11—O27^ix	98.5 (12)	K2^vii—O28—O20^vi	44.8 (9)
O12^xii—O11—O16	71.5 (8)	K2^vii—O28—O21	105.4 (10)
O12^xii—O11—O19	76.4 (11)	K2^vii—O28—O23^xvi	48.0 (7)
O12^xii—O11—O24	149.0 (13)	K2^vii—O28—O24^v	102.1 (11)
O12^xii—O11—O27^ix	138.4 (15)	K2ⁱ—O28—O12^v	107.5 (13)
O16—O11—O19	69.0 (9)	K2ⁱ—O28—O13ⁱⁱ	131.6 (11)
O16—O11—O24	109.2 (11)	K2ⁱ—O28—O14^v	44.1 (6)
O16—O11—O27^ix	124.6 (9)	K2ⁱ—O28—O16	53.6 (7)
O19—O11—O24	75.3 (12)	K2ⁱ—O28—O18	52.1 (7)
O19—O11—O27^ix	143.4 (16)	K2ⁱ—O28—O19^vi	131.0 (11)
O24—O11—O27^ix	68.1 (11)	K2ⁱ—O28—O20^vi	174.4 (16)
U1—O12—K1	114.1 (15)	K2ⁱ—O28—O21	114.2 (12)
U1—O12—O1	0.9 (9)	K2ⁱ—O28—O23^xvi	108.1 (14)
U1—O12—O2ⁱ	51.2 (8)	K2ⁱ—O28—O24^v	42.1 (6)
U1—O12—K2^xxiii	129.5 (11)	O12^v—O28—O13ⁱⁱ	119.6 (12)
U1—O12—O4	50.4 (9)	O12^v—O28—O14^v	96.0 (15)
U1—O12—O7	57.9 (11)	O12^v—O28—O16	155 (2)
U1—O12—O8	50.5 (10)	O12^v—O28—O18	90.4 (11)
U1—O12—O10	107.9 (15)	O12^v—O28—O19^vi	72.6 (11)
U1—O12—O11ⁱ	51.2 (11)	O12^v—O28—O20^vi	74.6 (11)
U1—O12—O14^xiv	87.9 (9)	O12^v—O28—O21	120.0 (14)
U1—O12—O16ⁱ	92.6 (10)	O12^v—O28—O23^xvi	80.9 (14)
U1—O12—O19ⁱ	101.6 (14)	O12^v—O28—O24^v	65.9 (11)
U1—O12—O20ⁱ	129.6 (14)	O13ⁱⁱ—O28—O14^v	116.3 (11)
U1—O12—O23^xv	165.1 (17)	O13ⁱⁱ—O28—O16	78.1 (11)
U1—O12—O24	88.9 (10)	O13ⁱⁱ—O28—O18	133 (2)
U1—O12—O28^viii	139.8 (14)	O13ⁱⁱ—O28—O19^vi	76.8 (13)
K1—O12—O1	113.3 (11)	O13ⁱⁱ—O28—O20^vi	47.8 (9)
K1—O12—O2ⁱ	132.0 (13)	O13ⁱⁱ—O28—O21	50.4 (12)
K1—O12—K2^xxiii	89.9 (9)	O13ⁱⁱ—O28—O23^xvi	71.2 (12)
K1—O12—O4	97.6 (9)	O13ⁱⁱ—O28—O24^v	163.0 (15)
K1—O12—O7	79.2 (10)	O14^v—O28—O16	59.6 (10)
K1—O12—O8	64.0 (9)	O14^v—O28—O18	93.6 (11)
K1—O12—O10	50.6 (7)	O14^v—O28—O19^vi	166.2 (13)
K1—O12—O11ⁱ	159.9 (10)	O14^v—O28—O20^vi	141.4 (13)
K1—O12—O14^xiv	96.2 (9)	O14^v—O28—O21	143.8 (11)
K1—O12—O16ⁱ	138.3 (9)	O14^v—O28—O23^xvi	64.2 (10)
K1—O12—O19ⁱ	136.1 (10)	O14^v—O28—O24^v	47.1 (7)
K1—O12—O20ⁱ	116.0 (10)	O16—O28—O18	88.2 (10)
K1—O12—O23^xv	52.4 (7)	O16—O28—O19^vi	131.0 (19)
K1—O12—O24	45.6 (6)	O16—O28—O20^vi	125.8 (15)
K1—O12—O28^viii	75.6 (11)	O16—O28—O21	84.2 (13)
O1—O12—O2ⁱ	51.4 (8)	O16—O28—O23^xvi	90.0 (11)
O1—O12—K2^xxiii	129.5 (8)	O16—O28—O24^v	92.4 (11)
O1—O12—O4	50.6 (8)	O18—O28—O19^vi	79.1 (11)
O1—O12—O7	57.3 (9)	O18—O28—O20^vi	123.3 (14)
O1—O12—O8	49.8 (9)	O18—O28—O21	83.5 (14)
O1—O12—O10	107.2 (11)	O18—O28—O23^xvi	155 (2)
O1—O12—O11ⁱ	52.1 (9)	O18—O28—O24^v	59.9 (10)
O1—O12—O14^xiv	87.7 (7)	O19^vi—O28—O20^vi	44.2 (9)
O1—O12—O16ⁱ	93.1 (8)	O19^vi—O28—O21	47.6 (10)
O1—O12—O19ⁱ	102.5 (10)	O19^vi—O28—O23^xvi	119.8 (12)
O1—O12—O20ⁱ	130.4 (10)	O19^vi—O28—O24^v	119.5 (10)
O1—O12—O23^xv	164.3 (13)	O20^vi—O28—O21	60.7 (11)
O1—O12—O24	88.4 (8)	O20^vi—O28—O23^xvi	77.2 (11)
O1—O12—O28^viii	140.1 (11)	O20^vi—O28—O24^v	140.6 (13)
O2ⁱ—O12—K2^xxiii	79.3 (7)	O21—O28—O23^xvi	121.3 (14)
O2ⁱ—O12—O4	98.3 (11)	O21—O28—O24^v	143.4 (11)
O2ⁱ—O12—O7	53.9 (10)	O23^xvi—O28—O24^v	95.1 (15)

