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Crystals of dl-2,4-bis(phenylthio)pentan-3-one, C17H18OS2, are orthorhombic (Iba2). Despite cell parameters that appear orthorhombic, crystals of dl-2,4-bis(2,6-dimethylphenylthio)pentan-3-one, C21H26OS2, are monoclinic (P21/n) and refine as two twinned components (57/43%) that mimic an orthorhombic lattice.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablocks global, shd2, shd3

hkl

Structure factor file (CIF format)
Contains datablock shd2

hkl

Structure factor file (CIF format)
Contains datablock shd3

CCDC references: 135763; 135764

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