Symmetry codes: (i) x, −y+1, z−1/2; (ii) x−1, y, z−1; (iii) x−1, −y+1, z−1/2; (iv) x−1, y, z; (v) x−1/2, y−1/2, z; (vi) x−1/2, −y+1/2, z−1/2; (vii) x−1/2, y−1/2, z−1; (viii) x+1/2, y+1/2, z; (ix) x+1/2, −y+3/2, z+1/2; (x) x+1, −y+1, z+1/2; (xi) x+1, y, z+1; (xii) x, −y+1, z+1/2; (xiii) x+1/2, y−1/2, z; (xiv) x−1/2, −y+3/2, z−1/2; (xv) x, y+1, z; (xvi) x−1/2, y+1/2, z; (xvii) x, y, z+1; (xviii) x−1/2, −y+3/2, z+1/2; (xix) x, y+1, z+1; (xx) x+1/2, y+1/2, z+1; (xxi) x+1/2, −y+1/2, z+1/2; (xxii) x+1, y, z; (xxiii) x, y, z−1; (xxiv) x, −y, z−1/2; (xxv) x+1/2, −y+3/2, z−1/2; (xxvi) x, y−1, z; (xxvii) x, y−1, z−1; (xxviii) x, −y, z+1/2.

Acknowledgements

We thank the two anonymous referees as well as the handling editor Helen Brand for their comments.

Funding information

This research was supported by the Czech Science Foundation (contract No. GACR 20-11949S) and by the OPVV project Geobarr (contract No. CZ.02.1.01/0.0/0.0/16026/0008459) (grant No. 20-11949S awarded to the Institute of Physics ASCR, v.v.i.).

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JOURNAL OF
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Volume 54| Part 6| December 2021| Pages 1656-1663

https://doi.org/10.1107/S1600576721009663

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research papers\(\def\hfill{\hskip 5em}\def\hfil{\hskip 3em}\def\eqno#1{\hfil {#1}}\)

Hidden and apparent twins in uranyl-oxide minerals agrinierite and rameauite: a demonstration of metric and reticular merohedry

1. Introduction

2. Methodology

2.1. Samples studied

2.2. Chemical composition of agrinierite

2.3. Single-crystal X-ray diffraction

3. Results

3.1. Twinning

3.2. The refined structures of agrinierite and rameauite

4. Implications: the careful handling of structures with `hidden' twinning

Supporting information

Acknowledgements

Funding information

References

research papers